####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_IPD14_7_1_13mer_refine5_hydro _audit_block_doi 10.5517/ccdc.csd.cc2g7g5c _database_code_depnum_ccdc_archive 'CCDC 2271282' loop_ _citation_id _citation_doi _citation_year 1 10.1038/s41467-025-59940-7 2025 loop_ _audit_author_name _audit_author_address 'Asim Bera' ;University of Washington United States of America ; _audit_update_record ; 2023-06-20 deposited with the CCDC. 2026-03-03 downloaded from the CCDC. ; _audit_creation_method SHELXL-2019/3 _shelx_SHELXL_version_number 2019/3 _chemical_name_systematic RH13.1 _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C47 H77 N9 O9 Zn0' _chemical_formula_weight 912.17 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0037 0.0018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0071 0.0036 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0122 0.0066 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2753 1.5037 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.270(2) _cell_length_b 18.000(4) _cell_length_c 22.050(4) _cell_angle_alpha 100.18(3) _cell_angle_beta 90.13(3) _cell_angle_gamma 101.85(3) _cell_volume 3923.3(15) _cell_formula_units_Z 1 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour ? _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 0.386 _exptl_crystal_F_000 494 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_absorpt_coefficient_mu 0.028 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.72932 _diffrn_radiation_type ? _diffrn_source ? _diffrn_measurement_device_type ? _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 26292 _diffrn_reflns_av_unetI/netI 0.4069 _diffrn_reflns_av_R_equivalents 0.4634 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_l_min 0 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_theta_min 1.206 _diffrn_reflns_theta_max 21.188 _diffrn_reflns_theta_full 21.188 _diffrn_measured_fraction_theta_max 0.910 _diffrn_measured_fraction_theta_full 0.910 _diffrn_reflns_Laue_measured_fraction_max 0.910 _diffrn_reflns_Laue_measured_fraction_full 0.910 _diffrn_reflns_point_group_measured_fraction_max 0.910 _diffrn_reflns_point_group_measured_fraction_full 0.910 _reflns_number_total 7275 _reflns_number_gt 3871 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2019/2 (Sheldrick, 2019)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1667P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 7275 _refine_ls_number_parameters 965 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.2137 _refine_ls_R_factor_gt 0.1703 _refine_ls_wR_factor_ref 0.3943 _refine_ls_wR_factor_gt 0.3709 _refine_ls_goodness_of_fit_ref 0.968 _refine_ls_restrained_S_all 0.968 _refine_ls_shift/su_max 0.088 _refine_ls_shift/su_mean 0.002 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N_1 N 0.2199(10) 0.2709(6) 0.6682(5) 0.064(3) Uani 1 1 d . . . . . H_1 H 0.214102 0.316655 0.685818 0.077 Uiso 1 1 calc R U . . . CA_1 C 0.3349(13) 0.2599(7) 0.6327(6) 0.071(4) Uani 1 1 d . . . . . HA_1 H 0.314975 0.208233 0.607188 0.085 Uiso 1 1 calc R U . . . C_1 C 0.4612(13) 0.2680(6) 0.6724(6) 0.057(4) Uani 1 1 d . . . . . O_1 O 0.5571(9) 0.2456(4) 0.6492(4) 0.065(3) Uani 1 1 d . . . . . CB_1 C 0.3646(17) 0.3208(11) 0.5894(6) 0.099(5) Uani 1 1 d . . . . . HB_1 H 0.443643 0.312849 0.566419 0.119 Uiso 1 1 calc R U . . . CG2_1 C 0.249(2) 0.3083(18) 0.5439(9) 0.157(10) Uani 1 1 d . . . . . HG2A_1 H 0.270183 0.343389 0.515491 0.236 Uiso 1 1 calc R U . . . HG2B_1 H 0.171382 0.317315 0.565488 0.236 Uiso 1 1 calc R U . . . HG2C_1 H 0.232778 0.256166 0.521580 0.236 Uiso 1 1 calc R U . . . OG1_1 O 0.3966(12) 0.3921(6) 0.6289(5) 0.105(4) Uani 1 1 d . . . . . N_2 N 0.4608(9) 0.2996(5) 0.7311(4) 0.056(3) Uani 1 1 d . . . . . H_2 H 0.389645 0.312521 0.745986 0.068 Uiso 1 1 calc R U . . . CA_2 C 0.5796(12) 0.3128(6) 0.7710(5) 0.061(4) Uani 1 1 d . . . . . HAA_2 H 0.610142 0.264822 0.768041 0.073 Uiso 1 1 calc R U . . . HAB_2 H 0.556707 0.328158 0.813338 0.073 Uiso 1 1 calc R U . . . C_2 C 0.6913(13) 0.3738(6) 0.7550(5) 0.052(3) Uani 1 1 d . . . . . O_2 O 0.8051(10) 0.3748(4) 0.7731(4) 0.067(3) Uani 1 1 d . . . . . N_3 N 0.6639(9) 0.4232(5) 0.7231(4) 0.058(3) Uani 1 1 d . . . . . H_3 H 0.582365 0.420758 0.712350 0.069 Uiso 1 1 calc R U . . . CA_3 C 0.7660(14) 0.4815(6) 0.7051(6) 0.068(4) Uani 1 1 d . . . . . HA_3 H 0.840265 0.490516 0.735318 0.082 Uiso 1 1 calc R U . . . C_3 C 0.7175(13) 0.5573(6) 0.7121(5) 0.055(3) Uani 1 1 d . . . . . O_3 O 0.6005(10) 0.5588(4) 0.7155(4) 0.065(3) Uani 1 1 d . . . . . CB_3 C 0.8219(17) 0.4582(8) 0.6418(7) 0.092(5) Uani 1 1 d . . . . . HBA_3 H 0.886703 0.501965 0.633006 0.110 Uiso 1 1 calc R U . . . HBB_3 H 0.868656 0.417036 0.644067 0.110 Uiso 1 1 calc R U . . . CG_3 C 0.7222(18) 0.4321(12) 0.5898(9) 0.122(7) Uani 1 1 d . . . . . HGA_3 H 0.676530 0.473332 0.586358 0.146 Uiso 1 1 calc R U . . . HGB_3 H 0.656598 0.388407 0.598182 0.146 Uiso 1 1 calc R U . . . CD_3 C 0.787(2) 0.4079(11) 0.5267(8) 0.119(7) Uani 1 1 d . . . . . OD1_3 O 0.7746(13) 0.3417(7) 0.5001(5) 0.116(5) Uani 1 1 d . . . . . OD2_3 O 0.8543(13) 0.4621(7) 0.5068(6) 0.114(5) Uani 1 1 d . . . . . N_4 N 0.8083(10) 0.6209(5) 0.7126(4) 0.060(3) Uani 1 1 d . . . . . H_4 H 0.890377 0.617661 0.709193 0.072 Uiso 1 1 calc R U . . . CA_4 C 0.7748(11) 0.6959(6) 0.7187(5) 0.057(3) Uani 1 1 d . . . . . HA_4 H 0.710064 0.699937 0.751059 0.069 Uiso 1 1 calc R U . . . C_4 C 0.7112(15) 0.7053(7) 0.6593(6) 0.075(4) Uani 1 1 d . . . . . O_4 O 0.7512(12) 0.6805(6) 0.6067(4) 0.103(4) Uani 1 1 d . . . . . CB_4 C 0.8949(12) 0.7605(7) 0.7370(5) 0.064(4) Uani 1 1 d . . . . . HBA_4 H 0.873109 0.809201 0.732422 0.077 Uiso 1 1 calc R U . . . HBB_4 H 0.967119 0.751941 0.710146 0.077 Uiso 1 1 calc R U . . . CG_4 C 0.9393(12) 0.7643(6) 0.8040(6) 0.061(4) Uani 1 1 d . . . . . CD1_4 C 0.8750(13) 0.8047(7) 0.8530(6) 0.071(4) Uani 1 1 d . . . . . HD1_4 H 0.808183 0.829279 0.843684 0.085 Uiso 1 1 calc R U . . . CD2_4 C 1.0380(14) 0.7292(7) 0.8205(6) 0.071(4) Uani 1 1 d . . . . . HD2_4 H 1.082965 0.704290 0.789323 0.085 Uiso 1 1 calc R U . . . CE1_4 C 0.9104(14) 0.8075(7) 0.9129(6) 0.073(4) Uani 1 1 d . . . . . HE1_4 H 0.870895 0.835600 0.944383 0.088 Uiso 1 1 calc R U . . . CE2_4 C 1.0737(13) 0.7290(7) 0.8811(6) 0.073(4) Uani 1 1 d . . . . . HE2_4 H 1.139618 0.704138 0.891001 0.087 Uiso 1 1 calc R U . . . CZ_4 C 1.0058(13) 0.7681(7) 0.9264(5) 0.071(4) Uani 1 1 d . . . . . OH_4 O 1.0432(10) 0.7719(6) 0.9891(4) 0.095(4) Uani 1 1 d . . . . . N_5 N 0.6160(10) 0.7444(5) 0.6646(4) 0.063(3) Uani 1 1 d . . . . . H_5 H 0.583123 0.754827 0.700180 0.075 Uiso 1 1 calc R U . . . CA_5 C 0.5639(13) 0.7707(7) 0.6130(5) 0.066(4) Uani 1 1 d . . . . . HA_5 H 0.565554 0.731669 0.575992 0.080 Uiso 1 1 calc R U . . . C_5 C 0.6482(13) 0.8439(6) 0.6027(5) 0.058(3) Uani 1 1 d . . . . . O_5 O 0.7510(9) 0.8759(5) 0.6336(4) 0.068(3) Uani 1 1 d . . . . . CB_5 C 0.4200(15) 0.7752(8) 0.6239(6) 0.080(4) Uani 1 1 d . . . . . HBA_5 H 0.373785 0.725993 0.633007 0.097 Uiso 1 1 calc R U . . . HBB_5 H 0.380497 0.781646 0.585671 0.097 Uiso 1 1 calc R U . . . CG_5 C 0.3936(17) 0.8381(8) 0.6746(6) 0.073(4) Uani 1 1 d . . . . . OD1_5 O 0.4802(10) 0.8920(5) 0.6938(4) 0.080(3) Uani 1 1 d . . . . . OD2_5 O 0.2716(13) 0.8317(6) 0.6903(4) 0.098(4) Uani 1 1 d . . . . . N_6 N 0.6110(11) 0.8729(5) 0.5558(4) 0.066(3) Uani 1 1 d . . . . . H_6 H 0.538287 0.850519 0.535060 0.079 Uiso 1 1 calc R U . . . CA_6 C 0.6935(14) 0.9439(7) 0.5387(6) 0.067(4) Uani 1 1 d . . . . . HA_6 H 0.786122 0.937752 0.537244 0.081 Uiso 1 1 calc R U . . . C_6 C 0.6881(14) 1.0148(7) 0.5852(6) 0.070(4) Uani 1 1 d . . . . . O_6 O 0.7666(12) 1.0734(6) 0.5805(6) 0.109(5) Uani 1 1 d . . . . . CB_6 C 0.6496(18) 0.9527(8) 0.4736(6) 0.089(5) Uani 1 1 d . . . . . HBA_6 H 0.693175 0.922522 0.443043 0.133 Uiso 1 1 calc R U . . . HBB_6 H 0.673453 1.006018 0.469629 0.133 Uiso 1 1 calc R U . . . HBC_6 H 0.554860 0.935087 0.467747 0.133 Uiso 1 1 calc R U . . . N_7 N 0.6005(10) 1.0123(5) 0.6300(5) 0.066(3) Uani 1 1 d . . . . . H_7 H 0.541701 0.970526 0.629149 0.079 Uiso 1 1 calc R U . . . CA_7 C 0.5996(12) 1.0759(6) 0.6795(5) 0.062(4) Uani 1 1 d . . . . . HA_7 H 0.635015 1.123873 0.664387 0.075 Uiso 1 1 calc R U . . . C_7 C 0.6858(14) 1.0739(7) 0.7355(6) 0.070(4) Uani 1 1 d . . . . . O_7 O 0.6979(10) 1.1276(5) 0.7798(5) 0.091(4) Uani 1 1 d . . . . . CB_7 C 0.4562(14) 1.0762(7) 0.6977(6) 0.073(4) Uani 1 1 d . . . . . HBA_7 H 0.410558 1.093731 0.666720 0.110 Uiso 1 1 calc R U . . . HBB_7 H 0.456345 1.110207 0.736545 0.110 Uiso 1 1 calc R U . . . HBC_7 H 0.411627 1.024917 0.701357 0.110 Uiso 1 1 calc R U . . . N_8 N 0.7388(10) 1.0135(5) 0.7364(5) 0.065(3) Uani 1 1 d . . . . . H_8 H 0.732760 0.978494 0.703836 0.078 Uiso 1 1 calc R U . . . CA_8 C 0.8082(13) 1.0053(7) 0.7923(6) 0.072(4) Uani 1 1 d . . . . . HAA_8 H 0.854602 1.056152 0.812607 0.087 Uiso 1 1 calc R U . . . HAB_8 H 0.875002 0.975097 0.780049 0.087 Uiso 1 1 calc R U . . . C_8 C 0.7230(14) 0.9684(7) 0.8382(7) 0.072(4) Uani 1 1 d . . . . . O_8 O 0.7700(10) 0.9746(5) 0.8906(4) 0.088(3) Uani 1 1 d . . . . . N_9 N 0.6033(10) 0.9258(5) 0.8189(4) 0.063(3) Uani 1 1 d . . . . . H_9 H 0.575010 0.924558 0.781937 0.075 Uiso 1 1 calc R U . . . CA_9 C 0.5191(11) 0.8813(6) 0.8585(6) 0.062(4) Uani 1 1 d . . . . . HA_9 H 0.543824 0.901459 0.902148 0.074 Uiso 1 1 calc R U . . . C_9 C 0.5319(11) 0.7967(6) 0.8406(6) 0.059(4) Uani 1 1 d . . . . . O_9 O 0.5355(10) 0.7656(5) 0.7875(4) 0.076(3) Uani 1 1 d . . . . . CB_9 C 0.3687(16) 0.8801(7) 0.8443(7) 0.083(5) Uani 1 1 d . . . . . HBA_9 H 0.349118 0.861000 0.800599 0.099 Uiso 1 1 calc R U . . . HBB_9 H 0.314181 0.843859 0.866451 0.099 Uiso 1 1 calc R U . . . CG_9 C 0.3285(17) 0.9569(8) 0.8610(7) 0.090(5) Uani 1 1 d . . . . . HGA_9 H 0.383428 0.994326 0.840065 0.108 Uiso 1 1 calc R U . . . HGB_9 H 0.342044 0.975445 0.905122 0.108 Uiso 1 1 calc R U . . . CD_9 C 0.1817(15) 0.9482(8) 0.8422(8) 0.088(5) Uani 1 1 d . . . . . HDA_9 H 0.130399 0.901524 0.853746 0.105 Uiso 1 1 calc R U . . . HDB_9 H 0.148616 0.991623 0.864416 0.105 Uiso 1 1 calc R U . . . NE_9 N 0.1624(13) 0.9444(7) 0.7756(6) 0.089(4) Uani 1 1 d . . . . . HE_9 H 0.158096 0.901136 0.750958 0.106 Uiso 1 1 calc R U . . . CZ_9 C 0.1514(15) 1.0078(10) 0.7522(8) 0.091(5) Uani 1 1 d . . . . . NH1_9 N 0.1629(13) 1.0763(6) 0.7850(7) 0.098(5) Uani 1 1 d . . . . . HH1A_9 H 0.247277 1.094558 0.798179 0.148 Uiso 1 1 calc R U . . . HH1B_9 H 0.111160 1.073904 0.817184 0.148 Uiso 1 1 calc R U . . . HH1C_9 H 0.138165 1.107360 0.761998 0.148 Uiso 1 1 calc R U . . . NH2_9 N 0.1224(14) 0.9962(8) 0.6923(8) 0.115(5) Uani 1 1 d . . . . . HH2A_9 H 0.080158 0.947486 0.679579 0.172 Uiso 1 1 calc R U . . . HH2B_9 H 0.197245 1.005577 0.672083 0.172 Uiso 1 1 calc R U . . . HH2C_9 H 0.070385 1.027774 0.684876 0.172 Uiso 1 1 calc R U . . . N_10 N 0.5302(10) 0.7581(5) 0.8888(5) 0.066(3) Uani 1 1 d . . . . . H_10 H 0.523764 0.780782 0.926082 0.079 Uiso 1 1 calc R U . . . CA_10 C 0.5397(13) 0.6761(7) 0.8748(6) 0.068(4) Uani 1 1 d . . . . . HA_10 H 0.598148 0.667612 0.840275 0.081 Uiso 1 1 calc R U . . . C_10 C 0.4010(14) 0.6283(6) 0.8580(5) 0.062(4) Uani 1 1 d . . . . . O_10 O 0.3122(9) 0.6270(5) 0.8952(4) 0.077(3) Uani 1 1 d . . . . . CB_10 C 0.6006(14) 0.6585(7) 0.9344(6) 0.072(4) Uani 1 1 d . . . . . HBA_10 H 0.686887 0.692696 0.944586 0.086 Uiso 1 1 calc R U . . . HBB_10 H 0.543319 0.668647 0.968439 0.086 Uiso 1 1 calc R U . . . CG_10 C 0.6171(14) 0.5737(7) 0.9265(6) 0.071(4) Uani 1 1 d . . . . . HG_10 H 0.528887 0.540538 0.915773 0.085 Uiso 1 1 calc R U . . . CD1_10 C 0.7077(18) 0.5522(9) 0.8756(7) 0.100(5) Uani 1 1 d . . . . . HD1A_10 H 0.725196 0.502208 0.877431 0.150 Uiso 1 1 calc R U . . . HD1B_10 H 0.789978 0.589694 0.880644 0.150 Uiso 1 1 calc R U . . . HD1C_10 H 0.665527 0.550898 0.836463 0.150 Uiso 1 1 calc R U . . . CD2_10 C 0.6625(17) 0.5597(9) 0.9897(7) 0.092(5) Uani 1 1 d . . . . . HD2A_10 H 0.661164 0.505775 0.987383 0.139 Uiso 1 1 calc R U . . . HD2B_10 H 0.603147 0.575645 1.020613 0.139 Uiso 1 1 calc R U . . . HD2C_10 H 0.751182 0.588963 1.000448 0.139 Uiso 1 1 calc R U . . . N_11 N 0.3815(11) 0.5875(5) 0.8007(5) 0.069(3) Uani 1 1 d . . . . . H_11 H 0.446471 0.590113 0.776068 0.083 Uiso 1 1 calc R U . . . CA_11 C 0.2508(13) 0.5381(7) 0.7787(6) 0.066(4) Uani 1 1 d . . . . . HA_11 H 0.179048 0.563251 0.795172 0.079 Uiso 1 1 calc R U . . . C_11 C 0.2368(15) 0.4603(7) 0.7985(6) 0.074(4) Uani 1 1 d . . . . . O_11 O 0.3145(9) 0.4176(4) 0.7796(4) 0.069(3) Uani 1 1 d . . . . . CB_11 C 0.2438(16) 0.5246(8) 0.7065(6) 0.084(4) Uani 1 1 d . . . . . HBA_11 H 0.333875 0.528817 0.692318 0.101 Uiso 1 1 calc R U . . . HBB_11 H 0.196308 0.472040 0.691526 0.101 Uiso 1 1 calc R U . . . CG_11 C 0.1797(13) 0.5769(7) 0.6778(5) 0.065(4) Uani 1 1 d . . . . . OG1_11 O 0.0844(10) 0.5996(5) 0.7037(4) 0.085(3) Uani 1 1 d . . . . . OG2_11 O 0.2215(11) 0.5911(5) 0.6258(5) 0.091(4) Uani 1 1 d . . . . . N_12 N 0.1370(10) 0.4377(5) 0.8346(4) 0.062(3) Uani 1 1 d . . . . . CA_12 C 0.1237(14) 0.3656(7) 0.8550(6) 0.070(4) Uani 1 1 d . . . . . HA_12 H 0.202657 0.366380 0.880289 0.084 Uiso 1 1 calc R U . . . C_12 C 0.1063(13) 0.2969(7) 0.8003(6) 0.069(4) Uani 1 1 d . . . . . O_12 O 0.1652(10) 0.2424(5) 0.8034(4) 0.082(3) Uani 1 1 d . . . . . CB_12 C 0.0031(13) 0.3597(8) 0.8944(6) 0.078(4) Uani 1 1 d . . . . . HBA_12 H 0.012628 0.332085 0.927615 0.093 Uiso 1 1 calc R U . . . HBB_12 H -0.077754 0.334446 0.870093 0.093 Uiso 1 1 calc R U . . . CG_12 C 0.0032(13) 0.4438(8) 0.9190(7) 0.080(4) Uani 1 1 d . . . . . HGA_12 H -0.085194 0.450173 0.930969 0.096 Uiso 1 1 calc R U . . . HGB_12 H 0.064210 0.463219 0.954603 0.096 Uiso 1 1 calc R U . . . CD_12 C 0.0472(12) 0.4855(7) 0.8675(5) 0.066(4) Uani 1 1 d . . . . . HDA_12 H 0.094620 0.537907 0.882878 0.080 Uiso 1 1 calc R U . . . HDB_12 H -0.027736 0.486489 0.841042 0.080 Uiso 1 1 calc R U . . . N_13 N 0.0272(9) 0.2971(5) 0.7536(4) 0.059(3) Uani 1 1 d . . . . . H_13 H -0.007433 0.336563 0.752887 0.071 Uiso 1 1 calc R U . . . CA_13 C -0.0025(13) 0.2323(7) 0.7036(6) 0.071(4) Uani 1 1 d . . . . . HA_13 H -0.047811 0.187227 0.720262 0.085 Uiso 1 1 calc R U . . . C_13 C 0.1269(14) 0.2137(8) 0.6739(6) 0.072(4) Uani 1 1 d . . . . . O_13 O 0.1316(10) 0.1459(5) 0.6539(5) 0.095(4) Uani 1 1 d . . . . . CB_13 C -0.0961(15) 0.2472(8) 0.6554(7) 0.085(5) Uani 1 1 d . . . . . HBA_13 H -0.054873 0.292350 0.639548 0.127 Uiso 1 1 calc R U . . . HBB_13 H -0.177792 0.255091 0.674010 0.127 Uiso 1 1 calc R U . . . HBC_13 H -0.114685 0.203552 0.622289 0.127 Uiso 1 1 calc R U . . . Zn_20 Zn 0.11932(19) 0.63848(9) 0.57406(8) 0.086(2) Uani 1 1 d . . . . . O1_21 O 0.6112(9) 0.2031(6) 0.5267(4) 0.087(3) Uani 1 1 d . . . . . O2_22 O 0.1047(11) 0.7426(6) 0.6141(5) 0.099(4) Uani 1 1 d . . . . . O3_23 O -0.0711(11) 0.6051(5) 0.5564(5) 0.096(4) Uani 1 1 d . . . . . O4_24 O 0.0024(13) 0.8622(7) 0.5932(6) 0.112(4) Uani 1 1 d . . . . . O5_25 O 0.9929(13) 1.0808(7) 0.5186(7) 0.129(5) Uani 1 1 d . . . . . O6_26 O 0.453(2) 0.5321(13) 0.5750(12) 0.210(9) Uani 1 1 d . . . . . O7_27 O 0.241(3) 0.1379(17) 0.9102(17) 0.35(3) Uani 1 1 d . . . . . O8_28 O 0.364(2) 0.2636(11) 0.8911(8) 0.173(7) Uani 1 1 d . . . . . O9_29 O 0.2396(11) 0.6983(7) 1.0042(5) 0.112(4) Uani 1 1 d . . . . . O10_30 O 0.4759(15) 0.1547(8) 0.9924(6) 0.138(5) Uani 1 1 d . . . . . O11_31 O 0.584(3) 1.1835(11) 0.8888(14) 0.269(16) Uani 1 1 d . . . . . O12_32 O 0.9954(18) 1.066(2) 0.9497(11) 0.29(2) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 N_1 0.066(7) 0.061(6) 0.059(7) -0.010(4) -0.004(5) 0.021(5) CA_1 0.076(10) 0.086(8) 0.049(8) -0.011(6) 0.004(6) 0.033(7) C_1 0.063(9) 0.052(6) 0.059(9) 0.013(5) 0.000(6) 0.018(5) O_1 0.071(6) 0.070(5) 0.060(5) 0.009(4) 0.009(4) 0.032(4) CB_1 0.105(12) 0.174(16) 0.041(8) 0.036(9) 0.017(7) 0.065(11) CG2_1 0.122(17) 0.31(3) 0.092(14) 0.071(16) 0.016(11) 0.131(19) OG1_1 0.145(10) 0.106(8) 0.092(8) 0.045(6) 0.047(7) 0.070(7) N_2 0.062(7) 0.061(6) 0.048(7) 0.006(4) 0.014(5) 0.021(4) CA_2 0.069(9) 0.069(7) 0.051(7) 0.009(5) 0.004(6) 0.027(6) C_2 0.064(9) 0.052(7) 0.041(6) 0.007(5) 0.004(5) 0.019(6) O_2 0.076(7) 0.068(5) 0.058(5) 0.008(4) -0.002(4) 0.020(4) N_3 0.054(6) 0.055(6) 0.063(6) 0.003(5) 0.006(4) 0.013(4) CA_3 0.089(10) 0.058(7) 0.055(8) -0.003(5) 0.009(6) 0.020(6) C_3 0.047(9) 0.071(8) 0.055(7) 0.015(5) 0.022(5) 0.028(6) O_3 0.069(7) 0.062(5) 0.064(6) 0.014(4) 0.008(4) 0.013(4) CB_3 0.122(13) 0.064(8) 0.080(10) 0.008(7) 0.030(9) 0.003(7) CG_3 0.094(13) 0.132(14) 0.114(16) 0.029(11) 0.008(10) -0.043(10) CD_3 0.186(19) 0.084(11) 0.065(11) 0.000(9) 0.017(11) -0.011(11) OD1_3 0.164(11) 0.110(9) 0.054(6) -0.011(6) 0.033(6) 0.005(7) OD2_3 0.145(11) 0.098(8) 0.093(9) 0.007(6) 0.050(7) 0.021(7) N_4 0.062(7) 0.062(6) 0.057(6) 0.012(4) 0.001(4) 0.018(5) CA_4 0.066(8) 0.057(7) 0.050(7) 0.005(5) 0.008(5) 0.018(5) C_4 0.111(12) 0.059(7) 0.052(9) 0.001(6) 0.008(7) 0.019(7) O_4 0.148(10) 0.131(8) 0.055(7) 0.014(5) 0.020(6) 0.090(7) CB_4 0.076(9) 0.068(7) 0.047(7) 0.009(5) 0.004(6) 0.014(6) CG_4 0.064(9) 0.061(7) 0.064(8) 0.024(6) 0.014(6) 0.014(6) CD1_4 0.078(10) 0.069(7) 0.066(9) 0.006(6) -0.004(7) 0.023(6) CD2_4 0.083(10) 0.065(7) 0.061(9) 0.002(6) 0.006(6) 0.018(6) CE1_4 0.074(10) 0.088(9) 0.053(9) 0.004(6) 0.012(6) 0.016(7) CE2_4 0.072(9) 0.086(8) 0.063(9) 0.003(6) -0.005(6) 0.031(7) CZ_4 0.076(10) 0.086(8) 0.044(8) 0.010(6) 0.005(6) 0.005(7) OH_4 0.101(8) 0.123(8) 0.057(7) 0.000(5) 0.001(5) 0.026(6) N_5 0.089(8) 0.065(6) 0.040(6) 0.005(4) 0.008(5) 0.034(5) CA_5 0.085(10) 0.074(8) 0.042(7) 0.002(5) -0.004(6) 0.029(6) C_5 0.064(9) 0.066(7) 0.045(7) 0.004(6) 0.009(6) 0.022(6) O_5 0.073(7) 0.075(5) 0.061(6) 0.016(4) 0.007(5) 0.024(4) CB_5 0.091(11) 0.083(9) 0.070(9) 0.026(7) -0.003(7) 0.014(7) CG_5 0.073(11) 0.072(9) 0.074(9) 0.013(7) -0.004(8) 0.016(8) OD1_5 0.104(8) 0.071(6) 0.062(6) 0.012(4) 0.003(5) 0.012(5) OD2_5 0.129(11) 0.109(8) 0.066(7) 0.020(5) 0.016(6) 0.047(6) N_6 0.079(8) 0.075(7) 0.046(6) 0.006(5) 0.001(5) 0.025(5) CA_6 0.075(9) 0.077(8) 0.057(8) 0.015(6) 0.005(6) 0.028(6) C_6 0.082(10) 0.071(8) 0.058(8) 0.011(6) 0.021(7) 0.016(7) O_6 0.126(9) 0.077(7) 0.112(9) -0.002(5) 0.063(7) 0.008(6) CB_6 0.140(13) 0.085(9) 0.054(8) 0.019(6) 0.014(8) 0.044(8) N_7 0.072(7) 0.068(6) 0.062(7) 0.018(5) 0.011(5) 0.021(5) CA_7 0.070(9) 0.066(7) 0.057(8) 0.013(6) 0.019(6) 0.025(6) C_7 0.088(10) 0.064(8) 0.054(8) 0.002(6) 0.019(6) 0.012(7) O_7 0.111(8) 0.087(6) 0.077(7) 0.009(5) 0.010(5) 0.032(5) CB_7 0.109(11) 0.063(7) 0.052(8) 0.013(5) 0.015(7) 0.026(6) N_8 0.072(7) 0.064(6) 0.061(7) 0.008(4) 0.010(5) 0.021(5) CA_8 0.060(9) 0.078(8) 0.082(10) 0.013(6) -0.001(6) 0.023(6) C_8 0.076(10) 0.063(7) 0.076(11) 0.007(6) 0.015(8) 0.019(7) O_8 0.108(8) 0.103(7) 0.050(6) 0.002(4) -0.022(5) 0.028(5) N_9 0.072(8) 0.066(6) 0.052(6) 0.014(4) 0.007(5) 0.015(5) CA_9 0.055(9) 0.074(8) 0.059(8) 0.014(6) -0.003(5) 0.015(6) C_9 0.059(8) 0.068(7) 0.052(9) 0.013(6) 0.011(5) 0.013(5) O_9 0.113(8) 0.083(6) 0.043(6) 0.010(4) 0.018(4) 0.048(5) CB_9 0.122(13) 0.061(7) 0.072(9) 0.022(6) 0.029(8) 0.026(7) CG_9 0.120(14) 0.077(9) 0.078(10) 0.015(7) 0.028(9) 0.031(8) CD_9 0.075(12) 0.076(9) 0.118(14) 0.026(8) 0.021(8) 0.021(7) NE_9 0.098(10) 0.086(8) 0.086(9) 0.024(6) 0.004(6) 0.021(6) CZ_9 0.067(10) 0.125(14) 0.095(12) 0.051(11) 0.006(7) 0.022(8) NH1_9 0.100(10) 0.055(7) 0.142(12) 0.015(7) 0.025(8) 0.020(6) NH2_9 0.101(11) 0.119(11) 0.130(15) 0.044(9) 0.000(9) 0.016(8) N_10 0.083(8) 0.068(6) 0.049(6) 0.009(5) 0.006(5) 0.023(5) CA_10 0.085(10) 0.066(7) 0.060(8) 0.018(6) 0.013(6) 0.028(6) C_10 0.089(10) 0.066(7) 0.041(7) 0.018(6) 0.017(7) 0.033(6) O_10 0.091(7) 0.083(6) 0.053(6) -0.002(4) 0.003(5) 0.026(4) CB_10 0.077(9) 0.084(8) 0.057(8) 0.022(6) 0.001(6) 0.017(6) CG_10 0.073(9) 0.085(8) 0.060(8) 0.022(6) -0.004(6) 0.023(6) CD1_10 0.133(14) 0.111(11) 0.072(10) 0.016(8) 0.008(9) 0.063(10) CD2_10 0.114(12) 0.104(10) 0.069(9) 0.033(7) -0.001(8) 0.031(8) N_11 0.085(8) 0.060(6) 0.066(8) 0.009(5) 0.012(5) 0.024(5) CA_11 0.082(10) 0.066(7) 0.054(8) -0.003(5) -0.001(6) 0.039(6) C_11 0.095(11) 0.078(8) 0.045(7) 0.003(6) -0.005(7) 0.020(8) O_11 0.079(6) 0.069(5) 0.062(6) 0.002(4) 0.016(4) 0.029(4) CB_11 0.109(12) 0.100(9) 0.048(8) 0.008(7) 0.013(7) 0.036(8) CG_11 0.077(9) 0.082(8) 0.046(8) 0.013(6) 0.014(6) 0.036(7) OG1_11 0.087(7) 0.103(7) 0.076(7) 0.022(5) 0.008(5) 0.042(5) OG2_11 0.118(9) 0.092(7) 0.078(7) 0.028(5) 0.022(6) 0.049(5) N_12 0.063(7) 0.072(6) 0.053(6) 0.006(5) 0.006(5) 0.022(5) CA_12 0.082(10) 0.075(8) 0.052(8) 0.000(6) -0.008(6) 0.021(6) C_12 0.063(9) 0.077(8) 0.070(9) 0.015(6) 0.015(7) 0.020(7) O_12 0.089(7) 0.080(6) 0.087(7) 0.023(5) 0.012(5) 0.034(5) CB_12 0.074(10) 0.105(10) 0.066(9) 0.033(7) 0.023(6) 0.033(7) CG_12 0.062(9) 0.102(10) 0.073(10) -0.005(7) 0.009(6) 0.031(7) CD_12 0.067(9) 0.085(8) 0.045(7) -0.004(6) 0.006(5) 0.027(6) N_13 0.062(7) 0.057(6) 0.062(7) 0.008(4) -0.004(5) 0.021(4) CA_13 0.074(10) 0.059(7) 0.077(9) 0.001(6) 0.001(7) 0.019(6) C_13 0.072(10) 0.080(9) 0.064(9) 0.001(7) -0.006(6) 0.026(8) O_13 0.098(8) 0.067(6) 0.113(9) -0.021(5) -0.002(6) 0.031(5) CB_13 0.084(11) 0.077(8) 0.091(11) -0.003(7) -0.004(8) 0.028(7) Zn_20 0.106(3) 0.091(2) 0.068(2) 0.0253(9) 0.0114(9) 0.0292(10) O1_21 0.086(7) 0.115(7) 0.055(6) 0.004(5) 0.001(4) 0.020(5) O2_22 0.109(8) 0.104(7) 0.089(8) 0.025(5) 0.006(6) 0.026(6) O3_23 0.125(9) 0.094(6) 0.079(7) 0.019(5) 0.000(6) 0.040(6) O4_24 0.124(10) 0.114(8) 0.111(9) 0.031(6) 0.013(7) 0.048(6) O5_25 0.111(10) 0.112(9) 0.173(13) 0.051(8) 0.029(8) 0.021(6) O6_26 0.22(2) 0.24(2) 0.23(2) 0.138(17) 0.046(16) 0.100(16) O7_27 0.28(3) 0.28(3) 0.40(5) -0.24(3) -0.17(3) 0.14(2) O8_28 0.228(18) 0.203(16) 0.112(12) 0.039(10) 0.009(11) 0.092(13) O9_29 0.101(8) 0.173(11) 0.067(7) 0.013(6) 0.008(5) 0.045(7) O10_30 0.184(13) 0.135(10) 0.078(8) 0.007(7) 0.021(8) 0.006(9) O11_31 0.31(3) 0.185(15) 0.37(3) 0.112(17) 0.28(3) 0.122(16) O12_32 0.125(15) 0.48(4) 0.18(2) -0.15(3) -0.029(13) 0.032(18) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag N_1 C_13 1.276(16) . ? N_1 CA_1 1.447(16) . ? CA_1 C_1 1.531(18) . ? CA_1 CB_1 1.56(2) . ? C_1 O_1 1.220(14) . ? C_1 N_2 1.318(15) . ? CB_1 OG1_1 1.39(2) . ? CB_1 CG2_1 1.51(3) . ? N_2 CA_2 1.456(15) . ? CA_2 C_2 1.505(17) . ? C_2 O_2 1.229(13) . ? C_2 N_3 1.300(15) . ? N_3 CA_3 1.434(15) . ? CA_3 C_3 1.528(16) . ? CA_3 CB_3 1.533(18) . ? C_3 O_3 1.209(13) . ? C_3 N_4 1.319(14) . ? CB_3 CG_3 1.48(2) . ? CG_3 CD_3 1.57(3) . ? CD_3 OD1_3 1.213(19) . ? CD_3 OD2_3 1.223(19) . ? CD_3 Zn_20 2.497(18) 2_666 ? OD1_3 Zn_20 2.010(10) 2_666 ? OD2_3 Zn_20 2.365(10) 2_666 ? N_4 CA_4 1.444(14) . ? CA_4 CB_4 1.510(16) . ? CA_4 C_4 1.514(18) . ? C_4 O_4 1.267(16) . ? C_4 N_5 1.312(17) . ? CB_4 CG_4 1.531(17) . ? CG_4 CD2_4 1.378(18) . ? CG_4 CD1_4 1.434(18) . ? CD1_4 CE1_4 1.357(19) . ? CD2_4 CE2_4 1.385(19) . ? CE1_4 CZ_4 1.382(19) . ? CE2_4 CZ_4 1.391(18) . ? CZ_4 OH_4 1.420(17) . ? N_5 CA_5 1.448(16) . ? CA_5 C_5 1.475(18) . ? CA_5 CB_5 1.513(19) . ? C_5 O_5 1.233(14) . ? C_5 N_6 1.326(16) . ? CB_5 CG_5 1.512(19) . ? CG_5 OD1_5 1.187(15) . ? CG_5 OD2_5 1.289(17) . ? N_6 CA_6 1.489(16) . ? CA_6 C_6 1.500(17) . ? CA_6 CB_6 1.548(19) . ? C_6 O_6 1.210(14) . ? C_6 N_7 1.338(15) . ? N_7 CA_7 1.436(14) . ? CA_7 CB_7 1.529(17) . ? CA_7 C_7 1.528(19) . ? C_7 O_7 1.234(14) . ? C_7 N_8 1.314(16) . ? N_8 CA_8 1.469(17) . ? CA_8 C_8 1.495(19) . ? C_8 O_8 1.229(17) . ? C_8 N_9 1.332(16) . ? N_9 CA_9 1.456(16) . ? CA_9 C_9 1.536(16) . ? CA_9 CB_9 1.57(2) . ? C_9 O_9 1.210(13) . ? C_9 N_10 1.367(16) . ? CB_9 CG_9 1.507(18) . ? CG_9 CD_9 1.53(2) . ? CD_9 NE_9 1.47(2) . ? NE_9 CZ_9 1.36(2) . ? CZ_9 NH1_9 1.30(2) . ? CZ_9 NH2_9 1.32(2) . ? N_10 CA_10 1.477(15) . ? CA_10 C_10 1.513(19) . ? CA_10 CB_10 1.564(18) . ? C_10 O_10 1.228(14) . ? C_10 N_11 1.338(15) . ? CB_10 CG_10 1.549(17) . ? CG_10 CD1_10 1.51(2) . ? CG_10 CD2_10 1.547(19) . ? N_11 CA_11 1.477(16) . ? CA_11 C_11 1.519(19) . ? CA_11 CB_11 1.565(18) . ? C_11 O_11 1.241(16) . ? C_11 N_12 1.340(17) . ? CB_11 CG_11 1.48(2) . ? CG_11 OG1_11 1.239(15) . ? CG_11 OG2_11 1.275(15) . ? OG2_11 Zn_20 1.958(10) . ? N_12 CA_12 1.429(16) . ? N_12 CD_12 1.492(15) . ? CA_12 CB_12 1.512(17) . ? CA_12 C_12 1.547(17) . ? C_12 O_12 1.266(15) . ? C_12 N_13 1.311(17) . ? CB_12 CG_12 1.514(18) . ? CG_12 CD_12 1.49(2) . ? N_13 CA_13 1.438(15) . ? CA_13 CB_13 1.53(2) . ? CA_13 C_13 1.554(18) . ? C_13 O_13 1.234(15) . ? Zn_20 O3_23 1.942(12) . ? Zn_20 O2_22 1.961(10) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C_13 N_1 CA_1 121.0(10) . . ? N_1 CA_1 C_1 113.6(10) . . ? N_1 CA_1 CB_1 109.7(11) . . ? C_1 CA_1 CB_1 107.6(11) . . ? O_1 C_1 N_2 122.8(11) . . ? O_1 C_1 CA_1 119.7(10) . . ? N_2 C_1 CA_1 117.6(10) . . ? OG1_1 CB_1 CG2_1 117.2(16) . . ? OG1_1 CB_1 CA_1 105.2(10) . . ? CG2_1 CB_1 CA_1 109.5(16) . . ? C_1 N_2 CA_2 120.7(9) . . ? N_2 CA_2 C_2 113.2(10) . . ? O_2 C_2 N_3 122.8(10) . . ? O_2 C_2 CA_2 118.2(10) . . ? N_3 C_2 CA_2 119.0(11) . . ? C_2 N_3 CA_3 121.8(11) . . ? N_3 CA_3 C_3 109.5(10) . . ? N_3 CA_3 CB_3 114.5(9) . . ? C_3 CA_3 CB_3 113.4(11) . . ? O_3 C_3 N_4 121.2(10) . . ? O_3 C_3 CA_3 121.5(11) . . ? N_4 C_3 CA_3 117.2(11) . . ? CG_3 CB_3 CA_3 115.5(15) . . ? CB_3 CG_3 CD_3 112.3(16) . . ? OD1_3 CD_3 OD2_3 122.3(17) . . ? OD1_3 CD_3 CG_3 123.7(16) . . ? OD2_3 CD_3 CG_3 114.0(15) . . ? OD1_3 CD_3 Zn_20 52.8(9) . 2_666 ? OD2_3 CD_3 Zn_20 69.5(10) . 2_666 ? CG_3 CD_3 Zn_20 176.4(12) . 2_666 ? CD_3 OD1_3 Zn_20 98.5(11) . 2_666 ? CD_3 OD2_3 Zn_20 81.5(10) . 2_666 ? C_3 N_4 CA_4 122.4(10) . . ? N_4 CA_4 CB_4 112.0(10) . . ? N_4 CA_4 C_4 110.8(9) . . ? CB_4 CA_4 C_4 109.5(10) . . ? O_4 C_4 N_5 120.8(12) . . ? O_4 C_4 CA_4 122.6(13) . . ? N_5 C_4 CA_4 116.6(10) . . ? CA_4 CB_4 CG_4 110.2(9) . . ? CD2_4 CG_4 CD1_4 117.1(12) . . ? CD2_4 CG_4 CB_4 123.3(10) . . ? CD1_4 CG_4 CB_4 119.6(12) . . ? CE1_4 CD1_4 CG_4 120.8(13) . . ? CG_4 CD2_4 CE2_4 123.5(11) . . ? CD1_4 CE1_4 CZ_4 119.3(11) . . ? CD2_4 CE2_4 CZ_4 116.5(13) . . ? CE1_4 CZ_4 CE2_4 122.7(12) . . ? CE1_4 CZ_4 OH_4 118.9(11) . . ? CE2_4 CZ_4 OH_4 118.2(13) . . ? C_4 N_5 CA_5 122.6(10) . . ? N_5 CA_5 C_5 111.0(10) . . ? N_5 CA_5 CB_5 108.6(11) . . ? C_5 CA_5 CB_5 113.6(10) . . ? O_5 C_5 N_6 120.5(11) . . ? O_5 C_5 CA_5 123.2(11) . . ? N_6 C_5 CA_5 116.3(11) . . ? CA_5 CB_5 CG_5 117.3(12) . . ? OD1_5 CG_5 OD2_5 124.2(13) . . ? OD1_5 CG_5 CB_5 120.1(14) . . ? OD2_5 CG_5 CB_5 115.4(12) . . ? C_5 N_6 CA_6 120.9(10) . . ? N_6 CA_6 C_6 112.1(10) . . ? N_6 CA_6 CB_6 110.1(10) . . ? C_6 CA_6 CB_6 110.9(11) . . ? O_6 C_6 N_7 122.0(11) . . ? O_6 C_6 CA_6 117.1(10) . . ? N_7 C_6 CA_6 120.9(11) . . ? C_6 N_7 CA_7 123.4(10) . . ? N_7 CA_7 CB_7 109.3(10) . . ? N_7 CA_7 C_7 112.6(10) . . ? CB_7 CA_7 C_7 110.4(10) . . ? O_7 C_7 N_8 122.1(13) . . ? O_7 C_7 CA_7 118.5(12) . . ? N_8 C_7 CA_7 119.3(10) . . ? C_7 N_8 CA_8 120.7(10) . . ? N_8 CA_8 C_8 116.1(12) . . ? O_8 C_8 N_9 123.3(12) . . ? O_8 C_8 CA_8 118.4(13) . . ? N_9 C_8 CA_8 118.1(13) . . ? C_8 N_9 CA_9 122.0(11) . . ? N_9 CA_9 C_9 108.0(9) . . ? N_9 CA_9 CB_9 110.0(10) . . ? C_9 CA_9 CB_9 104.8(9) . . ? O_9 C_9 N_10 122.6(10) . . ? O_9 C_9 CA_9 122.3(11) . . ? N_10 C_9 CA_9 115.0(10) . . ? CG_9 CB_9 CA_9 115.2(12) . . ? CB_9 CG_9 CD_9 109.7(12) . . ? NE_9 CD_9 CG_9 111.9(12) . . ? CZ_9 NE_9 CD_9 121.3(13) . . ? NH1_9 CZ_9 NH2_9 119.7(16) . . ? NH1_9 CZ_9 NE_9 124.2(17) . . ? NH2_9 CZ_9 NE_9 116.1(17) . . ? C_9 N_10 CA_10 117.9(10) . . ? N_10 CA_10 C_10 107.9(10) . . ? N_10 CA_10 CB_10 106.2(10) . . ? C_10 CA_10 CB_10 112.4(10) . . ? O_10 C_10 N_11 122.3(12) . . ? O_10 C_10 CA_10 121.6(11) . . ? N_11 C_10 CA_10 116.0(10) . . ? CG_10 CB_10 CA_10 112.1(10) . . ? CD1_10 CG_10 CD2_10 112.8(12) . . ? CD1_10 CG_10 CB_10 113.6(11) . . ? CD2_10 CG_10 CB_10 108.1(10) . . ? C_10 N_11 CA_11 121.4(10) . . ? N_11 CA_11 C_11 109.9(10) . . ? N_11 CA_11 CB_11 108.4(11) . . ? C_11 CA_11 CB_11 108.3(9) . . ? O_11 C_11 N_12 121.0(12) . . ? O_11 C_11 CA_11 120.0(12) . . ? N_12 C_11 CA_11 119.0(12) . . ? CG_11 CB_11 CA_11 116.8(10) . . ? OG1_11 CG_11 OG2_11 124.8(12) . . ? OG1_11 CG_11 CB_11 118.0(11) . . ? OG2_11 CG_11 CB_11 117.0(11) . . ? CG_11 OG2_11 Zn_20 120.8(9) . . ? C_11 N_12 CA_12 120.0(10) . . ? C_11 N_12 CD_12 127.4(11) . . ? CA_12 N_12 CD_12 111.6(10) . . ? N_12 CA_12 CB_12 105.4(10) . . ? N_12 CA_12 C_12 112.0(10) . . ? CB_12 CA_12 C_12 111.4(10) . . ? O_12 C_12 N_13 123.1(11) . . ? O_12 C_12 CA_12 118.9(12) . . ? N_13 C_12 CA_12 117.9(11) . . ? CA_12 CB_12 CG_12 102.0(10) . . ? CD_12 CG_12 CB_12 105.7(10) . . ? CG_12 CD_12 N_12 102.0(10) . . ? C_12 N_13 CA_13 121.0(10) . . ? N_13 CA_13 CB_13 110.5(10) . . ? N_13 CA_13 C_13 111.2(10) . . ? CB_13 CA_13 C_13 110.7(11) . . ? O_13 C_13 N_1 123.6(12) . . ? O_13 C_13 CA_13 119.1(12) . . ? N_1 C_13 CA_13 117.2(11) . . ? O3_23 Zn_20 OG2_11 124.1(4) . . ? O3_23 Zn_20 O2_22 93.2(4) . . ? OG2_11 Zn_20 O2_22 111.8(4) . . ? O3_23 Zn_20 OD1_3 114.0(5) . 2_666 ? OG2_11 Zn_20 OD1_3 108.2(5) . 2_666 ? O2_22 Zn_20 OD1_3 102.6(5) . 2_666 ? O3_23 Zn_20 OD2_3 87.0(4) . 2_666 ? OG2_11 Zn_20 OD2_3 85.9(5) . 2_666 ? O2_22 Zn_20 OD2_3 157.9(5) . 2_666 ? OD1_3 Zn_20 OD2_3 57.7(4) 2_666 2_666 ? O3_23 Zn_20 CD_3 102.2(6) . 2_666 ? OG2_11 Zn_20 CD_3 97.4(6) . 2_666 ? O2_22 Zn_20 CD_3 130.8(5) . 2_666 ? OD1_3 Zn_20 CD_3 28.7(5) 2_666 2_666 ? OD2_3 Zn_20 CD_3 29.0(4) 2_666 2_666 ? _refine_diff_density_max 0.065 _refine_diff_density_min -0.019 _refine_diff_density_rms 0.005 _shelx_res_file ; TITL IPD0014_7_1_mergable_a.res in P-1 IPD14_7_1_13mer_refine5_hydro.res created by SHELXL-2019/3 at 13:02:41 on 02-May-2023 REM Old TITL IPD0014_7_1 REM SHELXT solution in P-1: R1 0.340, Rweak 0.041, Alpha 0.138 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C66 N18 O24 Cl CELL 0.72932 10.2700 18.0000 22.0500 100.180 90.130 101.850 ZERR 1.000 0.0020 0.0040 0.0040 0.030 0.030 0.030 LATT 1 SFAC C H N O Zn DISP $C 0.00368 0.00180 11.94056!source kissel DISP $H -0.00002 0.00000 0.66634!source kissel DISP $N 0.00711 0.00363 20.61353!source kissel DISP $O 0.01216 0.00659 34.24495!source kissel DISP $Zn 0.27531 1.50374 6286.83626!source kissel UNIT 47 77 9 9 0 ACTA L.S. 20 BOND LIST 6 FMAP 2 PLAN 20 WPDB WGHT 0.166700 SWAT 0.971714 0.0024 FVAR 5.68706 RESI 1 THR N 3 0.219878 0.270899 0.668222 11.00000 0.06643 0.06098 = 0.05938 -0.01018 -0.00447 0.02088 AFIX 43 H 2 0.214102 0.316655 0.685818 11.00000 -1.20000 AFIX 0 CA 1 0.334884 0.259926 0.632702 11.00000 0.07601 0.08608 = 0.04875 -0.01097 0.00419 0.03297 AFIX 13 HA 2 0.314975 0.208233 0.607188 11.00000 -1.20000 AFIX 0 C 1 0.461199 0.268047 0.672419 11.00000 0.06314 0.05221 = 0.05882 0.01336 0.00041 0.01843 O 4 0.557096 0.245590 0.649208 11.00000 0.07064 0.07033 = 0.06041 0.00879 0.00879 0.03176 CB 1 0.364630 0.320791 0.589438 11.00000 0.10501 0.17363 = 0.04074 0.03584 0.01725 0.06536 AFIX 13 HB 2 0.443643 0.312849 0.566419 11.00000 -1.20000 AFIX 0 CG2 1 0.249286 0.308281 0.543868 11.00000 0.12227 0.30897 = 0.09161 0.07093 0.01583 0.13085 AFIX 137 HG2A 2 0.270183 0.343389 0.515491 11.00000 -1.50000 HG2B 2 0.171382 0.317315 0.565488 11.00000 -1.50000 HG2C 2 0.232778 0.256166 0.521580 11.00000 -1.50000 AFIX 0 OG1 4 0.396608 0.392136 0.628903 11.00000 0.14526 0.10587 = 0.09215 0.04461 0.04696 0.07029 RESI 2 GLY N 3 0.460799 0.299609 0.731103 11.00000 0.06234 0.06079 = 0.04815 0.00572 0.01364 0.02146 AFIX 43 H 2 0.389645 0.312521 0.745986 11.00000 -1.20000 AFIX 0 CA 1 0.579595 0.312825 0.770965 11.00000 0.06866 0.06895 = 0.05071 0.00931 0.00404 0.02742 AFIX 23 HAA 2 0.610142 0.264822 0.768041 11.00000 -1.20000 HAB 2 0.556707 0.328158 0.813338 11.00000 -1.20000 AFIX 0 C 1 0.691286 0.373791 0.755041 11.00000 0.06432 0.05211 = 0.04064 0.00714 0.00448 0.01861 O 4 0.805051 0.374779 0.773144 11.00000 0.07639 0.06834 = 0.05838 0.00819 -0.00217 0.02039 RESI 3 GLU N 3 0.663919 0.423174 0.723053 11.00000 0.05431 0.05461 = 0.06270 0.00301 0.00566 0.01339 AFIX 43 H 2 0.582365 0.420758 0.712350 11.00000 -1.20000 AFIX 0 CA 1 0.765970 0.481547 0.705132 11.00000 0.08882 0.05788 = 0.05501 -0.00294 0.00943 0.01996 AFIX 13 HA 2 0.840265 0.490516 0.735318 11.00000 -1.20000 AFIX 0 C 1 0.717462 0.557281 0.712057 11.00000 0.04738 0.07143 = 0.05495 0.01528 0.02243 0.02817 O 4 0.600531 0.558750 0.715499 11.00000 0.06924 0.06197 = 0.06352 0.01414 0.00799 0.01337 CB 1 0.821899 0.458198 0.641832 11.00000 0.12248 0.06427 = 0.08027 0.00831 0.02959 0.00259 AFIX 23 HBA 2 0.886703 0.501965 0.633006 11.00000 -1.20000 HBB 2 0.868656 0.417036 0.644067 11.00000 -1.20000 AFIX 0 CG 1 0.722249 0.432059 0.589770 11.00000 0.09350 0.13205 = 0.11355 0.02910 0.00798 -0.04315 AFIX 23 HGA 2 0.676530 0.473332 0.586358 11.00000 -1.20000 HGB 2 0.656598 0.388407 0.598182 11.00000 -1.20000 AFIX 0 CD 1 0.787420 0.407912 0.526709 11.00000 0.18552 0.08441 = 0.06468 0.00039 0.01713 -0.01112 OD1 4 0.774558 0.341680 0.500073 11.00000 0.16379 0.11037 = 0.05351 -0.01076 0.03339 0.00487 OD2 4 0.854329 0.462144 0.506769 11.00000 0.14495 0.09814 = 0.09284 0.00702 0.04977 0.02050 RESI 4 TYR N 3 0.808252 0.620933 0.712597 11.00000 0.06217 0.06220 = 0.05725 0.01166 0.00138 0.01773 AFIX 43 H 2 0.890377 0.617661 0.709193 11.00000 -1.20000 AFIX 0 CA 1 0.774810 0.695911 0.718692 11.00000 0.06625 0.05651 = 0.04994 0.00472 0.00753 0.01815 AFIX 13 HA 2 0.710064 0.699937 0.751059 11.00000 -1.20000 AFIX 0 C 1 0.711246 0.705278 0.659251 11.00000 0.11063 0.05939 = 0.05238 0.00104 0.00833 0.01931 O 4 0.751197 0.680479 0.606709 11.00000 0.14842 0.13103 = 0.05533 0.01444 0.01998 0.08952 CB 1 0.894947 0.760506 0.737019 11.00000 0.07555 0.06781 = 0.04747 0.00939 0.00414 0.01360 AFIX 23 HBA 2 0.873109 0.809201 0.732422 11.00000 -1.20000 HBB 2 0.967119 0.751941 0.710146 11.00000 -1.20000 AFIX 0 CG 1 0.939319 0.764256 0.804028 11.00000 0.06441 0.06083 = 0.06443 0.02432 0.01417 0.01417 CD1 1 0.874969 0.804692 0.853018 11.00000 0.07794 0.06890 = 0.06575 0.00559 -0.00353 0.02291 AFIX 43 HD1 2 0.808183 0.829279 0.843684 11.00000 -1.20000 AFIX 0 CD2 1 1.037994 0.729182 0.820526 11.00000 0.08325 0.06526 = 0.06088 0.00168 0.00551 0.01772 AFIX 43 HD2 2 1.082965 0.704290 0.789323 11.00000 -1.20000 AFIX 0 CE1 1 0.910398 0.807502 0.912857 11.00000 0.07378 0.08841 = 0.05296 0.00356 0.01201 0.01596 AFIX 43 HE1 2 0.870895 0.835600 0.944383 11.00000 -1.20000 AFIX 0 CE2 1 1.073724 0.729048 0.881125 11.00000 0.07233 0.08560 = 0.06272 0.00311 -0.00475 0.03096 AFIX 43 HE2 2 1.139618 0.704138 0.891001 11.00000 -1.20000 AFIX 0 CZ 1 1.005818 0.768148 0.926422 11.00000 0.07578 0.08609 = 0.04417 0.00968 0.00531 0.00513 OH 4 1.043233 0.771941 0.989126 11.00000 0.10052 0.12338 = 0.05709 -0.00004 0.00079 0.02615 RESI 5 ASP N 3 0.615958 0.744383 0.664602 11.00000 0.08855 0.06546 = 0.03974 0.00484 0.00844 0.03425 AFIX 43 H 2 0.583123 0.754827 0.700180 11.00000 -1.20000 AFIX 0 CA 1 0.563860 0.770664 0.612965 11.00000 0.08493 0.07383 = 0.04232 0.00160 -0.00362 0.02918 AFIX 13 HA 2 0.565554 0.731669 0.575992 11.00000 -1.20000 AFIX 0 C 1 0.648172 0.843860 0.602709 11.00000 0.06448 0.06589 = 0.04487 0.00371 0.00940 0.02227 O 4 0.751046 0.875880 0.633616 11.00000 0.07299 0.07535 = 0.06114 0.01577 0.00662 0.02430 CB 1 0.420039 0.775189 0.623885 11.00000 0.09083 0.08315 = 0.06963 0.02551 -0.00326 0.01354 AFIX 23 HBA 2 0.373785 0.725993 0.633007 11.00000 -1.20000 HBB 2 0.380497 0.781646 0.585671 11.00000 -1.20000 AFIX 0 CG 1 0.393629 0.838143 0.674573 11.00000 0.07272 0.07188 = 0.07434 0.01319 -0.00434 0.01591 OD1 4 0.480214 0.891976 0.693814 11.00000 0.10429 0.07107 = 0.06210 0.01189 0.00307 0.01164 OD2 4 0.271573 0.831658 0.690261 11.00000 0.12905 0.10949 = 0.06630 0.01976 0.01588 0.04678 RESI 6 ALA N 3 0.610999 0.872930 0.555834 11.00000 0.07938 0.07509 = 0.04581 0.00573 0.00144 0.02494 AFIX 43 H 2 0.538287 0.850519 0.535060 11.00000 -1.20000 AFIX 0 CA 1 0.693465 0.943851 0.538691 11.00000 0.07468 0.07718 = 0.05678 0.01507 0.00533 0.02805 AFIX 13 HA 2 0.786122 0.937752 0.537244 11.00000 -1.20000 AFIX 0 C 1 0.688060 1.014779 0.585195 11.00000 0.08178 0.07128 = 0.05761 0.01108 0.02104 0.01646 O 4 0.766576 1.073409 0.580539 11.00000 0.12607 0.07670 = 0.11193 -0.00229 0.06309 0.00784 CB 1 0.649570 0.952711 0.473596 11.00000 0.14031 0.08454 = 0.05354 0.01901 0.01429 0.04443 AFIX 137 HBA 2 0.693175 0.922522 0.443043 11.00000 -1.50000 HBB 2 0.673453 1.006018 0.469629 11.00000 -1.50000 HBC 2 0.554860 0.935087 0.467747 11.00000 -1.50000 AFIX 0 RESI 7 ALA N 3 0.600498 1.012333 0.630004 11.00000 0.07243 0.06772 = 0.06198 0.01770 0.01109 0.02126 AFIX 43 H 2 0.541701 0.970526 0.629149 11.00000 -1.20000 AFIX 0 CA 1 0.599633 1.075933 0.679465 11.00000 0.06961 0.06603 = 0.05734 0.01312 0.01882 0.02541 AFIX 13 HA 2 0.635015 1.123873 0.664387 11.00000 -1.20000 AFIX 0 C 1 0.685796 1.073858 0.735478 11.00000 0.08804 0.06369 = 0.05358 0.00176 0.01924 0.01165 O 4 0.697860 1.127589 0.779787 11.00000 0.11131 0.08665 = 0.07676 0.00861 0.00969 0.03211 CB 1 0.456200 1.076224 0.697720 11.00000 0.10865 0.06273 = 0.05236 0.01332 0.01456 0.02614 AFIX 137 HBA 2 0.410558 1.093731 0.666720 11.00000 -1.50000 HBB 2 0.456345 1.110207 0.736545 11.00000 -1.50000 HBC 2 0.411627 1.024917 0.701357 11.00000 -1.50000 AFIX 0 RESI 8 GLY N 3 0.738786 1.013520 0.736361 11.00000 0.07218 0.06372 = 0.06090 0.00793 0.00995 0.02064 AFIX 43 H 2 0.732760 0.978494 0.703836 11.00000 -1.20000 AFIX 0 CA 1 0.808199 1.005275 0.792316 11.00000 0.05978 0.07841 = 0.08219 0.01274 -0.00081 0.02317 AFIX 23 HAA 2 0.854602 1.056152 0.812607 11.00000 -1.20000 HAB 2 0.875002 0.975097 0.780049 11.00000 -1.20000 AFIX 0 C 1 0.722996 0.968389 0.838217 11.00000 0.07566 0.06327 = 0.07646 0.00723 0.01483 0.01884 O 4 0.770048 0.974603 0.890607 11.00000 0.10845 0.10256 = 0.04995 0.00224 -0.02186 0.02839 RESI 9 ARG N 3 0.603339 0.925789 0.818908 11.00000 0.07158 0.06594 = 0.05156 0.01366 0.00729 0.01469 AFIX 43 H 2 0.575010 0.924558 0.781937 11.00000 -1.20000 AFIX 0 CA 1 0.519080 0.881255 0.858498 11.00000 0.05480 0.07383 = 0.05874 0.01439 -0.00342 0.01525 AFIX 13 HA 2 0.543824 0.901459 0.902148 11.00000 -1.20000 AFIX 0 C 1 0.531920 0.796732 0.840639 11.00000 0.05874 0.06788 = 0.05158 0.01254 0.01079 0.01333 O 4 0.535512 0.765623 0.787532 11.00000 0.11344 0.08252 = 0.04260 0.01038 0.01797 0.04829 CB 1 0.368659 0.880098 0.844306 11.00000 0.12189 0.06146 = 0.07198 0.02199 0.02916 0.02615 AFIX 23 HBA 2 0.349118 0.861000 0.800599 11.00000 -1.20000 HBB 2 0.314181 0.843859 0.866451 11.00000 -1.20000 AFIX 0 CG 1 0.328548 0.956902 0.861046 11.00000 0.12041 0.07693 = 0.07836 0.01541 0.02821 0.03136 AFIX 23 HGA 2 0.383428 0.994326 0.840065 11.00000 -1.20000 HGB 2 0.342044 0.975445 0.905122 11.00000 -1.20000 AFIX 0 CD 1 0.181669 0.948166 0.842235 11.00000 0.07478 0.07645 = 0.11789 0.02617 0.02142 0.02103 AFIX 23 HDA 2 0.130399 0.901524 0.853746 11.00000 -1.20000 HDB 2 0.148616 0.991623 0.864416 11.00000 -1.20000 AFIX 0 NE 3 0.162433 0.944382 0.775615 11.00000 0.09764 0.08642 = 0.08563 0.02369 0.00393 0.02094 AFIX 43 HE 2 0.158096 0.901136 0.750958 11.00000 -1.20000 AFIX 0 CZ 1 0.151371 1.007781 0.752219 11.00000 0.06677 0.12486 = 0.09475 0.05089 0.00593 0.02153 NH1 3 0.162896 1.076265 0.784960 11.00000 0.10037 0.05466 = 0.14155 0.01547 0.02510 0.02045 AFIX 137 HH1A 2 0.247277 1.094558 0.798179 11.00000 -1.50000 HH1B 2 0.111160 1.073904 0.817184 11.00000 -1.50000 HH1C 2 0.138165 1.107360 0.761998 11.00000 -1.50000 AFIX 0 NH2 3 0.122415 0.996205 0.692273 11.00000 0.10057 0.11892 = 0.12952 0.04410 0.00042 0.01607 AFIX 137 HH2A 2 0.080158 0.947486 0.679579 11.00000 -1.50000 HH2B 2 0.197245 1.005577 0.672083 11.00000 -1.50000 HH2C 2 0.070385 1.027774 0.684876 11.00000 -1.50000 AFIX 0 RESI 10 LEU N 3 0.530198 0.758082 0.888804 11.00000 0.08323 0.06773 = 0.04936 0.00894 0.00602 0.02286 AFIX 43 H 2 0.523764 0.780782 0.926082 11.00000 -1.20000 AFIX 0 CA 1 0.539741 0.676063 0.874778 11.00000 0.08509 0.06645 = 0.05989 0.01755 0.01348 0.02832 AFIX 13 HA 2 0.598148 0.667612 0.840275 11.00000 -1.20000 AFIX 0 C 1 0.400978 0.628259 0.858042 11.00000 0.08930 0.06631 = 0.04129 0.01830 0.01720 0.03255 O 4 0.312174 0.627013 0.895249 11.00000 0.09115 0.08337 = 0.05296 -0.00232 0.00328 0.02592 CB 1 0.600637 0.658451 0.934410 11.00000 0.07698 0.08420 = 0.05718 0.02234 0.00074 0.01663 AFIX 23 HBA 2 0.686887 0.692696 0.944586 11.00000 -1.20000 HBB 2 0.543319 0.668647 0.968439 11.00000 -1.20000 AFIX 0 CG 1 0.617127 0.573690 0.926515 11.00000 0.07273 0.08518 = 0.05973 0.02213 -0.00366 0.02293 AFIX 13 HG 2 0.528887 0.540538 0.915773 11.00000 -1.20000 AFIX 0 CD1 1 0.707677 0.552169 0.875645 11.00000 0.13326 0.11085 = 0.07167 0.01609 0.00822 0.06347 AFIX 137 HD1A 2 0.725196 0.502208 0.877431 11.00000 -1.50000 HD1B 2 0.789978 0.589694 0.880644 11.00000 -1.50000 HD1C 2 0.665527 0.550898 0.836463 11.00000 -1.50000 AFIX 0 CD2 1 0.662455 0.559690 0.989737 11.00000 0.11385 0.10411 = 0.06932 0.03267 -0.00057 0.03073 AFIX 137 HD2A 2 0.661164 0.505775 0.987383 11.00000 -1.50000 HD2B 2 0.603147 0.575645 1.020613 11.00000 -1.50000 HD2C 2 0.751182 0.588963 1.000448 11.00000 -1.50000 AFIX 0 RESI 11 ASP N 3 0.381494 0.587506 0.800671 11.00000 0.08474 0.05978 = 0.06612 0.00896 0.01242 0.02422 AFIX 43 H 2 0.446471 0.590113 0.776068 11.00000 -1.20000 AFIX 0 CA 1 0.250816 0.538125 0.778652 11.00000 0.08248 0.06623 = 0.05413 -0.00318 -0.00062 0.03854 AFIX 13 HA 2 0.179048 0.563251 0.795172 11.00000 -1.20000 AFIX 0 C 1 0.236826 0.460328 0.798467 11.00000 0.09532 0.07799 = 0.04467 0.00259 -0.00474 0.01967 O 4 0.314457 0.417600 0.779568 11.00000 0.07898 0.06877 = 0.06229 0.00192 0.01625 0.02920 CB 1 0.243783 0.524581 0.706532 11.00000 0.10880 0.10034 = 0.04765 0.00755 0.01271 0.03639 AFIX 23 HBA 2 0.333875 0.528817 0.692318 11.00000 -1.20000 HBB 2 0.196308 0.472040 0.691526 11.00000 -1.20000 AFIX 0 CG 1 0.179680 0.576910 0.677779 11.00000 0.07723 0.08176 = 0.04645 0.01328 0.01444 0.03557 OG1 4 0.084364 0.599559 0.703666 11.00000 0.08731 0.10347 = 0.07571 0.02245 0.00841 0.04152 OG2 4 0.221508 0.591113 0.625790 11.00000 0.11818 0.09216 = 0.07841 0.02803 0.02244 0.04874 RESI 12 PRO N 3 0.137031 0.437750 0.834580 11.00000 0.06268 0.07190 = 0.05251 0.00566 0.00568 0.02203 CA 1 0.123668 0.365560 0.854957 11.00000 0.08165 0.07539 = 0.05185 0.00023 -0.00756 0.02123 AFIX 13 HA 2 0.202657 0.366380 0.880289 11.00000 -1.20000 AFIX 0 C 1 0.106313 0.296916 0.800308 11.00000 0.06335 0.07701 = 0.06967 0.01525 0.01538 0.02045 O 4 0.165212 0.242366 0.803436 11.00000 0.08878 0.07980 = 0.08689 0.02259 0.01242 0.03416 CB 1 0.003061 0.359745 0.894446 11.00000 0.07429 0.10519 = 0.06597 0.03253 0.02262 0.03300 AFIX 23 HBA 2 0.012628 0.332085 0.927615 11.00000 -1.20000 HBB 2 -0.077754 0.334446 0.870093 11.00000 -1.20000 AFIX 0 CG 1 0.003249 0.443797 0.919014 11.00000 0.06247 0.10167 = 0.07290 -0.00516 0.00887 0.03099 AFIX 23 HGA 2 -0.085194 0.450173 0.930969 11.00000 -1.20000 HGB 2 0.064210 0.463219 0.954603 11.00000 -1.20000 AFIX 0 CD 1 0.047169 0.485450 0.867527 11.00000 0.06719 0.08516 = 0.04528 -0.00442 0.00558 0.02664 AFIX 23 HDA 2 0.094620 0.537907 0.882878 11.00000 -1.20000 HDB 2 -0.027736 0.486489 0.841042 11.00000 -1.20000 AFIX 0 RESI 13 ALA N 3 0.027220 0.297091 0.753620 11.00000 0.06177 0.05656 = 0.06197 0.00766 -0.00413 0.02086 AFIX 43 H 2 -0.007433 0.336563 0.752887 11.00000 -1.20000 AFIX 0 CA 1 -0.002475 0.232292 0.703616 11.00000 0.07430 0.05883 = 0.07676 0.00141 0.00145 0.01870 AFIX 13 HA 2 -0.047811 0.187227 0.720262 11.00000 -1.20000 AFIX 0 C 1 0.126855 0.213734 0.673852 11.00000 0.07236 0.07962 = 0.06441 0.00056 -0.00576 0.02560 O 4 0.131605 0.145878 0.653910 11.00000 0.09843 0.06746 = 0.11274 -0.02062 -0.00154 0.03149 CB 1 -0.096149 0.247205 0.655391 11.00000 0.08414 0.07748 = 0.09077 -0.00279 -0.00373 0.02763 AFIX 137 HBA 2 -0.054873 0.292350 0.639548 11.00000 -1.50000 HBB 2 -0.177792 0.255091 0.674010 11.00000 -1.50000 HBC 2 -0.114685 0.203552 0.622289 11.00000 -1.50000 AFIX 0 RESI 20 Zn ZN 5 0.119325 0.638484 0.574062 11.00000 0.10629 0.09145 = 0.06768 0.02526 0.01139 0.02917 RESI 21 HOH O1 4 0.611181 0.203095 0.526681 11.00000 0.08598 0.11549 = 0.05533 0.00402 0.00080 0.01973 RESI 22 HOH O2 4 0.104669 0.742634 0.614073 11.00000 0.10872 0.10392 = 0.08931 0.02505 0.00564 0.02568 RESI 23 HOH O3 4 -0.071134 0.605129 0.556391 11.00000 0.12491 0.09384 = 0.07902 0.01940 -0.00022 0.03959 RESI 24 HOH O4 4 0.002374 0.862179 0.593212 11.00000 0.12425 0.11410 = 0.11081 0.03077 0.01297 0.04838 RESI 25 HOH O5 4 0.992937 1.080817 0.518618 11.00000 0.11076 0.11178 = 0.17257 0.05108 0.02885 0.02109 RESI 26 HOH O6 4 0.453011 0.532132 0.575003 11.00000 0.22498 0.23666 = 0.22828 0.13771 0.04566 0.10008 RESI 27 HOH O7 4 0.240961 0.137938 0.910209 11.00000 0.28072 0.28477 = 0.39807 -0.24367 -0.16955 0.14446 RESI 28 HOH O8 4 0.363743 0.263583 0.891071 11.00000 0.22789 0.20265 = 0.11237 0.03861 0.00891 0.09185 RESI 29 HOH O9 4 0.239589 0.698255 1.004212 11.00000 0.10095 0.17341 = 0.06658 0.01271 0.00785 0.04526 RESI 30 HOH O10 4 0.475923 0.154657 0.992440 11.00000 0.18370 0.13515 = 0.07794 0.00659 0.02121 0.00579 RESI 31 HOH O11 4 0.584028 1.183526 0.888847 11.00000 0.30982 0.18524 = 0.36806 0.11185 0.28440 0.12227 RESI 32 HOH O12 4 0.995412 1.066394 0.949712 11.00000 0.12535 0.47942 = 0.17974 -0.15279 -0.02909 0.03202 HKLF 4 REM IPD0014_7_1_mergable_a.res in P-1 REM wR2 = 0.3943, GooF = S = 0.968, Restrained GooF = 0.968 for all data REM R1 = 0.1703 for 3871 Fo > 4sig(Fo) and 0.2137 for all 7275 data REM 965 parameters refined using 0 restraints END WGHT 0.1108 0.0000 REM Highest difference peak 0.065, deepest hole -0.019, 1-sigma level 0.005 Q1 1 0.0461 0.5678 0.5582 11.00000 0.05 0.07 Q2 1 0.3297 0.7222 1.0521 11.00000 0.05 0.05 Q3 1 0.5988 0.1401 0.9696 11.00000 0.05 0.03 Q4 1 0.5481 1.1675 0.8670 11.00000 0.05 0.03 Q5 1 0.2097 0.7038 0.5942 11.00000 0.05 0.03 Q6 1 0.8323 0.7408 0.7412 11.00000 0.05 0.02 Q7 1 0.6127 0.7154 0.6716 11.00000 0.05 0.02 Q8 1 0.1265 0.5351 0.6158 11.00000 0.05 0.02 Q9 1 0.6611 1.1859 0.9244 11.00000 0.05 0.02 Q10 1 0.2554 1.0474 0.9876 11.00000 0.05 0.02 Q11 1 0.4936 0.3157 0.7528 11.00000 0.05 0.02 Q12 1 0.0124 0.6745 0.5908 11.00000 0.05 0.02 Q13 1 0.4086 0.2656 0.6748 11.00000 0.05 0.02 Q14 1 0.7268 1.1756 0.9056 11.00000 0.05 0.02 Q15 1 0.0655 0.2853 0.8092 11.00000 0.05 0.02 Q16 1 0.0297 0.2848 0.7834 11.00000 0.05 0.02 Q17 1 0.3274 0.4760 0.5471 11.00000 0.05 0.02 Q18 1 0.0815 0.2997 0.8189 11.00000 0.05 0.02 Q19 1 0.6952 0.9455 0.8166 11.00000 0.05 0.02 Q20 1 0.6847 0.8613 0.6325 11.00000 0.05 0.02 ; _shelx_res_checksum 33150 _shelx_hkl_file ; -9 2 10 33.61 13.22 -9 3 9 0.07 0.33 -9 3 10 18.91 7.47 -9 4 7 7.59 3.01 -9 4 8 24.48 9.63 -9 4 9 4.87 2.00 -9 5 8 2.67 1.51 -9 6 4 7.90 42.71 -9 6 5 16.44 6.56 -9 6 5 7.41 34.13 -9 6 6 10.89 4.43 -9 6 6 -1.07 19.13 -9 6 7 52.97 20.87 -9 6 7 2.23 20.63 -9 6 8 0.31 1.28 -9 6 8 -3.85 21.64 -9 7 1 12.25 4.90 -9 7 1 -22.71 55.64 -9 7 2 10.15 4.09 -9 7 3 15.14 6.06 -9 7 4 2.54 1.28 -9 7 4 -7.75 27.87 -9 7 4 5.45 29.94 -9 7 5 216.64 84.93 -9 7 7 29.03 11.60 -9 7 7 0.41 24.22 -9 7 8 6.90 3.36 -9 7 8 -0.09 20.57 -9 8 1 7.32 66.51 -9 8 2 -7.67 66.62 -9 8 2 33.38 107.86 -9 8 3 58.41 23.00 -9 8 4 14.64 5.93 -9 8 5 2.26 1.46 -9 8 6 67.53 26.67 -9 8 6 -2.66 22.47 -9 8 7 14.86 6.27 -9 8 7 -11.50 25.63 -9 8 7 -5.84 19.54 -9 9 1 9.25 3.94 -9 9 1 2.11 64.28 -9 9 2 0.23 1.12 -9 9 2 -13.12 80.48 -9 9 3 21.44 8.64 -9 9 3 13.38 83.11 -9 9 4 0.64 1.38 -9 9 4 8.53 91.03 -9 9 4 0.98 127.48 -9 9 5 19.51 8.01 -9 10 1 2.58 1.65 -9 10 1 -12.79 77.00 -9 10 2 25.24 10.14 -9 10 2 11.03 71.81 -9 10 3 9.20 3.97 -9 10 3 -12.84 82.88 -9 10 4 1.32 1.35 -9 10 4 -10.69 84.53 -9 11 1 89.89 35.37 -9 11 1 37.18 87.04 -8 -7 1 -0.48 4.66 -8 -7 1 1.58 31.82 -8 -7 2 4.63 4.93 -8 -7 2 -2.52 24.67 -8 -7 3 1.00 3.10 -8 -7 3 -2.79 22.38 -8 -7 4 5.64 3.71 -8 -7 4 4.34 20.32 -8 -7 5 -0.23 2.63 -8 -7 5 -3.76 10.20 -8 -7 6 -0.26 2.20 -8 -7 7 53.52 21.15 -8 -6 1 18.38 8.31 -8 -6 1 13.18 32.19 -8 -6 2 0.27 2.93 -8 -6 3 8.14 4.32 -8 -6 4 23.09 9.39 -8 -6 5 6.98 3.48 -8 -6 6 11.76 5.11 -8 -6 6 9.95 8.81 -8 -6 7 3.75 2.03 -8 -6 8 0.38 1.39 -8 -6 8 -1.20 7.79 -8 -6 9 0.56 1.05 -8 -5 1 31.13 12.74 -8 -5 2 14.73 6.45 -8 -5 6 -0.61 1.45 -8 -5 7 25.19 9.99 -8 -5 8 1.88 1.25 -8 -5 8 1.37 6.19 -8 -5 9 24.61 9.76 -8 -5 9 28.33 13.55 -8 -5 10 39.30 15.50 -8 -5 10 27.99 15.29 -8 -4 8 12.67 5.08 -8 -4 9 4.84 2.10 -8 -4 9 5.18 6.27 -8 -4 10 0.63 0.84 -8 -4 10 -1.72 8.04 -8 -3 9 1.48 0.92 -8 -3 10 0.97 0.78 -8 -3 10 -0.23 5.44 -8 -3 11 16.42 6.54 -8 -3 11 20.05 11.84 -8 -3 12 4.64 2.03 -8 -3 12 4.05 10.68 -8 -2 9 14.74 5.86 -8 -2 10 7.93 3.20 -8 -2 10 7.69 4.38 -8 -2 11 50.99 20.04 -8 -2 11 47.17 19.66 -8 -2 12 2.41 1.18 -8 -2 12 2.86 7.38 -8 -2 13 1.14 0.79 -8 -2 13 1.83 9.20 -8 -1 9 31.31 12.31 -8 -1 10 0.24 0.42 -8 -1 10 0.65 2.89 -8 -1 11 44.19 17.36 -8 -1 11 40.11 16.57 -8 -1 12 4.15 1.79 -8 -1 12 4.69 6.05 -8 -1 13 0.52 0.64 -8 -1 13 0.74 7.31 -8 0 9 35.95 14.12 -8 0 10 0.61 0.48 -8 0 10 1.34 2.45 -8 0 11 2.14 1.00 -8 0 11 1.89 3.72 -8 0 12 67.02 26.31 -8 0 12 75.41 30.52 -8 0 13 4.06 1.77 -8 0 13 0.14 6.92 -8 1 8 0.10 0.32 -8 1 9 10.23 4.06 -8 1 9 6.49 3.03 -8 1 10 90.98 35.65 -8 1 10 100.27 39.47 -8 1 12 1.12 0.67 -8 1 12 0.14 4.65 -8 1 13 22.45 8.89 -8 1 13 12.44 8.20 -8 2 7 23.35 9.17 -8 2 8 0.85 0.45 -8 2 8 0.32 0.79 -8 2 9 4.43 1.80 -8 2 9 1.63 1.77 -8 2 10 2.26 0.99 -8 2 10 3.19 2.47 -8 2 11 1.69 0.85 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124.40 49.91 0 2 19 57.61 87.50 0 2 20 26.31 12.34 0 2 20 31.11 63.20 0 2 20 30.48 14.72 0 2 20 -3.60 81.34 0 3 0 315.03 123.32 0 3 0 647.40 253.48 0 3 0 301.85 118.19 0 3 0 157.60 61.89 0 3 1 280.69 109.92 0 3 1 149.84 58.75 0 3 1 290.84 113.85 0 3 1 163.36 64.06 0 3 2 21.44 8.48 0 3 2 5.97 3.05 0 3 2 21.26 8.39 0 3 2 6.14 3.18 0 3 3 204.94 80.25 0 3 3 99.19 39.07 0 3 3 194.90 76.32 0 3 3 117.73 46.29 0 3 4 22.40 8.86 0 3 4 27.32 12.10 0 3 4 21.07 8.33 0 3 4 25.46 10.70 0 3 5 307.61 120.47 0 3 5 510.96 200.72 0 3 5 279.89 109.63 0 3 5 374.98 146.99 0 3 6 7.44 23.60 0 3 6 2.34 1.28 0 3 10 49.39 19.47 0 3 10 79.06 130.05 0 3 10 72.84 28.73 0 3 10 41.20 25.20 0 3 11 4.38 2.16 0 3 11 -51.58 217.95 0 3 11 7.13 3.35 0 3 11 10.82 26.22 0 3 12 1.54 1.55 0 3 12 58.35 302.99 0 3 12 6.54 3.33 0 3 12 3.34 29.59 0 3 13 13.95 5.90 0 3 13 -97.99 390.95 0 3 13 19.66 8.28 0 3 13 15.95 47.63 0 3 14 29.59 11.94 0 3 14 47.12 62.34 0 3 15 3.96 2.80 0 3 15 34.99 186.18 0 3 15 3.34 3.58 0 3 15 10.29 55.80 0 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81.97 32.20 0 4 8 80.65 32.76 0 4 9 29.95 11.85 0 4 9 38.45 15.25 0 4 12 -22.55 307.96 0 4 12 28.20 27.83 0 4 13 -3.30 321.25 0 4 14 21.91 8.94 0 4 14 54.79 176.08 0 4 14 38.26 15.62 0 4 14 19.59 39.27 0 4 15 72.15 28.55 0 4 15 79.46 225.65 0 4 15 113.28 44.89 0 4 15 99.76 57.67 0 4 16 14.47 6.27 0 4 16 -28.96 261.58 0 4 16 18.86 8.70 0 4 16 11.12 41.02 0 4 17 9.34 4.59 0 4 17 -9.18 111.45 0 4 17 15.44 7.96 0 4 17 19.05 47.26 0 4 18 -0.14 2.68 0 4 18 -0.30 73.92 0 4 18 -0.33 5.17 0 4 18 4.02 51.70 0 4 19 8.65 5.40 0 4 19 -13.95 33.36 0 4 19 1.75 6.78 0 4 19 6.82 56.66 0 4 20 8.85 5.50 0 4 20 2.61 39.44 0 4 20 8.80 8.25 0 4 20 8.04 56.46 0 5 0 206.48 80.88 0 5 0 425.97 167.12 0 5 0 198.33 77.69 0 5 0 64.17 26.25 0 5 1 12.77 5.10 0 5 1 15.86 7.26 0 5 1 11.12 4.46 0 5 1 20.35 10.40 0 5 2 792.28 310.12 0 5 2 747.79 292.95 0 5 2 768.32 300.77 0 5 2 701.01 274.53 0 5 3 105.01 41.16 0 5 3 257.25 101.02 0 5 3 115.73 45.36 0 5 3 219.77 86.36 0 5 5 3.64 1.63 0 5 5 37.52 15.81 0 5 5 4.39 1.93 0 5 5 39.98 16.54 0 5 6 89.44 35.08 0 5 6 225.99 90.24 0 5 6 90.86 35.66 0 5 6 187.55 74.15 0 5 7 80.54 31.61 0 5 7 448.16 179.05 0 5 7 105.64 41.45 0 5 7 271.34 107.01 0 5 8 28.63 11.33 0 5 8 41.15 42.38 0 5 8 31.87 12.63 0 5 8 37.70 16.70 0 5 9 42.24 16.66 0 5 9 -12.94 100.10 0 5 9 52.56 20.73 0 5 9 69.30 29.34 0 5 10 21.73 8.68 0 5 10 0.98 54.38 0 5 10 23.25 9.37 0 5 10 22.52 14.30 0 5 11 21.92 8.82 0 5 11 -3.20 97.14 0 5 11 33.02 13.26 0 5 11 28.75 18.74 0 5 12 1.13 1.35 0 5 12 2.24 2.35 0 5 14 -102.90 247.95 0 5 15 -250.92 376.35 0 5 15 1.75 25.70 0 5 16 40.89 16.35 0 5 16 51.31 20.96 0 5 16 49.06 40.17 0 5 17 5.07 3.20 0 5 17 -21.62 65.31 0 5 17 7.77 5.61 0 5 17 -7.23 33.35 0 5 19 2.43 3.95 0 5 19 7.16 7.89 0 5 19 5.37 48.06 0 6 0 576.10 225.59 0 6 0 1105.99 433.39 0 6 0 573.82 224.56 0 6 0 296.55 117.39 0 6 1 14.70 7.55 0 6 1 10.99 4.40 0 6 3 78.94 30.96 0 6 3 57.15 23.03 0 6 3 73.87 28.98 0 6 3 43.94 18.29 0 6 4 11.64 4.67 0 6 4 6.15 6.02 0 6 4 13.07 5.25 0 6 4 5.41 6.25 0 6 5 29.27 11.55 0 6 5 24.36 11.54 0 6 5 29.48 11.64 0 6 5 22.84 11.03 0 6 6 146.99 57.61 0 6 6 265.06 104.90 0 6 6 147.73 57.89 0 6 6 260.33 102.67 0 6 7 94.69 37.16 0 6 7 195.42 79.17 0 6 7 103.13 40.48 0 6 7 169.24 67.25 0 6 8 60.52 23.81 0 6 8 244.70 106.55 0 6 8 74.66 29.36 0 6 8 143.85 57.67 0 6 9 14.98 6.07 0 6 9 5.05 49.76 0 6 9 15.75 6.45 0 6 9 16.67 12.46 0 6 10 22.70 9.10 0 6 10 -17.86 128.74 0 6 10 23.04 9.37 0 6 10 28.87 18.45 0 6 11 1.22 1.27 0 6 11 5.80 99.25 0 6 11 1.65 2.05 0 6 11 6.92 17.13 0 6 12 0.60 1.33 0 6 12 7.82 107.58 0 6 12 2.11 2.42 0 6 12 -4.08 21.15 0 6 13 0.10 1.57 0 6 13 -18.79 160.51 0 6 13 0.78 2.59 0 6 13 3.84 24.06 0 6 14 -0.37 1.70 0 6 14 1.00 3.29 0 6 14 16.49 29.15 0 6 15 45.28 18.05 0 6 15 80.82 32.30 0 6 16 42.39 124.06 0 6 18 7.34 4.81 0 6 18 -9.83 22.95 0 6 18 -1.57 45.27 0 7 0 59.32 23.28 0 7 0 159.03 63.37 0 7 0 52.99 20.80 0 7 0 18.32 20.33 0 7 1 11.22 4.50 0 7 1 19.22 10.19 0 7 1 10.21 4.11 0 7 1 31.55 19.83 0 7 2 157.31 61.66 0 7 2 139.18 55.34 0 7 2 165.36 64.80 0 7 2 177.74 72.38 0 7 3 403.27 157.88 0 7 3 538.74 211.44 0 7 3 429.79 168.27 0 7 3 460.02 180.99 0 7 4 32.92 12.99 0 7 4 50.84 21.31 0 7 4 35.36 13.95 0 7 4 44.06 19.29 0 7 5 63.66 25.01 0 7 5 113.79 45.49 0 7 5 74.49 29.26 0 7 5 114.19 45.96 0 7 6 7.23 3.02 0 7 6 6.76 7.82 0 7 6 7.68 3.26 0 7 6 15.62 9.42 0 7 7 47.23 18.60 0 7 7 48.00 23.98 0 7 7 44.36 17.51 0 7 7 54.08 23.56 0 7 8 61.49 24.21 0 7 8 103.87 49.87 0 7 8 64.63 25.46 0 7 8 105.18 43.90 0 7 9 1.23 1.14 0 7 9 -3.32 64.91 0 7 9 1.68 1.81 0 7 9 11.63 16.94 0 7 10 16.55 6.72 0 7 10 13.14 99.08 0 7 10 3.58 173.11 0 7 10 21.65 8.89 0 7 10 30.46 22.06 0 7 11 68.62 27.04 0 7 11 -25.41 177.56 0 7 11 102.16 40.27 0 7 11 222.62 92.92 0 7 12 9.38 4.15 0 7 12 22.06 80.31 0 7 12 15.28 6.72 0 7 12 5.26 24.30 0 7 13 1.15 1.71 0 7 13 -23.25 86.76 0 7 13 3.41 3.44 0 7 13 3.40 25.23 0 7 14 10.11 4.48 0 7 14 33.09 224.85 0 7 14 13.27 6.45 0 7 14 17.73 31.57 0 7 15 10.06 4.61 0 7 15 -82.02 140.09 0 7 15 13.92 7.02 0 7 15 13.82 33.74 0 7 16 -0.40 2.16 0 7 16 0.83 4.37 0 7 16 -20.69 40.25 0 7 17 69.87 27.98 0 7 17 100.50 40.70 0 7 17 90.06 63.14 0 7 18 4.94 4.46 0 7 18 15.89 10.08 0 8 0 117.33 46.00 0 8 0 113.11 46.20 0 8 0 97.71 38.32 0 8 0 13.07 27.29 0 8 1 37.50 14.77 0 8 1 26.67 13.65 0 8 1 30.02 11.85 0 8 1 20.39 24.35 0 8 2 11.03 4.44 0 8 2 11.03 8.70 0 8 2 11.13 4.51 0 8 2 77.06 41.83 0 8 3 50.92 20.02 0 8 3 62.80 26.16 0 8 3 52.47 20.64 0 8 3 63.20 32.73 0 8 4 212.98 83.45 0 8 4 310.18 122.35 0 8 4 233.98 91.66 0 8 4 326.72 129.42 0 8 5 142.54 55.90 0 8 5 231.07 91.60 0 8 5 146.25 57.32 0 8 5 169.01 67.48 0 8 6 11.65 4.75 0 8 6 28.05 14.57 0 8 6 13.88 5.66 0 8 6 33.30 17.91 0 8 7 65.37 25.72 0 8 7 150.13 61.49 0 8 7 66.79 26.29 0 8 7 173.00 70.22 0 8 8 18.58 7.48 0 8 8 77.92 41.78 0 8 8 22.71 9.17 0 8 8 71.81 34.59 0 8 9 373.49 163.36 0 8 9 159.31 62.57 0 8 10 0.99 1.27 0 8 10 24.34 82.02 0 8 10 1.51 2.05 0 8 10 6.34 30.09 0 8 11 19.99 8.14 0 8 11 -27.70 139.86 0 8 11 26.43 10.89 0 8 11 44.10 32.45 0 8 12 1.81 1.73 0 8 12 20.42 127.88 0 8 12 2.19 3.17 0 8 12 -2.95 28.01 0 8 13 44.97 17.86 0 8 13 -40.81 113.91 0 8 13 70.50 28.16 0 8 13 78.37 43.53 0 8 14 13.18 5.66 0 8 14 9.30 80.82 0 8 14 24.12 10.58 0 8 14 24.49 34.79 0 8 15 3.22 2.37 0 8 15 -38.09 85.50 0 8 15 4.99 5.05 0 8 15 -10.20 36.33 0 8 16 20.69 8.87 0 8 16 23.29 46.95 0 8 17 -0.13 3.09 0 8 17 -2.41 27.32 0 8 17 2.12 6.36 0 8 17 -9.22 45.79 0 9 0 38.59 15.20 0 9 0 16.76 13.31 0 9 0 33.32 13.15 0 9 0 15.26 50.84 0 9 1 7.60 3.13 0 9 1 2.19 10.55 0 9 1 6.13 2.63 0 9 1 13.87 33.00 0 9 2 17.29 6.88 0 9 2 10.51 10.50 0 9 2 17.69 7.07 0 9 2 21.04 34.39 0 9 3 52.63 20.71 0 9 3 58.75 25.44 0 9 3 54.52 21.46 0 9 3 27.00 32.82 0 9 4 123.95 48.63 0 9 4 179.33 71.76 0 9 4 127.83 50.17 0 9 4 182.64 78.71 0 9 5 80.94 31.81 0 9 5 101.93 42.00 0 9 5 84.36 33.16 0 9 5 101.24 46.50 0 9 6 16.11 6.49 0 9 6 24.79 16.11 0 9 6 16.76 6.83 0 9 6 21.44 23.77 0 9 7 7.79 3.33 0 9 7 9.66 15.04 0 9 7 8.16 3.57 0 9 7 30.38 26.46 0 9 9 0.42 1.20 0 9 9 -20.43 46.50 0 9 9 0.87 1.82 0 9 9 0.60 33.43 0 9 10 1.50 1.56 0 9 10 -3.94 65.60 0 9 10 1.19 2.35 0 9 10 2.12 24.95 0 9 11 4.25 2.35 0 9 11 8.15 61.89 0 9 11 -46.24 112.14 0 9 11 5.38 3.73 0 9 11 -1.61 30.51 0 9 12 0.62 1.46 0 9 12 -69.99 203.52 0 9 12 -0.89 3.24 0 9 12 -1.50 29.62 0 9 13 0.09 1.52 0 9 13 0.44 3.71 0 9 13 1.05 38.26 0 9 14 47.07 18.75 0 9 14 10.44 74.72 0 9 14 76.78 30.97 0 9 14 77.46 55.15 0 9 15 1.47 2.20 0 9 16 13.43 6.21 0 9 16 -4.79 36.39 0 9 16 23.04 11.98 0 9 16 13.48 58.24 0 10 0 121.72 47.74 0 10 0 151.44 62.91 0 10 0 116.47 45.69 0 10 1 16.08 6.47 0 10 1 14.21 17.86 0 10 1 15.32 6.18 0 10 1 11.73 78.03 0 10 2 87.61 34.41 0 10 2 78.60 35.43 0 10 2 79.63 31.28 0 10 2 73.01 66.17 0 10 3 1.74 1.07 0 10 3 5.89 13.55 0 10 3 2.45 1.48 0 10 3 12.87 66.51 0 10 4 8.65 3.59 0 10 4 33.29 19.67 0 10 4 12.96 5.39 0 10 4 124.52 87.56 0 10 5 3.44 1.70 0 10 5 10.30 14.08 0 10 5 3.52 2.02 0 10 5 21.34 52.07 0 10 7 8.18 3.50 0 10 7 15.23 20.35 0 10 7 9.58 4.20 0 10 7 18.48 47.38 0 10 8 9.67 4.12 0 10 8 -4.24 26.65 0 10 8 7.89 3.70 0 10 8 26.40 33.90 0 10 9 77.29 30.45 0 10 9 97.48 54.75 0 10 9 92.40 36.47 0 10 9 122.52 57.89 0 10 10 -0.12 1.33 0 10 10 2.86 45.62 0 10 10 1.04 2.59 0 10 10 7.59 31.12 0 10 11 0.58 1.53 0 10 11 -11.76 100.79 0 10 11 0.19 3.07 0 10 11 -10.92 31.83 0 10 12 0.12 1.69 0 10 12 28.30 79.74 0 10 12 -6.97 140.49 0 10 12 0.84 3.50 0 10 12 -4.42 40.95 0 10 13 59.83 23.72 0 10 13 -10.20 143.57 0 10 13 96.40 38.50 0 10 13 126.29 72.84 0 10 14 15.43 6.70 0 10 14 12.39 55.05 0 10 15 24.94 10.40 0 10 15 -13.35 40.47 0 10 15 56.34 24.01 0 10 15 31.02 64.80 0 11 0 1.93 1.18 0 11 0 4.01 27.84 0 11 0 1.37 1.23 0 11 0 47.27 111.40 0 11 1 8.16 3.43 0 11 1 -1.20 23.02 0 11 1 5.82 2.68 0 11 1 -12.39 140.26 0 11 2 -0.09 0.86 0 11 2 -3.37 23.55 0 11 2 0.09 1.16 0 11 2 -43.30 107.35 0 11 3 17.47 7.03 0 11 3 65.42 37.91 0 11 3 18.60 7.50 0 11 3 8.86 94.00 0 11 5 5.43 2.46 0 11 5 28.63 23.79 0 11 5 8.23 3.72 0 11 5 57.95 113.62 0 11 6 3.95 1.95 0 11 6 10.36 19.82 0 11 6 5.79 2.95 0 11 6 15.50 74.95 0 11 7 3.18 1.77 0 11 7 4.66 18.47 0 11 7 3.42 2.39 0 11 7 4.93 46.20 0 11 8 36.05 14.35 0 11 8 43.24 32.30 0 11 8 38.07 15.26 0 11 8 53.51 48.61 0 11 9 0.98 1.33 0 11 9 26.11 41.98 0 11 9 1.03 2.10 0 11 9 1.14 35.99 0 11 10 -0.22 1.41 0 11 10 -25.09 50.01 0 11 10 0.70 2.71 0 11 10 -10.01 42.97 0 11 11 3.27 2.17 0 11 11 -12.51 73.41 0 11 11 4.21 4.15 0 11 11 10.18 42.08 0 11 12 12.98 5.54 0 11 12 22.56 74.95 0 11 12 -38.05 132.67 0 11 12 27.65 12.15 0 11 12 16.83 64.68 0 11 13 9.35 4.47 0 11 13 -14.33 139.00 0 11 13 19.52 10.40 0 11 13 37.11 60.40 0 11 14 5.17 3.43 0 11 14 12.50 9.24 0 11 14 15.35 65.60 0 12 1 10.99 4.55 0 12 2 5.27 2.51 0 12 2 3.02 1.77 0 12 2 -79.00 207.22 0 12 3 38.84 15.41 0 12 3 94.69 50.16 0 12 3 35.52 14.13 0 12 3 27.46 156.34 0 12 4 0.45 1.03 0 12 4 14.41 20.10 0 12 4 3.18 2.27 0 12 4 -24.36 129.25 0 12 5 2.12 1.38 0 12 5 2.87 18.87 0 12 5 1.35 1.93 0 12 5 -19.91 116.47 0 12 6 48.67 19.26 0 12 6 55.80 32.26 0 12 6 58.86 23.34 0 12 6 51.19 83.33 0 12 7 38.05 15.12 0 12 7 50.61 31.63 0 12 7 43.34 17.28 0 12 7 45.92 69.07 0 12 8 13.58 5.65 0 12 8 10.84 30.74 0 12 8 13.30 5.79 0 12 8 -9.64 57.00 0 12 9 1.41 1.47 0 12 9 -12.51 36.41 0 12 9 2.37 2.73 0 12 9 19.22 62.34 0 12 10 -0.09 1.43 0 12 10 14.43 52.22 0 12 10 0.31 3.24 0 12 10 11.63 52.92 0 12 12 17.27 7.32 0 12 12 5.78 79.85 0 12 12 33.68 15.30 0 12 12 7.20 65.25 0 13 0 61.15 24.10 0 13 0 56.05 45.45 0 13 0 53.52 21.16 0 13 0 40.20 160.68 0 13 1 1.33 1.27 0 13 1 11.36 33.08 0 13 1 1.97 1.74 0 13 1 -15.94 138.21 0 13 2 127.14 49.94 0 13 2 221.43 94.17 0 13 2 109.57 43.08 0 13 2 -7.79 166.78 0 13 3 107.06 42.10 0 13 3 166.33 74.09 0 13 3 102.67 40.41 0 13 3 12.94 109.12 0 13 4 2.91 1.81 0 13 4 11.88 22.11 0 13 4 3.58 2.49 0 13 4 20.22 98.85 0 13 5 21.17 8.54 0 13 5 36.07 28.41 0 13 5 24.36 9.91 0 13 5 -17.13 97.88 0 13 6 22.48 9.09 0 13 6 58.64 35.91 0 13 6 30.59 12.38 0 13 6 23.24 122.81 0 13 7 4.38 2.28 0 13 7 4.46 24.26 0 13 7 4.53 2.96 0 13 7 68.68 121.21 0 13 8 33.39 13.35 0 13 8 32.86 36.88 0 13 8 40.42 16.28 0 13 8 64.00 83.11 0 13 9 1.32 1.54 0 13 9 1.17 43.64 0 13 9 0.48 2.94 0 13 9 9.84 63.83 0 13 10 37.55 15.02 0 13 10 27.70 56.36 0 13 10 63.49 25.83 0 13 10 -11.92 78.83 0 13 11 3.79 2.48 0 13 11 4.70 60.12 0 13 11 5.13 6.68 0 13 11 -12.54 70.04 0 14 0 43.69 17.31 0 14 0 26.61 43.15 0 14 0 40.88 16.27 0 14 0 22.82 90.35 0 14 1 0.79 1.28 0 14 1 7.90 38.12 0 14 1 1.30 1.69 0 14 1 28.28 115.96 0 14 2 10.24 4.36 0 14 2 26.67 34.78 0 14 2 7.67 3.52 0 14 2 -10.97 138.09 0 14 3 0.90 1.34 0 14 3 6.14 32.14 0 14 3 1.51 2.03 0 14 3 62.06 191.94 0 14 4 3.66 2.11 0 14 4 5.72 25.20 0 14 4 3.68 2.73 0 14 4 -35.27 181.96 0 14 5 6.02 2.93 0 14 5 1.14 26.79 0 14 5 6.17 3.55 0 14 5 0.92 103.93 0 14 6 0.18 1.26 0 14 6 -4.90 27.54 0 14 6 1.07 2.47 0 14 6 -6.43 85.79 0 14 7 9.71 4.23 0 14 7 9.99 33.94 0 14 7 12.68 5.92 0 14 7 -12.83 66.96 0 14 8 10.75 4.67 0 14 8 11.46 44.27 0 14 8 14.76 7.31 0 14 8 32.95 107.23 0 14 9 13.66 5.78 0 14 9 14.68 46.42 0 14 9 28.31 12.47 0 14 9 23.26 71.53 0 15 0 8.35 3.65 0 15 0 -11.62 51.43 0 15 0 6.75 3.40 0 15 0 -36.46 276.98 0 15 1 11.37 4.81 0 15 1 -3.69 47.12 0 15 1 11.56 5.09 0 15 1 -56.79 120.64 0 15 2 6.75 3.21 0 15 2 4.93 39.61 0 15 2 6.63 3.38 0 15 2 24.77 84.65 0 15 3 13.20 5.55 0 15 3 18.25 33.83 0 15 3 14.04 6.14 0 15 3 44.68 119.04 0 15 4 3.26 2.02 0 15 4 28.42 38.31 0 15 4 3.74 2.99 0 15 4 4.13 86.59 0 15 6 2.95 2.03 0 15 6 4.63 34.87 0 15 6 5.64 4.49 0 15 6 -13.63 113.34 0 15 7 40.43 16.12 0 15 7 41.77 40.63 0 15 7 68.45 27.58 0 15 7 9.44 71.24 0 16 0 49.50 19.59 0 16 0 65.42 87.78 0 16 0 41.10 16.40 0 16 0 23.04 86.70 0 16 1 60.35 73.12 0 16 1 36.16 14.57 0 16 1 25.71 79.68 0 16 3 4.15 2.24 0 16 3 7.34 38.84 0 16 3 4.64 3.72 0 16 4 0.21 1.37 0 16 4 2.26 36.97 0 16 4 1.78 3.80 0 16 4 13.67 115.45 0 17 0 18.49 7.60 0 17 0 -64.00 89.38 0 17 0 19.17 8.33 0 17 0 -59.55 121.89 0 17 1 13.39 5.65 0 17 1 33.17 67.48 0 17 1 14.64 6.61 0 17 1 -20.16 114.14 1 -17 0 0.52 2.63 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3 3.62 102.67 1 -16 3 53.19 21.04 1 -16 3 -12.29 67.88 1 -16 4 8.22 3.74 1 -16 4 6.99 89.95 1 -16 4 13.33 5.54 1 -16 4 1.01 92.69 1 -16 5 7.72 3.54 1 -16 5 9.99 78.77 1 -16 5 9.91 4.20 1 -16 5 25.11 107.23 1 -16 6 3.39 2.04 1 -16 6 13.11 70.16 1 -16 6 8.62 3.69 1 -16 6 24.81 104.44 1 -16 7 5.99 2.92 1 -16 7 -15.54 69.42 1 -16 7 14.43 5.92 1 -16 7 4.40 90.46 1 -16 8 14.27 5.98 1 -16 8 -0.72 59.55 1 -16 8 25.67 10.27 1 -16 8 13.29 73.07 1 -16 10 2.81 1.59 1 -16 11 0.73 1.44 1 -16 11 11.26 28.31 1 -16 11 0.85 0.98 1 -16 11 24.53 147.73 1 -16 12 6.66 3.17 1 -16 12 1.03 27.41 1 -16 12 10.29 4.32 1 -16 12 -43.85 110.60 1 -15 0 37.14 14.88 1 -15 0 28.83 271.39 1 -15 0 40.17 15.94 1 -15 0 29.36 56.21 1 -15 1 50.19 19.92 1 -15 1 -2.26 243.05 1 -15 1 61.72 24.35 1 -15 1 12.79 61.15 1 -15 2 10.26 4.47 1 -15 2 -72.10 202.55 1 -15 2 11.92 4.99 1 -15 2 -14.33 58.47 1 -15 3 20.91 8.49 1 -15 3 28.55 11.42 1 -15 3 33.40 70.79 1 -15 4 16.66 6.83 1 -15 4 62.40 127.25 1 -15 4 26.24 10.51 1 -15 4 10.24 107.86 1 -15 5 6.05 2.86 1 -15 5 -7.30 89.55 1 -15 5 10.76 4.50 1 -15 5 -28.20 133.13 1 -15 6 0.67 1.34 1 -15 6 -20.15 77.40 1 -15 6 -0.01 0.94 1 -15 6 50.94 172.49 1 -15 7 82.94 32.67 1 -15 7 -20.03 79.28 1 -15 7 115.28 45.29 1 -15 7 13.65 186.58 1 -15 8 97.37 38.32 1 -15 8 70.79 82.19 1 -15 8 125.77 49.40 1 -15 9 3.10 1.90 1 -15 9 20.45 60.01 1 -15 9 3.46 1.77 1 -15 9 -8.22 165.19 1 -15 10 0.13 1.28 1 -15 10 5.48 47.02 1 -15 10 0.23 0.87 1 -15 10 13.49 113.05 1 -15 11 1.79 1.52 1 -15 11 7.65 37.58 1 -15 11 3.38 1.69 1 -15 11 20.52 90.81 1 -15 12 0.40 1.30 1 -15 12 -11.03 92.12 1 -15 13 26.84 10.77 1 -15 13 14.37 23.80 1 -15 13 42.39 16.79 1 -15 13 -23.73 140.09 1 -15 14 0.87 1.34 1 -15 14 -11.52 26.25 1 -15 14 -0.03 0.82 1 -15 14 39.25 172.94 1 -15 14 1.15 45.27 1 -14 0 29.79 11.95 1 -14 0 -0.67 78.09 1 -14 0 35.91 14.25 1 -14 0 16.81 47.30 1 -14 1 9.43 4.14 1 -14 1 6.78 91.38 1 -14 1 11.76 4.87 1 -14 1 -12.82 50.66 1 -14 2 47.22 18.70 1 -14 2 29.10 106.49 1 -14 2 59.49 23.46 1 -14 2 7.39 56.07 1 -14 3 0.38 1.18 1 -14 3 0.26 0.97 1 -14 3 -14.60 90.18 1 -14 4 18.81 7.61 1 -14 4 -12.47 108.66 1 -14 4 28.18 11.22 1 -14 4 -24.64 111.23 1 -14 5 0.19 1.17 1 -14 5 16.26 105.35 1 -14 5 0.82 0.95 1 -14 5 -2.61 124.46 1 -14 6 3.40 1.92 1 -14 6 -8.62 113.68 1 -14 6 5.69 2.53 1 -14 6 39.52 112.65 1 -14 7 31.72 12.63 1 -14 7 32.84 108.03 1 -14 7 41.96 16.59 1 -14 8 1.77 1.43 1 -14 8 1.94 78.09 1 -14 8 1.51 1.08 1 -14 8 15.04 157.60 1 -14 9 1.69 1.44 1 -14 9 -29.15 57.10 1 -14 9 2.63 1.46 1 -14 9 28.60 155.38 1 -14 10 119.67 47.01 1 -14 10 50.15 52.16 1 -14 10 153.55 60.23 1 -14 10 12.71 211.33 1 -14 11 227.99 89.38 1 -14 11 101.81 63.43 1 -14 11 317.60 124.46 1 -14 11 91.15 423.00 1 -14 12 4.03 2.09 1 -14 12 -2.82 30.57 1 -14 12 11.84 4.84 1 -14 12 29.13 157.20 1 -14 13 35.68 14.19 1 -14 13 16.31 29.46 1 -14 13 61.20 24.12 1 -14 13 -4.52 155.60 1 -14 14 13.96 116.82 1 -14 14 8.56 64.63 1 -14 15 0.65 1.26 1 -14 15 -3.28 20.15 1 -14 15 0.20 0.84 1 -14 15 -36.38 117.56 1 -14 15 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350.39 195.19 1 -13 11 10.43 4.35 1 -13 11 24.64 29.13 1 -13 11 10.03 4.12 1 -13 11 6.78 204.71 1 -13 12 10.20 4.31 1 -13 12 23.39 28.17 1 -13 12 8.84 3.70 1 -13 12 -32.62 264.89 1 -13 13 22.79 9.16 1 -13 13 26.20 40.38 1 -13 13 41.19 16.30 1 -13 13 -44.25 389.06 1 -13 13 20.29 90.52 1 -13 14 105.41 41.45 1 -13 14 74.09 40.02 1 -13 14 169.18 66.34 1 -13 14 -11.49 93.89 1 -13 14 1.80 47.93 1 -13 15 2.22 1.48 1 -13 15 7.85 25.41 1 -13 15 9.97 4.16 1 -13 15 9.85 87.67 1 -13 15 20.32 179.62 1 -13 16 6.21 2.95 1 -13 16 7.27 17.32 1 -13 16 19.31 7.80 1 -13 16 -5.84 108.55 1 -13 17 6.15 2.90 1 -13 17 5.89 12.17 1 -12 0 34.42 55.43 1 -12 1 109.97 43.17 1 -12 1 129.19 156.69 1 -12 1 81.00 64.97 1 -12 2 45.90 18.12 1 -12 2 36.32 164.33 1 -12 2 60.12 23.67 1 -12 2 17.60 85.96 1 -12 3 2.09 1.32 1 -12 3 7.74 137.18 1 -12 3 2.53 1.40 1 -12 3 32.99 110.31 1 -12 4 2.17 1.37 1 -12 4 -9.50 110.37 1 -12 4 1.29 1.12 1 -12 4 -24.73 105.58 1 -12 5 118.64 46.58 1 -12 5 37.42 80.08 1 -12 5 -5.72 111.80 1 -12 7 11.90 73.35 1 -12 7 1.96 1.16 1 -12 8 2.98 1.59 1 -12 8 -2.57 76.32 1 -12 8 1.35 0.98 1 -12 8 7.47 263.58 1 -12 9 21.09 8.43 1 -12 9 4.63 40.79 1 -12 9 26.92 10.70 1 -12 9 -74.61 394.83 1 -12 10 2.34 1.40 1 -12 10 8.07 27.99 1 -12 10 2.54 1.32 1 -12 11 38.35 15.18 1 -12 11 19.36 24.52 1 -12 11 62.52 24.60 1 -12 11 -37.45 198.95 1 -12 12 9.95 4.17 1 -12 12 -2.40 19.94 1 -12 12 27.37 10.87 1 -12 12 31.09 90.06 1 -12 13 38.46 15.24 1 -12 13 29.64 24.83 1 -12 13 65.14 25.64 1 -12 13 -1.73 134.78 1 -12 13 -139.58 344.57 1 -12 14 0.27 1.09 1 -12 14 12.35 28.63 1 -12 14 0.57 0.78 1 -12 14 -1.39 122.81 1 -12 14 65.65 249.32 1 -12 15 55.16 21.79 1 -12 15 57.72 31.51 1 -12 15 89.49 35.19 1 -12 15 8.48 96.05 1 -12 15 -3.36 129.14 1 -12 16 49.86 19.71 1 -12 16 40.39 21.14 1 -12 16 23.51 74.78 1 -12 17 -0.28 9.79 1 -12 17 -20.46 82.08 1 -12 18 -0.15 1.16 1 -12 18 3.12 9.17 1 -12 18 -2.64 23.84 1 -11 1 30.85 12.23 1 -11 1 38.70 15.28 1 -11 2 9.43 3.89 1 -11 2 -11.11 97.88 1 -11 2 10.19 4.16 1 -11 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24.60 1 0 6 51.89 20.38 1 0 6 38.64 24.62 1 0 7 290.10 113.62 1 0 7 1239.47 490.48 1 0 7 377.09 147.67 1 0 7 1140.79 449.30 1 0 8 459.00 179.73 1 0 8 1549.76 610.89 1 0 9 153.32 60.12 1 0 9 444.56 236.20 1 0 9 226.62 88.87 1 0 9 451.35 196.44 1 0 10 236.60 92.75 1 0 10 522.20 274.36 1 0 10 -147.28 360.03 1 0 10 307.56 120.58 1 0 10 540.51 229.53 1 0 11 12.12 5.13 1 0 11 -7.22 193.93 1 0 11 -13.81 392.32 1 0 11 10.79 5.05 1 0 12 48.72 19.30 1 0 12 56.38 350.22 1 0 12 -85.84 606.33 1 0 12 61.03 24.26 1 0 12 7.28 62.34 1 0 13 42.22 16.83 1 0 13 -194.85 428.19 1 0 13 125.26 604.05 1 0 13 46.33 18.66 1 0 13 -0.23 62.00 1 0 14 73.30 29.03 1 0 14 33.04 378.17 1 0 14 -26.96 490.37 1 0 14 92.57 36.78 1 0 14 41.27 223.54 1 0 14 -2.68 93.60 1 0 15 107.35 42.37 1 0 15 136.38 54.10 1 0 15 19.99 83.68 1 0 16 27.36 11.44 1 0 16 -80.20 257.59 1 0 16 27.25 12.47 1 0 16 45.65 189.83 1 0 16 13.99 63.77 1 0 17 63.31 25.38 1 0 17 74.15 306.53 1 0 17 58.81 24.32 1 0 17 1.40 145.51 1 0 18 231.58 91.15 1 0 18 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71.41 1 1 11 44.19 17.46 1 1 11 50.53 199.81 1 1 11 65.94 26.07 1 1 11 6.15 118.64 1 1 12 122.29 48.04 1 1 12 92.63 296.72 1 1 12 176.19 69.25 1 1 12 -37.57 119.50 1 1 13 8.31 3.87 1 1 13 -50.64 394.94 1 1 13 6.62 3.72 1 1 13 16.38 180.76 1 1 14 13.46 5.94 1 1 14 32.93 279.21 1 1 14 60.86 449.70 1 1 14 16.87 7.63 1 1 15 19.09 8.11 1 1 15 -57.95 176.54 1 1 15 26.14 11.48 1 1 16 14.90 6.65 1 1 16 67.31 215.49 1 1 16 -33.08 308.36 1 1 16 16.88 8.55 1 1 17 5.43 4.01 1 1 17 -55.64 310.07 1 1 17 85.22 418.67 1 1 17 6.18 5.74 1 1 17 -29.65 94.17 1 1 18 100.33 39.91 1 1 18 99.13 40.02 1 1 18 50.19 106.72 1 1 19 2.53 4.74 1 1 19 7.01 91.60 1 1 19 1.46 6.59 1 1 19 -43.12 103.98 1 1 20 99.53 40.24 1 1 20 -27.98 79.34 1 1 20 58.81 25.23 1 1 20 89.67 109.57 1 2 0 26.27 10.32 1 2 0 5.85 3.03 1 2 0 21.03 8.27 1 2 0 4.25 2.98 1 2 1 151.72 59.43 1 2 1 71.13 27.96 1 2 1 144.88 56.74 1 2 1 54.95 21.64 1 2 2 496.41 194.33 1 2 2 345.54 135.35 1 2 2 510.33 199.75 1 2 2 502.80 196.90 1 2 3 71.58 28.06 1 2 3 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3 10 100.90 46.47 1 3 11 171.18 67.13 1 3 11 178.59 274.87 1 3 11 238.03 93.37 1 3 11 338.02 137.92 1 3 12 46.05 18.26 1 3 12 -78.09 409.20 1 3 12 61.94 24.57 1 3 12 90.46 56.54 1 3 13 38.78 15.46 1 3 13 46.89 259.93 1 3 13 44.80 17.97 1 3 13 80.03 64.23 1 3 14 3.55 2.48 1 3 14 84.76 149.21 1 3 14 8.56 4.82 1 3 14 8.44 57.67 1 3 15 3.26 2.66 1 3 15 9.07 204.60 1 3 15 4.99 4.11 1 3 15 -11.06 53.44 1 3 16 0.95 2.54 1 3 16 27.29 295.52 1 3 16 -1.50 4.02 1 3 16 -22.42 52.13 1 3 17 0.01 2.60 1 3 17 -2.52 140.37 1 3 17 0.57 4.82 1 3 17 -11.93 62.69 1 3 18 3.16 3.56 1 3 18 -6.98 71.70 1 3 18 -31.41 100.10 1 3 18 5.72 6.33 1 3 18 -0.28 65.03 1 3 19 10.58 102.44 1 3 20 8.71 6.46 1 3 20 -4.87 45.56 1 3 20 9.48 9.06 1 3 20 0.20 68.10 1 4 0 0.98 0.76 1 4 0 16.11 7.72 1 4 0 0.78 0.64 1 4 0 0.99 6.38 1 4 1 1010.17 395.28 1 4 1 881.83 345.37 1 4 1 855.02 334.59 1 4 1 815.09 319.36 1 4 2 0.68 0.72 1 4 2 4.16 3.02 1 4 2 1.15 0.83 1 4 2 9.92 5.20 1 4 3 141.80 55.54 1 4 3 215.44 84.59 1 4 3 151.55 59.38 1 4 3 276.70 108.55 1 4 4 35.32 13.89 1 4 4 116.47 46.09 1 4 4 36.68 14.43 1 4 4 125.26 49.44 1 4 6 127.77 50.07 1 4 6 256.22 104.50 1 4 6 144.71 56.72 1 4 6 203.86 80.48 1 4 7 95.94 37.62 1 4 7 102.33 54.54 1 4 7 119.95 47.03 1 4 7 171.75 68.16 1 4 8 2.42 1.34 1 4 8 -2.42 61.72 1 4 8 5.89 2.67 1 4 8 10.68 7.96 1 4 9 24.71 9.81 1 4 9 11.15 40.83 1 4 9 35.67 14.19 1 4 9 25.01 13.17 1 4 10 0.42 0.97 1 4 10 -0.38 104.44 1 4 10 0.25 1.43 1 4 10 -4.78 11.19 1 4 11 15.94 6.49 1 4 11 6.41 207.97 1 4 11 17.00 7.03 1 4 11 12.06 17.41 1 4 12 3.11 1.93 1 4 12 -63.54 359.52 1 4 12 2.68 2.37 1 4 12 2.56 23.41 1 4 13 14.80 6.19 1 4 14 47.09 18.74 1 4 14 104.90 41.56 1 4 14 101.07 57.21 1 4 15 5.04 3.04 1 4 15 -24.00 277.33 1 4 15 7.95 4.85 1 4 15 2.75 36.35 1 4 16 99.31 39.15 1 4 16 9.04 230.55 1 4 16 169.41 66.96 1 4 16 172.66 85.96 1 4 17 10.11 4.82 1 4 17 -21.57 80.14 1 4 17 8.90 6.19 1 4 17 11.47 49.48 1 4 18 42.04 17.04 1 4 18 -16.16 75.58 1 4 18 63.09 26.14 1 4 18 48.62 65.71 1 4 19 56.14 22.84 1 4 19 3.60 31.04 1 4 19 63.71 26.95 1 4 19 68.73 64.00 1 5 0 2.15 1.08 1 5 0 33.99 14.36 1 5 0 3.12 1.38 1 5 0 1.92 8.39 1 5 1 69.76 27.36 1 5 1 254.22 99.82 1 5 1 92.35 36.20 1 5 1 284.63 112.08 1 5 2 173.46 67.93 1 5 2 109.23 43.19 1 5 2 162.11 63.49 1 5 2 90.75 36.23 1 5 3 562.18 220.06 1 5 3 727.82 285.14 1 5 3 636.56 249.20 1 5 3 647.97 254.00 1 5 4 74.38 29.17 1 5 4 112.42 44.52 1 5 5 10.99 4.42 1 5 5 34.38 15.97 1 5 5 12.10 4.86 1 5 5 25.19 11.90 1 5 6 12.87 5.16 1 5 6 49.58 24.93 1 5 6 17.92 7.15 1 5 6 36.36 15.75 1 5 7 175.74 68.85 1 5 7 375.78 152.35 1 5 7 206.71 81.00 1 5 7 285.88 112.65 1 5 8 2.56 1.43 1 5 8 34.83 51.06 1 5 8 6.75 3.05 1 5 8 18.14 11.27 1 5 9 135.98 53.33 1 5 9 5.91 105.69 1 5 9 151.95 59.61 1 5 9 194.56 77.80 1 5 10 7.91 3.38 1 5 10 13.90 57.72 1 5 10 9.74 4.23 1 5 10 9.10 11.52 1 5 11 0.45 1.25 1 5 11 -24.85 136.38 1 5 11 0.96 1.88 1 5 11 6.05 14.93 1 5 13 4.41 2.41 1 5 13 37.19 144.14 1 5 13 6.47 3.95 1 5 13 7.91 24.68 1 5 14 14.53 6.18 1 5 14 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10 -75.52 167.47 1 6 10 0.53 1.80 1 6 10 -1.85 14.25 1 6 11 7.08 117.22 1 6 11 3.54 2.53 1 6 12 18.50 7.57 1 6 12 2.65 93.89 1 6 12 25.65 10.60 1 6 12 40.49 31.54 1 6 13 36.29 14.54 1 6 13 -58.81 184.98 1 6 13 51.79 20.81 1 6 13 81.39 43.41 1 6 14 3.02 2.27 1 6 14 -90.75 232.66 1 6 14 4.79 3.97 1 6 14 -15.17 28.60 1 6 15 40.28 16.14 1 6 15 -20.27 143.68 1 6 15 63.49 25.61 1 6 15 67.19 44.85 1 6 16 -0.11 2.08 1 6 16 9.85 74.38 1 6 16 3.26 4.97 1 6 16 -1.70 38.44 1 6 18 7.30 5.09 1 6 18 -3.85 22.31 1 6 18 8.40 7.97 1 6 18 -0.61 45.92 1 7 0 100.56 39.41 1 7 0 157.94 63.03 1 7 0 82.08 32.17 1 7 0 25.79 26.05 1 7 1 1.51 0.86 1 7 1 6.78 6.71 1 7 1 1.87 1.01 1 7 1 37.89 22.75 1 7 2 46.04 18.09 1 7 2 50.15 21.20 1 7 2 45.07 17.71 1 7 2 45.64 25.03 1 7 3 16.09 6.40 1 7 3 26.27 12.27 1 7 3 18.22 7.25 1 7 3 31.86 17.54 1 7 4 20.87 8.28 1 7 4 21.52 10.88 1 7 4 21.72 8.64 1 7 4 17.29 11.29 1 7 5 53.52 21.05 1 7 5 47.39 20.52 1 7 5 53.30 20.97 1 7 5 48.91 21.57 1 7 6 98.96 38.84 1 7 6 198.44 79.28 1 7 6 104.38 40.97 1 7 6 195.36 77.57 1 7 7 42.85 16.91 1 7 7 59.95 30.91 1 7 7 39.97 15.81 1 7 7 63.03 28.10 1 7 8 5.44 2.47 1 7 8 33.45 37.49 1 7 8 7.50 3.39 1 7 8 22.74 16.70 1 7 9 0.40 1.16 1 7 9 11.92 79.00 1 7 9 0.62 1.72 1 7 9 1.84 17.72 1 7 10 31.24 12.69 1 7 11 5.31 2.62 1 7 11 -20.46 153.15 1 7 11 10.67 5.00 1 7 11 16.54 26.86 1 7 12 4.82 2.65 1 7 12 20.81 74.44 1 7 12 5.15 3.40 1 7 12 2.02 22.58 1 7 13 48.91 19.46 1 7 13 3.12 95.77 1 7 13 69.30 27.73 1 7 13 90.01 47.43 1 7 14 7.61 3.72 1 7 14 28.24 178.02 1 7 14 18.51 8.48 1 7 14 8.62 33.25 1 7 15 88.92 35.15 1 7 15 7.76 74.55 1 7 15 120.07 47.76 1 7 15 150.47 73.81 1 7 16 26.16 10.84 1 7 16 -16.91 71.47 1 7 16 36.19 15.65 1 7 16 55.43 54.76 1 7 17 10.79 5.69 1 7 17 3.68 27.29 1 7 17 20.40 10.98 1 7 17 33.97 51.25 1 8 0 7.74 3.16 1 8 0 24.44 14.33 1 8 0 6.73 2.77 1 8 0 13.72 41.83 1 8 1 17.51 6.95 1 8 1 18.90 11.13 1 8 1 17.58 6.99 1 8 1 11.95 31.56 1 8 2 81.51 31.98 1 8 2 108.38 43.80 1 8 2 82.36 32.32 1 8 2 80.20 45.46 1 8 3 99.76 39.12 1 8 3 142.60 57.10 1 8 3 107.35 42.10 1 8 3 176.94 75.35 1 8 4 15.82 6.31 1 8 4 82.82 34.12 1 8 4 23.90 9.49 1 8 4 95.60 40.70 1 8 5 29.89 11.82 1 8 5 26.28 14.04 1 8 5 29.26 11.61 1 8 5 26.15 16.96 1 8 6 89.72 35.24 1 8 6 110.94 45.50 1 8 6 89.72 35.24 1 8 6 132.10 54.50 1 8 7 71.41 28.09 1 8 7 153.89 65.31 1 8 7 80.43 31.65 1 8 7 168.95 70.04 1 8 8 2.34 1.49 1 8 8 18.10 37.73 1 8 8 3.12 1.97 1 8 8 7.88 24.30 1 8 10 14.68 6.05 1 8 10 3.10 79.63 1 8 10 30.66 160.68 1 8 10 17.01 7.23 1 8 10 47.65 37.43 1 8 11 34.50 13.78 1 8 11 -55.43 126.91 1 8 11 37.27 15.10 1 8 11 48.53 33.66 1 8 12 -0.02 1.45 1 8 12 0.23 3.06 1 8 12 -0.67 30.53 1 8 13 29.10 11.73 1 8 13 -30.66 94.69 1 8 13 38.28 15.77 1 8 13 27.63 34.67 1 8 14 28.34 11.49 1 8 14 -5.96 71.36 1 8 14 46.04 19.11 1 8 14 45.92 40.46 1 8 15 131.53 51.81 1 8 15 -32.97 84.93 1 8 15 215.32 84.99 1 8 15 271.79 122.58 1 8 16 18.34 8.07 1 8 16 3.92 33.61 1 8 16 32.51 14.97 1 8 16 19.21 47.20 1 9 0 0.23 0.62 1 9 0 7.88 12.47 1 9 0 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82.59 51.69 1 13 1 52.53 20.78 1 13 1 26.91 83.16 1 13 2 0.05 1.11 1 13 2 -4.74 29.16 1 13 2 0.91 1.51 1 13 2 16.70 125.71 1 13 3 44.15 17.52 1 13 3 74.04 39.15 1 13 3 47.81 18.99 1 13 3 7.02 99.42 1 13 4 19.76 8.05 1 13 4 32.80 26.33 1 13 4 21.21 8.69 1 13 4 -28.31 102.39 1 13 5 15.38 6.36 1 13 5 16.01 23.12 1 13 5 17.41 7.36 1 13 5 -47.87 132.73 1 13 6 27.89 11.19 1 13 6 32.32 27.42 1 13 6 35.81 14.44 1 13 6 44.71 125.49 1 13 7 0.80 1.33 1 13 7 -1.41 24.78 1 13 7 0.19 2.42 1 13 7 18.01 90.52 1 13 8 12.17 5.16 1 13 8 10.14 37.81 1 13 8 18.53 8.07 1 13 8 4.42 62.91 1 13 10 4.74 2.65 1 13 10 -5.28 54.78 1 13 10 6.95 6.21 1 13 10 14.08 67.42 1 14 0 9.46 4.06 1 14 0 -3.46 41.92 1 14 0 7.67 3.58 1 14 0 -34.01 155.32 1 14 1 -0.32 1.26 1 14 1 0.49 1.57 1 14 1 -52.94 173.51 1 14 2 12.18 5.13 1 14 2 20.68 38.03 1 14 2 13.39 5.76 1 14 3 10.23 4.46 1 14 3 12.28 27.21 1 14 3 11.09 5.04 1 14 3 -84.82 196.39 1 14 4 34.25 13.71 1 14 4 47.35 32.74 1 14 4 38.45 15.52 1 14 4 -5.02 107.06 1 14 5 1.68 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1 32.20 12.86 2 -17 1 -10.96 97.71 2 -17 2 16.19 6.88 2 -17 2 2.75 72.10 2 -17 2 21.00 8.51 2 -17 2 -35.87 102.33 2 -17 3 0.33 1.74 2 -17 3 18.90 69.82 2 -17 3 0.41 1.21 2 -17 4 10.75 4.77 2 -17 4 21.39 8.65 2 -17 5 2.76 2.00 2 -17 5 6.33 2.90 2 -17 6 2.27 1.77 2 -17 6 2.56 31.61 2 -17 6 3.15 1.78 2 -17 6 -12.46 145.68 2 -17 7 11.41 4.93 2 -17 7 10.97 29.02 2 -17 7 21.85 8.81 2 -17 7 15.02 136.78 2 -17 8 49.77 19.76 2 -17 8 23.36 27.85 2 -17 8 90.64 35.69 2 -17 8 27.57 103.98 2 -17 9 38.35 15.31 2 -17 9 -1.59 23.47 2 -17 9 71.98 28.40 2 -17 9 -14.28 93.77 2 -17 10 18.08 7.54 2 -17 10 -1.37 24.64 2 -17 10 47.78 18.93 2 -16 0 1.11 2.05 2 -16 0 11.12 90.64 2 -16 0 2.07 1.61 2 -16 0 24.40 68.96 2 -16 1 1.87 2.06 2 -16 1 1.90 102.56 2 -16 1 0.86 1.31 2 -16 1 13.02 65.82 2 -16 2 2.77 2.11 2 -16 2 3.82 98.56 2 -16 2 5.39 2.59 2 -16 2 16.48 65.65 2 -16 3 3.46 2.18 2 -16 3 22.98 101.99 2 -16 3 5.81 2.73 2 -16 3 -11.23 73.81 2 -16 4 19.25 7.88 2 -16 4 -13.85 81.97 2 -16 4 27.21 10.90 2 -16 4 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18 154.58 61.03 2 3 18 11.07 77.23 2 3 18 51.19 141.46 2 3 18 212.19 84.08 2 3 18 198.38 109.06 2 3 19 21.73 10.11 2 3 19 1.14 41.95 2 3 19 7.49 90.75 2 3 19 17.99 11.40 2 3 19 -0.92 66.96 2 4 0 380.34 148.93 2 4 0 535.54 209.85 2 4 0 329.92 129.14 2 4 0 140.89 56.19 2 4 1 114.19 44.74 2 4 1 224.16 88.01 2 4 1 136.49 53.47 2 4 1 251.20 99.02 2 4 2 43.24 16.98 2 4 2 22.48 9.43 2 4 2 44.50 17.48 2 4 2 19.19 8.67 2 4 3 174.48 68.33 2 4 3 144.14 56.76 2 4 3 164.62 64.45 2 4 3 181.96 71.53 2 4 4 79.46 31.15 2 4 4 117.62 46.95 2 4 4 82.02 32.16 2 4 4 107.35 42.57 2 4 5 0.93 0.80 2 4 5 3.96 5.95 2 4 6 11.46 4.61 2 4 6 10.36 35.18 2 4 6 12.60 5.09 2 4 6 15.01 8.96 2 4 7 48.19 18.96 2 4 7 8.78 58.75 2 4 7 63.77 25.07 2 4 7 74.04 30.43 2 4 8 29.79 11.79 2 4 8 2.59 41.03 2 4 8 33.13 13.16 2 4 8 29.11 14.78 2 4 9 22.09 8.78 2 4 9 21.65 64.34 2 4 9 28.63 11.44 2 4 9 18.93 12.44 2 4 10 80.65 31.71 2 4 10 -21.69 149.79 2 4 10 104.50 41.09 2 4 10 98.56 41.31 2 4 11 102.44 40.28 2 4 11 -37.26 327.23 2 4 11 138.89 54.62 2 4 11 114.93 50.06 2 4 12 1.34 1.58 2 4 12 -37.33 277.78 2 4 12 0.83 2.37 2 4 12 0.33 23.79 2 4 13 1.68 1.81 2 4 13 33.11 169.58 2 4 13 2.79 3.05 2 4 13 2.32 34.63 2 4 14 1.36 1.99 2 4 14 -80.25 245.78 2 4 14 3.05 3.39 2 4 14 -3.18 31.66 2 4 15 2.71 2.36 2 4 15 39.30 236.43 2 4 15 4.97 4.50 2 4 15 6.93 42.59 2 4 16 5.54 3.32 2 4 16 0.23 100.45 2 4 16 6.21 5.32 2 4 16 -3.01 41.96 2 4 17 76.32 30.31 2 4 17 2.88 64.34 2 4 17 108.15 43.42 2 4 17 139.69 78.31 2 4 19 -0.68 3.99 2 4 19 1.70 33.82 2 4 19 4.32 91.09 2 4 19 2.00 7.63 2 4 19 -15.51 60.40 2 5 0 70.22 27.54 2 5 0 48.60 19.82 2 5 0 58.52 22.95 2 5 0 11.21 14.00 2 5 1 18.31 7.24 2 5 1 23.96 9.43 2 5 1 84.02 35.73 2 5 2 30.33 11.94 2 5 2 37.50 15.49 2 5 2 33.72 13.26 2 5 2 33.34 15.25 2 5 3 284.91 112.14 2 5 3 188.23 73.75 2 5 4 30.10 11.86 2 5 4 29.01 13.19 2 5 4 29.91 11.80 2 5 4 23.08 11.12 2 5 5 25.81 10.19 2 5 5 39.93 19.39 2 5 5 25.29 9.99 2 5 5 32.94 14.91 2 5 6 11.56 4.67 2 5 6 18.96 21.78 2 5 6 10.27 4.21 2 5 6 5.92 7.29 2 5 7 29.20 11.56 2 5 7 48.61 59.43 2 5 7 32.30 12.82 2 5 7 32.48 15.95 2 5 8 122.86 48.20 2 5 8 39.89 91.72 2 5 8 132.67 52.06 2 5 8 190.11 76.03 2 5 9 13.89 5.67 2 5 9 -0.81 49.30 2 5 9 16.03 6.57 2 5 9 22.25 14.83 2 5 10 7.71 3.40 2 5 10 6.94 109.69 2 5 10 7.24 3.60 2 5 10 1.45 14.66 2 5 11 3.49 1.94 2 5 11 91.09 221.37 2 5 11 5.48 3.15 2 5 11 2.02 17.50 2 5 12 106.72 41.98 2 5 12 194.85 83.39 2 5 13 93.49 36.85 2 5 13 -37.33 232.72 2 5 13 127.31 50.28 2 5 13 136.32 61.15 2 5 14 42.92 17.15 2 5 14 -100.90 337.84 2 5 14 68.85 27.61 2 5 14 66.45 41.18 2 5 15 20.66 8.56 2 5 15 26.80 11.69 2 5 15 23.56 34.73 2 5 16 99.71 39.39 2 5 16 -10.35 64.45 2 5 16 159.03 63.03 2 5 16 137.01 69.02 2 5 17 3.60 3.07 2 5 17 -9.01 56.07 2 5 17 4.28 5.51 2 5 17 14.23 47.90 2 5 18 51.56 21.00 2 5 18 -3.03 23.33 2 5 18 59.66 25.48 2 5 18 47.54 53.19 2 6 0 309.10 121.67 2 6 0 180.13 70.56 2 6 2 0.50 0.60 2 6 2 3.06 5.98 2 6 2 0.89 0.78 2 6 2 8.34 15.37 2 6 3 78.89 30.95 2 6 3 96.80 38.80 2 6 3 82.48 32.36 2 6 3 83.39 34.69 2 6 4 16.29 6.49 2 6 4 11.05 6.97 2 6 4 16.38 6.54 2 6 4 11.50 9.12 2 6 5 270.48 105.98 2 6 5 258.16 102.21 2 6 5 234.94 92.06 2 6 5 247.78 97.94 2 6 6 78.66 30.88 2 6 6 110.49 48.93 2 6 6 77.92 30.61 2 6 6 93.43 38.38 2 6 7 1.33 1.03 2 6 7 -13.75 31.41 2 6 7 1.61 1.43 2 6 7 2.90 10.63 2 6 8 30.74 12.21 2 6 8 46.50 65.03 2 6 8 31.53 12.58 2 6 8 35.27 18.45 2 6 9 6.54 2.96 2 6 9 -17.73 152.92 2 6 9 6.38 3.21 2 6 9 2.36 14.84 2 6 10 9.75 4.12 2 6 10 11.91 5.25 2 6 10 12.77 20.09 2 6 12 24.68 10.02 2 6 12 4.21 158.17 2 6 12 24.74 10.34 2 6 12 43.60 31.40 2 6 13 13.85 5.95 2 6 13 34.30 232.72 2 6 13 12.69 6.21 2 6 13 21.40 30.32 2 6 14 5.06 2.84 2 6 14 -72.78 200.89 2 6 14 8.53 5.02 2 6 14 13.04 35.39 2 6 15 8.86 4.34 2 6 15 8.62 89.15 2 6 15 23.35 10.68 2 6 15 14.20 36.80 2 6 16 86.70 34.37 2 6 16 128.85 51.35 2 6 16 149.73 80.31 2 6 17 36.86 15.28 2 6 17 60.58 55.01 2 7 0 105.47 41.34 2 7 0 54.16 23.23 2 7 0 87.67 34.39 2 7 0 8.69 41.44 2 7 1 201.23 78.83 2 7 1 334.19 131.59 2 7 1 202.38 79.28 2 7 1 203.92 88.30 2 7 2 31.38 12.38 2 7 2 28.84 13.73 2 7 2 33.29 13.14 2 7 2 10.14 27.74 2 7 3 154.35 60.52 2 7 3 205.46 81.39 2 7 3 149.61 58.64 2 7 3 197.58 80.88 2 7 4 288.51 112.99 2 7 4 352.28 138.89 2 7 4 285.37 111.80 2 7 4 325.35 128.85 2 7 5 0.85 0.89 2 7 5 0.83 7.70 2 7 5 0.62 1.04 2 7 5 2.08 10.36 2 7 6 23.27 9.27 2 7 6 39.97 21.49 2 7 6 23.09 9.21 2 7 6 45.98 23.02 2 7 7 0.26 1.05 2 7 7 -12.99 30.82 2 7 7 0.09 1.47 2 7 7 2.80 16.96 2 7 8 11.66 4.83 2 7 8 47.47 76.15 2 7 8 13.97 5.95 2 7 8 21.71 21.42 2 7 9 8.20 3.55 2 7 9 3.33 105.58 2 7 9 -67.99 189.03 2 7 9 10.22 4.63 2 7 9 26.29 29.08 2 7 11 49.78 19.75 2 7 11 30.77 73.98 2 7 11 54.72 21.86 2 7 11 79.23 40.59 2 7 12 16.06 6.74 2 7 12 -39.44 77.86 2 7 12 26.11 11.02 2 7 12 37.26 31.30 2 7 13 20.99 8.60 2 7 13 -18.17 198.33 2 7 13 25.80 11.00 2 7 13 27.29 33.04 2 7 14 17.81 7.54 2 7 14 -25.07 102.78 2 7 14 23.73 10.58 2 7 14 31.21 37.57 2 7 15 5.23 3.27 2 7 15 7.81 63.37 2 7 15 9.99 6.58 2 7 15 10.05 44.69 2 7 16 -6.11 27.56 2 7 17 44.05 18.12 2 7 17 65.71 27.86 2 7 17 69.53 58.52 2 8 0 13.92 5.57 2 8 0 15.61 12.10 2 8 0 13.50 5.41 2 8 0 -4.01 61.94 2 8 1 2.80 1.36 2 8 1 12.16 10.90 2 8 1 3.02 1.50 2 8 1 24.07 40.59 2 8 2 39.87 15.71 2 8 2 37.10 17.57 2 8 2 39.19 15.45 2 8 2 28.29 43.51 2 8 3 140.43 55.05 2 8 3 239.57 95.14 2 8 3 161.71 63.43 2 8 3 300.31 126.68 2 8 4 72.10 28.33 2 8 4 153.61 61.72 2 8 4 86.70 34.06 2 8 4 179.22 75.24 2 8 5 1.60 1.14 2 8 5 2.98 9.95 2 8 5 1.26 1.37 2 8 5 -5.19 22.13 2 8 6 133.76 52.49 2 8 6 174.43 72.15 2 8 6 136.27 53.49 2 8 6 189.37 79.40 2 8 7 0.90 1.10 2 8 7 5.21 28.31 2 8 7 1.61 1.65 2 8 7 4.83 34.08 2 8 8 21.47 8.65 2 8 8 41.35 54.22 2 8 8 25.87 10.48 2 8 8 39.03 37.35 2 8 9 1.62 1.51 2 8 9 6.74 30.44 2 8 10 72.50 28.58 2 8 10 76.72 76.95 2 8 10 -4.72 124.12 2 8 10 79.80 31.59 2 8 10 107.18 51.86 2 8 11 14.28 5.99 2 8 11 -36.51 115.62 2 8 11 24.53 10.43 2 8 11 18.20 31.38 2 8 12 0.21 1.55 2 8 12 29.96 99.42 2 8 12 -0.15 3.04 2 8 12 -11.04 32.84 2 8 13 25.06 10.24 2 8 13 18.48 70.84 2 8 13 32.66 13.91 2 8 13 18.66 40.63 2 8 14 12.64 5.60 2 8 14 -21.86 80.77 2 8 14 18.79 9.12 2 8 14 12.05 48.23 2 8 16 4.60 3.67 2 8 16 -4.81 27.00 2 8 16 5.84 7.91 2 8 16 19.50 49.77 2 9 0 137.64 53.96 2 9 0 147.85 61.20 2 9 0 128.00 50.20 2 9 1 21.36 8.50 2 9 1 32.05 19.56 2 9 1 22.60 9.00 2 9 1 12.34 80.48 2 9 2 38.03 15.03 2 9 2 68.22 31.10 2 9 2 40.57 16.02 2 9 2 9.02 69.64 2 9 3 30.58 12.11 2 9 3 71.93 32.17 2 9 3 39.32 15.58 2 9 3 69.99 95.88 2 9 4 6.06 2.63 2 9 4 6.15 12.43 2 9 4 7.38 3.32 2 9 4 18.50 66.11 2 9 5 12.65 5.17 2 9 5 38.16 21.34 2 9 5 15.93 6.49 2 9 5 34.51 52.98 2 9 6 149.50 58.64 2 9 6 138.43 58.18 2 9 6 126.40 49.62 2 9 6 288.33 127.54 2 9 8 30.78 12.30 2 9 8 36.18 42.34 2 9 8 34.39 13.84 2 9 8 26.50 29.95 2 9 9 9.10 4.03 2 9 9 18.20 49.63 2 9 9 13.67 6.21 2 9 9 20.41 30.81 2 9 10 7.88 3.64 2 9 10 18.62 79.23 2 9 10 -10.78 142.26 2 9 10 9.62 5.01 2 9 10 11.62 31.74 2 9 11 0.69 1.61 2 9 11 -9.99 137.98 2 9 11 0.04 2.98 2 9 11 1.23 39.39 2 9 12 16.30 6.90 2 9 12 22.15 10.02 2 9 12 26.65 43.77 2 9 13 3.07 2.34 2 9 13 4.67 61.55 2 9 13 5.89 5.11 2 9 13 -9.86 56.89 2 9 15 1.92 2.78 2 9 15 -4.82 35.73 2 9 15 3.06 7.27 2 9 15 -9.82 61.49 2 10 0 10.54 4.35 2 10 0 18.24 24.88 2 10 0 12.03 4.96 2 10 0 -21.08 111.51 2 10 1 6.61 2.82 2 10 1 16.26 25.71 2 10 1 7.55 3.27 2 10 1 4.59 155.43 2 10 2 5.72 2.53 2 10 2 4.61 24.16 2 10 2 6.14 2.74 2 10 2 -8.75 99.93 2 10 3 69.25 27.26 2 10 3 113.91 49.58 2 10 3 65.65 25.86 2 10 3 24.73 99.25 2 10 4 60.69 23.91 2 10 4 86.53 39.85 2 10 4 63.88 25.19 2 10 4 64.17 116.30 2 10 5 191.88 79.97 2 10 5 168.38 66.17 2 10 6 14.05 5.77 2 10 6 24.04 20.76 2 10 6 15.50 6.50 2 10 6 19.75 53.84 2 10 7 1.23 1.27 2 10 7 1.23 23.81 2 10 7 1.67 2.10 2 10 7 6.71 41.25 2 10 8 8.20 3.65 2 10 8 -10.51 32.56 2 10 8 8.81 4.35 2 10 8 -6.74 37.41 2 10 9 18.33 7.51 2 10 9 55.51 67.42 2 10 9 21.64 9.13 2 10 9 34.11 39.80 2 10 10 25.40 10.29 2 10 10 -17.03 66.57 2 10 10 36.65 15.04 2 10 10 28.37 48.26 2 10 11 21.60 8.94 2 10 11 32.27 76.95 2 10 11 -0.63 130.05 2 10 11 37.30 15.58 2 10 11 21.98 43.12 2 10 12 8.00 3.86 2 10 12 -28.31 124.00 2 10 12 10.40 6.15 2 10 12 39.80 72.38 2 11 0 171.18 67.13 2 11 0 203.57 92.92 2 11 0 131.82 51.73 2 11 0 121.78 171.46 2 11 1 7.60 3.25 2 11 1 8.24 3.56 2 11 1 -26.09 253.88 2 11 2 10.61 31.14 2 11 2 1.06 1.30 2 11 2 46.44 168.89 2 11 4 38.09 15.10 2 11 4 61.94 31.66 2 11 4 49.86 19.80 2 11 4 48.12 134.73 2 11 5 6.10 2.78 2 11 5 3.88 17.41 2 11 5 8.35 3.96 2 11 5 -3.59 92.63 2 11 6 13.25 5.49 2 11 6 16.68 20.51 2 11 6 15.66 6.63 2 11 6 -2.35 72.78 2 11 7 21.95 8.90 2 11 7 21.96 29.81 2 11 7 21.20 8.74 2 11 7 39.29 67.25 2 11 8 7.34 3.38 2 11 8 3.46 34.01 2 11 8 7.99 4.01 2 11 8 25.42 66.34 2 11 9 18.60 7.67 2 11 9 1.96 47.79 2 11 9 25.43 10.75 2 11 9 25.91 55.57 2 11 10 8.82 4.08 2 11 10 -16.55 64.91 2 11 10 15.91 7.69 2 11 10 19.86 54.35 2 11 11 0.32 1.67 2 11 11 -4.97 74.89 2 11 11 6.35 132.16 2 11 11 1.92 4.93 2 11 11 1.02 66.45 2 11 12 51.63 20.64 2 11 12 119.21 48.24 2 11 12 53.06 75.29 2 12 0 54.82 21.61 2 12 0 38.53 37.15 2 12 0 48.91 19.36 2 12 0 0.08 157.60 2 12 1 0.50 0.94 2 12 1 1.31 25.51 2 12 1 0.04 1.40 2 12 2 4.72 2.26 2 12 2 10.18 27.62 2 12 2 4.15 2.35 2 12 2 43.92 139.97 2 12 3 29.15 11.64 2 12 3 56.75 32.05 2 12 3 32.55 13.07 2 12 3 36.72 105.87 2 12 4 5.70 2.74 2 12 4 -5.16 18.65 2 12 4 6.65 3.30 2 12 4 -1.37 99.53 2 12 5 8.77 3.81 2 12 5 10.57 21.10 2 12 5 9.75 4.41 2 12 5 -34.28 96.51 2 12 6 0.30 1.23 2 12 6 -0.93 21.32 2 12 6 0.16 1.93 2 12 6 23.44 133.87 2 12 7 20.14 8.19 2 12 7 26.23 30.80 2 12 7 27.74 11.36 2 12 7 51.46 90.29 2 12 8 13.58 5.72 2 12 8 6.23 35.63 2 12 8 17.57 7.71 2 12 8 33.72 71.24 2 12 9 54.41 21.57 2 12 9 50.43 53.33 2 12 9 73.41 29.33 2 12 9 108.38 84.13 2 12 10 25.71 61.60 2 12 11 15.45 6.63 2 12 11 10.46 73.92 2 12 11 34.37 15.60 2 12 11 6.34 78.20 2 13 0 -0.08 1.14 2 13 0 11.96 40.12 2 13 0 0.16 1.62 2 13 0 -6.61 118.41 2 13 1 6.70 3.07 2 13 1 2.38 31.35 2 13 1 5.02 2.62 2 13 1 18.14 123.03 2 13 2 2.51 1.67 2 13 2 5.30 29.19 2 13 2 4.50 2.60 2 13 2 -35.24 187.72 2 13 3 0.86 1.37 2 13 3 16.97 25.15 2 13 3 1.49 2.18 2 13 3 56.30 231.07 2 13 4 17.33 7.14 2 13 4 18.62 25.06 2 13 4 21.46 8.89 2 13 4 -0.14 148.76 2 13 5 76.26 30.10 2 13 5 82.42 43.22 2 13 5 83.68 33.07 2 13 5 7.23 103.41 2 13 6 105.47 41.53 2 13 6 158.40 71.47 2 13 6 136.95 53.94 2 13 6 68.62 84.13 2 13 7 32.07 12.84 2 13 7 34.78 40.54 2 13 7 41.96 16.96 2 13 7 3.09 72.55 2 13 8 11.92 5.13 2 13 8 -7.88 40.70 2 13 8 24.25 10.77 2 13 8 -13.96 106.21 2 13 9 0.42 1.49 2 13 9 -15.78 48.37 2 13 9 -2.21 5.11 2 13 9 -47.96 72.67 2 14 0 18.15 7.40 2 14 0 3.94 47.63 2 14 0 17.32 7.18 2 14 0 -12.95 178.25 2 14 1 104.32 41.05 2 14 1 146.19 73.35 2 14 1 86.53 34.11 2 14 1 16.64 97.02 2 14 2 1.26 1.44 2 14 2 4.03 28.91 2 14 2 0.68 2.10 2 14 2 -59.09 93.66 2 14 3 0.99 1.37 2 14 3 -1.89 29.63 2 14 3 1.44 2.48 2 14 3 11.24 110.26 2 14 4 5.77 2.92 2 14 4 7.51 33.03 2 14 4 8.80 4.51 2 14 4 -4.26 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13 -0.09 0.85 3 -15 13 3.30 141.12 3 -15 14 5.11 2.55 3 -15 14 8.54 23.43 3 -15 14 10.26 4.29 3 -15 14 3.99 184.07 3 -15 14 -21.12 48.72 3 -14 0 2.12 1.74 3 -14 0 -11.03 87.61 3 -14 0 1.96 1.41 3 -14 0 -9.51 51.48 3 -14 1 157.49 61.77 3 -14 1 -22.20 97.42 3 -14 1 217.03 85.10 3 -14 1 23.09 55.64 3 -14 2 6.15 2.84 3 -14 2 -5.32 97.82 3 -14 2 9.63 4.06 3 -14 2 0.66 62.52 3 -14 3 4.27 2.14 3 -14 3 -8.01 102.10 3 -14 3 4.20 2.06 3 -14 3 33.98 97.42 3 -14 4 2.74 1.66 3 -14 4 -4.21 93.94 3 -14 4 4.50 2.16 3 -14 4 -42.55 112.60 3 -14 5 1.64 1.33 3 -14 5 -12.01 102.78 3 -14 5 1.52 1.12 3 -14 5 41.30 129.02 3 -14 6 3.65 1.97 3 -14 6 45.03 103.58 3 -14 6 2.85 1.50 3 -14 6 67.65 116.93 3 -14 7 17.09 6.96 3 -14 7 3.20 82.14 3 -14 7 27.85 11.09 3 -14 7 50.62 151.44 3 -14 8 3.33 1.82 3 -14 8 17.49 64.17 3 -14 8 5.47 2.44 3 -14 8 47.99 175.91 3 -14 9 2.65 1.58 3 -14 9 -10.03 45.26 3 -14 9 7.18 3.10 3 -14 9 16.98 159.42 3 -14 10 192.28 75.41 3 -14 10 107.29 63.26 3 -14 10 292.90 114.76 3 -14 10 47.90 293.87 3 -14 11 4.03 2.07 3 -14 11 1.99 31.58 3 -14 11 4.13 1.93 3 -14 11 25.98 232.78 3 -14 12 1.89 1.46 3 -14 12 9.38 24.62 3 -14 12 2.00 1.21 3 -14 12 -32.33 138.66 3 -14 13 30.53 12.19 3 -14 13 23.43 25.92 3 -14 13 53.39 21.08 3 -14 13 -67.31 116.30 3 -14 13 3.86 78.54 3 -14 14 6.42 46.66 3 -14 15 112.31 44.16 3 -14 15 85.90 41.60 3 -14 15 241.96 94.86 3 -14 15 25.92 102.27 3 -14 15 -36.84 117.16 3 -13 0 2.09 1.67 3 -13 0 -44.03 192.11 3 -13 0 1.81 1.30 3 -13 0 6.12 44.44 3 -13 1 62.63 24.69 3 -13 1 -25.43 195.02 3 -13 1 68.39 26.91 3 -13 1 14.74 54.79 3 -13 2 26.52 10.58 3 -13 2 -1.33 226.33 3 -13 2 34.11 13.53 3 -13 2 38.49 99.19 3 -13 3 0.56 1.02 3 -13 3 -3.89 193.08 3 -13 3 0.87 1.00 3 -13 3 -1.78 116.65 3 -13 4 0.78 1.09 3 -13 4 4.53 130.56 3 -13 4 0.95 1.05 3 -13 4 -19.32 161.65 3 -13 5 9.70 4.09 3 -13 5 -40.09 113.79 3 -13 5 13.70 5.56 3 -13 5 31.39 154.92 3 -13 6 9.37 3.99 3 -13 6 15.61 127.37 3 -13 6 14.32 5.80 3 -13 6 76.83 208.08 3 -13 7 99.53 39.11 3 -13 7 125.66 132.62 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12.11 25.73 3 13 3 8.80 4.30 3 13 3 49.83 127.25 3 13 4 19.23 7.89 3 13 4 37.13 35.62 3 13 4 23.22 9.69 3 13 4 2.67 70.84 3 13 5 5.42 2.75 3 13 5 6.07 29.88 3 13 5 8.28 4.48 3 13 5 4.95 81.39 3 13 6 -0.21 1.38 3 13 6 8.72 30.48 3 13 6 0.37 3.36 3 13 6 15.19 115.45 3 13 7 3.56 2.11 3 13 7 -4.68 43.67 3 13 7 5.89 4.99 3 13 7 12.01 76.60 3 14 0 1.76 1.58 3 14 0 3.01 57.55 3 14 0 0.80 1.72 3 14 0 -6.96 82.65 3 14 1 4.52 2.32 3 14 1 2.26 45.89 3 14 1 4.19 2.79 3 14 1 13.39 71.19 3 14 2 10.44 4.52 3 14 2 25.68 36.23 3 14 2 14.70 6.75 3 14 2 19.94 82.65 3 14 3 5.10 2.58 3 14 3 2.84 31.45 3 14 3 8.43 4.95 3 14 4 8.73 3.95 3 14 4 4.32 32.11 3 14 4 15.29 7.41 3 14 4 -27.12 118.59 3 14 5 1.41 1.59 3 14 5 9.14 33.70 3 14 5 0.39 3.85 3 14 5 -15.46 79.51 3 15 0 2.76 1.87 3 15 0 3.97 59.26 3 15 0 3.77 3.04 3 15 0 20.44 119.61 3 15 1 6.74 3.21 3 15 1 20.92 43.81 3 15 1 9.65 5.21 3 15 1 -38.75 119.67 4 -17 0 0.45 2.53 4 -17 0 12.11 119.33 4 -17 0 1.00 1.44 4 -17 0 -48.30 109.23 4 -17 1 0.43 2.45 4 -17 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155.26 60.92 4 -11 6 -26.60 139.29 4 -11 7 61.83 24.35 4 -11 7 37.61 40.57 4 -11 7 90.41 35.51 4 -11 7 87.38 242.08 4 -11 8 59.04 23.23 4 -11 8 163.59 359.52 4 -11 9 2.06 21.67 4 -11 9 3.74 1.74 4 -11 10 31.49 12.49 4 -11 10 24.02 19.74 4 -11 10 46.12 18.20 4 -11 10 31.95 251.94 4 -11 10 31.31 227.13 4 -11 11 2.90 1.56 4 -11 11 2.59 17.39 4 -11 11 9.66 3.98 4 -11 11 23.25 114.08 4 -11 12 0.96 1.04 4 -11 12 7.83 18.24 4 -11 12 6.74 2.88 4 -11 12 -35.29 97.88 4 -11 12 40.74 514.72 4 -11 13 1.32 1.08 4 -11 13 5.75 15.76 4 -11 13 1.89 1.20 4 -11 13 -37.98 100.39 4 -11 13 -22.74 742.08 4 -11 14 17.90 7.23 4 -11 14 15.08 12.40 4 -11 14 11.11 91.32 4 -11 15 9.67 4.06 4 -11 15 6.15 9.25 4 -11 15 19.74 72.21 4 -11 15 -12.92 96.40 4 -11 16 14.96 6.10 4 -11 16 9.67 9.39 4 -11 16 -4.45 53.95 4 -11 16 -13.65 133.36 4 -11 18 1.07 1.21 4 -11 18 0.51 8.71 4 -11 18 2.96 25.78 4 -10 0 69.07 27.16 4 -10 0 145.16 136.21 4 -10 0 66.68 26.21 4 -10 0 42.54 36.94 4 -10 1 13.55 5.46 4 -10 1 143.51 141.86 4 -10 1 10.17 4.14 4 -10 1 83.51 59.43 4 -10 2 14.49 5.82 4 -10 2 48.87 99.08 4 -10 2 14.35 5.77 4 -10 2 40.88 77.40 4 -10 3 93.89 36.85 4 -10 3 65.99 70.50 4 -10 3 105.69 41.48 4 -10 3 96.00 90.01 4 -10 4 68.50 26.93 4 -10 4 36.79 63.09 4 -10 4 90.01 35.34 4 -10 4 -2.53 127.94 4 -10 5 9.74 4.03 4 -10 5 96.45 73.69 4 -10 5 5.34 2.30 4 -10 5 1.43 122.18 4 -10 6 11.87 4.82 4 -10 6 19.22 39.40 4 -10 6 11.14 4.52 4 -10 6 58.12 144.48 4 -10 7 9.85 4.05 4 -10 7 29.34 25.16 4 -10 7 10.84 4.41 4 -10 7 -20.41 183.44 4 -10 8 2.11 1.22 4 -10 8 6.74 16.34 4 -10 8 4.35 1.93 4 -10 8 -22.57 206.37 4 -10 9 38.47 15.21 4 -10 9 34.70 21.35 4 -10 9 48.82 19.24 4 -10 9 102.73 169.75 4 -10 10 -50.09 172.26 4 -10 10 86.76 197.07 4 -10 11 38.48 15.23 4 -10 11 48.42 26.05 4 -10 11 56.63 22.30 4 -10 11 56.74 164.22 4 -10 11 36.41 368.59 4 -10 12 14.63 5.92 4 -10 12 24.20 17.54 4 -10 12 12.92 5.25 4 -10 12 14.62 118.87 4 -10 13 2.74 1.47 4 -10 13 1.82 8.33 4 -10 13 7.52 81.74 4 -10 14 19.39 7.79 4 -10 14 15.81 10.23 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62.23 25.81 4 0 18 -17.92 87.27 4 0 18 30.81 15.62 4 0 18 13.44 110.37 4 0 19 -10.50 78.89 4 1 0 263.75 103.24 4 1 0 57.21 30.94 4 1 0 205.68 80.54 4 1 0 76.32 30.57 4 1 1 0.93 0.53 4 1 1 2.69 1.20 4 1 1 6.47 3.96 4 1 2 2.08 0.98 4 1 2 -0.35 48.57 4 1 2 2.94 1.38 4 1 2 2.09 4.17 4 1 3 105.07 41.17 4 1 3 32.22 58.47 4 1 3 119.50 46.82 4 1 3 88.18 35.23 4 1 4 32.56 12.81 4 1 4 -6.19 70.16 4 1 4 42.95 16.91 4 1 4 33.99 15.37 4 1 5 3.42 1.63 4 1 5 11.44 93.32 4 1 5 8.93 3.81 4 1 6 67.25 26.40 4 1 6 0.13 134.27 4 1 6 69.93 27.52 4 1 6 55.73 30.78 4 1 7 249.15 97.65 4 1 7 126.68 200.55 4 1 7 282.69 110.83 4 1 7 374.35 155.60 4 1 8 0.78 1.32 4 1 8 103.81 237.34 4 1 8 1.41 1.92 4 1 8 29.23 59.21 4 1 9 45.05 17.85 4 1 9 64.51 308.01 4 1 9 45.73 18.25 4 1 9 5.77 67.48 4 1 10 75.86 29.95 4 1 10 -12.65 358.38 4 1 10 -132.22 592.07 4 1 10 72.50 28.78 4 1 10 45.53 118.59 4 1 11 62.91 24.96 4 1 11 -5.56 247.32 4 1 11 164.05 413.99 4 1 11 57.32 23.07 4 1 11 76.32 152.98 4 1 12 83.39 33.00 4 1 12 72.55 159.65 4 1 12 0.11 239.51 4 1 12 94.34 37.67 4 1 12 113.28 131.36 4 1 13 23.57 10.02 4 1 13 -24.18 190.11 4 1 13 -19.66 262.04 4 1 13 27.19 12.28 4 1 13 37.06 104.04 4 1 14 6.96 4.48 4 1 14 -0.54 222.80 4 1 14 6.57 6.13 4 1 14 -1.71 81.97 4 1 15 14.32 7.13 4 1 15 -122.75 583.51 4 1 15 10.54 7.72 4 1 15 -28.39 143.00 4 1 16 60.80 24.62 4 1 16 36.72 132.16 4 1 16 54.03 23.05 4 1 16 32.43 96.51 4 1 17 35.79 15.34 4 1 17 -11.49 119.78 4 1 17 17.64 10.93 4 1 17 12.77 99.31 4 1 18 6.00 7.15 4 1 18 28.15 76.89 4 1 18 0.15 8.42 4 1 18 0.43 90.01 4 2 0 34.43 13.51 4 2 0 12.84 6.71 4 2 0 16.94 6.66 4 2 1 141.46 55.39 4 2 1 113.85 49.00 4 2 1 124.52 48.77 4 2 1 141.91 56.70 4 2 2 46.66 18.30 4 2 2 1.11 17.99 4 2 2 43.74 17.17 4 2 2 21.82 9.77 4 2 3 175.28 68.62 4 2 3 -1.85 25.76 4 2 3 174.26 68.28 4 2 3 150.87 59.61 4 2 4 3.24 1.53 4 2 4 -7.93 68.90 4 2 4 2.91 1.60 4 2 4 0.45 5.31 4 2 5 20.19 8.01 4 2 5 2.09 86.53 4 2 5 30.51 12.08 4 2 5 16.34 9.03 4 2 7 40.09 15.81 4 2 7 47.90 18.94 4 2 7 40.48 20.95 4 2 8 1.18 1.30 4 2 8 -6.19 193.53 4 2 8 1.44 1.79 4 2 8 -3.15 17.68 4 2 9 86.59 34.07 4 2 9 159.20 349.54 4 2 9 91.49 36.09 4 2 9 104.27 52.66 4 2 10 79.63 31.38 4 2 10 -143.97 315.88 4 2 10 92.46 36.54 4 2 10 128.34 70.33 4 2 11 12.46 5.39 4 2 11 18.20 224.39 4 2 11 24.53 10.41 4 2 11 25.07 57.55 4 2 12 16.97 7.21 4 2 12 -5.81 171.18 4 2 12 16.15 7.68 4 2 12 19.05 63.88 4 2 14 0.24 2.74 4 2 14 50.73 274.19 4 2 14 -32.78 421.46 4 2 14 -0.67 5.23 4 2 14 9.91 63.71 4 2 15 3.43 3.46 4 2 15 31.55 131.65 4 2 15 0.60 194.50 4 2 15 6.20 7.02 4 2 15 -20.47 71.41 4 2 16 13.52 6.79 4 2 16 11.81 62.23 4 2 16 -7.51 94.00 4 2 16 15.75 9.93 4 2 16 26.56 74.21 4 2 17 99.42 39.59 4 2 17 46.59 84.87 4 2 17 0.96 99.93 4 2 17 99.13 40.39 4 2 17 122.98 94.17 4 2 18 -2.16 5.28 4 2 18 -41.11 87.44 4 2 18 -1.20 8.46 4 2 18 0.12 81.45 4 3 0 65.03 25.48 4 3 0 35.31 14.46 4 3 0 49.07 19.24 4 3 1 30.66 12.05 4 3 1 34.84 14.90 4 3 1 30.45 11.97 4 3 1 28.54 20.76 4 3 2 89.55 35.10 4 3 2 82.02 35.77 4 3 2 83.05 32.58 4 3 2 47.30 20.23 4 3 3 77.80 30.51 4 3 3 24.17 26.10 4 3 3 61.83 24.26 4 3 3 34.33 14.93 4 3 4 9.93 4.00 4 3 4 8.58 37.24 4 3 4 10.53 4.32 4 3 4 6.13 6.33 4 3 5 2.64 1.70 4 3 6 22.93 9.10 4 3 6 5.77 107.63 4 3 6 22.73 9.10 4 3 6 22.11 12.54 4 3 7 8.45 3.56 4 3 7 35.82 137.35 4 3 7 7.31 3.37 4 3 7 9.54 10.90 4 3 8 9.67 4.11 4 3 8 69.70 277.73 4 3 8 6.76 3.42 4 3 8 9.90 13.79 4 3 9 433.78 169.92 4 3 9 117.79 339.10 4 3 9 566.86 222.05 4 3 9 448.16 178.08 4 3 10 0.30 1.36 4 3 10 42.44 216.75 4 3 10 1.34 2.51 4 3 10 13.54 21.89 4 3 11 177.56 69.70 4 3 11 -3.65 124.57 4 3 11 270.08 106.09 4 3 11 308.18 129.31 4 3 12 40.39 16.16 4 3 12 -65.37 199.30 4 3 12 44.47 18.15 4 3 12 44.91 40.05 4 3 13 42.85 17.19 4 3 13 67.82 27.35 4 3 13 66.62 49.11 4 3 14 75.58 29.93 4 3 14 33.59 268.54 4 3 14 82.82 33.33 4 3 14 139.12 74.78 4 3 15 23.51 9.92 4 3 15 42.05 104.84 4 3 15 19.66 9.91 4 3 15 39.68 52.02 4 3 16 29.11 12.21 4 3 16 -3.63 79.28 4 3 16 -16.19 133.13 4 3 16 36.59 16.79 4 3 16 50.64 66.05 4 3 17 3.43 4.57 4 3 17 -0.70 37.99 4 3 17 -17.44 81.91 4 3 17 3.98 8.58 4 3 17 37.93 63.14 4 4 0 100.16 39.25 4 4 0 105.52 41.83 4 4 0 104.50 40.95 4 4 1 17.79 7.04 4 4 1 12.17 6.65 4 4 1 18.13 7.18 4 4 1 24.87 27.09 4 4 2 29.17 11.49 4 4 2 48.18 20.71 4 4 2 33.04 13.01 4 4 2 46.73 24.94 4 4 3 0.04 0.61 4 4 3 3.37 17.88 4 4 3 0.12 0.82 4 4 3 1.10 7.91 4 4 5 2.68 1.37 4 4 5 5.08 77.29 4 4 5 2.95 1.63 4 4 5 1.31 8.90 4 4 6 8.08 3.41 4 4 6 -11.29 36.26 4 4 6 6.29 2.96 4 4 6 8.73 10.68 4 4 7 85.90 33.77 4 4 7 46.03 94.74 4 4 7 87.96 34.65 4 4 7 98.96 42.55 4 4 8 95.66 37.61 4 4 8 -74.44 226.45 4 4 8 106.21 41.81 4 4 8 127.71 54.24 4 4 9 142.54 55.94 4 4 9 76.60 174.08 4 4 9 179.45 70.50 4 4 9 251.09 102.67 4 4 10 2.76 1.95 4 4 10 -27.74 128.34 4 4 10 2.50 3.13 4 4 10 9.87 25.48 4 4 11 12.70 5.48 4 4 11 11.72 199.92 4 4 11 15.35 7.18 4 4 11 17.21 24.82 4 4 12 3.19 2.42 4 4 12 -2.39 27.34 4 4 13 73.24 28.96 4 4 13 11.04 221.48 4 4 13 98.62 39.33 4 4 13 114.31 58.69 4 4 14 43.14 17.31 4 4 14 -64.06 107.92 4 4 14 65.60 26.68 4 4 14 74.95 46.45 4 4 15 1.52 2.66 4 4 15 2.68 5.74 4 4 15 -6.18 38.04 4 4 16 2.29 3.58 4 4 16 12.71 36.33 4 4 16 5.52 7.48 4 4 16 -11.03 47.82 4 4 17 1.60 4.17 4 4 17 -0.55 36.08 4 4 17 1.15 8.15 4 4 17 -5.57 46.75 4 5 0 315.14 123.38 4 5 0 281.09 110.71 4 5 0 257.02 100.62 4 5 1 92.97 36.46 4 5 1 105.64 42.39 4 5 1 90.64 35.55 4 5 1 113.91 59.15 4 5 2 20.12 7.99 4 5 2 35.47 15.69 4 5 2 26.99 10.66 4 5 3 192.68 75.52 4 5 3 162.73 67.02 4 5 4 109.23 42.84 4 5 4 156.63 67.93 4 5 4 108.32 42.51 4 5 4 102.50 43.42 4 5 5 0.03 0.90 4 5 5 9.50 50.77 4 5 5 0.04 1.25 4 5 5 -4.62 13.19 4 5 6 3.09 1.66 4 5 6 1.82 136.38 4 5 6 2.01 1.73 4 5 6 8.63 19.87 4 5 7 -0.09 1.08 4 5 7 0.64 1.94 4 5 7 -2.41 20.73 4 5 8 3.35 1.89 4 5 8 3.68 91.66 4 5 8 5.27 3.20 4 5 8 10.62 21.69 4 5 9 1.71 1.64 4 5 9 -8.13 132.39 4 5 9 1.75 2.65 4 5 9 7.45 25.57 4 5 10 2.84 2.19 4 5 10 -0.11 190.00 4 5 10 3.65 3.50 4 5 10 7.04 24.69 4 5 12 25.44 10.38 4 5 12 -77.46 233.75 4 5 12 35.19 14.79 4 5 12 41.32 36.93 4 5 13 11.61 5.26 4 5 13 21.26 9.98 4 5 13 25.82 36.57 4 5 14 77.63 30.78 4 5 14 3.56 62.69 4 5 14 100.73 40.38 4 5 14 94.86 55.36 4 5 15 10.97 5.41 4 5 15 6.88 50.60 4 5 15 12.15 8.05 4 5 15 9.71 49.28 4 5 16 11.51 6.21 4 5 16 -1.69 22.74 4 5 16 11.64 9.21 4 5 16 4.26 47.73 4 6 1 199.12 78.03 4 6 1 182.64 97.59 4 6 2 85.05 33.38 4 6 2 97.08 39.60 4 6 2 90.58 35.55 4 6 2 175.34 92.80 4 6 3 7.09 2.96 4 6 3 3.41 8.23 4 6 3 5.99 2.64 4 6 3 0.40 39.03 4 6 4 3.91 1.84 4 6 4 -2.15 21.91 4 6 4 2.41 1.63 4 6 4 -1.21 28.47 4 6 5 1.43 1.17 4 6 5 17.32 45.29 4 6 5 1.99 1.76 4 6 5 12.04 23.98 4 6 6 -0.30 1.07 4 6 6 -2.18 98.85 4 6 6 -0.45 1.72 4 6 6 13.89 34.86 4 6 7 8.74 3.77 4 6 7 43.68 170.49 4 6 7 13.86 5.93 4 6 7 12.66 35.87 4 6 8 131.25 51.52 4 6 8 141.69 55.73 4 6 8 255.37 108.77 4 6 9 19.71 8.06 4 6 9 19.99 73.24 4 6 9 20.10 8.66 4 6 9 23.71 29.25 4 6 11 2.03 1.94 4 6 11 -55.76 226.45 4 6 11 0.60 3.58 4 6 11 6.45 29.07 4 6 12 1.83 2.22 4 6 12 -11.97 91.49 4 6 12 2.69 4.37 4 6 12 -2.05 32.97 4 6 13 103.93 41.05 4 6 13 -15.14 60.52 4 6 13 146.02 58.01 4 6 13 140.20 70.16 4 6 14 25.43 10.62 4 6 14 27.57 12.71 4 6 14 43.30 53.16 4 6 15 0.76 3.47 4 6 15 4.66 22.55 4 6 15 3.60 7.05 4 6 15 6.67 45.28 4 7 0 8.56 3.52 4 7 0 11.74 14.43 4 7 0 7.51 3.15 4 7 0 34.57 99.08 4 7 1 67.59 26.56 4 7 1 77.06 33.49 4 7 1 65.03 25.59 4 7 1 18.20 150.76 4 7 2 62.57 24.61 4 7 2 92.29 39.16 4 7 2 72.73 28.61 4 7 2 131.13 128.51 4 7 3 19.23 7.67 4 7 3 20.99 14.72 4 7 3 18.80 7.58 4 7 3 57.27 95.03 4 7 4 5.52 2.45 4 7 4 5.81 20.93 4 7 4 4.52 2.24 4 7 4 76.15 75.18 4 7 5 20.34 8.15 4 7 5 24.36 38.26 4 7 5 21.00 8.51 4 7 5 -3.96 50.63 4 7 6 2.58 1.58 4 7 6 0.19 56.17 4 7 6 1.59 2.08 4 7 6 20.43 44.79 4 7 7 11.06 4.66 4 7 7 -23.01 76.20 4 7 7 26.13 129.88 4 7 7 9.91 4.70 4 7 7 0.43 33.24 4 7 8 22.10 8.97 4 7 8 -23.97 132.79 4 7 8 21.94 9.20 4 7 8 15.57 29.07 4 7 10 49.68 19.70 4 7 10 -16.78 98.17 4 7 10 63.71 25.54 4 7 10 58.18 42.45 4 7 11 5.29 2.89 4 7 11 5.39 60.86 4 7 11 9.43 5.81 4 7 11 20.47 41.61 4 7 12 45.82 18.32 4 7 12 -11.50 70.96 4 7 12 54.64 22.47 4 7 12 74.61 52.38 4 7 13 54.72 21.82 4 7 13 3.57 45.80 4 7 13 76.55 31.05 4 7 13 136.67 83.90 4 7 14 19.58 8.52 4 7 14 -11.53 22.74 4 7 14 27.74 13.55 4 7 14 62.06 56.68 4 8 0 12.88 5.22 4 8 0 17.73 25.66 4 8 0 8.32 3.47 4 8 0 5.19 119.27 4 8 1 52.77 20.79 4 8 1 87.16 39.45 4 8 1 47.24 18.63 4 8 1 28.37 160.34 4 8 2 10.02 4.14 4 8 2 20.36 16.94 4 8 2 11.07 4.59 4 8 2 4.19 102.16 4 8 3 1.94 1.20 4 8 3 9.40 15.58 4 8 3 2.29 1.58 4 8 3 -5.82 126.80 4 8 4 41.48 16.40 4 8 4 33.24 24.42 4 8 4 39.51 15.67 4 8 4 46.22 126.06 4 8 5 105.52 41.47 4 8 5 166.61 75.12 4 8 5 95.66 37.63 4 8 5 185.61 109.69 4 8 6 7.66 3.41 4 8 6 17.07 44.18 4 8 6 7.68 3.84 4 8 6 4.11 43.37 4 8 7 13.88 5.80 4 8 7 21.82 57.32 4 8 7 15.26 6.80 4 8 7 -9.62 35.89 4 8 8 3.07 2.04 4 8 8 -4.78 36.69 4 8 9 6.75 3.31 4 8 9 57.38 184.29 4 8 9 7.93 4.57 4 8 9 12.46 40.72 4 8 10 22.26 9.16 4 8 10 -4.28 60.80 4 8 10 31.22 13.22 4 8 10 27.00 45.55 4 8 11 32.78 13.22 4 8 11 0.37 53.10 4 8 11 44.85 18.78 4 8 11 23.49 44.87 4 8 12 11.20 5.09 4 8 12 12.31 57.67 4 8 12 19.07 9.89 4 8 12 26.35 67.08 4 8 13 5.62 3.47 4 8 13 12.74 32.26 4 8 13 6.51 7.64 4 8 13 0.88 60.92 4 9 0 33.52 13.27 4 9 0 41.91 36.84 4 9 0 23.60 9.41 4 9 0 48.76 233.86 4 9 1 6.34 2.78 4 9 1 8.76 21.20 4 9 1 6.13 2.87 4 9 2 39.29 15.56 4 9 2 53.14 29.83 4 9 2 36.94 14.69 4 9 2 49.47 177.79 4 9 3 2.10 1.39 4 9 3 9.76 18.39 4 9 3 3.46 2.20 4 9 3 -55.95 144.20 4 9 4 22.17 8.90 4 9 4 12.15 19.23 4 9 4 22.94 9.32 4 9 4 58.58 136.55 4 9 5 36.41 14.46 4 9 5 32.92 31.34 4 9 5 34.79 13.95 4 9 5 67.08 89.95 4 9 7 7.51 3.41 4 9 7 -41.22 71.53 4 9 7 6.76 4.19 4 9 7 20.02 53.50 4 9 8 -0.43 1.52 4 9 8 57.72 75.18 4 9 8 0.93 3.34 4 9 8 -15.08 62.23 4 9 9 38.88 15.60 4 9 9 13.41 126.46 4 9 9 54.40 22.14 4 9 9 30.03 53.50 4 9 10 63.66 25.24 4 9 10 82.71 33.13 4 9 10 82.71 79.40 4 9 11 80.54 31.87 4 9 11 -2.23 41.74 4 9 11 139.92 55.85 4 9 11 58.47 77.17 4 9 12 2.13 2.69 4 9 12 -4.75 27.61 4 9 12 3.93 7.93 4 9 12 -8.29 72.15 4 10 0 19.66 7.90 4 10 0 20.93 27.60 4 10 0 16.72 6.81 4 10 0 -33.57 143.17 4 10 1 55.50 21.94 4 10 1 73.07 37.46 4 10 1 48.87 19.37 4 10 1 40.29 114.14 4 10 2 73.87 29.11 4 10 2 100.05 46.67 4 10 2 72.78 28.72 4 10 2 8.52 140.60 4 10 3 69.07 27.22 4 10 3 90.41 43.18 4 10 3 69.47 27.44 4 10 3 93.72 124.06 4 10 5 22.67 9.14 4 10 5 26.87 36.29 4 10 5 21.91 8.98 4 10 5 -14.86 96.85 4 10 6 8.08 3.60 4 10 6 36.77 43.29 4 10 6 8.82 4.43 4 10 6 -45.04 122.92 4 10 7 69.93 27.63 4 10 7 53.61 58.47 4 10 7 85.22 33.86 4 10 7 97.31 92.75 4 10 8 3.70 2.30 4 10 8 -6.34 68.28 4 10 8 5.80 4.81 4 10 8 -22.37 71.64 4 10 9 1.92 1.88 4 10 9 8.48 70.22 4 10 9 5.38 115.16 4 10 9 4.02 4.76 4 10 9 4.74 83.33 4 10 10 38.75 15.61 4 10 10 -18.80 119.27 4 10 10 65.37 26.98 4 10 10 16.28 75.29 4 10 11 2.47 2.62 4 10 11 3.19 7.06 4 10 11 -18.77 82.36 4 11 0 45.39 17.98 4 11 0 35.19 36.23 4 11 0 31.73 12.66 4 11 0 98.85 163.59 4 11 2 2.31 1.57 4 11 3 1.76 1.52 4 11 3 9.56 24.16 4 11 3 2.32 2.25 4 11 3 38.12 219.72 4 11 4 -0.48 1.31 4 11 4 0.04 23.05 4 11 4 -0.18 2.03 4 11 4 5.86 155.20 4 11 5 6.13 2.96 4 11 5 1.29 33.64 4 11 5 6.47 3.63 4 11 5 12.82 94.74 4 11 6 5.85 2.90 4 11 6 -6.77 40.49 4 11 6 8.16 4.51 4 11 6 -0.88 77.29 4 11 7 16.78 6.96 4 11 7 -1.76 49.74 4 11 7 23.41 10.18 4 11 7 24.09 71.13 4 11 8 -0.19 1.52 4 11 8 -11.75 63.14 4 11 8 -2.84 5.58 4 11 8 30.40 105.01 4 11 9 1.09 1.82 4 11 9 -1.03 79.23 4 11 9 15.54 140.43 4 11 9 1.87 6.47 4 11 9 18.18 79.97 4 12 0 6.73 3.08 4 12 0 2.67 39.92 4 12 0 5.44 2.88 4 12 0 -96.45 244.81 4 12 1 21.66 8.76 4 12 1 23.80 30.86 4 12 1 21.45 8.88 4 12 1 3.58 115.05 4 12 2 23.97 9.70 4 12 2 21.99 29.35 4 12 2 28.27 11.53 4 12 3 0.72 1.43 4 12 3 -2.37 27.97 4 12 3 1.37 2.35 4 12 3 -7.67 121.32 4 12 4 2.24 1.80 4 12 4 7.01 32.11 4 12 4 1.06 2.63 4 12 4 11.85 71.93 4 12 5 0.95 1.57 4 12 5 8.28 34.61 4 12 5 -0.35 2.78 4 12 5 3.05 84.87 4 12 6 1.33 1.63 4 12 6 17.97 45.13 4 12 6 4.28 4.27 4 12 6 -6.29 116.25 4 12 7 7.31 3.47 4 12 7 -18.44 54.10 4 12 7 16.19 8.56 4 12 7 9.13 80.25 4 13 0 2.30 1.74 4 13 0 -3.57 53.48 4 13 0 2.79 2.34 4 13 0 13.07 86.93 4 13 1 5.93 2.87 4 13 1 16.94 37.68 4 13 1 6.56 3.74 4 13 1 0.44 69.47 4 13 2 2.62 1.89 4 13 2 -3.55 31.69 4 13 2 4.16 3.58 4 13 2 -8.08 85.73 4 13 3 13.80 5.85 4 13 3 24.95 33.93 4 13 3 22.74 9.92 4 13 4 40.27 16.08 4 13 4 36.01 37.42 4 13 4 61.49 24.78 4 13 4 91.60 129.71 4 13 5 6.57 3.22 4 13 5 3.43 33.15 4 13 5 9.67 5.61 4 13 5 9.90 91.15 4 14 0 13.20 5.61 4 14 0 29.76 55.05 4 14 0 14.89 6.86 4 14 0 -57.67 120.30 4 14 1 5.63 2.83 4 14 1 13.30 39.97 4 14 1 10.91 5.92 4 14 1 8.72 126.57 5 -16 0 12.84 5.72 5 -16 0 -16.54 93.60 5 -16 0 15.39 6.34 5 -16 0 11.29 86.30 5 -16 1 17.73 7.48 5 -16 1 3.89 80.60 5 -16 1 22.69 9.19 5 -16 1 16.28 99.53 5 -16 2 0.66 1.82 5 -16 2 9.85 52.23 5 -16 2 2.05 1.48 5 -16 2 3.27 111.34 5 -16 3 0.47 1.68 5 -16 3 -1.09 35.56 5 -16 3 1.28 1.27 5 -16 3 -50.88 113.68 5 -16 4 1.72 1.69 5 -16 4 4.81 30.69 5 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7 26.24 77.69 5 9 8 3.25 2.20 5 9 8 -76.72 126.46 5 9 8 -10.08 77.06 5 9 10 0.61 2.51 5 9 10 1.71 7.88 5 9 10 -5.63 90.12 5 10 0 1.62 1.90 5 10 1 27.58 11.22 5 10 2 45.40 18.17 5 10 3 8.72 4.20 5 10 5 1.40 1.49 5 10 5 1.55 3.05 5 10 5 6.28 90.01 5 10 6 9.58 4.22 5 10 6 12.91 6.62 5 10 6 -24.00 69.64 5 10 7 0.14 1.46 5 10 7 -5.02 73.24 5 10 7 1.41 5.88 5 10 7 -7.04 103.70 5 10 8 21.72 8.94 5 10 8 -4.76 77.52 5 10 8 0.14 121.72 5 10 8 48.15 20.54 5 10 8 -30.28 86.30 5 10 9 56.57 22.51 5 10 9 17.95 100.45 5 10 9 96.85 39.23 5 10 9 70.96 92.23 5 11 0 58.92 40.36 5 11 0 58.29 23.13 5 11 2 3.21 1.97 5 11 2 6.75 29.88 5 11 2 4.66 3.04 5 11 2 -19.97 80.03 5 11 3 2.26 1.70 5 11 3 13.77 32.84 5 11 3 2.83 2.73 5 11 3 -8.31 104.38 5 11 4 45.97 18.29 5 11 4 49.81 48.11 5 11 4 46.81 18.84 5 11 4 4.03 88.53 5 11 5 48.75 19.39 5 11 5 36.89 50.83 5 11 5 73.24 29.43 5 11 5 42.20 126.23 5 11 6 28.11 11.36 5 11 6 56.12 60.01 5 11 6 60.29 24.85 5 11 6 -13.95 85.39 5 11 7 7.77 3.61 5 11 7 34.06 72.04 5 11 7 17.93 9.94 5 11 7 39.61 84.93 5 12 0 3.93 2.15 5 12 0 6.78 37.63 5 12 0 6.14 3.71 5 12 0 -10.49 86.36 5 12 1 6.16 2.92 5 12 1 14.44 34.96 5 12 1 12.09 6.01 5 12 1 5.91 96.68 5 12 2 4.42 2.36 5 12 2 27.65 34.67 5 12 2 6.98 4.58 5 12 2 -9.53 85.90 5 12 3 0.24 1.27 5 12 3 -4.11 32.31 5 12 3 0.06 3.71 5 12 4 0.98 1.44 5 12 4 1.40 42.26 5 12 4 1.87 4.05 5 12 4 31.20 122.75 5 13 0 50.89 20.18 5 13 0 72.78 52.23 5 13 0 74.09 29.64 5 13 0 5.94 127.94 6 -16 0 0.63 2.41 6 -16 0 7.71 90.98 6 -16 0 0.77 1.40 6 -16 0 -18.01 98.68 6 -16 1 11.36 5.29 6 -16 1 -6.27 50.19 6 -16 1 16.18 6.66 6 -16 1 -9.61 119.67 6 -16 2 39.02 15.74 6 -16 2 -2.81 31.18 6 -16 2 47.34 18.78 6 -16 2 0.44 117.27 6 -16 3 6.52 3.46 6 -16 3 -1.46 24.90 6 -16 3 10.39 4.44 6 -16 3 -5.14 116.42 6 -16 4 15.66 6.65 6 -16 4 -6.75 24.93 6 -16 4 24.05 9.68 6 -16 4 22.56 103.70 6 -16 5 1.67 1.73 6 -16 5 -1.13 22.18 6 -16 5 3.81 2.00 6 -16 5 12.94 103.36 6 -16 6 -0.10 1.44 6 -16 6 -11.17 23.85 6 -16 6 0.07 1.00 6 -16 6 -1.23 101.47 6 -15 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12.79 5.42 6 -14 2 0.50 78.60 6 -14 2 15.05 6.15 6 -14 2 -47.32 78.60 6 -14 3 3.05 1.94 6 -14 3 9.53 70.27 6 -14 3 7.32 3.22 6 -14 3 6.14 87.10 6 -14 4 35.42 14.09 6 -14 4 -10.01 75.18 6 -14 4 56.11 22.15 6 -14 4 12.45 104.21 6 -14 5 2.24 1.60 6 -14 5 -6.34 68.28 6 -14 5 1.49 1.20 6 -14 5 -6.58 106.72 6 -14 6 0.46 1.28 6 -14 6 -0.80 52.82 6 -14 6 -0.22 0.87 6 -14 6 19.10 94.97 6 -14 7 0.23 1.17 6 -14 7 17.61 39.48 6 -14 7 -0.05 0.89 6 -14 7 19.00 77.69 6 -14 8 6.86 3.14 6 -14 8 3.12 32.86 6 -14 8 17.34 7.02 6 -14 8 13.32 99.08 6 -14 9 0.94 1.25 6 -14 9 7.26 26.11 6 -14 9 1.56 1.19 6 -14 9 -31.03 130.68 6 -14 10 5.27 2.56 6 -14 10 -0.76 20.64 6 -14 10 14.93 6.10 6 -14 10 -63.14 112.31 6 -14 10 13.91 60.18 6 -14 11 8.90 3.87 6 -14 11 9.64 23.90 6 -14 11 23.31 9.37 6 -14 11 58.69 121.84 6 -14 11 13.16 73.24 6 -14 12 7.44 3.34 6 -14 12 -4.19 21.91 6 -14 12 18.06 7.31 6 -14 12 5.92 142.03 6 -14 12 -21.14 119.04 6 -13 0 0.65 1.55 6 -13 0 0.78 1.13 6 -13 0 29.58 60.46 6 -13 1 1.04 1.55 6 -13 1 8.32 138.49 6 -13 1 1.85 1.30 6 -13 1 -24.47 74.21 6 -13 2 1.80 1.55 6 -13 2 10.07 83.05 6 -13 2 1.82 1.25 6 -13 2 11.26 90.18 6 -13 3 4.43 2.27 6 -13 3 1.13 72.95 6 -13 3 6.35 2.79 6 -13 3 -29.42 124.12 6 -13 4 0.52 1.15 6 -13 4 -5.67 71.36 6 -13 4 0.14 0.87 6 -13 4 6.80 165.30 6 -13 5 1.67 1.43 6 -13 5 -15.85 67.88 6 -13 5 6.31 2.77 6 -13 5 -83.73 185.44 6 -13 6 29.49 11.77 6 -13 6 -8.86 54.50 6 -13 6 55.38 21.85 6 -13 6 6.98 177.62 6 -13 7 55.67 21.99 6 -13 7 17.27 47.29 6 -13 7 87.84 34.56 6 -13 7 10.08 171.18 6 -13 8 3.10 1.75 6 -13 8 4.74 30.58 6 -13 8 1.14 0.96 6 -13 8 63.94 143.23 6 -13 9 2.46 1.54 6 -13 9 6.30 26.10 6 -13 9 3.61 1.75 6 -13 9 -10.55 96.17 6 -13 10 1.30 1.25 6 -13 10 -4.41 26.79 6 -13 10 3.53 1.76 6 -13 10 -12.19 94.80 6 -13 10 -39.75 117.22 6 -13 11 30.25 12.06 6 -13 11 27.36 25.68 6 -13 11 71.01 27.98 6 -13 11 18.19 108.60 6 -13 11 50.87 124.17 6 -13 12 12.91 5.35 6 -13 12 12.93 21.25 6 -13 12 33.07 13.16 6 -13 12 52.97 118.93 6 -13 13 1.02 1.22 6 -13 13 3.56 18.38 6 -13 13 0.25 0.92 6 -13 13 14.46 168.55 6 -12 0 8.82 3.84 6 -12 0 6.49 53.13 6 -12 1 10.61 4.48 6 -12 1 17.53 100.96 6 -12 1 11.97 4.95 6 -12 1 0.40 62.00 6 -12 2 14.58 5.96 6 -12 2 -6.11 79.91 6 -12 2 17.60 7.11 6 -12 2 -12.87 75.29 6 -12 3 3.03 1.66 6 -12 3 -29.01 83.28 6 -12 3 17.90 96.00 6 -12 4 -12.97 107.41 6 -12 6 77.57 30.54 6 -12 6 17.14 38.46 6 -12 6 114.59 45.00 6 -12 7 0.40 1.08 6 -12 7 -5.15 30.05 6 -12 7 0.77 0.84 6 -12 7 12.99 180.07 6 -12 8 3.12 1.74 6 -12 8 -8.63 33.57 6 -12 8 8.17 3.43 6 -12 8 -2.59 243.22 6 -12 9 18.73 7.56 6 -12 9 17.19 32.50 6 -12 9 31.35 12.45 6 -12 9 -34.02 128.91 6 -12 10 35.64 14.15 6 -12 10 45.04 31.91 6 -12 10 69.13 27.23 6 -12 10 -22.07 121.09 6 -12 11 15.70 6.42 6 -12 11 33.56 28.47 6 -12 11 30.94 12.29 6 -12 11 77.52 127.08 6 -12 11 48.22 158.17 6 -12 12 36.72 14.58 6 -12 12 34.53 24.91 6 -12 12 106.44 41.83 6 -12 12 14.37 108.60 6 -12 13 40.90 16.22 6 -12 13 40.63 21.25 6 -12 13 0.58 63.60 6 -12 13 -25.26 99.31 6 -12 14 0.47 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184.29 6 -11 12 8.12 3.51 6 -11 12 6.25 12.53 6 -11 12 -22.88 100.45 6 -11 12 -2.22 114.02 6 -11 13 0.33 0.98 6 -11 13 0.74 10.30 6 -11 13 -16.67 71.41 6 -11 13 -30.37 158.23 6 -11 14 52.07 20.59 6 -11 14 49.38 22.96 6 -11 15 113.28 44.53 6 -11 15 100.10 41.52 6 -11 15 2.63 33.53 6 -10 0 167.41 65.65 6 -10 0 239.28 226.62 6 -10 0 220.46 86.41 6 -10 0 154.06 80.37 6 -10 1 0.68 0.96 6 -10 1 46.41 115.79 6 -10 1 0.95 0.91 6 -10 1 -9.28 62.46 6 -10 2 7.98 3.34 6 -10 2 12.93 96.85 6 -10 2 20.33 8.11 6 -10 2 -32.00 98.79 6 -10 3 70.04 27.54 6 -10 3 122.06 101.87 6 -10 3 115.79 45.43 6 -10 3 40.14 144.99 6 -10 4 -0.11 0.84 6 -10 4 -18.99 66.85 6 -10 4 0.36 0.71 6 -10 4 34.11 140.66 6 -10 5 34.88 13.80 6 -10 5 26.87 33.26 6 -10 5 48.04 18.93 6 -10 5 -14.33 189.54 6 -10 6 1.52 1.09 6 -10 6 -0.84 19.64 6 -10 6 2.84 1.39 6 -10 6 -3.40 157.71 6 -10 7 10.05 4.14 6 -10 7 7.45 17.81 6 -10 7 27.94 11.08 6 -10 7 8.31 229.81 6 -10 8 3.30 1.65 6 -10 8 10.92 18.40 6 -10 8 6.66 2.83 6 -10 8 -30.92 100.10 6 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6 -9 6 3.49 16.07 6 -9 6 1.15 0.82 6 -9 6 16.16 227.42 6 -9 6 71.30 187.20 6 -9 7 2.45 1.28 6 -9 7 -4.29 15.49 6 -9 7 9.00 3.70 6 -9 7 34.08 225.31 6 -9 7 71.07 218.00 6 -9 8 14.23 5.74 6 -9 8 19.35 18.13 6 -9 8 32.61 12.90 6 -9 8 -101.13 221.66 6 -9 8 -66.57 339.73 6 -9 9 26.29 10.46 6 -9 9 32.46 19.41 6 -9 9 38.38 15.16 6 -9 9 -9.11 107.46 6 -9 10 2.85 1.48 6 -9 10 2.01 8.61 6 -9 10 -10.38 86.93 6 -9 10 -79.17 374.41 6 -9 12 15.73 6.36 6 -9 12 16.92 11.04 6 -9 12 -42.75 85.05 6 -9 13 50.23 19.83 6 -9 13 79.17 33.25 6 -9 13 8.02 66.34 6 -9 14 0.94 1.02 6 -9 14 6.92 10.06 6 -9 14 15.86 57.61 6 -9 15 18.87 7.61 6 -9 15 37.87 18.57 6 -9 15 17.19 32.03 6 -9 15 -20.19 52.93 6 -9 16 33.53 13.37 6 -9 16 37.71 18.66 6 -9 16 -5.67 23.02 6 -9 16 -12.55 36.17 6 -8 0 1.38 1.05 6 -8 0 34.89 87.44 6 -8 0 2.56 1.28 6 -8 0 5.73 41.51 6 -8 1 37.73 14.87 6 -8 1 42.57 57.50 6 -8 1 48.59 19.12 6 -8 1 40.97 56.59 6 -8 2 10.31 4.18 6 -8 2 7.50 47.55 6 -8 2 23.56 9.34 6 -8 2 -9.34 77.12 6 -8 3 16.90 6.74 6 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-5 4 -68.85 216.29 8 -5 5 101.81 40.62 8 -5 5 -3.49 81.91 8 -5 5 -10.74 179.45 8 -5 5 -92.12 217.38 8 -5 7 38.23 16.27 8 -5 7 -14.22 97.31 8 -5 8 41.55 17.60 8 -5 8 4.53 73.98 8 -5 9 20.87 10.63 8 -5 9 33.32 48.19 8 -5 10 29.18 13.78 8 -5 10 4.20 47.19 8 -5 10 2.24 84.08 8 -5 11 1.69 1.07 8 -5 11 2.98 7.67 8 -5 11 17.65 47.34 8 -5 11 29.94 82.14 8 -5 12 8.84 3.67 8 -5 12 8.37 10.19 8 -5 12 7.99 23.68 8 -5 12 17.86 40.76 8 -5 13 0.59 0.88 8 -5 13 1.29 10.06 8 -5 13 -0.11 19.93 8 -5 13 -1.54 38.13 8 -4 2 6.97 15.16 8 -4 3 19.56 43.88 8 -4 4 125.94 49.73 8 -4 5 6.48 5.29 8 -4 5 36.29 75.86 8 -4 6 -0.05 4.70 8 -4 6 19.34 78.89 8 -4 6 19.51 173.80 8 -4 7 9.67 6.02 8 -4 7 11.83 178.25 8 -4 8 -14.80 49.08 8 -4 8 -7.26 172.77 8 -4 9 5.58 6.27 8 -4 9 -13.61 43.12 8 -4 9 -2.06 196.27 8 -4 10 3.87 6.15 8 -4 10 -13.08 45.39 8 -4 10 -72.84 218.00 8 -4 10 6.84 57.44 8 -4 11 -0.08 7.64 8 -4 11 -5.89 33.82 8 -4 11 -40.75 205.17 8 -4 11 -35.54 56.18 8 -4 12 29.77 11.79 8 -4 12 29.74 16.51 8 -4 12 278.12 112.02 8 -4 12 4.09 212.64 8 -4 12 -12.14 35.97 8 -4 13 39.80 20.48 8 -4 13 93.09 199.92 8 -4 13 4.36 35.99 8 -3 4 -13.03 41.63 8 -3 4 46.30 42.20 8 -3 5 51.16 20.64 8 -3 5 -18.37 74.38 8 -3 5 34.03 81.74 8 -3 6 4.22 4.22 8 -3 6 -4.89 65.03 8 -3 6 49.00 125.03 8 -3 8 31.45 54.07 8 -3 9 8.42 6.29 8 -3 9 11.28 35.04 8 -3 10 18.15 9.41 8 -3 10 13.00 28.10 8 -3 11 73.52 30.44 8 -3 11 6.34 24.11 8 -3 12 11.48 4.64 8 -3 12 3.56 8.97 8 -3 12 -7.72 18.47 8 -2 4 4.22 2.10 8 -2 4 0.94 46.28 8 -2 5 2.85 2.18 8 -2 5 2.74 28.94 8 -2 6 2.60 2.82 8 -2 6 -0.76 41.86 8 -2 6 9.10 54.28 8 -2 8 -1.31 31.78 8 -2 8 -35.54 80.94 8 -2 9 -6.67 21.04 8 -2 9 103.01 116.65 8 -2 10 1.76 4.81 8 -2 10 -3.37 18.65 8 -2 10 21.77 107.52 8 -2 11 27.01 13.51 8 -2 11 3.51 16.70 8 -2 11 54.36 125.20 8 -2 12 5.88 9.38 8 -2 12 3.17 16.00 8 -2 12 28.90 121.04 8 -1 4 1.94 1.04 8 -1 4 11.54 43.56 8 -1 5 -5.08 32.92 8 -1 5 2.33 27.94 8 -1 6 19.66 8.05 8 -1 6 7.67 28.98 8 -1 6 27.97 39.18 8 -1 8 -1.97 16.42 8 -1 8 -0.97 46.66 8 -1 9 -6.09 15.59 8 -1 9 51.64 78.71 8 -1 10 -4.84 17.84 8 -1 10 -6.76 86.47 8 -1 11 13.21 8.42 8 -1 11 7.63 15.13 8 -1 11 37.45 81.39 8 -1 12 6.04 2.54 8 -1 12 3.93 7.10 8 -1 12 4.81 16.54 8 0 4 -17.28 31.99 8 0 5 -8.37 19.62 8 0 5 16.92 39.83 8 0 6 0.06 17.43 8 0 6 2.85 47.38 8 0 8 11.10 15.64 8 0 8 13.25 51.01 8 0 9 -1.15 15.29 8 0 9 -3.47 73.87 8 0 10 2.62 3.33 8 0 10 4.39 14.47 8 0 10 -24.81 64.80 8 0 11 -0.71 4.61 8 0 11 -2.86 13.97 8 0 11 -10.12 60.06 8 0 12 74.55 29.28 8 0 12 27.79 12.74 8 0 12 8.49 16.25 8 0 12 43.17 68.39 8 1 4 1.64 14.60 8 1 5 10.26 16.50 8 1 5 11.61 61.03 8 1 6 8.47 14.57 8 1 6 -28.01 63.09 8 1 7 -0.54 11.93 8 1 7 -28.47 59.72 8 1 8 -1.84 10.64 8 1 8 11.54 64.11 8 1 9 5.62 10.17 8 1 9 -4.23 75.69 8 1 10 -1.55 3.53 8 1 10 -0.27 9.17 8 1 10 -5.33 64.80 8 1 11 23.40 10.86 8 1 11 5.28 9.22 8 1 11 26.27 64.45 8 2 3 2.46 14.43 8 2 4 0.89 10.34 8 2 4 -19.76 107.41 8 2 5 8.01 6.99 8 2 5 -30.47 95.08 8 2 6 -1.67 5.80 8 2 7 5.35 6.42 8 2 7 27.73 93.94 8 2 8 2.95 6.14 8 2 8 23.96 100.79 8 2 9 4.25 7.59 8 2 9 24.69 91.38 8 2 10 46.16 19.02 8 2 10 12.76 9.02 8 2 10 24.33 69.87 8 3 2 35.15 15.59 8 3 3 0.85 3.66 8 3 3 -53.04 129.42 8 3 4 0.81 4.14 8 3 4 26.79 84.42 8 3 5 9.75 6.31 8 3 5 40.22 108.03 8 3 6 5.21 6.25 8 3 6 1.64 105.92 8 3 7 1.44 5.58 8 3 7 -21.69 125.14 8 3 8 0.50 6.29 8 3 8 -10.11 140.32 8 3 9 11.53 8.37 8 3 9 -20.56 106.66 8 4 1 7.55 4.93 8 4 2 7.77 5.11 8 4 3 7.28 5.26 8 4 3 -5.04 73.07 8 4 4 25.22 11.38 8 4 4 24.94 103.41 8 4 5 19.49 10.32 8 4 5 -15.53 72.90 8 4 6 3.13 6.62 8 4 6 33.30 123.43 8 4 7 -0.56 6.19 8 4 7 57.84 138.38 8 4 8 1.46 6.50 8 4 8 -43.87 116.53 8 5 0 0.88 3.12 8 5 1 14.01 6.54 8 5 1 -7.49 48.77 8 5 2 4.00 3.92 8 5 3 -0.26 3.88 8 5 3 -6.41 81.57 8 5 4 14.43 8.01 8 5 5 1.18 5.73 8 5 5 -71.87 145.62 8 5 6 -0.14 5.80 8 5 6 44.50 115.68 8 5 7 -1.42 6.20 8 5 7 -37.32 106.26 8 6 0 16.06 7.92 8 6 1 1.05 4.41 8 6 1 2.45 30.96 8 6 3 6.89 6.41 8 6 3 19.55 93.43 8 6 4 30.04 13.93 8 6 5 19.85 10.01 8 6 5 31.66 118.76 8 7 1 -0.97 6.61 8 7 1 -0.40 38.48 8 7 2 10.66 8.17 8 7 2 26.19 136.15 8 7 3 -0.06 6.10 8 7 3 29.39 161.76 9 -11 0 1.40 1.25 9 -11 0 19.36 80.82 9 -11 1 164.62 64.63 9 -11 1 112.08 111.85 9 -11 2 8.54 3.64 9 -11 2 -3.48 117.39 9 -11 2 -4.11 53.01 9 -11 3 5.43 23.40 9 -11 3 108.26 42.55 9 -11 3 30.94 130.05 9 -11 3 36.48 96.05 9 -11 4 21.38 8.58 9 -11 4 0.21 117.79 9 -11 4 5.79 103.24 9 -10 0 1.07 1.27 9 -10 0 -1.08 76.09 9 -10 0 -2.78 38.82 9 -10 1 0.24 1.03 9 -10 1 -5.66 92.06 9 -10 1 15.43 44.72 9 -10 2 0.43 1.08 9 -10 2 56.11 111.11 9 -10 2 -22.32 59.32 9 -10 3 10.13 4.26 9 -10 3 52.47 129.65 9 -10 4 53.31 21.06 9 -10 4 -55.28 118.76 9 -10 5 10.31 4.31 9 -10 5 1.26 84.02 9 -10 6 7.76 13.30 9 -10 6 28.96 82.99 9 -10 7 6.93 77.80 9 -9 0 1.14 1.12 9 -9 0 -2.02 66.11 9 -9 1 181.33 71.13 9 -9 1 64.40 90.18 9 -9 2 2.89 1.62 9 -9 2 -15.12 98.39 9 -9 3 16.18 6.57 9 -9 3 14.74 113.68 9 -9 4 242.19 94.97 9 -9 4 -26.11 116.93 9 -9 5 39.00 116.59 9 -9 6 4.05 105.75 9 -9 8 17.32 13.80 9 -9 8 0.46 72.38 9 -8 0 2.65 59.78 9 -8 1 91.15 73.81 9 -8 2 9.73 4.00 9 -8 3 -17.78 117.10 9 -8 4 28.45 91.26 9 -8 5 -49.04 85.67 9 -8 6 -26.88 100.50 9 -8 6 -13.77 55.55 9 -8 7 82.08 131.13 9 -8 7 12.37 46.15 9 -8 8 41.41 91.72 9 -8 8 9.05 36.29 9 -8 9 -25.10 117.67 9 -8 9 4.84 29.86 9 -7 0 76.78 30.15 9 -7 0 10.37 45.39 9 -7 1 19.72 44.06 9 -7 2 10.48 51.75 9 -7 3 -18.40 79.74 9 -7 4 -6.66 71.47 9 -7 5 57.78 83.39 9 -7 6 21.95 50.31 9 -7 7 -4.07 64.97 9 -7 7 -3.88 37.50 9 -7 8 -39.21 99.02 9 -7 8 10.66 30.02 9 -7 8 -1.95 31.40 9 -7 9 -26.02 116.30 9 -7 9 11.17 28.65 9 -7 9 -6.29 26.94 9 -6 1 52.04 45.86 9 -6 2 14.14 36.63 9 -6 3 9.07 38.92 9 -6 3 -1.04 52.33 9 -6 4 -15.87 64.28 9 -6 5 -8.05 46.97 9 -6 8 14.39 83.73 9 -6 9 -19.37 55.83 9 -6 9 -0.02 35.63 9 -5 3 4.58 28.68 9 -5 4 3.11 56.62 9 -5 4 -13.04 37.94 9 -5 5 -1.73 48.60 9 -5 6 16.68 42.71 9 -5 8 -2.27 47.03 9 -5 9 -26.67 210.36 9 -5 9 -17.77 32.50 9 -5 10 -5.17 26.79 9 -5 10 -106.21 241.62 9 -5 10 5.03 30.52 9 -4 5 -25.06 56.43 9 -4 6 3.01 87.73 9 -4 7 -15.61 65.60 9 -4 8 -0.44 130.28 9 -4 9 -4.08 22.57 9 -4 10 -1.39 18.20 9 -3 5 -10.42 56.78 9 -3 6 -23.46 57.89 9 -3 6 10.62 66.28 9 -3 7 -12.30 77.75 9 -3 8 4.13 24.41 9 -3 8 -26.91 91.89 9 -3 9 4.05 17.02 9 -3 9 -11.42 112.25 9 -2 6 -4.49 36.70 9 -2 7 2.20 22.79 9 -2 7 -26.53 59.21 9 -2 8 22.60 63.54 9 -2 9 -8.75 19.14 9 -2 9 13.13 85.96 9 -1 6 -6.46 28.96 9 -1 7 5.91 15.20 9 -1 7 51.45 81.11 9 -1 8 63.88 82.42 9 -1 9 -1.02 16.34 9 -1 9 -30.15 85.05 9 0 6 -4.26 13.41 9 0 7 -3.25 13.82 9 0 7 34.14 97.77 9 0 8 -3.72 16.27 9 0 8 -5.70 95.83 9 1 6 -6.73 12.44 9 1 7 1.80 14.03 9 2 5 1.82 10.71 9 2 6 1.46 12.74 9 3 4 3.18 11.67 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 9338 _exptl_crystal_recrystallization_method 'Sitting drop vapor diffusion'