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train_7900
What is described in this image?
Figure 3. 1H NMR spectrum of urethane acrylate oligomer.
train_7901
What is described in this image?
Figure 1 SEM Images of carbon nanotubes at (a) at low resolution (b) at high resolution.
train_7902
What is described in this image?
Fig. 1.3 Schematic representation of burette
train_7903
What is described in this image?
Fig. 15 Analysis of semicrystalline PPO with TMDC and DSC. The apparent heat capacity curves show a full separation of the latent heat measured by DSC and the underlying glass transition by TMDC. The solid fractions due to crystallinity are calculated from the latent heat by DSC, and the glass transition of the RAF is ...
train_7904
What is described in this image?
Fig. 7 The magnetic entropy change and its field exponent for Heusler-type alloy. The overshoot of exponent n occurs near the FOPT of Ni–Mn–In–Co Heusler alloy. Characteristic spikes shown in the shaded gray region
train_7905
What is described in this image?
Fig. 5. Particle size distribution for microcapsules prepared using different mass ratios of monomers/paraffin: (a) in volume and (b) in number.
train_7906
What is described in this image?
Fig. 1. Impedance spectrum of PEO-15wt% (LiCF3SO3) solid polymer electrolytes.
train_7907
What is described in this image?
Figure 1 Graphical representation of chemical structures of block copolymer PHB-b-PHHx (A), random copolymer P(HB-co-HHx) (B) and blend of PHB and PHHx (C).
train_7908
What is described in this image?
Fig. 4 DSC traces of the powder with 88 mass% amorphous fraction for the Ti48Cu39.5Ni10Co2.5 (at.%) alloy. The amorphous nanocrystalline powders are produced by a different ball-to-powder ratio (BPR) by mechanical milling (heating rate: 40 °C min-1) [42]
train_7909
What is described in this image?
Figure 5. Topographic image of bitumen B2 (20 μm × 20 μm).
train_7910
What is described in this image?
Fig. 6. Effect of angular frequency (0.1 to 100 rad/s) and temperature on the complex viscosity: a Affinisol™ 15 cP, b Affinisol™ 100 cP, cAffinisol™ 4 M, dKollidon® VA 64, and e comparison of the effect of angular frequency on the complex viscosity for different polymers at 150°C
train_7911
What is described in this image?
Fig. 11. Weight loss for neat PLA and PLEAs in NaHNO3/NaOH buffer solution (pH 10.7) plotted against time during hydrolytic degradation; PLA (j), PLEA10 (d), PLEA20 ( ), PLEA30 (N), and PLEA40 (.).
train_7912
What is described in this image?
FIG. 4. Semilogariphmic plots of the DSC cooling rate against reciprocal of absolute Tg inflection and Tg onset glass transition temperatures.
train_7913
What is described in this image?
Figure 1 The core shell model used to fit the SANS data showing the dimensions that can be calculated from the model.
train_7914
What is described in this image?
Table 3 Thermal stability parameters for pure PEG and PEG@MXene
train_7915
What is described in this image?
Figure 3. DSC thermograms of PIL (a) block and (b) random copolymers (with TFSI counteranions) at various PIL compositions from 0 to ca. 15 mol % (ca. 45 vol %, Table 1). (c) Glass transition temperatures as a function of PIL composition. The solid line corresponds to the Gordon−Taylor equation, and the dashed lines co...
train_7916
What is described in this image?
Table 3. Optical and Thermal Properties of DPP−Based Oligophenylenethiophenes
train_7917
What is described in this image?
Fig. 2. DSC curves for epoxy furan binding agent upon (1) first, (2) second, and (3) third heatings depending on (a) temperature and (b) time [6].
train_7918
What is described in this image?
Figure 12. SEM images of residues from FR-PLA composites after LOI tests: (a) PLA/30AHP, 300× magnification; (b) PLA/30AHP, 2000× magnification.
train_7919
What is described in this image?
Fig. 4. Scanning electron microscope (SEM) micrographs of untreated and WEPS-treated asphalts taken at × 3000 magnification. A. AP-5 WEPS 0 wt. %; B. AP-5 WEPS 3 wt. %; C. AP-5 WEPS 6 wt. %; D. AP-5 WEPS 9 wt. %.
train_7920
What is described in this image?
Table 2. Glass Transition Temperature (Tg) of the Poly(furfuryl methacrylate)-b-poly(2 ethylhexyl acrylate)-b-poly(furfuryl methacrylate) (FEF) Triblock Copolymers
train_7921
What is described in this image?
Fig. 1 Effect of storage time on the peroxide value and residual encapsulated oil of fish oil microencapsulated within SMP at a drying air temperature of 180 °C
train_7922
What is described in this image?
Fig. 10 – Temperature evolutions of the heat storage unit during heat storage and retrieval. (a) Pure paraffin and (b) EG(10)/paraffin(90) composite.
train_7923
What is described in this image?
Table 2 Thermophysical characteristics determined through experiments and compared with literature of PCMs investigated for temperature regulation of photovoltaics.
train_7924
What is described in this image?
Figure 8. Tapping mode AFM height images of C6PT1C6 (a and b), C6PT2C6 (c and d), C6PT3C6 (e and f), EHPT2C6 (g and h), and C6PT2C6 (i and j) films at conditions of as-cast (left) and after thermal annealing (right). Annealing conditions: 100 °C for 10 min. Scan size: 2 μm × 2 μm.
train_7925
What is described in this image?
Table 4 Calorimetric data obtained for DMPC SUVs upon addition of dendrimers (concentration 1 mol%)
train_7926
What is described in this image?
Figure 3. Dynamic mechanical analysis demonstrates the effects of (a) increasing supramolecular cross-links via UPyA concentration (upper), (b) increasing supramolecular cross-links via UPyMA concentration (middle), and (c) increasing covalent cross-links via BPAEDA concentration (lower). The glass transition increases...
train_7927
What is described in this image?
Fig. 5 XRD patterns and DSC curve observed during the dehydration process and decomposition of GCV, analyzed by a Combined XRD–DSC. (Color figure online)
train_7928
What is described in this image?
Table 2 DSC characteristic temperatures for the ball-milled Ni-Mn-Ga powder 'A', and sintered samples in vacuum 'B' and argon 'C' atmospheres from Fig. 8.
train_7929
What is described in this image?
FIG. 9. ECE as a function of applied electric field for the three different temperature regions by indirect measurement. Arrows indicate increasing temperature: from 60 C to 90 C for region I, from 97 C to 125 C for region II, and from 130 C to 165 C for region III.
train_7930
What is described in this image?
Fig. 7. Temperature dependence of E’ for PCL based materials.
train_7931
What is described in this image?
Fig. 1. (a) A typical tapping-mode atomic force microscopy (AFM) image of GONS
train_7932
What is described in this image?
Table 3 Thermal properties of MicroPCMs with various type of emulsion temperature.
train_7933
What is described in this image?
Fig. 2. Crystallization rate versus temperature for nonisothermal cold crystallization of PET at several heating rates (indicated). Notice the differences in vertical scale.
train_7934
What is described in this image?
FIGURE 2 Schematic diagram of the apparatus used in the testing of the Tg. (color figure available online).
train_7935
What is described in this image?
Fig. 18 AFM surface topography images of Bit-C as a function of temperature and corresponding DSC heating curve (images: courtesy Lab 3)
train_7936
What is described in this image?
Fig. 4. Plot of the phase angle vs. temperature observed by TMDSC and DMA with an ABS sample.
train_7937
What is described in this image?
Table 1 Chemical composition in at.-% of the selected areas on SEM micrographs in Fig. 3.
train_7938
What is described in this image?
FIG. 14. Raman line-shape parameters associated with the ES mode: top panel n(x), middle panel A2(x)/A , and bottom panel G(x). The ES mode splits into a majority and minority mode in regions II and III. See text for details. The error bars on mode frequencies are 60.1 cm21 and represent the size of the data points.
train_7939
What is described in this image?
Fig. 1. Chemical structure of ETPU.
train_7940
What is described in this image?
Figure 5. Boson peak frequency ωbos plots as a function of temperature for the (TeO2)0.9(ZnO)0.1 and (TeO2)0.8(ZnO)0.2 glasses. The inset shows the respective plot for the high-frequency molecular band at 750 cm−1 of the latter glass.
train_7941
What is described in this image?
Figure 5 shows the TEM image of T7 sample, and Fig.6 shows EDS analysis diagrams of A, B and C particles indicated in Fig.5. EDS analysis of A point showed that this region was basically composed of Zr, Ti and O, and the proportion of Zr was approximately equal to Ti. Combined with the XRD analysis, it could be inferre...
train_7942
What is described in this image?
Table 2 The electron energy shells corresponding to X-ray emission for C, Au, O and Zn elements and the values of weight, atomic and compound percentage of these elements along with their chemical formula in the (PVA–PVP)–x wt% ZnO polymer nanocomposite (PNC) films obtained from the EDX spectra.
train_7943
What is described in this image?
Fig. 8. TEM images and corresponding SAED patterns of the 292 J/mm3-printed TiNi SMA: Bright-field images of (a) cellular ultrafine martensites with (b) nanotwins marked by red rectangle in (a), (c) darkfield image of nano-sized Ti2Ni precipitates along grain boundaries of ultrafine martensites marked by yellow rectang...
train_7944
What is described in this image?
Table 3 Temperature scan rates and the frequency transformed with Eq. (12) at glass transition of polystyrene in the condition of bd2 ¼ const. in He flow.
train_7945
What is described in this image?
Table 4 Infrared spectral analysis of the samples before and after degradation PBAT band position cm−1 Position of band 25/75 cm−1 Position of band 75/25 cm−1 PLA band position cm−1
train_7946
What is described in this image?
Figure 9. Subsequent heating scans at 80 C/min after isothermal crystallization until saturation of the PLLA block within the block copolymers indicated. Left: at 120 C. Right: at 128 C.
train_7947
What is described in this image?
Fig. 2. Storage modulus (G′) of emulsion as function of frequency.
train_7948
What is described in this image?
Fig. 3. Absorbance of regolith simulants in (a) the visible
train_7949
What is described in this image?
Fig. 3. Yield (%) of acid-modified tapioca starches hydrolyzed with 6% and 12% HCl at 25 °C.
train_7950
What is described in this image?
Fig. 5 Thermal diffusivity, specific heat, and density change of the PTFE material
train_7951
What is described in this image?
Figure 6: ZTACH ACE curing using a magnetic plate with particle position represented through the process (ZTACH ACE)
train_7952
What is described in this image?
Table 2 Fraction of retained austenite in TRIP samples.
train_7953
What is described in this image?
Figure 3. The onset-temperatures of In melting and the Tni transition as a function of (re)heating rate.
train_7954
What is described in this image?
Fig. 8. DSC and TGA curves of themosets polymerized at 250 C of bis(MI-npda).
train_7955
What is described in this image?
Figure 5. Above: Crystallization and melting temperatures (obtained from the data reported in Figures 1 and 2 andTable 2) corresponding to the PCL blocks and the glass-transition temperature of the PLLAblock (data obtained from ref 29) within all copolymers versus PLLA content. Below: Crystallization and melting enthal...
train_7956
What is described in this image?
Fig. 7. Exportation window from the Setaram Calisto software (v1.088).
train_7957
What is described in this image?
Fig. 2. First DSC scans for PHB, PLA and theirs blends.
train_7958
What is described in this image?
Figure 2. Differential scanning calorimetry (DSC) thermograms of PNIPAM aqueous solution with the addition of urea at four different heating−cooling cycles (cycles 1, 5, 10, 15), where both the heating and cooling rates were 1.00 °C/min, and the PNIPAM concentration (CPNIPAM) and urea concentration (Curea) were 1.0 mg/...
train_7959
What is described in this image?
Figure 5. (a) Plot of ln T 2 g /β versus 1000/Tg of the analysed material. (b) Plot of ln β versus 1000/Tg of the studied glass β in K s−1.
train_7960
What is described in this image?
Figure 10. Calculated κlatt with application of various scattering mechanisms in comparison with the experiment values for the samples of pristine SnSe, Pb alloyed Sn0.95Pb0.05Se, Na doped and Pb alloyed Na0.01(Sn0.95Pb0.05)0.99Se.
train_7961
What is described in this image?
Fig. 10.3 Schematic representation of components of NMR spectrophotometer
train_7962
What is described in this image?
Fig. 4. (W) lnða=T2 g Þ versus ð1000=TgÞ for Ga5Se95 glass. (X) lnðaÞ versus ð1000=TgÞ for Ga5Se95 glass.
train_7963
What is described in this image?
FIG. 17. Raman mode frequency variation of CS tetrahedra ~top panel!, ES tetrahedra ~middle panel!, and CM ~bottom panel! as a function of x in SixSe12x glasses. See text for details. The error bars on mode frequencies are 60.1 cm21 and represent the size of the data points.
train_7964
What is described in this image?
Fig. 4. Thermal properties of the native cornstarch against moisture content: the melting temperature of ice (d), the glass transition temperature (j), the gelatinization (G endotherm) temperature of cornstarch (n), the melting (M1 endotherm) temperature of cornstarch (m), and the melting (M2 endotherm) temperature of ...
train_7965
What is described in this image?
Figure 6. DSC non-isothermal crystallization traces of PLA samples.
train_7966
What is described in this image?
Figure 7. (a) IR spectra of the carbonyl region of (from top to bottom) solid dispersion samples containing indomethacin and 50% PVPVA immediately after preparation, the same sample after 1-day storage at 75% RH, and the same sample after 7-day storage at 94% RH (7 days), pure amorphous indomethacin, and pure PVPVA. Th...
train_7967
What is described in this image?
Fig. 2. FT-IR spectra of the (a) PA, (b) TiO2, (c) MPCM1, (d) MPCM2 and (e) MPCM3. Fig. 3. XRD patterns of the (a) PA, (b) TiO2, (c) MPCM1, (d) MPCM2 and (e) MPCM3.
train_7968
What is described in this image?
Figure 11. DSC thermogram showing melting of sugar.
train_7969
What is described in this image?
Figure 13. Influence of cooling rate on heat effects obtained with 10%, w/w, PLLA in 57/43, w/w, mixtures. The importance of solid-liquid demixing processes increases with decreasing cooling rates. Arrows indicate the onset of solid-liquid demixing, and the line indicates the onset of liquid-liquid demixing.
train_7970
What is described in this image?
Figure 2 Tack as a function of calculated Tg-DSC (using DSC component values and the Fox equation).
train_7971
What is described in this image?
Figure 4. FESEM micrographs of the cross-section of (a) GO1/PVA and (b) gGO1.4/PVA composites at 20K magnifications and (c) gGO1.4/PVA composites at lower (10K) and (d) at higher (30K) magnifications.
train_7972
What is described in this image?
Table 4 Mechanical properties of PHBV materials.
train_7973
What is described in this image?
Figure 7 Three kinds of crosslink densities as a function of the loading amount of ZDMA.
train_7974
What is described in this image?
Fig. 14 Photograph of the gauge used as a measurement cell. (a) The rectangular 2×3 mm2 silicon frame supporting the submicron silicon nitride membrane, which is bonded to a standard chip holder. (b) Photograph of the central part of the XEN-39240 with the 60×60 μm2 heated region in the middle and six hot junctions of ...
train_7975
What is described in this image?
Figure 2. ln(ln1/(1 − α)) versus 1/T curves for Se90Sb10−xAgx glassy alloys. (a) Variation of ln(ln1/(1 − α)) versus 1/T for Se90Sb8Ag2; (b) Variation of ln(ln1/(1 − α)) versus 1/T for Se90Sb6Ag4; (c) Variation of ln(ln1/(1 − α)) versus 1/T for Se90Sb10−xAgx.
train_7976
What is described in this image?
Fig. 7 Heating DSC curves for the different cured resins.
train_7977
What is described in this image?
Figure 7. Near-infrared spectrum of pure PHMB over quartz plate (black line); deconvoluted spectrum (gray line) improves visualization of small bands.
train_7978
What is described in this image?
Fig. 3. Experimental X-ray powder patterns for 1b at room temperature (black curve) and after heating up to 100 C (orange curve), 130 C (green curve), 150 C (brown curve) and 170 C (pale green curve). At the bottom e theoretical XRD curve for polymorph 1b (blue curve) and polymorph 1a (red curve) calculated on the basi...
train_7979
What is described in this image?
Table 1 Thermal characteristic of freeze-dried milk and its fractions
train_7980
What is described in this image?
Fig. 5. Viscosity increase due to the intermolecular hydrogen bonds formation via
train_7981
What is described in this image?
Figure 1 Displacement ellipsoid plots of glutaric acid–glycine co-crystal (a) phase (I) and (b) phase (II) showing the atom-numbering scheme and 50% probability displacement ellipsoids at 300 and 200 K, respectively. H atoms are shown as arbitrary spheres.
train_7982
What is described in this image?
Fig. 16. Actual glass transition temperature and start temperature for postcuring reaction as function of curing time at 180 C.
train_7983
What is described in this image?
Fig. 2 Differential scanning calorimetry thermograms of DPPC, DPPC ? 1, and DPPC ? 2 at x = 0.01, x = 0.05, x = 0.10, and x = 0.20 using scanning rate of 2.5 C/min
train_7984
What is described in this image?
Fig. 2. The DSC scans of PMAAM-co-PMMA copolymers.
train_7985
What is described in this image?
Fig. 4. DSC (left) and TGA (right) curves overlay
train_7986
What is described in this image?
Fig. 1. Chemical structures of monomers, surfactant and
train_7987
What is described in this image?
Fig. 2. (a) Differential Scanning Calorimetry (DSC) and (b) Temperature History Method (THM) curves for paraffins wax RT 20 [42].
train_7988
What is described in this image?
Fig. 6 Quantitative 13C NMR spectra of the AD-IS, AD-PD, FDCA-PD, and FDCA-IS resins. IS isosorbide, PD propanediol, G glycerol
train_7989
What is described in this image?
Figure 5. Variable-temperature unit cell data of Form II from SCXRD, showing that the Form II crystal could transform to Form I at 225 K on heating. Vertical error bars are contained within the markers. Inset: partial enlarged detail picture, showing the very different expansion coefficients with temperature for all ax...
train_7990
What is described in this image?
Fig. 5. Microstructure of the ASTM A335 P91 steel after cooling at (a) 5 ºC/min, (b) 2 ºC/min; (c) 1.5 ºC/min.
train_7991
What is described in this image?
Figure 10. Dermal fibroblast cells surface coverage on the electrospun PVA/PHB nanofibers mats with different blend compositions after 3, 7, and 14 days.
train_7992
What is described in this image?
Fig. 8 Raman curve of the residue of PVA (PVA0) and PVA/MoS2 nanocomposite (PVA3) after calcination at 600 uC for 20 min in air.
train_7993
What is described in this image?
Figure 4. Effect of PEB7.5 amount on the DSC traces of 4% C32 in decane. Cooling scan rate: 10 °C/min and the curves for top to bottom denote with 0.8% PEB7.5, with 0.3% PEB7.5, with 0.1% PEB7.5, with 0.05% PEB7.5, and without PEB7.5.
train_7994
What is described in this image?
Table 1 Parameters used for TMDSC measurements with the Setaram BT 2.15 (first line) and the Mettler Toledo Flash DSC 1.
train_7995
What is described in this image?
Fig. 4. Temperature–time profile for the annealing experiments. The sample was melted, quenched, and then annealed at different temperatures, Ta, and times, ta. All cooling and heating rates except the final measurement for analysis (5000 K/s, red) were performed at 70,000 K/s to avoid ordering, e.g. formation of homog...
train_7996
What is described in this image?
Table 1 Onset temperature, Ton, of the calorimetric glass transition signal for different heating rates, q
train_7997
What is described in this image?
Fig. 7. Normalized heat capacity (CPN) versus temperature (T) on heating at 10 K/min as a function of the cooling rate (q).
train_7998
What is described in this image?
Fig. 5. Heat capacity at constant frequency (p = 80s) and underlying heating rate (q = 1 Kimin), but different modulation amplitudes. The maximum heating and cooling rates due to modulation are 1.18,4.71, and 47.12 K/min (from top to bottom).
train_7999
What is described in this image?
Fig. 2. Thermoanalytical curves obtained by TGA analysis of loratadine (A), PVP K30 (B), the physical mixture (C), or of the solid dispersions obtained by rotary evaporation (D) or spray-drying (E).