activity_comment
string
activity_id
int64
assay_chembl_id
string
assay_description
string
assay_type
string
bao_format
string
bao_label
string
canonical_smiles
string
data_validity_comment
null
document_chembl_id
string
document_journal
string
document_year
int64
molecule_chembl_id
string
molecule_pref_name
string
pchembl_value
float64
potential_duplicate
int64
qudt_units
string
record_id
int64
relation
string
src_id
int64
standard_flag
int64
standard_relation
string
standard_type
string
standard_units
string
standard_value
float64
target_chembl_id
string
target_organism
string
target_pref_name
string
target_tax_id
string
text_value
null
type
string
units
string
uo_units
string
value
string
ligand_efficiency__bei
string
ligand_efficiency__le
string
ligand_efficiency__lle
string
ligand_efficiency__sei
string
availability_type
float64
black_box_warning
int64
chirality
int64
first_approval
float64
helm_notation
string
inorganic_flag
int64
max_phase
string
molecule_type
string
natural_product
int64
oral
bool
parenteral
bool
polymer_flag
int64
pref_name
string
prodrug
int64
structure_type
string
therapeutic_flag
bool
topical
bool
usan_stem
string
usan_year
float64
withdrawn_flag
bool
molecule_structures__canonical_smiles
string
molecule_structures__molfile
string
molecule_structures__standard_inchi
string
molecule_structures__standard_inchi_key
string
molecule_properties__alogp
float64
molecule_properties__aromatic_rings
float64
molecule_properties__full_molformula
string
molecule_properties__full_mwt
string
molecule_properties__hba
float64
molecule_properties__hbd
float64
molecule_properties__heavy_atoms
float64
molecule_properties__mw_freebase
float64
molecule_properties__np_likeness_score
string
molecule_properties__num_ro5_violations
float64
molecule_properties__psa
float64
molecule_properties__qed_weighted
float64
molecule_properties__ro3_pass
string
molecule_properties__rtb
float64
molecule_hierarchy__active_chembl_id
string
molecule_hierarchy__molecule_chembl_id
string
molecule_hierarchy__parent_chembl_id
string
molecule_synonyms_flat
string
cross_references_flat
string
assay_category
null
assay_cell_type
string
assay_organism
string
assay_strain
string
assay_subcellular_fraction
string
assay_tax_id
float64
assay_tissue
string
assay_type_assay
string
assay_type_description
string
bao_format_assay
string
bao_label_assay
string
cell_chembl_id
string
confidence_description
string
confidence_score
int64
description
string
document_chembl_id_assay
string
relationship_description
string
relationship_type
string
src_assay_id
null
src_id_assay
int64
target_chembl_id_assay
string
tissue_chembl_id
string
variant_sequence
null
assay_parameters_flat
string
target_organism_enriched
string
target_pref_name_enriched
string
species_group_flag
bool
target_type
string
tax_id
float64
uniprot_accession
string
component_description
string
component_type
string
component_id
float64
n_components
float64
mechanism_of_action
string
action_type
string
direct_interaction
float64
disease_efficacy
float64
mechanism_comment
string
selectivity_comment
string
binding_site_comment
string
mesh_headings
string
efo_terms
string
max_phase_for_ind
string
n_indications
float64
doc__abstract
string
doc__authors
string
doc__doi
string
doc__doi_chembl
null
doc__first_page
string
doc__issue
string
doc__journal
string
doc__patent_id
null
doc__pubmed_id
float64
doc__src_id
int64
doc__title
string
doc__volume
string
doc__year
int64
null
40,611
CHEMBL750936
In vitro inhibitory activity of compound against AGT (O6-alkylguanine-DNA alkyltransferase) at a concentration of 10 uM using breast cancer MCF-7 cells, expressed as Fmol O6-MeG removed/mg of protein
B
BAO_0000219
cell-based format
Nc1nc(OCc2ccccc2)c2nc[nH]c2n1
null
CHEMBL1136584
Bioorg Med Chem Lett
2,003
CHEMBL407874
6-O-BENZYLGUANINE
null
0
null
309,926
=
1
0
=
Activity
(fM of O6-MeG removed) (mg of protein)-1
50
CHEMBL2864
Homo sapiens
Methylated-DNA--protein-cysteine methyltransferase
9606
null
Activity
(fM of O6-MeG removed) (mg of protein)-1
null
50.0
null
null
null
null
null
0
2
null
null
0
3.0
Small molecule
1
false
false
0
6-O-BENZYLGUANINE
0
MOL
false
false
null
null
false
Nc1nc(OCc2ccccc2)c2nc[nH]c2n1
RDKit 2D 18 20 0 0 0 0 0 0 0 0999 V2000 0.6696 1.8243 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3841 2.2368 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.0449 -0.2382 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.0449 0.5868 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6696 0.9993 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.6696 -0.6507 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5440 0.7443 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.6696 -1.4757 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5440 2.0792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.3841 -1.8882 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0449 2.2368 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.3841 -2.7132 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6696 -3.1257 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0449 -2.7132 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0449 -1.8882 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7594 0.9993 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0289 1.4118 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7594 1.8243 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1 2 1 0 1 5 2 0 1 11 1 0 4 3 1 0 6 3 1 0 4 5 1 0 16 4 2 0 6 8 1 0 16 7 1 0 17 7 2 0 8 10 2 0 8 15 1 0 17 9 1 0 18 9 1 0 10 12 1 0 18 11 2 0 12 13 2 0 13 14 1 0 14 15 2 0 16 18 1 0 M END > <chembl_id> CHEMBL407874 > <chembl_pref_name> 6-O-BENZYLGUANINE
InChI=1S/C12H11N5O/c13-12-16-10-9(14-7-15-10)11(17-12)18-6-8-4-2-1-3-5-8/h1-5,7H,6H2,(H3,13,14,15,16,17)
KRWMERLEINMZFT-UHFFFAOYSA-N
1.51
3
C12H11N5O
241.25
5
2
18
241.25
-0.67
0
89.71
0.73
N
3
CHEMBL407874
CHEMBL407874
CHEMBL407874
6-o-benzylguanine [OTHER] | NSC-637037 [RESEARCH_CODE] | O6-benzylguanine [OTHER] | O(6)-benzylguanine [OTHER]
null
null
MCF7
null
null
null
null
null
B
Binding
BAO_0000219
cell-based format
CHEMBL3308403
Homologous single protein target assigned
8
In vitro inhibitory activity of compound against AGT (O6-alkylguanine-DNA alkyltransferase) at a concentration of 10 uM using breast cancer MCF-7 cells, expressed as Fmol O6-MeG removed/mg of protein
CHEMBL1136584
Homologous protein target assigned
H
null
1
CHEMBL2864
null
null
null
Homo sapiens
Methylated-DNA--protein-cysteine methyltransferase
false
SINGLE PROTEIN
9,606
P16455
Methylated-DNA--protein-cysteine methyltransferase
PROTEIN
1,194
1
null
null
null
null
null
null
null
Melanoma | Glioblastoma | Lymphoma | Neoplasms | Sarcoma | Multiple Myeloma | Lymphoma, T-Cell, Cutaneous | Sezary Syndrome | Mycosis Fungoides | Gliosarcoma | Central Nervous System Neoplasms | Colorectal Neoplasms
cutaneous melanoma | glioblastoma multiforme | lymphoma | neoplasm | sarcoma | multiple myeloma | Cutaneous T-cell lymphoma | Sezary's disease | mycosis fungoides | gliosarcoma | Central Nervous System Neoplasm | colorectal cancer
3.0
12
Novel radiolabeled O(6)-benzylguanine derivatives, 6-O-[(11)C]-[(methoxymethyl)benzyl]guanines ([(11)C]p-O(6)-MMBG, 1a; [(11)C]m-O(6)-MMBG, 1b; ([(11)C]o-O(6)-MMBG, 1c), have been synthesized for evaluation as new potential positron emission tomography (PET) breast cancer imaging agents for DNA repair protein, O(6)-alkylguanine-DNA alkyltransferase (AGT).
Liu X, Zheng QH, Fei X, Wang JQ, Ohannesian DW, Erickson LC, Stone KL, Hutchins GD.
10.1016/s0960-894x(02)01048-x
null
641
4
Bioorg Med Chem Lett
null
12,639,548
1
Synthesis and preliminary biological evaluation of 6-O-[11C]-[(methoxymethyl)benzyl]guanines, new potential PET breast cancer imaging agents for the DNA repair protein AGT.
13
2,003
null
40,612
CHEMBL713457
In vitro inhibitory activity of compound against AGT (O6-alkylguanine-DNA alkyltransferase) at a concentration of 50 uM using breast cancer MCF-7 cells, expressed as Fmol O6-MeG removed/mg of protein
B
BAO_0000219
cell-based format
Nc1nc(OCc2ccccc2)c2nc[nH]c2n1
null
CHEMBL1136584
Bioorg Med Chem Lett
2,003
CHEMBL407874
6-O-BENZYLGUANINE
null
0
null
309,926
=
1
0
=
Activity
(fM of O6-MeG removed) (mg of protein)-1
19
CHEMBL2864
Homo sapiens
Methylated-DNA--protein-cysteine methyltransferase
9606
null
Activity
(fM of O6-MeG removed) (mg of protein)-1
null
19.0
null
null
null
null
null
0
2
null
null
0
3.0
Small molecule
1
false
false
0
6-O-BENZYLGUANINE
0
MOL
false
false
null
null
false
Nc1nc(OCc2ccccc2)c2nc[nH]c2n1
RDKit 2D 18 20 0 0 0 0 0 0 0 0999 V2000 0.6696 1.8243 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3841 2.2368 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.0449 -0.2382 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.0449 0.5868 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6696 0.9993 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.6696 -0.6507 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5440 0.7443 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.6696 -1.4757 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5440 2.0792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.3841 -1.8882 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0449 2.2368 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.3841 -2.7132 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6696 -3.1257 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0449 -2.7132 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0449 -1.8882 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7594 0.9993 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0289 1.4118 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7594 1.8243 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1 2 1 0 1 5 2 0 1 11 1 0 4 3 1 0 6 3 1 0 4 5 1 0 16 4 2 0 6 8 1 0 16 7 1 0 17 7 2 0 8 10 2 0 8 15 1 0 17 9 1 0 18 9 1 0 10 12 1 0 18 11 2 0 12 13 2 0 13 14 1 0 14 15 2 0 16 18 1 0 M END > <chembl_id> CHEMBL407874 > <chembl_pref_name> 6-O-BENZYLGUANINE
InChI=1S/C12H11N5O/c13-12-16-10-9(14-7-15-10)11(17-12)18-6-8-4-2-1-3-5-8/h1-5,7H,6H2,(H3,13,14,15,16,17)
KRWMERLEINMZFT-UHFFFAOYSA-N
1.51
3
C12H11N5O
241.25
5
2
18
241.25
-0.67
0
89.71
0.73
N
3
CHEMBL407874
CHEMBL407874
CHEMBL407874
6-o-benzylguanine [OTHER] | NSC-637037 [RESEARCH_CODE] | O6-benzylguanine [OTHER] | O(6)-benzylguanine [OTHER]
null
null
MCF7
null
null
null
null
null
B
Binding
BAO_0000219
cell-based format
CHEMBL3308403
Homologous single protein target assigned
8
In vitro inhibitory activity of compound against AGT (O6-alkylguanine-DNA alkyltransferase) at a concentration of 50 uM using breast cancer MCF-7 cells, expressed as Fmol O6-MeG removed/mg of protein
CHEMBL1136584
Homologous protein target assigned
H
null
1
CHEMBL2864
null
null
null
Homo sapiens
Methylated-DNA--protein-cysteine methyltransferase
false
SINGLE PROTEIN
9,606
P16455
Methylated-DNA--protein-cysteine methyltransferase
PROTEIN
1,194
1
null
null
null
null
null
null
null
Melanoma | Glioblastoma | Lymphoma | Neoplasms | Sarcoma | Multiple Myeloma | Lymphoma, T-Cell, Cutaneous | Sezary Syndrome | Mycosis Fungoides | Gliosarcoma | Central Nervous System Neoplasms | Colorectal Neoplasms
cutaneous melanoma | glioblastoma multiforme | lymphoma | neoplasm | sarcoma | multiple myeloma | Cutaneous T-cell lymphoma | Sezary's disease | mycosis fungoides | gliosarcoma | Central Nervous System Neoplasm | colorectal cancer
3.0
12
Novel radiolabeled O(6)-benzylguanine derivatives, 6-O-[(11)C]-[(methoxymethyl)benzyl]guanines ([(11)C]p-O(6)-MMBG, 1a; [(11)C]m-O(6)-MMBG, 1b; ([(11)C]o-O(6)-MMBG, 1c), have been synthesized for evaluation as new potential positron emission tomography (PET) breast cancer imaging agents for DNA repair protein, O(6)-alkylguanine-DNA alkyltransferase (AGT).
Liu X, Zheng QH, Fei X, Wang JQ, Ohannesian DW, Erickson LC, Stone KL, Hutchins GD.
10.1016/s0960-894x(02)01048-x
null
641
4
Bioorg Med Chem Lett
null
12,639,548
1
Synthesis and preliminary biological evaluation of 6-O-[11C]-[(methoxymethyl)benzyl]guanines, new potential PET breast cancer imaging agents for the DNA repair protein AGT.
13
2,003
null
40,613
CHEMBL857692
Inhibitory concentration against HCV NS3 protease was determined
B
BAO_0000357
single protein format
CC[C@H](NC(=O)[C@H](CC1CCCCC1)NC(=O)[C@@H](NC(=O)[C@H](CC(C)C)NC(=O)c1cnccn1)[C@@H](C)CC)C(=O)C(=O)N[C@H](C(=O)O)C(C)C
null
CHEMBL1136650
Bioorg Med Chem Lett
2,003
CHEMBL13442
null
5.44
0
http://www.openphacts.org/units/Nanomolar
12,748
=
1
1
=
IC50
nM
3,600
CHEMBL4620
Hepatitis C virus genotype 1a (isolate 1) (HCV)
Genome polyprotein
11104
null
IC50
uM
UO_0000065
3.6
7.60
0.15
3.14
2.41
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CC[C@H](NC(=O)[C@H](CC1CCCCC1)NC(=O)[C@@H](NC(=O)[C@H](CC(C)C)NC(=O)c1cnccn1)[C@@H](C)CC)C(=O)C(=O)N[C@H](C(=O)O)C(C)C
RDKit 2D 51 52 0 0 1 0 0 0 0 0999 V2000 9.0417 -3.5792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.3250 -3.1667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0375 -3.1667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.7542 -3.1667 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.6042 -3.1667 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.8917 -3.5792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.2583 -3.1667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.1792 -3.5792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.7542 -3.5792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.4667 -3.5792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.8917 -3.1667 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.3250 -3.5792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9750 -3.5917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 10.4667 -3.5792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.4667 -3.1667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.1792 -3.1667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.6125 -3.5792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 11.1875 -3.1667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.6958 -3.1792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 8.3250 -2.3417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 9.0417 -4.4042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.0375 -2.3417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.2583 -2.3417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.8917 -4.4042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 6.1792 -4.4042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.4667 -2.3417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 11.1792 -2.3417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.6958 -4.8292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.1792 -2.3417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3250 -4.4042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 10.4750 -4.4042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 11.9000 -3.5792 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.9750 -4.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.8750 -1.6167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.6125 -4.4042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -3.5917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3917 -1.5417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -4.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0417 -4.8167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.7542 -4.8167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 11.1875 -4.8167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.6125 -4.8167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.7000 -1.6167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.4542 -0.9042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.8042 -0.9542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1875 -1.3167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.3250 -4.8167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0417 -5.6542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.8667 -0.1917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1042 -0.9042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.6917 -0.1792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 9 1 0 4 1 1 0 12 5 1 6 6 5 1 0 7 10 1 0 8 11 1 0 9 15 1 0 10 16 1 0 11 17 1 0 12 3 1 0 13 7 1 0 14 4 1 0 15 8 1 0 16 6 1 0 17 2 1 0 18 14 1 0 19 13 2 0 20 2 2 0 21 1 2 0 22 3 2 0 23 7 2 0 24 6 2 0 25 8 2 0 15 26 1 1 27 18 2 0 28 33 2 0 16 29 1 1 30 12 1 0 14 31 1 6 32 18 1 0 33 13 1 0 34 26 1 0 17 35 1 6 36 19 1 0 37 29 1 0 38 28 1 0 39 30 1 0 40 31 1 0 41 31 1 0 30 42 1 6 43 34 1 0 44 34 1 0 45 37 1 0 46 37 1 0 47 35 1 0 48 39 1 0 49 44 1 0 50 43 1 0 51 49 1 0 51 50 1 0 38 36 2 0 M END > <chembl_id> CHEMBL13442 > <chembl_pref_name> None
InChI=1S/C36H57N7O8/c1-8-22(7)29(43-32(46)25(17-20(3)4)40-33(47)27-19-37-15-16-38-27)34(48)41-26(18-23-13-11-10-12-14-23)31(45)39-24(9-2)30(44)35(49)42-28(21(5)6)36(50)51/h15-16,19-26,28-29H,8-14,17-18H2,1-7H3,(H,39,45)(H,40,47)(H,41,48)(H,42,49)(H,43,46)(H,50,51)/t22-,24-,25-,26-,28-,29-/m0/s1
DIROIABUGPDKJH-HPWCXNRPSA-N
2.3
1
C36H57N7O8
715.89
9
6
51
715.89
-0.19
2
225.65
0.11
N
20
CHEMBL13442
CHEMBL13442
CHEMBL13442
null
null
null
null
null
null
null
null
null
B
Binding
BAO_0000357
single protein format
null
Homologous single protein target assigned
8
Inhibitory concentration against HCV NS3 protease was determined
CHEMBL1136650
Homologous protein target assigned
H
null
1
CHEMBL4620
null
null
null
Hepatitis C virus genotype 1a (isolate 1) (HCV)
Genome polyprotein
false
SINGLE PROTEIN
11,104
P26664
Genome polyprotein
PROTEIN
5,042
1
null
null
null
null
null
null
null
null
null
null
null
Using a tetrapeptide-based alpha-ketoamide template, various amines and amino acids were incorporated to explore the prime side of the HCV NS3 protease catalytic site. Glycine carboxylic acid was found to be the most effective prime group. Further optimization yielded an inhibitor with IC(50) of 0.060 microM.
Han W, Hu Z, Jiang X, Wasserman ZR, Decicco CP.
10.1016/s0960-894x(03)00031-3
null
1111
6
Bioorg Med Chem Lett
null
12,643,923
1
Glycine alpha-ketoamides as HCV NS3 protease inhibitors.
13
2,003
null
40,615
CHEMBL615267
Inhibitory activity against inosine 5'-inosine monophosphate dehydrogenase type II (IMPDH II)
B
BAO_0000357
single protein format
Nc1ccc2cnccc2c1Br
null
CHEMBL1136691
Bioorg Med Chem Lett
2,003
CHEMBL27011
null
6.26
0
http://www.openphacts.org/units/Nanomolar
39,739
=
1
1
=
IC50
nM
550
CHEMBL2002
Homo sapiens
Inosine-5'-monophosphate dehydrogenase 2
9606
null
IC50
uM
UO_0000065
0.55
28.06
0.71
3.68
16.09
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
Nc1ccc2cnccc2c1Br
RDKit 2D 12 13 0 0 0 0 0 0 0 0999 V2000 0.4542 0.2833 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.2583 0.6958 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.1750 0.6958 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.6708 1.5208 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.2500 1.5208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.1750 1.5208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.4625 1.9333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.4500 -0.5417 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 1.8875 0.2833 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.9625 1.9375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9625 0.2875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.6708 0.6958 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 2 0 4 12 1 0 5 2 2 0 6 3 1 0 7 6 2 0 8 1 1 0 9 3 1 0 10 5 1 0 11 2 1 0 12 11 2 0 5 7 1 0 10 4 2 0 M END > <chembl_id> CHEMBL27011 > <chembl_pref_name> None
InChI=1S/C9H7BrN2/c10-9-7-3-4-12-5-6(7)1-2-8(9)11/h1-5H,11H2
JDEBLBVBKMBILY-UHFFFAOYSA-N
2.58
2
C9H7BrN2
223.07
2
1
12
223.07
-0.61
0
38.91
0.7
Y
0
CHEMBL27011
CHEMBL27011
CHEMBL27011
null
null
null
null
null
null
null
null
null
B
Binding
BAO_0000357
single protein format
null
Homologous single protein target assigned
8
Inhibitory activity against inosine 5'-inosine monophosphate dehydrogenase type II (IMPDH II)
CHEMBL1136691
Homologous protein target assigned
H
null
1
CHEMBL2002
null
null
null
Homo sapiens
Inosine-5'-monophosphate dehydrogenase 2
false
SINGLE PROTEIN
9,606
P12268
Inosine-5'-monophosphate dehydrogenase 2
PROTEIN
333
1
null
null
null
null
null
null
null
null
null
null
null
Screening of our in-house compound collection led to the discovery of 5-bromo-6-amino-2-isoquinoline 1 as a weak inhibitor of IMPDH. Subsequent optimization of 1 afforded a series of novel 2-isoquinolinoaminooxazole-based inhibitors, represented by 17, with single-digit nanomolar potency against the enzyme.
Chen P, Norris D, Haslow KD, Murali Dhar TG, Pitts WJ, Watterson SH, Cheney DL, Bassolino DA, Fleener CA, Rouleau KA, Hollenbaugh DL, Townsend RM, Barrish JC, Iwanowicz EJ.
10.1016/s0960-894x(03)00107-0
null
1345
7
Bioorg Med Chem Lett
null
12,657,279
1
Identification of novel and potent isoquinoline aminooxazole-based IMPDH inhibitors.
13
2,003
null
40,616
CHEMBL761409
Ability to displace [3H]oxytocin from human OT receptor (hOT)
B
BAO_0000357
single protein format
Cc1cc2cc(C(=O)N3CCC(N4C(=O)OCc5ccccc54)CC3)ccc2[nH]1
null
CHEMBL1135944
Bioorg Med Chem Lett
2,002
CHEMBL32740
null
6.9
0
http://www.openphacts.org/units/Nanomolar
45,869
=
1
1
=
Ki
nM
125.89
CHEMBL2049
Homo sapiens
Oxytocin receptor
9606
null
Log Ki
null
UO_0000065
-6.9
17.72
0.32
2.66
10.51
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
Cc1cc2cc(C(=O)N3CCC(N4C(=O)OCc5ccccc54)CC3)ccc2[nH]1
RDKit 2D 29 33 0 0 0 0 0 0 0 0999 V2000 4.6792 -0.6667 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4000 -0.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6625 -3.9667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6667 -3.1417 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.5792 -5.4750 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.9667 -0.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.7917 -4.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.4000 0.5708 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.3750 -4.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.0667 -4.8042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.5875 -4.1292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.7917 -5.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.0792 -3.9750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6792 -1.4917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9667 0.5708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9625 -1.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3917 -1.9042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3875 -2.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9542 -2.7167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6792 0.9875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.1125 -0.6667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.9417 -4.3750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.3667 -5.2042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.0750 -5.6250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2542 -0.6667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.8917 -4.8042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2542 0.9833 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5417 -0.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5417 0.5708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 4 1 0 4 18 1 0 5 12 1 0 6 1 1 0 7 13 2 0 8 2 1 0 9 3 1 0 10 11 2 0 11 7 1 0 12 24 2 0 13 9 1 0 14 1 1 0 15 6 1 0 16 14 1 0 17 14 1 0 18 17 1 0 19 16 1 0 20 15 1 0 21 2 2 0 22 3 2 0 23 9 2 0 24 23 1 0 25 6 2 0 26 10 1 0 27 15 2 0 28 25 1 0 29 28 2 0 19 4 1 0 8 20 1 0 27 29 1 0 7 12 1 0 5 10 1 0 M END > <chembl_id> CHEMBL32740 > <chembl_pref_name> None
InChI=1S/C23H23N3O3/c1-15-12-18-13-16(6-7-20(18)24-15)22(27)25-10-8-19(9-11-25)26-21-5-3-2-4-17(21)14-29-23(26)28/h2-7,12-13,19,24H,8-11,14H2,1H3
CBFKPANXJWRIIF-UHFFFAOYSA-N
4.24
3
C23H23N3O3
389.45
3
1
29
389.45
-0.97
0
65.64
0.71
N
2
CHEMBL32740
CHEMBL32740
CHEMBL32740
null
null
null
null
null
null
null
null
null
B
Binding
BAO_0000357
single protein format
null
Homologous single protein target assigned
8
Ability to displace [3H]oxytocin from human OT receptor (hOT)
CHEMBL1135944
Homologous protein target assigned
H
null
1
CHEMBL2049
null
null
null
Homo sapiens
Oxytocin receptor
false
SINGLE PROTEIN
9,606
P30559
Oxytocin receptor
PROTEIN
389
1
null
null
null
null
null
null
null
null
null
null
null
Studies to discover novel, potent and selective oxytocin antagonists are reported. Combinatorial libraries designed to find novel replacements of fragments of oxytocin antagonist L-371,257, identified pyrimidine, thiazole, indole and benzofuran as potential alternatives to the benzoic acid moiety of L-371,257. Additional investigations identified indole and benzofuran derivatives with potent oxytocin antagonist activity.
Wyatt PG, Allen MJ, Chilcott J, Foster A, Livermore DG, Mordaunt JE, Scicinski J, Woollard PM.
10.1016/s0960-894x(02)00159-2
null
1399
10
Bioorg Med Chem Lett
null
11,992,786
1
Identification of potent and selective oxytocin antagonists. Part 1: indole and benzofuran derivatives.
12
2,002
null
40,617
CHEMBL808229
Minimum fungicidal concentration against Saccharomyces cerevisiae(no antifungal activity)
F
BAO_0000218
organism-based format
CCCCCCCCOC(=O)c1cccc(O)c1
null
CHEMBL1134164
Bioorg Med Chem Lett
2,001
CHEMBL117843
null
null
0
http://www.openphacts.org/units/MicrogramPerMilliliter
222,259
=
1
0
=
MIC
ug.mL-1
null
CHEMBL361
Saccharomyces cerevisiae
Saccharomyces cerevisiae
4932
null
MIC
ug ml-1
UO_0000274
null
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCCCCCCOC(=O)c1cccc(O)c1
RDKit 2D 18 18 0 0 0 0 0 0 0 0999 V2000 2.9375 -2.6667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4042 -2.9750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8792 -2.6667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.9417 -2.0667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.3667 -2.9750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.4542 -2.9750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.8375 -2.6625 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.4042 -3.5792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8792 -3.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3667 -3.5750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.4542 -3.5750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9667 -3.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0042 -6.2875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0042 -5.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4875 -5.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9667 -4.4792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4875 -4.7792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.5167 -6.5875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 2 2 0 4 1 2 0 5 3 1 0 6 1 1 0 7 5 1 0 8 2 1 0 9 8 2 0 10 9 1 0 11 6 1 0 12 11 1 0 13 14 1 0 14 15 1 0 15 17 1 0 16 12 1 0 17 16 1 0 18 13 1 0 10 5 2 0 M END > <chembl_id> CHEMBL117843 > <chembl_pref_name> None
InChI=1S/C15H22O3/c1-2-3-4-5-6-7-11-18-15(17)13-9-8-10-14(16)12-13/h8-10,12,16H,2-7,11H2,1H3
LAJACIZEQBXWOS-UHFFFAOYSA-N
3.91
1
C15H22O3
250.34
3
1
18
250.34
0.16
0
46.53
0.56
N
8
CHEMBL117843
CHEMBL117843
CHEMBL117843
null
null
null
null
Saccharomyces cerevisiae
null
null
4,932
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Minimum fungicidal concentration against Saccharomyces cerevisiae(no antifungal activity)
CHEMBL1134164
Non-molecular target assigned
N
null
1
CHEMBL361
null
null
null
Saccharomyces cerevisiae
Saccharomyces cerevisiae
false
ORGANISM
4,932
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Octyl gallate (3,4,5-trihydroxybenzoate) was found to possess antifungal activity against Saccharomyces cerevisiae and Zygosaccharomyces bailii, in addition to its potent antioxidant activity. Catechol moiety is essential to elicit this activity. The primary fungicidal activity of octyl gallate comes from its ability to act as a nonionic surface-active agent (surfactant). The length of the alkyl chain is not a major contributor but plays an important role in eliciting the activity.
Kubo I, Xiao P, Fujita K.
10.1016/s0960-894x(00)00656-9
null
347
3
Bioorg Med Chem Lett
null
11,212,107
1
Antifungal activity of octyl gallate: structural criteria and mode of action.
11
2,001
null
40,618
CHEMBL763559
Concentration required for maximal in vitro inhibition of aggregation of human platelet rich plasma (hPRP)
F
BAO_0000218
organism-based format
CCCCNC(=N)c1ccc(C2=NOC(CC(=O)NCCC(=O)O)C2)cc1
null
CHEMBL1133917
Bioorg Med Chem Lett
2,001
CHEMBL71066
null
7.7
0
http://www.openphacts.org/units/Nanomolar
123,884
=
1
1
=
IC50
nM
20
CHEMBL372
Homo sapiens
Homo sapiens
9606
null
IC50
uM
UO_0000065
0.02
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCCNC(=N)c1ccc(C2=NOC(CC(=O)NCCC(=O)O)C2)cc1
RDKit 2D 27 28 0 0 0 0 0 0 0 0999 V2000 3.0542 -4.0542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.5792 -3.3917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8417 -3.8125 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.7250 -3.3667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5250 -2.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0667 -2.7250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.2750 -2.8500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8542 -2.9875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.1167 -2.5750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7542 -3.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.1000 -3.3667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.1333 -2.6500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.3667 -2.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3542 -3.6667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 8.7917 -2.0917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.3375 -4.0917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3417 -2.6625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5042 -4.0875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5167 -2.6542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.9417 -2.3667 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.1458 -4.0792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.6917 -2.7125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.2000 -3.3917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.7208 -1.9375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.1250 -1.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7083 -0.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.1208 0.2083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 2 0 3 1 1 0 4 11 1 0 5 8 1 0 6 2 1 0 7 5 1 0 8 3 1 0 9 13 1 0 10 2 1 0 11 19 1 0 12 4 1 0 13 22 1 0 14 7 2 0 15 9 2 0 16 10 2 0 17 10 1 0 18 16 1 0 19 17 2 0 20 7 1 0 21 4 2 0 22 20 1 0 23 9 1 0 24 12 1 0 25 24 1 0 26 25 1 0 27 26 1 0 8 6 1 0 11 18 2 0 M END > <chembl_id> CHEMBL71066 > <chembl_pref_name> None
InChI=1S/C19H26N4O4/c1-2-3-9-22-19(20)14-6-4-13(5-7-14)16-11-15(27-23-16)12-17(24)21-10-8-18(25)26/h4-7,15H,2-3,8-12H2,1H3,(H2,20,22)(H,21,24)(H,25,26)
WFZZJCOUKAUMBN-UHFFFAOYSA-N
1.88
1
C19H26N4O4
374.44
5
4
27
374.44
-0.61
0
123.87
0.28
N
10
CHEMBL71066
CHEMBL71066
CHEMBL71066
null
null
null
null
Homo sapiens
null
null
9,606
Plasma
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Concentration required for maximal in vitro inhibition of aggregation of human platelet rich plasma (hPRP)
CHEMBL1133917
Non-molecular target assigned
N
null
1
CHEMBL372
CHEMBL3559721
null
null
Homo sapiens
Homo sapiens
false
ORGANISM
9,606
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Selective antagonism of the platelet GPIIb/IIIa receptor represents an attractive mechanism for the prevention and treatment of a number of thrombotic disease states. The antiplatelet activity of the oral GPIIb/IIIa receptor antagonists DMP 754 and DMP 802 have been disclosed. In this paper, the synthesis and biological evaluation of a series of potent N-substituted benzamidine isoxazolines are explored. The effect of benzamidine substitution on the duration of antiplatelet efficacy in dog is presented.
Sielecki TM, Liu J, Mousa SA, Racanelli AL, Hausner EA, Wexler RR, Olson RE.
10.1016/s0960-894x(01)00406-1
null
2201
16
Bioorg Med Chem Lett
null
11,514,170
1
Synthesis and pharmacology of modified amidine isoxazoline glycoprotein IIb/IIIa receptor antagonists.
11
2,001
null
40,619
CHEMBL763559
Concentration required for maximal in vitro inhibition of aggregation of human platelet rich plasma (hPRP)
F
BAO_0000218
organism-based format
COc1ccccc1CNC(=N)c1ccc(C2=NOC(CC(=O)NCCC(=O)O)C2)cc1
null
CHEMBL1133917
Bioorg Med Chem Lett
2,001
CHEMBL71111
null
7.5
0
http://www.openphacts.org/units/Nanomolar
123,888
=
1
1
=
IC50
nM
32
CHEMBL372
Homo sapiens
Homo sapiens
9606
null
IC50
uM
UO_0000065
0.032
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
COc1ccccc1CNC(=N)c1ccc(C2=NOC(CC(=O)NCCC(=O)O)C2)cc1
RDKit 2D 32 34 0 0 0 0 0 0 0 0999 V2000 3.0542 -4.0542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.5792 -3.3917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.1333 -2.6500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.7250 -3.3667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8417 -3.8125 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.5250 -2.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0667 -2.7250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.2750 -2.8500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8542 -2.9875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.1167 -2.5750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.1250 -1.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7542 -3.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.1000 -3.3667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7208 -1.9375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.3667 -2.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7083 -0.5125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3542 -3.6667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 8.7917 -2.0917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.3417 -2.6625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3375 -4.0917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5167 -2.6542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5042 -4.0875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.9417 -2.3667 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.1458 -4.0792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.6917 -2.7125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.2000 -3.3917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.1125 -0.5167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.9458 -1.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.1125 0.2083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5292 0.1958 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.3583 -0.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9458 0.2083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 2 0 3 4 1 0 4 13 1 0 5 1 1 0 6 9 1 0 7 2 1 0 8 6 1 0 9 5 1 0 10 15 1 0 11 14 1 0 12 2 1 0 13 22 1 0 14 3 1 0 15 25 1 0 16 11 2 0 17 8 2 0 18 10 2 0 19 12 2 0 20 12 1 0 21 19 1 0 22 20 2 0 23 8 1 0 24 4 2 0 25 23 1 0 26 10 1 0 27 16 1 0 28 11 1 0 29 16 1 0 30 27 1 0 31 28 2 0 32 31 1 0 9 7 1 0 21 13 2 0 29 32 2 0 M END > <chembl_id> CHEMBL71111 > <chembl_pref_name> None
InChI=1S/C23H26N4O5/c1-31-20-5-3-2-4-17(20)14-26-23(24)16-8-6-15(7-9-16)19-12-18(32-27-19)13-21(28)25-11-10-22(29)30/h2-9,18H,10-14H2,1H3,(H2,24,26)(H,25,28)(H,29,30)
HTKQOPDYLSNJQL-UHFFFAOYSA-N
2.28
2
C23H26N4O5
438.48
6
4
32
438.48
-0.74
0
133.1
0.33
N
10
CHEMBL71111
CHEMBL71111
CHEMBL71111
null
null
null
null
Homo sapiens
null
null
9,606
Plasma
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Concentration required for maximal in vitro inhibition of aggregation of human platelet rich plasma (hPRP)
CHEMBL1133917
Non-molecular target assigned
N
null
1
CHEMBL372
CHEMBL3559721
null
null
Homo sapiens
Homo sapiens
false
ORGANISM
9,606
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Selective antagonism of the platelet GPIIb/IIIa receptor represents an attractive mechanism for the prevention and treatment of a number of thrombotic disease states. The antiplatelet activity of the oral GPIIb/IIIa receptor antagonists DMP 754 and DMP 802 have been disclosed. In this paper, the synthesis and biological evaluation of a series of potent N-substituted benzamidine isoxazolines are explored. The effect of benzamidine substitution on the duration of antiplatelet efficacy in dog is presented.
Sielecki TM, Liu J, Mousa SA, Racanelli AL, Hausner EA, Wexler RR, Olson RE.
10.1016/s0960-894x(01)00406-1
null
2201
16
Bioorg Med Chem Lett
null
11,514,170
1
Synthesis and pharmacology of modified amidine isoxazoline glycoprotein IIb/IIIa receptor antagonists.
11
2,001
null
40,620
CHEMBL812612
Inhibitory concentration against potent thrombin receptor-1 (PAR-1) on human platelets
B
BAO_0000019
assay format
CCCCn1c(=N)n(CC(=O)c2cc(C(C)(C)C)c(O)c(C(C)(C)C)c2)c2ccccc21
null
CHEMBL1133830
Bioorg Med Chem Lett
2,001
CHEMBL97952
null
6.45
0
http://www.openphacts.org/units/Nanomolar
179,190
=
1
1
=
IC50
nM
359
CHEMBL3974
Homo sapiens
Proteinase-activated receptor 1
9606
null
IC50
nM
UO_0000065
359.0
14.80
0.28
0.53
9.08
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCCn1c(=N)n(CC(=O)c2cc(C(C)(C)C)c(O)c(C(C)(C)C)c2)c2ccccc21
RDKit 2D 32 34 0 0 0 0 0 0 0 0999 V2000 2.0292 -2.7250 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.5042 -3.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0292 -4.0542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.2417 -2.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2417 -3.8042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4042 -0.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0417 0.4083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8542 0.5833 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2792 -1.9375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3417 -0.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1500 -0.8167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7917 -0.3750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0875 -1.7667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3375 -3.3875 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.4917 1.0208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.2125 0.1375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.6417 -2.3792 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.1125 1.3708 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.8167 -4.8542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5250 -2.5667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5250 -4.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2250 1.3958 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7417 1.8083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.7667 -0.4750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.4667 0.9250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.1667 -0.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.6792 0.8458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3917 -5.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1792 -6.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.1875 -3.8042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.1875 -2.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7625 -6.8167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 2 1 0 4 1 1 0 5 4 1 0 6 11 1 0 7 12 2 0 8 7 1 0 9 1 1 0 10 13 1 0 11 10 2 0 12 10 1 0 13 9 1 0 14 2 2 0 15 7 1 0 16 6 1 0 17 13 2 0 18 8 1 0 19 3 1 0 20 4 2 0 21 5 2 0 22 15 1 0 23 15 1 0 24 16 1 0 25 16 1 0 26 16 1 0 27 15 1 0 28 19 1 0 29 28 1 0 30 31 2 0 31 20 1 0 32 29 1 0 3 5 1 0 21 30 1 0 8 6 2 0 M END > <chembl_id> CHEMBL97952 > <chembl_pref_name> None
InChI=1S/C27H37N3O2/c1-8-9-14-29-21-12-10-11-13-22(21)30(25(29)28)17-23(31)18-15-19(26(2,3)4)24(32)20(16-18)27(5,6)7/h10-13,15-16,28,32H,8-9,14,17H2,1-7H3
WWLIKMQMTCGMJV-UHFFFAOYSA-N
5.91
3
C27H37N3O2
435.61
5
2
32
435.61
-0.54
1
71.01
0.47
N
6
CHEMBL97952
CHEMBL97952
CHEMBL97952
null
null
null
null
Homo sapiens
null
null
9,606
null
B
Binding
BAO_0000019
assay format
null
Direct single protein target assigned
9
Inhibitory concentration against potent thrombin receptor-1 (PAR-1) on human platelets
CHEMBL1133830
Direct protein target assigned
D
null
1
CHEMBL3974
null
null
null
Homo sapiens
Proteinase-activated receptor 1
false
SINGLE PROTEIN
9,606
P25116
Proteinase-activated receptor 1
PROTEIN
2,293
1
null
null
null
null
null
null
null
null
null
null
null
Several benzimidazole derivatives have been identified as potent thrombin receptor (PAR-1) antagonists as represented by compound 1h, which showed an IC(50) of 33 nM.
Chackalamannil S, Doller D, Eagen K, Czarniecki M, Ahn HS, Foster CJ, Boykow G.
10.1016/s0960-894x(01)00555-8
null
2851
21
Bioorg Med Chem Lett
null
11,597,414
1
Potent, low molecular weight thrombin receptor antagonists.
11
2,001
null
40,621
CHEMBL699495
Inhibition of human platelet aggregation induced by high affinity thrombin receptor agonist peptide( ha-TRAP)
F
BAO_0000218
organism-based format
CCCCn1c(=N)n(CC(=O)c2cc(C(C)(C)C)c(O)c(C(C)(C)C)c2)c2ccccc21
null
CHEMBL1133830
Bioorg Med Chem Lett
2,001
CHEMBL97952
null
6.08
0
http://www.openphacts.org/units/Nanomolar
179,190
=
1
1
=
IC50
nM
825
CHEMBL372
Homo sapiens
Homo sapiens
9606
null
IC50
nM
UO_0000065
825.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCCn1c(=N)n(CC(=O)c2cc(C(C)(C)C)c(O)c(C(C)(C)C)c2)c2ccccc21
RDKit 2D 32 34 0 0 0 0 0 0 0 0999 V2000 2.0292 -2.7250 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.5042 -3.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0292 -4.0542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.2417 -2.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2417 -3.8042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4042 -0.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0417 0.4083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8542 0.5833 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2792 -1.9375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3417 -0.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1500 -0.8167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7917 -0.3750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0875 -1.7667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3375 -3.3875 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.4917 1.0208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.2125 0.1375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.6417 -2.3792 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.1125 1.3708 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.8167 -4.8542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5250 -2.5667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5250 -4.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2250 1.3958 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7417 1.8083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.7667 -0.4750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.4667 0.9250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.1667 -0.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.6792 0.8458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3917 -5.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1792 -6.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.1875 -3.8042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.1875 -2.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7625 -6.8167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 2 1 0 4 1 1 0 5 4 1 0 6 11 1 0 7 12 2 0 8 7 1 0 9 1 1 0 10 13 1 0 11 10 2 0 12 10 1 0 13 9 1 0 14 2 2 0 15 7 1 0 16 6 1 0 17 13 2 0 18 8 1 0 19 3 1 0 20 4 2 0 21 5 2 0 22 15 1 0 23 15 1 0 24 16 1 0 25 16 1 0 26 16 1 0 27 15 1 0 28 19 1 0 29 28 1 0 30 31 2 0 31 20 1 0 32 29 1 0 3 5 1 0 21 30 1 0 8 6 2 0 M END > <chembl_id> CHEMBL97952 > <chembl_pref_name> None
InChI=1S/C27H37N3O2/c1-8-9-14-29-21-12-10-11-13-22(21)30(25(29)28)17-23(31)18-15-19(26(2,3)4)24(32)20(16-18)27(5,6)7/h10-13,15-16,28,32H,8-9,14,17H2,1-7H3
WWLIKMQMTCGMJV-UHFFFAOYSA-N
5.91
3
C27H37N3O2
435.61
5
2
32
435.61
-0.54
1
71.01
0.47
N
6
CHEMBL97952
CHEMBL97952
CHEMBL97952
null
null
null
null
Homo sapiens
null
null
9,606
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Inhibition of human platelet aggregation induced by high affinity thrombin receptor agonist peptide( ha-TRAP)
CHEMBL1133830
Non-molecular target assigned
N
null
1
CHEMBL372
null
null
null
Homo sapiens
Homo sapiens
false
ORGANISM
9,606
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Several benzimidazole derivatives have been identified as potent thrombin receptor (PAR-1) antagonists as represented by compound 1h, which showed an IC(50) of 33 nM.
Chackalamannil S, Doller D, Eagen K, Czarniecki M, Ahn HS, Foster CJ, Boykow G.
10.1016/s0960-894x(01)00555-8
null
2851
21
Bioorg Med Chem Lett
null
11,597,414
1
Potent, low molecular weight thrombin receptor antagonists.
11
2,001
null
40,622
CHEMBL699496
Inhibition of human platelet aggregation induced by thrombin
F
BAO_0000218
organism-based format
CCCCn1c(=N)n(CC(=O)c2cc(C(C)(C)C)c(O)c(C(C)(C)C)c2)c2ccccc21
null
CHEMBL1133830
Bioorg Med Chem Lett
2,001
CHEMBL97952
null
5
0
http://www.openphacts.org/units/Nanomolar
179,190
=
1
1
=
IC50
nM
10,000
CHEMBL372
Homo sapiens
Homo sapiens
9606
null
IC50
nM
UO_0000065
10000.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCCn1c(=N)n(CC(=O)c2cc(C(C)(C)C)c(O)c(C(C)(C)C)c2)c2ccccc21
RDKit 2D 32 34 0 0 0 0 0 0 0 0999 V2000 2.0292 -2.7250 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.5042 -3.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0292 -4.0542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.2417 -2.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2417 -3.8042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4042 -0.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0417 0.4083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8542 0.5833 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2792 -1.9375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3417 -0.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1500 -0.8167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7917 -0.3750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0875 -1.7667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3375 -3.3875 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.4917 1.0208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.2125 0.1375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.6417 -2.3792 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.1125 1.3708 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.8167 -4.8542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5250 -2.5667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5250 -4.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2250 1.3958 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7417 1.8083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.7667 -0.4750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.4667 0.9250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.1667 -0.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.6792 0.8458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3917 -5.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1792 -6.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.1875 -3.8042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.1875 -2.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7625 -6.8167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 2 1 0 4 1 1 0 5 4 1 0 6 11 1 0 7 12 2 0 8 7 1 0 9 1 1 0 10 13 1 0 11 10 2 0 12 10 1 0 13 9 1 0 14 2 2 0 15 7 1 0 16 6 1 0 17 13 2 0 18 8 1 0 19 3 1 0 20 4 2 0 21 5 2 0 22 15 1 0 23 15 1 0 24 16 1 0 25 16 1 0 26 16 1 0 27 15 1 0 28 19 1 0 29 28 1 0 30 31 2 0 31 20 1 0 32 29 1 0 3 5 1 0 21 30 1 0 8 6 2 0 M END > <chembl_id> CHEMBL97952 > <chembl_pref_name> None
InChI=1S/C27H37N3O2/c1-8-9-14-29-21-12-10-11-13-22(21)30(25(29)28)17-23(31)18-15-19(26(2,3)4)24(32)20(16-18)27(5,6)7/h10-13,15-16,28,32H,8-9,14,17H2,1-7H3
WWLIKMQMTCGMJV-UHFFFAOYSA-N
5.91
3
C27H37N3O2
435.61
5
2
32
435.61
-0.54
1
71.01
0.47
N
6
CHEMBL97952
CHEMBL97952
CHEMBL97952
null
null
null
null
Homo sapiens
null
null
9,606
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Inhibition of human platelet aggregation induced by thrombin
CHEMBL1133830
Non-molecular target assigned
N
null
1
CHEMBL372
null
null
null
Homo sapiens
Homo sapiens
false
ORGANISM
9,606
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Several benzimidazole derivatives have been identified as potent thrombin receptor (PAR-1) antagonists as represented by compound 1h, which showed an IC(50) of 33 nM.
Chackalamannil S, Doller D, Eagen K, Czarniecki M, Ahn HS, Foster CJ, Boykow G.
10.1016/s0960-894x(01)00555-8
null
2851
21
Bioorg Med Chem Lett
null
11,597,414
1
Potent, low molecular weight thrombin receptor antagonists.
11
2,001
null
40,624
CHEMBL737009
Plasma cholesterol level was evaluated in Swiss white mice before treatment with the compound
F
BAO_0000218
organism-based format
O=C(O)c1ccccc1C(=O)Nc1ccc(Cl)cc1
null
CHEMBL1133800
Bioorg Med Chem Lett
2,001
CHEMBL90025
null
null
0
null
164,080
=
1
0
=
Cholesterol
mM l-1
2.3
CHEMBL375
Mus musculus
Mus musculus
10090
null
Cholesterol
mM l-1
null
2.3
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)c1ccccc1C(=O)Nc1ccc(Cl)cc1
RDKit 2D 19 20 0 0 0 0 0 0 0 0999 V2000 4.2875 -2.4792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1542 -4.3125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2792 -1.6542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.0792 -2.6917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.9417 -5.1042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.9917 -1.2375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -4.1000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 6.4125 -0.4042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.2042 -0.1875 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 4.9792 -0.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.7042 -1.6417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4167 -1.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6917 0.0083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -2.4875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -4.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 2 1 0 4 3 1 0 5 1 1 0 6 1 2 0 7 4 2 0 8 5 1 0 9 4 1 0 10 14 2 0 11 10 1 0 12 8 1 0 13 8 2 0 14 13 1 0 15 12 2 0 16 2 2 0 17 3 2 0 18 19 2 0 19 16 1 0 10 15 1 0 18 17 1 0 M END > <chembl_id> CHEMBL90025 > <chembl_pref_name> None
InChI=1S/C14H10ClNO3/c15-9-5-7-10(8-6-9)16-13(17)11-3-1-2-4-12(11)14(18)19/h1-8H,(H,16,17)(H,18,19)
WJSPLHRLEZJTRR-UHFFFAOYSA-N
3.29
2
C14H10ClNO3
275.69
2
2
19
275.69
-1.26
0
66.4
0.9
N
3
CHEMBL90025
CHEMBL90025
CHEMBL90025
null
null
null
null
Mus musculus
null
null
10,090
Plasma
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Plasma cholesterol level was evaluated in Swiss white mice before treatment with the compound
CHEMBL1133800
Non-molecular target assigned
N
null
1
CHEMBL375
CHEMBL3559721
null
null
Mus musculus
Mus musculus
false
ORGANISM
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of substituted N-arylphthalamic acids 3a-i has been synthesized by the reaction of phthalic anhydride 1 and aryl- or heterocyclic amines 2a-i, in the absence of solvents, in a domestic microwave oven. The formation of nine N-arylphthalamic acids was accomplished in 1-3 min giving excellent yields for compounds 3a-g, but moderate yield of compounds 3h and 3i, respectively. Compounds 3h and 3i are new. Interestingly, N-arylphthalamic acids 3a-i induced hyperlipidemia in Swiss white mice and also increased animals' body weight.
Sena VL, Srivastava RM, Oliveira SP, Lima VL.
10.1016/s0960-894x(01)00540-6
null
2671
20
Bioorg Med Chem Lett
null
11,591,498
1
Microwave assisted synthesis of N-arylphthalamic acids with hyperlipidemic activity.
11
2,001
null
40,626
CHEMBL745439
Plasma triglyceride level was evaluated in Swiss white mice before treatment with the compound
F
BAO_0000218
organism-based format
O=C(O)c1ccccc1C(=O)Nc1ccc(Cl)cc1
null
CHEMBL1133800
Bioorg Med Chem Lett
2,001
CHEMBL90025
null
null
0
null
164,080
=
1
0
=
Triglycerides
mM l-1
0.86
CHEMBL375
Mus musculus
Mus musculus
10090
null
Triglycerides
mM l-1
null
0.8600000000000001
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)c1ccccc1C(=O)Nc1ccc(Cl)cc1
RDKit 2D 19 20 0 0 0 0 0 0 0 0999 V2000 4.2875 -2.4792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1542 -4.3125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2792 -1.6542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.0792 -2.6917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.9417 -5.1042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.9917 -1.2375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -4.1000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 6.4125 -0.4042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.2042 -0.1875 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 4.9792 -0.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.7042 -1.6417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4167 -1.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6917 0.0083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -2.4875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -4.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 2 1 0 4 3 1 0 5 1 1 0 6 1 2 0 7 4 2 0 8 5 1 0 9 4 1 0 10 14 2 0 11 10 1 0 12 8 1 0 13 8 2 0 14 13 1 0 15 12 2 0 16 2 2 0 17 3 2 0 18 19 2 0 19 16 1 0 10 15 1 0 18 17 1 0 M END > <chembl_id> CHEMBL90025 > <chembl_pref_name> None
InChI=1S/C14H10ClNO3/c15-9-5-7-10(8-6-9)16-13(17)11-3-1-2-4-12(11)14(18)19/h1-8H,(H,16,17)(H,18,19)
WJSPLHRLEZJTRR-UHFFFAOYSA-N
3.29
2
C14H10ClNO3
275.69
2
2
19
275.69
-1.26
0
66.4
0.9
N
3
CHEMBL90025
CHEMBL90025
CHEMBL90025
null
null
null
null
Mus musculus
null
null
10,090
Plasma
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Plasma triglyceride level was evaluated in Swiss white mice before treatment with the compound
CHEMBL1133800
Non-molecular target assigned
N
null
1
CHEMBL375
CHEMBL3559721
null
null
Mus musculus
Mus musculus
false
ORGANISM
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of substituted N-arylphthalamic acids 3a-i has been synthesized by the reaction of phthalic anhydride 1 and aryl- or heterocyclic amines 2a-i, in the absence of solvents, in a domestic microwave oven. The formation of nine N-arylphthalamic acids was accomplished in 1-3 min giving excellent yields for compounds 3a-g, but moderate yield of compounds 3h and 3i, respectively. Compounds 3h and 3i are new. Interestingly, N-arylphthalamic acids 3a-i induced hyperlipidemia in Swiss white mice and also increased animals' body weight.
Sena VL, Srivastava RM, Oliveira SP, Lima VL.
10.1016/s0960-894x(01)00540-6
null
2671
20
Bioorg Med Chem Lett
null
11,591,498
1
Microwave assisted synthesis of N-arylphthalamic acids with hyperlipidemic activity.
11
2,001
null
40,628
CHEMBL733793
Animal body weight was evaluated in Swiss white mice before treatment with the compound
F
BAO_0000218
organism-based format
O=C(O)c1ccccc1C(=O)Nc1ccc(Cl)cc1
null
CHEMBL1133800
Bioorg Med Chem Lett
2,001
CHEMBL90025
null
null
0
http://qudt.org/vocab/unit#Gram
164,080
=
1
0
=
Body weight
g
25
CHEMBL375
Mus musculus
Mus musculus
10090
null
Body weight
g
UO_0000021
25.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)c1ccccc1C(=O)Nc1ccc(Cl)cc1
RDKit 2D 19 20 0 0 0 0 0 0 0 0999 V2000 4.2875 -2.4792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1542 -4.3125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2792 -1.6542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.0792 -2.6917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.9417 -5.1042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.9917 -1.2375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -4.1000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 6.4125 -0.4042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.2042 -0.1875 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 4.9792 -0.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.7042 -1.6417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4167 -1.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6917 0.0083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -2.4875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -4.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 2 1 0 4 3 1 0 5 1 1 0 6 1 2 0 7 4 2 0 8 5 1 0 9 4 1 0 10 14 2 0 11 10 1 0 12 8 1 0 13 8 2 0 14 13 1 0 15 12 2 0 16 2 2 0 17 3 2 0 18 19 2 0 19 16 1 0 10 15 1 0 18 17 1 0 M END > <chembl_id> CHEMBL90025 > <chembl_pref_name> None
InChI=1S/C14H10ClNO3/c15-9-5-7-10(8-6-9)16-13(17)11-3-1-2-4-12(11)14(18)19/h1-8H,(H,16,17)(H,18,19)
WJSPLHRLEZJTRR-UHFFFAOYSA-N
3.29
2
C14H10ClNO3
275.69
2
2
19
275.69
-1.26
0
66.4
0.9
N
3
CHEMBL90025
CHEMBL90025
CHEMBL90025
null
null
null
null
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Animal body weight was evaluated in Swiss white mice before treatment with the compound
CHEMBL1133800
Non-molecular target assigned
N
null
1
CHEMBL375
null
null
null
Mus musculus
Mus musculus
false
ORGANISM
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of substituted N-arylphthalamic acids 3a-i has been synthesized by the reaction of phthalic anhydride 1 and aryl- or heterocyclic amines 2a-i, in the absence of solvents, in a domestic microwave oven. The formation of nine N-arylphthalamic acids was accomplished in 1-3 min giving excellent yields for compounds 3a-g, but moderate yield of compounds 3h and 3i, respectively. Compounds 3h and 3i are new. Interestingly, N-arylphthalamic acids 3a-i induced hyperlipidemia in Swiss white mice and also increased animals' body weight.
Sena VL, Srivastava RM, Oliveira SP, Lima VL.
10.1016/s0960-894x(01)00540-6
null
2671
20
Bioorg Med Chem Lett
null
11,591,498
1
Microwave assisted synthesis of N-arylphthalamic acids with hyperlipidemic activity.
11
2,001
null
40,629
CHEMBL733794
Animal body weight was evaluated in Swiss white mice treated with 20 mg/kg/day of ip administration for 14 days
F
BAO_0000218
organism-based format
O=C(O)c1ccccc1C(=O)Nc1ccc(Cl)cc1
null
CHEMBL1133800
Bioorg Med Chem Lett
2,001
CHEMBL90025
null
null
0
http://qudt.org/vocab/unit#Gram
164,080
=
1
0
=
Body weight
g
28
CHEMBL375
Mus musculus
Mus musculus
10090
null
Body weight
g
UO_0000021
28.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)c1ccccc1C(=O)Nc1ccc(Cl)cc1
RDKit 2D 19 20 0 0 0 0 0 0 0 0999 V2000 4.2875 -2.4792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1542 -4.3125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2792 -1.6542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.0792 -2.6917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.9417 -5.1042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.9917 -1.2375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -4.1000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 6.4125 -0.4042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.2042 -0.1875 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 4.9792 -0.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.7042 -1.6417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4167 -1.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6917 0.0083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -2.4875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -4.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 2 1 0 4 3 1 0 5 1 1 0 6 1 2 0 7 4 2 0 8 5 1 0 9 4 1 0 10 14 2 0 11 10 1 0 12 8 1 0 13 8 2 0 14 13 1 0 15 12 2 0 16 2 2 0 17 3 2 0 18 19 2 0 19 16 1 0 10 15 1 0 18 17 1 0 M END > <chembl_id> CHEMBL90025 > <chembl_pref_name> None
InChI=1S/C14H10ClNO3/c15-9-5-7-10(8-6-9)16-13(17)11-3-1-2-4-12(11)14(18)19/h1-8H,(H,16,17)(H,18,19)
WJSPLHRLEZJTRR-UHFFFAOYSA-N
3.29
2
C14H10ClNO3
275.69
2
2
19
275.69
-1.26
0
66.4
0.9
N
3
CHEMBL90025
CHEMBL90025
CHEMBL90025
null
null
null
null
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Animal body weight was evaluated in Swiss white mice treated with 20 mg/kg/day of ip administration for 14 days
CHEMBL1133800
Non-molecular target assigned
N
null
1
CHEMBL375
null
null
ROUTE=None None
Mus musculus
Mus musculus
false
ORGANISM
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of substituted N-arylphthalamic acids 3a-i has been synthesized by the reaction of phthalic anhydride 1 and aryl- or heterocyclic amines 2a-i, in the absence of solvents, in a domestic microwave oven. The formation of nine N-arylphthalamic acids was accomplished in 1-3 min giving excellent yields for compounds 3a-g, but moderate yield of compounds 3h and 3i, respectively. Compounds 3h and 3i are new. Interestingly, N-arylphthalamic acids 3a-i induced hyperlipidemia in Swiss white mice and also increased animals' body weight.
Sena VL, Srivastava RM, Oliveira SP, Lima VL.
10.1016/s0960-894x(01)00540-6
null
2671
20
Bioorg Med Chem Lett
null
11,591,498
1
Microwave assisted synthesis of N-arylphthalamic acids with hyperlipidemic activity.
11
2,001
null
40,630
CHEMBL737009
Plasma cholesterol level was evaluated in Swiss white mice before treatment with the compound
F
BAO_0000218
organism-based format
O=C(O)c1ccccc1C(=O)Nn1cnnc1
null
CHEMBL1133800
Bioorg Med Chem Lett
2,001
CHEMBL262903
null
null
0
null
164,077
=
1
0
=
Cholesterol
mM l-1
2.46
CHEMBL375
Mus musculus
Mus musculus
10090
null
Cholesterol
mM l-1
null
2.46
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)c1ccccc1C(=O)Nn1cnnc1
RDKit 2D 17 18 0 0 0 0 0 0 0 0999 V2000 4.2875 -2.4792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9917 -1.2375 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.2917 -0.9500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.8750 -0.2417 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2792 -1.6542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.7417 -1.5667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0667 -0.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1542 -4.3125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0792 -2.6917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.9417 -5.1042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -4.1000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -2.4875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -4.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 6 1 0 3 8 2 0 4 9 2 0 5 1 1 0 6 1 1 0 7 5 1 0 8 2 1 0 9 2 1 0 10 7 1 0 11 1 2 0 12 10 2 0 13 10 1 0 14 5 2 0 15 7 2 0 16 17 2 0 17 14 1 0 4 3 1 0 15 16 1 0 M END > <chembl_id> CHEMBL262903 > <chembl_pref_name> None
InChI=1S/C10H8N4O3/c15-9(13-14-5-11-12-6-14)7-3-1-2-4-8(7)10(16)17/h1-6H,(H,13,15)(H,16,17)
JXXNYVAHSXIBNI-UHFFFAOYSA-N
0.36
2
C10H8N4O3
232.20
5
2
17
232.2
-1.14
0
97.11
0.8
N
3
CHEMBL262903
CHEMBL262903
CHEMBL262903
null
null
null
null
Mus musculus
null
null
10,090
Plasma
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Plasma cholesterol level was evaluated in Swiss white mice before treatment with the compound
CHEMBL1133800
Non-molecular target assigned
N
null
1
CHEMBL375
CHEMBL3559721
null
null
Mus musculus
Mus musculus
false
ORGANISM
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of substituted N-arylphthalamic acids 3a-i has been synthesized by the reaction of phthalic anhydride 1 and aryl- or heterocyclic amines 2a-i, in the absence of solvents, in a domestic microwave oven. The formation of nine N-arylphthalamic acids was accomplished in 1-3 min giving excellent yields for compounds 3a-g, but moderate yield of compounds 3h and 3i, respectively. Compounds 3h and 3i are new. Interestingly, N-arylphthalamic acids 3a-i induced hyperlipidemia in Swiss white mice and also increased animals' body weight.
Sena VL, Srivastava RM, Oliveira SP, Lima VL.
10.1016/s0960-894x(01)00540-6
null
2671
20
Bioorg Med Chem Lett
null
11,591,498
1
Microwave assisted synthesis of N-arylphthalamic acids with hyperlipidemic activity.
11
2,001
null
40,631
CHEMBL737010
Plasma cholesterol level was evaluated in Swiss white mice treated with 20 mg/kg/day of ip administration for 14 days
F
BAO_0000218
organism-based format
O=C(O)c1ccccc1C(=O)Nn1cnnc1
null
CHEMBL1133800
Bioorg Med Chem Lett
2,001
CHEMBL262903
null
null
0
null
164,077
=
1
0
=
Cholesterol
mM l-1
2.95
CHEMBL375
Mus musculus
Mus musculus
10090
null
Cholesterol
mM l-1
null
2.95
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)c1ccccc1C(=O)Nn1cnnc1
RDKit 2D 17 18 0 0 0 0 0 0 0 0999 V2000 4.2875 -2.4792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9917 -1.2375 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.2917 -0.9500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.8750 -0.2417 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2792 -1.6542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.7417 -1.5667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0667 -0.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1542 -4.3125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0792 -2.6917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.9417 -5.1042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -4.1000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -2.4875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -4.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 6 1 0 3 8 2 0 4 9 2 0 5 1 1 0 6 1 1 0 7 5 1 0 8 2 1 0 9 2 1 0 10 7 1 0 11 1 2 0 12 10 2 0 13 10 1 0 14 5 2 0 15 7 2 0 16 17 2 0 17 14 1 0 4 3 1 0 15 16 1 0 M END > <chembl_id> CHEMBL262903 > <chembl_pref_name> None
InChI=1S/C10H8N4O3/c15-9(13-14-5-11-12-6-14)7-3-1-2-4-8(7)10(16)17/h1-6H,(H,13,15)(H,16,17)
JXXNYVAHSXIBNI-UHFFFAOYSA-N
0.36
2
C10H8N4O3
232.20
5
2
17
232.2
-1.14
0
97.11
0.8
N
3
CHEMBL262903
CHEMBL262903
CHEMBL262903
null
null
null
null
Mus musculus
null
null
10,090
Plasma
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Plasma cholesterol level was evaluated in Swiss white mice treated with 20 mg/kg/day of ip administration for 14 days
CHEMBL1133800
Non-molecular target assigned
N
null
1
CHEMBL375
CHEMBL3559721
null
ROUTE=None None
Mus musculus
Mus musculus
false
ORGANISM
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of substituted N-arylphthalamic acids 3a-i has been synthesized by the reaction of phthalic anhydride 1 and aryl- or heterocyclic amines 2a-i, in the absence of solvents, in a domestic microwave oven. The formation of nine N-arylphthalamic acids was accomplished in 1-3 min giving excellent yields for compounds 3a-g, but moderate yield of compounds 3h and 3i, respectively. Compounds 3h and 3i are new. Interestingly, N-arylphthalamic acids 3a-i induced hyperlipidemia in Swiss white mice and also increased animals' body weight.
Sena VL, Srivastava RM, Oliveira SP, Lima VL.
10.1016/s0960-894x(01)00540-6
null
2671
20
Bioorg Med Chem Lett
null
11,591,498
1
Microwave assisted synthesis of N-arylphthalamic acids with hyperlipidemic activity.
11
2,001
null
40,632
CHEMBL745439
Plasma triglyceride level was evaluated in Swiss white mice before treatment with the compound
F
BAO_0000218
organism-based format
O=C(O)c1ccccc1C(=O)Nn1cnnc1
null
CHEMBL1133800
Bioorg Med Chem Lett
2,001
CHEMBL262903
null
null
0
null
164,077
=
1
0
=
Triglycerides
mM l-1
1.12
CHEMBL375
Mus musculus
Mus musculus
10090
null
Triglycerides
mM l-1
null
1.12
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)c1ccccc1C(=O)Nn1cnnc1
RDKit 2D 17 18 0 0 0 0 0 0 0 0999 V2000 4.2875 -2.4792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9917 -1.2375 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.2917 -0.9500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.8750 -0.2417 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2792 -1.6542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.7417 -1.5667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0667 -0.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1542 -4.3125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0792 -2.6917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.9417 -5.1042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -4.1000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -2.4875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -4.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 6 1 0 3 8 2 0 4 9 2 0 5 1 1 0 6 1 1 0 7 5 1 0 8 2 1 0 9 2 1 0 10 7 1 0 11 1 2 0 12 10 2 0 13 10 1 0 14 5 2 0 15 7 2 0 16 17 2 0 17 14 1 0 4 3 1 0 15 16 1 0 M END > <chembl_id> CHEMBL262903 > <chembl_pref_name> None
InChI=1S/C10H8N4O3/c15-9(13-14-5-11-12-6-14)7-3-1-2-4-8(7)10(16)17/h1-6H,(H,13,15)(H,16,17)
JXXNYVAHSXIBNI-UHFFFAOYSA-N
0.36
2
C10H8N4O3
232.20
5
2
17
232.2
-1.14
0
97.11
0.8
N
3
CHEMBL262903
CHEMBL262903
CHEMBL262903
null
null
null
null
Mus musculus
null
null
10,090
Plasma
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Plasma triglyceride level was evaluated in Swiss white mice before treatment with the compound
CHEMBL1133800
Non-molecular target assigned
N
null
1
CHEMBL375
CHEMBL3559721
null
null
Mus musculus
Mus musculus
false
ORGANISM
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of substituted N-arylphthalamic acids 3a-i has been synthesized by the reaction of phthalic anhydride 1 and aryl- or heterocyclic amines 2a-i, in the absence of solvents, in a domestic microwave oven. The formation of nine N-arylphthalamic acids was accomplished in 1-3 min giving excellent yields for compounds 3a-g, but moderate yield of compounds 3h and 3i, respectively. Compounds 3h and 3i are new. Interestingly, N-arylphthalamic acids 3a-i induced hyperlipidemia in Swiss white mice and also increased animals' body weight.
Sena VL, Srivastava RM, Oliveira SP, Lima VL.
10.1016/s0960-894x(01)00540-6
null
2671
20
Bioorg Med Chem Lett
null
11,591,498
1
Microwave assisted synthesis of N-arylphthalamic acids with hyperlipidemic activity.
11
2,001
null
40,634
CHEMBL733793
Animal body weight was evaluated in Swiss white mice before treatment with the compound
F
BAO_0000218
organism-based format
O=C(O)c1ccccc1C(=O)Nn1cnnc1
null
CHEMBL1133800
Bioorg Med Chem Lett
2,001
CHEMBL262903
null
null
0
http://qudt.org/vocab/unit#Gram
164,077
=
1
0
=
Body weight
g
35
CHEMBL375
Mus musculus
Mus musculus
10090
null
Body weight
g
UO_0000021
35.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)c1ccccc1C(=O)Nn1cnnc1
RDKit 2D 17 18 0 0 0 0 0 0 0 0999 V2000 4.2875 -2.4792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9917 -1.2375 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.2917 -0.9500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.8750 -0.2417 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2792 -1.6542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.7417 -1.5667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0667 -0.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1542 -4.3125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0792 -2.6917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.9417 -5.1042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -4.1000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -2.4875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -4.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 6 1 0 3 8 2 0 4 9 2 0 5 1 1 0 6 1 1 0 7 5 1 0 8 2 1 0 9 2 1 0 10 7 1 0 11 1 2 0 12 10 2 0 13 10 1 0 14 5 2 0 15 7 2 0 16 17 2 0 17 14 1 0 4 3 1 0 15 16 1 0 M END > <chembl_id> CHEMBL262903 > <chembl_pref_name> None
InChI=1S/C10H8N4O3/c15-9(13-14-5-11-12-6-14)7-3-1-2-4-8(7)10(16)17/h1-6H,(H,13,15)(H,16,17)
JXXNYVAHSXIBNI-UHFFFAOYSA-N
0.36
2
C10H8N4O3
232.20
5
2
17
232.2
-1.14
0
97.11
0.8
N
3
CHEMBL262903
CHEMBL262903
CHEMBL262903
null
null
null
null
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Animal body weight was evaluated in Swiss white mice before treatment with the compound
CHEMBL1133800
Non-molecular target assigned
N
null
1
CHEMBL375
null
null
null
Mus musculus
Mus musculus
false
ORGANISM
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of substituted N-arylphthalamic acids 3a-i has been synthesized by the reaction of phthalic anhydride 1 and aryl- or heterocyclic amines 2a-i, in the absence of solvents, in a domestic microwave oven. The formation of nine N-arylphthalamic acids was accomplished in 1-3 min giving excellent yields for compounds 3a-g, but moderate yield of compounds 3h and 3i, respectively. Compounds 3h and 3i are new. Interestingly, N-arylphthalamic acids 3a-i induced hyperlipidemia in Swiss white mice and also increased animals' body weight.
Sena VL, Srivastava RM, Oliveira SP, Lima VL.
10.1016/s0960-894x(01)00540-6
null
2671
20
Bioorg Med Chem Lett
null
11,591,498
1
Microwave assisted synthesis of N-arylphthalamic acids with hyperlipidemic activity.
11
2,001
null
40,635
CHEMBL733794
Animal body weight was evaluated in Swiss white mice treated with 20 mg/kg/day of ip administration for 14 days
F
BAO_0000218
organism-based format
O=C(O)c1ccccc1C(=O)Nn1cnnc1
null
CHEMBL1133800
Bioorg Med Chem Lett
2,001
CHEMBL262903
null
null
0
http://qudt.org/vocab/unit#Gram
164,077
=
1
0
=
Body weight
g
39
CHEMBL375
Mus musculus
Mus musculus
10090
null
Body weight
g
UO_0000021
39.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)c1ccccc1C(=O)Nn1cnnc1
RDKit 2D 17 18 0 0 0 0 0 0 0 0999 V2000 4.2875 -2.4792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9917 -1.2375 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.2917 -0.9500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.8750 -0.2417 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2792 -1.6542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5750 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.7417 -1.5667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0667 -0.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1542 -4.3125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0792 -2.6917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.9417 -5.1042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -4.1000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -2.4875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8542 -4.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -2.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 6 1 0 3 8 2 0 4 9 2 0 5 1 1 0 6 1 1 0 7 5 1 0 8 2 1 0 9 2 1 0 10 7 1 0 11 1 2 0 12 10 2 0 13 10 1 0 14 5 2 0 15 7 2 0 16 17 2 0 17 14 1 0 4 3 1 0 15 16 1 0 M END > <chembl_id> CHEMBL262903 > <chembl_pref_name> None
InChI=1S/C10H8N4O3/c15-9(13-14-5-11-12-6-14)7-3-1-2-4-8(7)10(16)17/h1-6H,(H,13,15)(H,16,17)
JXXNYVAHSXIBNI-UHFFFAOYSA-N
0.36
2
C10H8N4O3
232.20
5
2
17
232.2
-1.14
0
97.11
0.8
N
3
CHEMBL262903
CHEMBL262903
CHEMBL262903
null
null
null
null
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Animal body weight was evaluated in Swiss white mice treated with 20 mg/kg/day of ip administration for 14 days
CHEMBL1133800
Non-molecular target assigned
N
null
1
CHEMBL375
null
null
ROUTE=None None
Mus musculus
Mus musculus
false
ORGANISM
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of substituted N-arylphthalamic acids 3a-i has been synthesized by the reaction of phthalic anhydride 1 and aryl- or heterocyclic amines 2a-i, in the absence of solvents, in a domestic microwave oven. The formation of nine N-arylphthalamic acids was accomplished in 1-3 min giving excellent yields for compounds 3a-g, but moderate yield of compounds 3h and 3i, respectively. Compounds 3h and 3i are new. Interestingly, N-arylphthalamic acids 3a-i induced hyperlipidemia in Swiss white mice and also increased animals' body weight.
Sena VL, Srivastava RM, Oliveira SP, Lima VL.
10.1016/s0960-894x(01)00540-6
null
2671
20
Bioorg Med Chem Lett
null
11,591,498
1
Microwave assisted synthesis of N-arylphthalamic acids with hyperlipidemic activity.
11
2,001
null
34,377
CHEMBL636019
True partition coefficient corrected for ionization was determined
P
BAO_0000100
small-molecule physicochemical format
CN(C)CCc1c[nH]c2cccc(O)c12
null
CHEMBL1121785
J Med Chem
1,981
CHEMBL65547
PSILOCIN
null
0
null
113,388
=
1
0
=
pKa
null
42.1
CHEMBL2362975
null
No relevant target
null
null
pKa
null
null
42.1
null
null
null
null
null
0
2
null
null
0
2.0
Small molecule
1
false
false
0
PSILOCIN
0
MOL
false
false
deu-
null
false
CN(C)CCc1c[nH]c2cccc(O)c12
RDKit 2D 15 16 0 0 0 0 0 0 0 0999 V2000 3.0857 -19.6308 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0845 -20.4581 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7992 -20.8708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7974 -19.2180 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3025 -20.7133 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.7903 -20.0417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3020 -19.3703 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5127 -19.6272 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5130 -20.4572 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.5567 -18.5857 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.3635 -18.4139 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.6180 -17.6293 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.4248 -17.4574 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.0659 -17.0165 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7950 -18.3931 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1 2 2 0 8 4 2 0 5 6 1 0 7 8 1 0 9 5 1 0 4 1 1 0 7 10 1 0 8 9 1 0 10 11 1 0 11 12 1 0 2 3 1 0 12 13 1 0 6 7 2 0 12 14 1 0 3 9 2 0 4 15 1 0 M END > <chembl_id> CHEMBL65547 > <chembl_pref_name> PSILOCIN
InChI=1S/C12H16N2O/c1-14(2)7-6-9-8-13-10-4-3-5-11(15)12(9)10/h3-5,8,13,15H,6-7H2,1-2H3
SPCIYGNTAMCTRO-UHFFFAOYSA-N
1.98
2
C12H16N2O
204.27
2
2
15
204.27
0.31
0
39.26
0.8
Y
3
CHEMBL65547
CHEMBL65547
CHEMBL65547
4-ho-dmt [OTHER] | Psilocin [OTHER] | Psilocyn [OTHER]
null
null
null
null
null
null
null
null
P
Physicochemical
BAO_0000100
small-molecule physicochemical format
null
Default value - Target unknown or has yet to be assigned
0
True partition coefficient corrected for ionization was determined
CHEMBL1121785
Default value - Target has yet to be curated
U
null
1
CHEMBL2362975
null
null
null
null
No relevant target
false
NO TARGET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The 360-MHz 1H NMR spectra of bufotenin and psilocin were obtained, both as the free bases in CDCl3 and as protonated salts in D2O. Coupling constants for the side-chain methylenes were derived using the LAOCN3 program. These time-averaged coupling constants indicate that the trans and gauche rotamers of both compounds have about equal energy in D2O. There is a slight excess of the trans rotamer of bufotenin in CDCl3. For psilocin, in contrast, the gauche form is highly favored in CDCl3. The magnitude of this stabilization was estimated at about 1 kcal/mol using rotamer populations and free energy of transfer from published partitioning studies. It is suggested that this could result from a very weak hydrogen bond. On the other hand, the difference in partitioning between bufotenin and psilocin, which seems to be a major determinant of biological activity, is largely due to a difference in the basicity of the two compounds. The pKa values for the amino group of psilocin and bufotenin were determined to be 8.47 and 9.67, respectively.
Migliaccio GP, Shieh TL, Byrn SR, Hathaway BA, Nichols DE.
10.1021/jm00134a016
null
206
2
J Med Chem
null
6,259,355
1
Comparison of solution conformational preferences for the hallucinogens bufotenin and psilocin using 360-MHz proton NMR spectroscopy.
24
1,981
null
34,378
CHEMBL638404
Partition coefficient of octanol and water was determined
P
BAO_0000100
small-molecule physicochemical format
CN(C)CCc1c[nH]c2cccc(O)c12
null
CHEMBL1121785
J Med Chem
1,981
CHEMBL65547
PSILOCIN
null
0
null
113,388
=
1
0
=
Poct
null
0.68
CHEMBL2362975
null
No relevant target
null
null
Poct
null
null
0.68
null
null
null
null
null
0
2
null
null
0
2.0
Small molecule
1
false
false
0
PSILOCIN
0
MOL
false
false
deu-
null
false
CN(C)CCc1c[nH]c2cccc(O)c12
RDKit 2D 15 16 0 0 0 0 0 0 0 0999 V2000 3.0857 -19.6308 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0845 -20.4581 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7992 -20.8708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7974 -19.2180 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3025 -20.7133 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.7903 -20.0417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3020 -19.3703 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5127 -19.6272 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5130 -20.4572 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.5567 -18.5857 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.3635 -18.4139 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.6180 -17.6293 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.4248 -17.4574 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.0659 -17.0165 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7950 -18.3931 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1 2 2 0 8 4 2 0 5 6 1 0 7 8 1 0 9 5 1 0 4 1 1 0 7 10 1 0 8 9 1 0 10 11 1 0 11 12 1 0 2 3 1 0 12 13 1 0 6 7 2 0 12 14 1 0 3 9 2 0 4 15 1 0 M END > <chembl_id> CHEMBL65547 > <chembl_pref_name> PSILOCIN
InChI=1S/C12H16N2O/c1-14(2)7-6-9-8-13-10-4-3-5-11(15)12(9)10/h3-5,8,13,15H,6-7H2,1-2H3
SPCIYGNTAMCTRO-UHFFFAOYSA-N
1.98
2
C12H16N2O
204.27
2
2
15
204.27
0.31
0
39.26
0.8
Y
3
CHEMBL65547
CHEMBL65547
CHEMBL65547
4-ho-dmt [OTHER] | Psilocin [OTHER] | Psilocyn [OTHER]
null
null
null
null
null
null
null
null
P
Physicochemical
BAO_0000100
small-molecule physicochemical format
null
Default value - Target unknown or has yet to be assigned
0
Partition coefficient of octanol and water was determined
CHEMBL1121785
Default value - Target has yet to be curated
U
null
1
CHEMBL2362975
null
null
null
null
No relevant target
false
NO TARGET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The 360-MHz 1H NMR spectra of bufotenin and psilocin were obtained, both as the free bases in CDCl3 and as protonated salts in D2O. Coupling constants for the side-chain methylenes were derived using the LAOCN3 program. These time-averaged coupling constants indicate that the trans and gauche rotamers of both compounds have about equal energy in D2O. There is a slight excess of the trans rotamer of bufotenin in CDCl3. For psilocin, in contrast, the gauche form is highly favored in CDCl3. The magnitude of this stabilization was estimated at about 1 kcal/mol using rotamer populations and free energy of transfer from published partitioning studies. It is suggested that this could result from a very weak hydrogen bond. On the other hand, the difference in partitioning between bufotenin and psilocin, which seems to be a major determinant of biological activity, is largely due to a difference in the basicity of the two compounds. The pKa values for the amino group of psilocin and bufotenin were determined to be 8.47 and 9.67, respectively.
Migliaccio GP, Shieh TL, Byrn SR, Hathaway BA, Nichols DE.
10.1021/jm00134a016
null
206
2
J Med Chem
null
6,259,355
1
Comparison of solution conformational preferences for the hallucinogens bufotenin and psilocin using 360-MHz proton NMR spectroscopy.
24
1,981
null
34,379
CHEMBL637888
Partition coefficient (logP)
P
BAO_0000100
small-molecule physicochemical format
CN(C)CCc1c[nH]c2cccc(O)c12
null
CHEMBL1121785
J Med Chem
1,981
CHEMBL65547
PSILOCIN
null
0
null
113,388
=
1
1
=
LogP
null
1.45
CHEMBL2362975
null
No relevant target
null
null
logP
null
null
1.45
null
null
null
null
null
0
2
null
null
0
2.0
Small molecule
1
false
false
0
PSILOCIN
0
MOL
false
false
deu-
null
false
CN(C)CCc1c[nH]c2cccc(O)c12
RDKit 2D 15 16 0 0 0 0 0 0 0 0999 V2000 3.0857 -19.6308 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0845 -20.4581 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7992 -20.8708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7974 -19.2180 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3025 -20.7133 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.7903 -20.0417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3020 -19.3703 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5127 -19.6272 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5130 -20.4572 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.5567 -18.5857 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.3635 -18.4139 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.6180 -17.6293 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.4248 -17.4574 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.0659 -17.0165 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7950 -18.3931 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1 2 2 0 8 4 2 0 5 6 1 0 7 8 1 0 9 5 1 0 4 1 1 0 7 10 1 0 8 9 1 0 10 11 1 0 11 12 1 0 2 3 1 0 12 13 1 0 6 7 2 0 12 14 1 0 3 9 2 0 4 15 1 0 M END > <chembl_id> CHEMBL65547 > <chembl_pref_name> PSILOCIN
InChI=1S/C12H16N2O/c1-14(2)7-6-9-8-13-10-4-3-5-11(15)12(9)10/h3-5,8,13,15H,6-7H2,1-2H3
SPCIYGNTAMCTRO-UHFFFAOYSA-N
1.98
2
C12H16N2O
204.27
2
2
15
204.27
0.31
0
39.26
0.8
Y
3
CHEMBL65547
CHEMBL65547
CHEMBL65547
4-ho-dmt [OTHER] | Psilocin [OTHER] | Psilocyn [OTHER]
null
null
null
null
null
null
null
null
P
Physicochemical
BAO_0000100
small-molecule physicochemical format
null
Default value - Target unknown or has yet to be assigned
0
Partition coefficient (logP)
CHEMBL1121785
Default value - Target has yet to be curated
U
null
1
CHEMBL2362975
null
null
null
null
No relevant target
false
NO TARGET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The 360-MHz 1H NMR spectra of bufotenin and psilocin were obtained, both as the free bases in CDCl3 and as protonated salts in D2O. Coupling constants for the side-chain methylenes were derived using the LAOCN3 program. These time-averaged coupling constants indicate that the trans and gauche rotamers of both compounds have about equal energy in D2O. There is a slight excess of the trans rotamer of bufotenin in CDCl3. For psilocin, in contrast, the gauche form is highly favored in CDCl3. The magnitude of this stabilization was estimated at about 1 kcal/mol using rotamer populations and free energy of transfer from published partitioning studies. It is suggested that this could result from a very weak hydrogen bond. On the other hand, the difference in partitioning between bufotenin and psilocin, which seems to be a major determinant of biological activity, is largely due to a difference in the basicity of the two compounds. The pKa values for the amino group of psilocin and bufotenin were determined to be 8.47 and 9.67, respectively.
Migliaccio GP, Shieh TL, Byrn SR, Hathaway BA, Nichols DE.
10.1021/jm00134a016
null
206
2
J Med Chem
null
6,259,355
1
Comparison of solution conformational preferences for the hallucinogens bufotenin and psilocin using 360-MHz proton NMR spectroscopy.
24
1,981
null
34,380
CHEMBL668662
Inhibition of dihydrofolate reductase from bovine liver
B
BAO_0000019
assay format
CCCCCCCCOc1cccc(Cc2cnc(N)nc2N)c1
null
CHEMBL1121828
J Med Chem
1,981
CHEMBL31235
null
null
0
null
295,584
=
1
0
=
Log 1/Ki app
null
5.78
CHEMBL1075051
Bos taurus
Dihydrofolate reductase
9913
null
Log 1/Ki app
null
null
5.78
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCCCCCCOc1cccc(Cc2cnc(N)nc2N)c1
RDKit 2D 24 25 0 0 0 0 0 0 0 0999 V2000 0.7417 -4.2792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.2542 -3.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7792 -4.2792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.7417 -4.8792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2542 -5.1792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.7792 -4.8792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2917 -3.9667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8167 -4.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2500 -3.3792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.2167 -5.1792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.8167 -4.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3417 -5.1750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3417 -5.7750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.8667 -4.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3417 -3.9667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8667 -4.8667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8167 -6.0667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8125 -6.6625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2292 -8.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7542 -8.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7625 -7.8417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2917 -6.9542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2792 -7.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2250 -9.3250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 2 0 3 2 1 0 4 1 1 0 5 4 2 0 6 5 1 0 7 3 1 0 8 7 1 0 9 2 1 0 10 4 1 0 11 8 2 0 12 11 1 0 13 12 1 0 14 15 2 0 15 8 1 0 16 14 1 0 17 13 1 0 18 17 1 0 19 20 1 0 20 21 1 0 21 23 1 0 22 18 1 0 23 22 1 0 24 19 1 0 6 3 2 0 16 12 2 0 M END > <chembl_id> CHEMBL31235 > <chembl_pref_name> None
InChI=1S/C19H28N4O/c1-2-3-4-5-6-7-11-24-17-10-8-9-15(13-17)12-16-14-22-19(21)23-18(16)20/h8-10,13-14H,2-7,11-12H2,1H3,(H4,20,21,22,23)
RNZGHILIUCETNY-UHFFFAOYSA-N
3.97
2
C19H28N4O
328.46
5
2
24
328.46
-0.34
0
87.05
0.64
N
10
CHEMBL31235
CHEMBL31235
CHEMBL31235
null
null
null
null
Bos taurus
null
null
9,913
null
B
Binding
BAO_0000019
assay format
null
Direct single protein target assigned
9
Inhibition of dihydrofolate reductase from bovine liver
CHEMBL1121828
Direct protein target assigned
D
null
1
CHEMBL1075051
null
null
null
Bos taurus
Dihydrofolate reductase
false
SINGLE PROTEIN
9,913
P00376
Dihydrofolate reductase
PROTEIN
4,114
1
null
null
null
null
null
null
null
null
null
null
null
In our previous publication (Blaney, J. M.; Dietrich, S. W.; Reynolds, M. A.; Hansch, C. J. Med. Chem. 1979, 22, 614), correlation equations were presented for the inhibition of bovine liver and Escherichia coli dihydrofolate reductase (DHFR) by 5-(substituted benzyl)-2,4-diaminopyrimidines. These equations brought out differences in the way these two enzymes interact with substituents, which explain the high selectivity of drugs like trimethoprim. We have tested and further developed these equations in this report. It is of particular interest that our previously published correlation equation for E. coli DHFR accurately predicted the potency of a commercial competitor of trimethoprim (tetroxoprim) now in clinical use. We believe that new and effective competitors for trimethoprim can be designed by means of the two correlation equations.
Li RL, Dietrich SW, Hansch C.
10.1021/jm00137a012
null
538
5
J Med Chem
null
7,017,146
1
Quantitative structure-selectivity relationships. Comparison of the inhibition of Escherichia coli and bovine liver dihydrofolate reductase by 5-(substituted-benzyl)-2,4-diaminopyrimidines.
24
1,981
null
34,381
CHEMBL668773
Compound is evaluated for the inhibition of dihydrofolate reductase from Escherichia coli
B
BAO_0000357
single protein format
CCCCCCCCOc1cccc(Cc2cnc(N)nc2N)c1
null
CHEMBL1121828
J Med Chem
1,981
CHEMBL31235
null
null
0
null
295,584
=
1
0
=
Log 1/Ki app
null
6.25
CHEMBL1809
Escherichia coli
Dihydrofolate reductase
562
null
Log 1/Ki app
null
null
6.25
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCCCCCCOc1cccc(Cc2cnc(N)nc2N)c1
RDKit 2D 24 25 0 0 0 0 0 0 0 0999 V2000 0.7417 -4.2792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.2542 -3.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7792 -4.2792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.7417 -4.8792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2542 -5.1792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.7792 -4.8792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2917 -3.9667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8167 -4.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2500 -3.3792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.2167 -5.1792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.8167 -4.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3417 -5.1750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3417 -5.7750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.8667 -4.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3417 -3.9667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8667 -4.8667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8167 -6.0667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8125 -6.6625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2292 -8.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7542 -8.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7625 -7.8417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2917 -6.9542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2792 -7.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2250 -9.3250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 2 0 3 2 1 0 4 1 1 0 5 4 2 0 6 5 1 0 7 3 1 0 8 7 1 0 9 2 1 0 10 4 1 0 11 8 2 0 12 11 1 0 13 12 1 0 14 15 2 0 15 8 1 0 16 14 1 0 17 13 1 0 18 17 1 0 19 20 1 0 20 21 1 0 21 23 1 0 22 18 1 0 23 22 1 0 24 19 1 0 6 3 2 0 16 12 2 0 M END > <chembl_id> CHEMBL31235 > <chembl_pref_name> None
InChI=1S/C19H28N4O/c1-2-3-4-5-6-7-11-24-17-10-8-9-15(13-17)12-16-14-22-19(21)23-18(16)20/h8-10,13-14H,2-7,11-12H2,1H3,(H4,20,21,22,23)
RNZGHILIUCETNY-UHFFFAOYSA-N
3.97
2
C19H28N4O
328.46
5
2
24
328.46
-0.34
0
87.05
0.64
N
10
CHEMBL31235
CHEMBL31235
CHEMBL31235
null
null
null
null
Escherichia coli
null
null
562
null
B
Binding
BAO_0000357
single protein format
null
Direct single protein target assigned
9
Compound is evaluated for the inhibition of dihydrofolate reductase from Escherichia coli
CHEMBL1121828
Direct protein target assigned
D
null
1
CHEMBL1809
null
null
null
Escherichia coli
Dihydrofolate reductase
false
SINGLE PROTEIN
562
P0ABQ4
Dihydrofolate reductase
PROTEIN
103
1
null
null
null
null
null
null
null
null
null
null
null
In our previous publication (Blaney, J. M.; Dietrich, S. W.; Reynolds, M. A.; Hansch, C. J. Med. Chem. 1979, 22, 614), correlation equations were presented for the inhibition of bovine liver and Escherichia coli dihydrofolate reductase (DHFR) by 5-(substituted benzyl)-2,4-diaminopyrimidines. These equations brought out differences in the way these two enzymes interact with substituents, which explain the high selectivity of drugs like trimethoprim. We have tested and further developed these equations in this report. It is of particular interest that our previously published correlation equation for E. coli DHFR accurately predicted the potency of a commercial competitor of trimethoprim (tetroxoprim) now in clinical use. We believe that new and effective competitors for trimethoprim can be designed by means of the two correlation equations.
Li RL, Dietrich SW, Hansch C.
10.1021/jm00137a012
null
538
5
J Med Chem
null
7,017,146
1
Quantitative structure-selectivity relationships. Comparison of the inhibition of Escherichia coli and bovine liver dihydrofolate reductase by 5-(substituted-benzyl)-2,4-diaminopyrimidines.
24
1,981
null
34,382
CHEMBL847678
Sweet potency as logarithm of sweet potency (log SP) relative to sucrose
F
BAO_0000019
assay format
C[C@@H](Cc1ccco1)NC(=O)[C@H](N)CC(=O)O
null
CHEMBL1121833
J Med Chem
1,981
CHEMBL154919
null
null
0
null
302,439
=
1
0
=
Log SP
null
1.16
CHEMBL612545
null
Unchecked
null
null
Log SP
null
null
1.16
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
C[C@@H](Cc1ccco1)NC(=O)[C@H](N)CC(=O)O
RDKit 2D 17 17 0 0 1 0 0 0 0 0999 V2000 -2.0250 -0.9875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.0625 -0.9875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5083 -0.6875 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.5458 -0.6875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.5833 -0.6875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.0542 -0.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.1167 -1.5792 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.4708 -0.6875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0250 -1.5875 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.6000 -0.7375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.7042 -1.7042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0042 -1.1667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.5833 -0.0875 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.9833 -0.9875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.5458 -0.0875 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -4.1000 -0.9792 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.9833 -1.5875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 4 1 0 3 1 1 0 4 1 1 0 5 2 1 0 6 8 1 0 7 6 1 0 8 14 1 0 9 1 2 0 10 6 2 0 11 7 1 0 12 10 1 0 13 5 2 0 14 3 1 0 4 15 1 1 16 5 1 0 14 17 1 6 12 11 2 0 M END > <chembl_id> CHEMBL154919 > <chembl_pref_name> None
InChI=1S/C11H16N2O4/c1-7(5-8-3-2-4-17-8)13-11(16)9(12)6-10(14)15/h2-4,7,9H,5-6,12H2,1H3,(H,13,16)(H,14,15)/t7-,9+/m0/s1
VOQPIRFCQUFIFQ-IONNQARKSA-N
0.13
1
C11H16N2O4
240.26
4
3
17
240.26
-0.55
0
105.56
0.65
N
6
CHEMBL154919
CHEMBL154919
CHEMBL154919
null
null
null
null
null
null
null
null
null
F
Functional
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Sweet potency as logarithm of sweet potency (log SP) relative to sucrose
CHEMBL1121833
Default value - Target has yet to be curated
U
null
1
CHEMBL612545
null
null
null
null
Unchecked
false
UNCHECKED
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The relationship between structure and the sweet potency of L-aspartyl dipeptide analogues was investigated by physicochemical parameters and regression analysis. The dipeptide analogues reported were divided into the following four classes: L-aspartic acid amides, L-aspartylaminoethyl esters, L-aspartylaminopropionates, and L-aspartyl-aminoacetates. The analysis carried out for each class indicated that the electron-withdrawing effect of the substituents directed to the peptide bond and the steric dimensions of the molecules are important in eliciting the sweet taste. The values of coefficients of the electronic sigma terms in the correlations for L-aspartic acid amides, L-aspartylaminoethyl esters, and L-aspartylaminopropionates were approximately 0.7, indicating a common basic site on the receptor surface. The value for L-aspartylaminoacetates was approximately 1.5, and this value suggests, together with the factor of the participation of steric parameters, a closer or geometrically more proper fit to the receptor, explaining the generally higher potency of this class compared to the other three. The receptor model drawn based on these quantitative analyses appears to be consistent with other classes of sweeteners of apparently unrelated structures.
Iwamura H.
10.1021/jm00137a018
null
572
5
J Med Chem
null
7,241,515
1
Structure--sweetness relationship of L-aspartyl dipeptide analogues. A receptor site topology.
24
1,981
null
34,383
CHEMBL847678
Sweet potency as logarithm of sweet potency (log SP) relative to sucrose
F
BAO_0000019
assay format
CC[C@@H](Cc1ccccc1)NC(=O)[C@H](N)CC(=O)O
null
CHEMBL1121833
J Med Chem
1,981
CHEMBL345850
null
null
0
null
302,650
=
1
0
=
Log SP
null
0.89
CHEMBL612545
null
Unchecked
null
null
Log SP
null
null
0.89
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CC[C@@H](Cc1ccccc1)NC(=O)[C@H](N)CC(=O)O
RDKit 2D 19 19 0 0 1 0 0 0 0 0999 V2000 -1.5708 0.2208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.6083 0.2208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0500 0.5208 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.0958 0.5208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.1250 0.5208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5708 -0.3792 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.1250 1.1208 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.5333 0.2208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0875 1.1208 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.0125 0.5208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.6458 0.2250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.5042 0.2208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.5333 -0.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5042 -0.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0167 0.5250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0458 -0.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.5417 0.2333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0250 -0.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.5417 -0.3750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 4 1 0 3 1 1 0 4 1 1 0 5 2 1 0 6 1 2 0 7 5 2 0 8 3 1 0 4 9 1 1 10 8 1 0 11 5 1 0 12 10 1 0 8 13 1 6 14 12 2 0 15 12 1 0 16 13 1 0 17 15 2 0 18 14 1 0 19 17 1 0 19 18 2 0 M END > <chembl_id> CHEMBL345850 > <chembl_pref_name> None
InChI=1S/C14H20N2O3/c1-2-11(8-10-6-4-3-5-7-10)16-14(19)12(15)9-13(17)18/h3-7,11-12H,2,8-9,15H2,1H3,(H,16,19)(H,17,18)/t11-,12+/m0/s1
SIXSBZCTRDJENX-NWDGAFQWSA-N
0.93
1
C14H20N2O3
264.32
3
3
19
264.32
0.15
0
92.42
0.68
N
7
CHEMBL345850
CHEMBL345850
CHEMBL345850
null
null
null
null
null
null
null
null
null
F
Functional
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Sweet potency as logarithm of sweet potency (log SP) relative to sucrose
CHEMBL1121833
Default value - Target has yet to be curated
U
null
1
CHEMBL612545
null
null
null
null
Unchecked
false
UNCHECKED
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The relationship between structure and the sweet potency of L-aspartyl dipeptide analogues was investigated by physicochemical parameters and regression analysis. The dipeptide analogues reported were divided into the following four classes: L-aspartic acid amides, L-aspartylaminoethyl esters, L-aspartylaminopropionates, and L-aspartyl-aminoacetates. The analysis carried out for each class indicated that the electron-withdrawing effect of the substituents directed to the peptide bond and the steric dimensions of the molecules are important in eliciting the sweet taste. The values of coefficients of the electronic sigma terms in the correlations for L-aspartic acid amides, L-aspartylaminoethyl esters, and L-aspartylaminopropionates were approximately 0.7, indicating a common basic site on the receptor surface. The value for L-aspartylaminoacetates was approximately 1.5, and this value suggests, together with the factor of the participation of steric parameters, a closer or geometrically more proper fit to the receptor, explaining the generally higher potency of this class compared to the other three. The receptor model drawn based on these quantitative analyses appears to be consistent with other classes of sweeteners of apparently unrelated structures.
Iwamura H.
10.1021/jm00137a018
null
572
5
J Med Chem
null
7,241,515
1
Structure--sweetness relationship of L-aspartyl dipeptide analogues. A receptor site topology.
24
1,981
null
34,386
CHEMBL847678
Sweet potency as logarithm of sweet potency (log SP) relative to sucrose
F
BAO_0000019
assay format
C[C@@H](COC(=O)C1CCCC1)NC(=O)[C@H](N)CC(=O)O
null
CHEMBL1121833
J Med Chem
1,981
CHEMBL434078
null
null
0
null
302,608
=
1
0
=
Log SP
null
1.7
CHEMBL612545
null
Unchecked
null
null
Log SP
null
null
1.7
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
C[C@@H](COC(=O)C1CCCC1)NC(=O)[C@H](N)CC(=O)O
RDKit 2D 20 20 0 0 1 0 0 0 0 0999 V2000 -3.4458 -0.8667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.4833 -0.8667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.8458 -0.5625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.9250 -0.5667 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -3.9708 -0.5667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -5.0000 -0.5667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3708 -0.8625 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.4458 -1.4667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.8500 0.0375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -5.0000 0.0333 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.3250 -0.8542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.9625 0.0333 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -5.5208 -0.8625 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.8875 -0.5667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -0.8667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.2625 -1.4542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.2167 -0.6125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -1.4667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6250 -1.0542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.3250 -1.5792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 5 1 0 3 7 1 0 4 1 1 0 5 1 1 0 6 2 1 0 7 14 1 0 8 1 2 0 9 3 2 0 10 6 2 0 11 3 1 0 5 12 1 1 13 6 1 0 14 15 1 0 15 4 1 0 16 11 1 0 17 11 1 0 15 18 1 6 19 17 1 0 20 16 1 0 19 20 1 0 M END > <chembl_id> CHEMBL434078 > <chembl_pref_name> None
InChI=1S/C13H22N2O5/c1-8(15-12(18)10(14)6-11(16)17)7-20-13(19)9-4-2-3-5-9/h8-10H,2-7,14H2,1H3,(H,15,18)(H,16,17)/t8-,10+/m0/s1
CUSAUPTWLADOAS-WCBMZHEXSA-N
0.03
0
C13H22N2O5
286.33
5
3
20
286.33
-0.01
0
118.72
0.57
N
7
CHEMBL434078
CHEMBL434078
CHEMBL434078
null
null
null
null
null
null
null
null
null
F
Functional
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Sweet potency as logarithm of sweet potency (log SP) relative to sucrose
CHEMBL1121833
Default value - Target has yet to be curated
U
null
1
CHEMBL612545
null
null
null
null
Unchecked
false
UNCHECKED
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The relationship between structure and the sweet potency of L-aspartyl dipeptide analogues was investigated by physicochemical parameters and regression analysis. The dipeptide analogues reported were divided into the following four classes: L-aspartic acid amides, L-aspartylaminoethyl esters, L-aspartylaminopropionates, and L-aspartyl-aminoacetates. The analysis carried out for each class indicated that the electron-withdrawing effect of the substituents directed to the peptide bond and the steric dimensions of the molecules are important in eliciting the sweet taste. The values of coefficients of the electronic sigma terms in the correlations for L-aspartic acid amides, L-aspartylaminoethyl esters, and L-aspartylaminopropionates were approximately 0.7, indicating a common basic site on the receptor surface. The value for L-aspartylaminoacetates was approximately 1.5, and this value suggests, together with the factor of the participation of steric parameters, a closer or geometrically more proper fit to the receptor, explaining the generally higher potency of this class compared to the other three. The receptor model drawn based on these quantitative analyses appears to be consistent with other classes of sweeteners of apparently unrelated structures.
Iwamura H.
10.1021/jm00137a018
null
572
5
J Med Chem
null
7,241,515
1
Structure--sweetness relationship of L-aspartyl dipeptide analogues. A receptor site topology.
24
1,981
null
34,387
CHEMBL847678
Sweet potency as logarithm of sweet potency (log SP) relative to sucrose
F
BAO_0000019
assay format
CC[C@H](NC(=O)[C@H](N)CC(=O)O)C(=O)OC
null
CHEMBL1121833
J Med Chem
1,981
CHEMBL345229
null
null
0
null
302,539
=
1
0
=
Log SP
null
1.04
CHEMBL612545
null
Unchecked
null
null
Log SP
null
null
1.04
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CC[C@H](NC(=O)[C@H](N)CC(=O)O)C(=O)OC
RDKit 2D 16 15 0 0 1 0 0 0 0 0999 V2000 -1.3458 -1.0417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.8250 -0.7417 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.3833 -1.0417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.2125 -0.7417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.8708 -0.7417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.9000 -0.7417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3083 -1.0417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3458 -1.6417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.2125 -0.1417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.9000 -0.1417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.8625 -0.1417 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.7292 -1.0417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.4208 -1.0375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.3083 -1.6417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.7375 -1.6417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.8208 -1.9417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 5 1 0 4 7 1 0 5 1 1 0 6 3 1 0 7 2 1 0 8 1 2 0 9 4 2 0 10 6 2 0 5 11 1 1 12 4 1 0 13 6 1 0 7 14 1 6 15 12 1 0 16 14 1 0 M END > <chembl_id> CHEMBL345229 > <chembl_pref_name> None
InChI=1S/C9H16N2O5/c1-3-6(9(15)16-2)11-8(14)5(10)4-7(12)13/h5-6H,3-4,10H2,1-2H3,(H,11,14)(H,12,13)/t5-,6+/m1/s1
OEHNLOQCFKDMNG-RITPCOANSA-N
-1.14
0
C9H16N2O5
232.24
5
3
16
232.24
0.44
0
118.72
0.5
N
6
CHEMBL345229
CHEMBL345229
CHEMBL345229
null
null
null
null
null
null
null
null
null
F
Functional
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Sweet potency as logarithm of sweet potency (log SP) relative to sucrose
CHEMBL1121833
Default value - Target has yet to be curated
U
null
1
CHEMBL612545
null
null
null
null
Unchecked
false
UNCHECKED
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The relationship between structure and the sweet potency of L-aspartyl dipeptide analogues was investigated by physicochemical parameters and regression analysis. The dipeptide analogues reported were divided into the following four classes: L-aspartic acid amides, L-aspartylaminoethyl esters, L-aspartylaminopropionates, and L-aspartyl-aminoacetates. The analysis carried out for each class indicated that the electron-withdrawing effect of the substituents directed to the peptide bond and the steric dimensions of the molecules are important in eliciting the sweet taste. The values of coefficients of the electronic sigma terms in the correlations for L-aspartic acid amides, L-aspartylaminoethyl esters, and L-aspartylaminopropionates were approximately 0.7, indicating a common basic site on the receptor surface. The value for L-aspartylaminoacetates was approximately 1.5, and this value suggests, together with the factor of the participation of steric parameters, a closer or geometrically more proper fit to the receptor, explaining the generally higher potency of this class compared to the other three. The receptor model drawn based on these quantitative analyses appears to be consistent with other classes of sweeteners of apparently unrelated structures.
Iwamura H.
10.1021/jm00137a018
null
572
5
J Med Chem
null
7,241,515
1
Structure--sweetness relationship of L-aspartyl dipeptide analogues. A receptor site topology.
24
1,981
null
34,388
CHEMBL847678
Sweet potency as logarithm of sweet potency (log SP) relative to sucrose
F
BAO_0000019
assay format
CC(Cc1ccccc1)NC(=O)[C@H](N)CC(=O)O
null
CHEMBL1121833
J Med Chem
1,981
CHEMBL153822
null
null
0
null
302,489
=
1
0
=
Log SP
null
1.56
CHEMBL612545
null
Unchecked
null
null
Log SP
null
null
1.56
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CC(Cc1ccccc1)NC(=O)[C@H](N)CC(=O)O
RDKit 2D 18 18 0 0 1 0 0 0 0 0999 V2000 -1.2708 -0.6167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.3083 -0.6125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7458 -0.3167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.7875 -0.3167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.8208 -0.3125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.2708 -1.2167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.8208 0.2875 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.2250 -0.6167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.7833 0.2833 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.2917 -0.3167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3458 -0.6125 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.8125 -0.6125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.2250 -1.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3250 -0.3042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.8125 -1.2125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3292 -1.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8417 -0.6042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8500 -1.2042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 4 1 0 3 1 1 0 4 1 1 0 5 2 1 0 6 1 2 0 7 5 2 0 8 3 1 0 4 9 1 1 10 8 1 0 11 5 1 0 12 10 1 0 13 8 1 0 14 12 1 0 15 12 2 0 16 15 1 0 17 14 2 0 18 16 2 0 18 17 1 0 M END > <chembl_id> CHEMBL153822 > <chembl_pref_name> None
InChI=1S/C13H18N2O3/c1-9(7-10-5-3-2-4-6-10)15-13(18)11(14)8-12(16)17/h2-6,9,11H,7-8,14H2,1H3,(H,15,18)(H,16,17)/t9?,11-/m1/s1
DADLXGFKJVGHGU-HCCKASOXSA-N
0.54
1
C13H18N2O3
250.30
3
3
18
250.3
-0.14
0
92.42
0.69
N
6
CHEMBL153822
CHEMBL153822
CHEMBL153822
null
null
null
null
null
null
null
null
null
F
Functional
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Sweet potency as logarithm of sweet potency (log SP) relative to sucrose
CHEMBL1121833
Default value - Target has yet to be curated
U
null
1
CHEMBL612545
null
null
null
null
Unchecked
false
UNCHECKED
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The relationship between structure and the sweet potency of L-aspartyl dipeptide analogues was investigated by physicochemical parameters and regression analysis. The dipeptide analogues reported were divided into the following four classes: L-aspartic acid amides, L-aspartylaminoethyl esters, L-aspartylaminopropionates, and L-aspartyl-aminoacetates. The analysis carried out for each class indicated that the electron-withdrawing effect of the substituents directed to the peptide bond and the steric dimensions of the molecules are important in eliciting the sweet taste. The values of coefficients of the electronic sigma terms in the correlations for L-aspartic acid amides, L-aspartylaminoethyl esters, and L-aspartylaminopropionates were approximately 0.7, indicating a common basic site on the receptor surface. The value for L-aspartylaminoacetates was approximately 1.5, and this value suggests, together with the factor of the participation of steric parameters, a closer or geometrically more proper fit to the receptor, explaining the generally higher potency of this class compared to the other three. The receptor model drawn based on these quantitative analyses appears to be consistent with other classes of sweeteners of apparently unrelated structures.
Iwamura H.
10.1021/jm00137a018
null
572
5
J Med Chem
null
7,241,515
1
Structure--sweetness relationship of L-aspartyl dipeptide analogues. A receptor site topology.
24
1,981
null
34,389
CHEMBL847678
Sweet potency as logarithm of sweet potency (log SP) relative to sucrose
F
BAO_0000019
assay format
CCCCCC[C@H](C)NC(=O)[C@H](N)CC(=O)O
null
CHEMBL1121833
J Med Chem
1,981
CHEMBL154383
null
null
0
null
302,485
=
1
0
=
Log SP
null
1.58
CHEMBL612545
null
Unchecked
null
null
Log SP
null
null
1.58
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCCCC[C@H](C)NC(=O)[C@H](N)CC(=O)O
RDKit 2D 17 16 0 0 1 0 0 0 0 0999 V2000 -3.5375 -0.1917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.5833 -0.1917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.0208 0.1083 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -4.0583 0.1083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -5.0958 0.1083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.5375 -0.7917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -5.0958 0.7083 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -4.0583 0.7083 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -5.6125 -0.1875 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.4958 -0.1917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9833 0.1083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4958 -0.7917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.1000 0.1125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4208 -0.1875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4583 -0.1875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9458 0.1125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6167 -0.1917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 4 1 0 3 1 1 0 4 1 1 0 5 2 1 0 6 1 2 0 7 5 2 0 4 8 1 1 9 5 1 0 10 3 1 0 11 10 1 0 10 12 1 6 13 14 1 0 14 16 1 0 15 11 1 0 16 15 1 0 17 13 1 0 M END > <chembl_id> CHEMBL154383 > <chembl_pref_name> None
InChI=1S/C12H24N2O3/c1-3-4-5-6-7-9(2)14-12(17)10(13)8-11(15)16/h9-10H,3-8,13H2,1-2H3,(H,14,17)(H,15,16)/t9-,10+/m0/s1
KCYZZFRWSADIIG-VHSXEESVSA-N
1.26
0
C12H24N2O3
244.33
3
3
17
244.33
0.33
0
92.42
0.53
N
9
CHEMBL154383
CHEMBL154383
CHEMBL154383
null
null
null
null
null
null
null
null
null
F
Functional
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Sweet potency as logarithm of sweet potency (log SP) relative to sucrose
CHEMBL1121833
Default value - Target has yet to be curated
U
null
1
CHEMBL612545
null
null
null
null
Unchecked
false
UNCHECKED
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The relationship between structure and the sweet potency of L-aspartyl dipeptide analogues was investigated by physicochemical parameters and regression analysis. The dipeptide analogues reported were divided into the following four classes: L-aspartic acid amides, L-aspartylaminoethyl esters, L-aspartylaminopropionates, and L-aspartyl-aminoacetates. The analysis carried out for each class indicated that the electron-withdrawing effect of the substituents directed to the peptide bond and the steric dimensions of the molecules are important in eliciting the sweet taste. The values of coefficients of the electronic sigma terms in the correlations for L-aspartic acid amides, L-aspartylaminoethyl esters, and L-aspartylaminopropionates were approximately 0.7, indicating a common basic site on the receptor surface. The value for L-aspartylaminoacetates was approximately 1.5, and this value suggests, together with the factor of the participation of steric parameters, a closer or geometrically more proper fit to the receptor, explaining the generally higher potency of this class compared to the other three. The receptor model drawn based on these quantitative analyses appears to be consistent with other classes of sweeteners of apparently unrelated structures.
Iwamura H.
10.1021/jm00137a018
null
572
5
J Med Chem
null
7,241,515
1
Structure--sweetness relationship of L-aspartyl dipeptide analogues. A receptor site topology.
24
1,981
null
34,392
CHEMBL784534
Antiallergic activity was evaluated by passive cutaneous anaphylaxis test in egg albumin sensitized male Harlan-Sprague-Dawley rats when administered perorally
F
BAO_0000218
organism-based format
O=C1c2[nH]nnc2N(Cc2ccc(F)cc2)C2=NCCN12
null
CHEMBL1121553
J Med Chem
1,980
CHEMBL18489
null
null
0
null
22,459
=
1
1
=
ED50
mg.kg-1
17.7
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
ED50
mg kg-1
UO_0000308
17.7
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C1c2[nH]nnc2N(Cc2ccc(F)cc2)C2=NCCN12
RDKit 2D 21 24 0 0 0 0 0 0 0 0999 V2000 4.5792 -3.9792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.8667 -3.5667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3042 -3.5625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3000 -2.7375 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.8625 -2.7375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5792 -2.3167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0792 -3.8292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.5875 -3.1542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.0750 -2.4792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.0917 -3.8167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.5792 -4.8042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5875 -1.4917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 6.0792 -2.4792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.5667 -3.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8667 -5.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4375 -6.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7167 -6.4375 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 3.8667 -6.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.1542 -4.7917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4417 -5.2042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.1542 -6.4417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 1 0 4 3 1 0 5 2 2 0 6 4 1 0 7 2 1 0 8 7 2 0 9 5 1 0 10 3 2 0 11 1 1 0 12 6 2 0 13 4 1 0 14 10 1 0 15 11 1 0 16 20 2 0 17 16 1 0 18 15 1 0 19 15 2 0 20 19 1 0 21 18 2 0 13 14 1 0 6 5 1 0 8 9 1 0 16 21 1 0 M END > <chembl_id> CHEMBL18489 > <chembl_pref_name> None
InChI=1S/C13H11FN6O/c14-9-3-1-8(2-4-9)7-20-11-10(16-18-17-11)12(21)19-6-5-15-13(19)20/h1-4H,5-7H2,(H,16,17,18)
PZBVSAQNUMAWOE-UHFFFAOYSA-N
0.78
2
C13H11FN6O
286.27
5
1
21
286.27
-1.55
0
77.48
0.88
N
2
CHEMBL18489
CHEMBL18489
CHEMBL18489
null
null
null
null
Rattus norvegicus
null
null
10,116
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Antiallergic activity was evaluated by passive cutaneous anaphylaxis test in egg albumin sensitized male Harlan-Sprague-Dawley rats when administered perorally
CHEMBL1121553
Non-molecular target assigned
N
null
1
CHEMBL376
null
null
null
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The synthesis of a series of substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones is described. Several members of the series exhibit enhanced antiallergic and bronchodilator activity and reduced side effects as compared to theophylline. Structure-activity relationships and metabolic considerations are discussed for the series. Analogues substituted with a 4-(4-chlorobenzyl) moiety, such as 33 and 40, shown an optimal balance of antiallergic and bronchodilator activity and are of particular interest. Compound 33 is significantly more potent than theophylline against both metacholine- and antigen-induced bronchospasms, does not affect spontaneous motor activity, and shows minimal cardiovascular effects in the rat.
Temple DL, Yevich JP, Catt JD, Owens D, Hanning C, Covington RR, Seidehamel RJ, Dungan KW.
10.1021/jm00185a008
null
1188
11
J Med Chem
null
6,161,252
1
Substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones.
23
1,980
null
34,393
CHEMBL773605
Lowest active dose which cured rats with Entamoeba histolytica cecal infection was measured
F
BAO_0000218
organism-based format
CCCN1CCN(c2nc3ccc(/N=C/N(C)C)cc3nc2N2CCN(CCC)CC2)CC1
null
CHEMBL1121391
J Med Chem
1,980
CHEMBL66079
null
null
0
null
110,555
=
1
0
=
Dose
mg kg-1 day-1
50
CHEMBL612853
Entamoeba histolytica
Entamoeba histolytica
5759
null
Dose
mg kg-1 day-1
UO_0000311
50.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCN1CCN(c2nc3ccc(/N=C/N(C)C)cc3nc2N2CCN(CCC)CC2)CC1
RDKit 2D 33 36 0 0 0 0 0 0 0 0999 V2000 5.7000 -6.2125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6917 -5.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9875 -6.6292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.9792 -4.9750 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.4042 -4.9667 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.4167 -6.6167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.2667 -6.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2667 -5.3917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1250 -6.6292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.4125 -6.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.8292 -4.1292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.8417 -7.4417 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5542 -6.6292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1167 -5.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1250 -6.2000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4000 -4.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4167 -7.4417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8417 -6.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6917 -6.6292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5542 -4.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1125 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1292 -7.8542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.8292 -4.9625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.8417 -6.6167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8417 -5.3917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.5542 -7.8542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.5417 -3.7250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0208 -6.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6917 -7.4542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.2542 -4.1292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.2667 -7.4417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.9750 -3.7167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.9875 -7.8542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 2 0 4 2 2 0 5 2 1 0 6 1 1 0 7 3 1 0 8 7 1 0 9 18 1 0 10 9 2 0 11 21 1 0 12 22 1 0 13 7 2 0 14 5 1 0 15 6 1 0 16 5 1 0 17 6 1 0 18 13 1 0 19 10 1 0 20 8 2 0 21 16 1 0 22 17 1 0 23 14 1 0 24 15 1 0 25 18 2 0 26 12 1 0 27 11 1 0 28 19 1 0 29 19 1 0 30 27 1 0 31 26 1 0 32 30 1 0 33 31 1 0 24 12 1 0 4 8 1 0 23 11 1 0 20 25 1 0 M END > <chembl_id> CHEMBL66079 > <chembl_pref_name> None
InChI=1S/C25H40N8/c1-5-9-30-11-15-32(16-12-30)24-25(33-17-13-31(10-6-2)14-18-33)28-23-19-21(26-20-29(3)4)7-8-22(23)27-24/h7-8,19-20H,5-6,9-18H2,1-4H3/b26-20+
PYQRPNZZTJLWTE-LHLOQNFPSA-N
2.92
2
C25H40N8
452.65
7
0
33
452.65
-1.17
0
54.34
0.45
N
8
CHEMBL66079
CHEMBL66079
CHEMBL66079
null
null
null
null
Entamoeba histolytica
null
null
5,759
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Lowest active dose which cured rats with Entamoeba histolytica cecal infection was measured
CHEMBL1121391
Non-molecular target assigned
N
null
1
CHEMBL612853
null
null
null
Entamoeba histolytica
Entamoeba histolytica
false
ORGANISM
5,759
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of amidines and sulfonamides of 5- and 6-amino-2,3-bis(4-alkyl-1-piperazinyl)quinoxalines was synthesized and tested against cecal and hepatic forms of Entamoeba histolytica infections in rats and hamsters, respectively. Four compounds (5, 6, 8, and 9) were found to have acceptable activity against infections in both species but were too toxic to be considered for use in man.
Fabio PF, Lang SA, Lin YI, Tomcufcik AS.
10.1021/jm00176a017
null
201
2
J Med Chem
null
7,359,534
1
Antiamebic amidines and sulfonamides of 5- and 6-amino-2,3-bis(4-alkyl-1-piperazinyl)quinoxalines.
23
1,980
null
34,394
CHEMBL693881
Lowest active dose which cured hamsters with Entamoeba histolytica hepatic infection was measured
F
BAO_0000218
organism-based format
CCCN1CCN(c2nc3ccc(/N=C/N(C)C)cc3nc2N2CCN(CCC)CC2)CC1
null
CHEMBL1121391
J Med Chem
1,980
CHEMBL66079
null
null
0
null
110,555
=
1
0
=
Dose
mg kg-1 day-1
100
CHEMBL612853
Entamoeba histolytica
Entamoeba histolytica
5759
null
Dose
mg kg-1 day-1
UO_0000311
100.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCN1CCN(c2nc3ccc(/N=C/N(C)C)cc3nc2N2CCN(CCC)CC2)CC1
RDKit 2D 33 36 0 0 0 0 0 0 0 0999 V2000 5.7000 -6.2125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6917 -5.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9875 -6.6292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.9792 -4.9750 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.4042 -4.9667 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.4167 -6.6167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.2667 -6.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2667 -5.3917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1250 -6.6292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.4125 -6.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.8292 -4.1292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.8417 -7.4417 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5542 -6.6292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1167 -5.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1250 -6.2000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4000 -4.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4167 -7.4417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8417 -6.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6917 -6.6292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5542 -4.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1125 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1292 -7.8542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.8292 -4.9625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.8417 -6.6167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8417 -5.3917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.5542 -7.8542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.5417 -3.7250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0208 -6.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6917 -7.4542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.2542 -4.1292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.2667 -7.4417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.9750 -3.7167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.9875 -7.8542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 2 0 4 2 2 0 5 2 1 0 6 1 1 0 7 3 1 0 8 7 1 0 9 18 1 0 10 9 2 0 11 21 1 0 12 22 1 0 13 7 2 0 14 5 1 0 15 6 1 0 16 5 1 0 17 6 1 0 18 13 1 0 19 10 1 0 20 8 2 0 21 16 1 0 22 17 1 0 23 14 1 0 24 15 1 0 25 18 2 0 26 12 1 0 27 11 1 0 28 19 1 0 29 19 1 0 30 27 1 0 31 26 1 0 32 30 1 0 33 31 1 0 24 12 1 0 4 8 1 0 23 11 1 0 20 25 1 0 M END > <chembl_id> CHEMBL66079 > <chembl_pref_name> None
InChI=1S/C25H40N8/c1-5-9-30-11-15-32(16-12-30)24-25(33-17-13-31(10-6-2)14-18-33)28-23-19-21(26-20-29(3)4)7-8-22(23)27-24/h7-8,19-20H,5-6,9-18H2,1-4H3/b26-20+
PYQRPNZZTJLWTE-LHLOQNFPSA-N
2.92
2
C25H40N8
452.65
7
0
33
452.65
-1.17
0
54.34
0.45
N
8
CHEMBL66079
CHEMBL66079
CHEMBL66079
null
null
null
null
Entamoeba histolytica
null
null
5,759
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Lowest active dose which cured hamsters with Entamoeba histolytica hepatic infection was measured
CHEMBL1121391
Non-molecular target assigned
N
null
1
CHEMBL612853
null
null
null
Entamoeba histolytica
Entamoeba histolytica
false
ORGANISM
5,759
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of amidines and sulfonamides of 5- and 6-amino-2,3-bis(4-alkyl-1-piperazinyl)quinoxalines was synthesized and tested against cecal and hepatic forms of Entamoeba histolytica infections in rats and hamsters, respectively. Four compounds (5, 6, 8, and 9) were found to have acceptable activity against infections in both species but were too toxic to be considered for use in man.
Fabio PF, Lang SA, Lin YI, Tomcufcik AS.
10.1021/jm00176a017
null
201
2
J Med Chem
null
7,359,534
1
Antiamebic amidines and sulfonamides of 5- and 6-amino-2,3-bis(4-alkyl-1-piperazinyl)quinoxalines.
23
1,980
null
34,395
CHEMBL657542
Ability to destroy fluid-phase human complement 1 in the presence of complement 4 with appropriate serial twofold dilutions of the test compound using C1 assay
B
BAO_0000019
assay format
Cc1ccc(C(=O)Nc2ccc(S(=O)(=O)O)c3cc(S(=O)(=O)O)cc(S(=O)(=O)O)c23)cc1NC(=O)c1cccc(NC(=O)Nc2cccc(C(=O)Nc3cc(C(=O)Nc4ccc(S(=O)(=O)O)c5cc(S(=O)(=O)O)cc(S(=O)(=O)O)c45)ccc3C)c2)c1
null
CHEMBL1121398
J Med Chem
1,980
CHEMBL265502
SURAMIN
null
0
http://www.openphacts.org/units/MicrogramPerMilliliter
143,085
=
1
0
=
ED50
ug ml-1
21
CHEMBL612545
null
Unchecked
null
null
ED50
ug ml-1
UO_0000274
21.0
null
null
null
null
null
0
2
null
null
0
3.0
Small molecule
1
false
false
0
SURAMIN
0
MOL
false
false
null
1,997
false
Cc1ccc(C(=O)Nc2ccc(S(=O)(=O)O)c3cc(S(=O)(=O)O)cc(S(=O)(=O)O)c23)cc1NC(=O)c1cccc(NC(=O)Nc2cccc(C(=O)Nc3cc(C(=O)Nc4ccc(S(=O)(=O)O)c5cc(S(=O)(=O)O)cc(S(=O)(=O)O)c45)ccc3C)c2)c1
RDKit 2D 86 93 0 0 0 0 0 0 0 0999 V2000 -2.4083 -0.0667 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 2.8000 -1.2792 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -2.2167 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 1.3917 0.7458 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 -1.4708 -1.7000 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 0.9500 -1.2667 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -0.6000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.8833 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 -0.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.8833 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8167 -0.2125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8167 0.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -1.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4125 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -0.6000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7667 -0.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8750 -1.2917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 0.4625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7167 -0.0917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 1.7750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.3875 1.8208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 0.2000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.2500 -0.3542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.0125 2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4125 -0.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -1.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 2.0083 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.8625 2.1083 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.2542 1.7083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3333 1.8333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7292 0.8625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 1.0208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3333 1.2708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 1.1208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -1.5167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 0.4750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.9667 1.0750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -2.7542 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.0000 -1.9750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.5042 -1.5500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.8625 2.0500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9083 2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8208 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2375 0.6458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.4792 1.7833 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.4500 1.7833 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.9833 -0.0667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.8833 -0.0667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.0292 -0.8125 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.5417 -1.7667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.7375 1.1833 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.8083 -2.2167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.8958 -2.2167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.0792 0.3250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.7458 -2.1667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.6542 -0.8042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.2292 -1.7042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.2083 -1.2250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.7667 0.4083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8208 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7417 1.9583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 2.0875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.0125 2.6000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 1.2958 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.3042 -0.3917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.3875 1.3000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -4.2833 0.1958 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.4000 1.7750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4458 1.7583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9458 2.0333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9292 2.0500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.2958 1.2708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 1.1583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.2958 1.8333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 1.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8625 2.5708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9083 2.6208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4000 2.8458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3625 2.8583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9292 2.5708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9458 2.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 2.6333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7542 2.4958 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 7 1 0 3 14 1 0 4 13 1 0 5 16 1 0 6 15 1 0 7 10 1 0 8 1 1 0 9 8 1 0 10 18 1 0 11 9 2 0 12 10 2 0 13 47 2 0 14 11 1 0 15 28 2 0 16 19 1 0 17 9 1 0 18 26 1 0 19 8 2 0 20 7 2 0 21 25 1 0 22 34 1 0 23 44 1 0 24 31 1 0 25 17 1 0 26 22 1 0 27 49 1 0 28 12 1 0 29 16 2 0 30 23 1 0 31 33 1 0 32 30 1 0 33 36 1 0 34 37 2 0 35 21 1 0 36 35 2 0 37 32 1 0 38 2 1 0 39 1 1 0 40 4 1 0 41 3 1 0 42 5 1 0 43 6 1 0 44 71 2 0 45 24 1 0 46 63 1 0 47 62 1 0 48 27 1 0 49 73 1 0 50 1 2 0 51 1 2 0 52 2 2 0 53 2 2 0 54 4 2 0 55 3 2 0 56 3 2 0 57 4 2 0 58 5 2 0 59 6 2 0 60 6 2 0 61 5 2 0 62 18 2 0 63 17 2 0 64 32 2 0 65 77 1 0 66 27 2 0 67 23 2 0 68 22 2 0 69 24 2 0 70 21 2 0 71 74 1 0 72 45 1 0 73 72 2 0 74 48 1 0 75 35 1 0 76 78 2 0 77 75 2 0 78 64 1 0 79 81 2 0 80 45 2 0 81 83 1 0 82 80 1 0 83 74 2 0 84 82 2 0 85 65 1 0 86 64 1 0 11 29 1 0 14 46 2 0 33 65 2 0 73 84 1 0 44 79 1 0 34 76 1 0 12 13 1 0 20 15 1 0 M END > <chembl_id> CHEMBL265502 > <chembl_pref_name> SURAMIN
InChI=1S/C51H40N6O23S6/c1-25-9-11-29(49(60)54-37-13-15-41(83(69,70)71)35-21-33(81(63,64)65)23-43(45(35)37)85(75,76)77)19-39(25)56-47(58)27-5-3-7-31(17-27)52-51(62)53-32-8-4-6-28(18-32)48(59)57-40-20-30(12-10-26(40)2)50(61)55-38-14-16-42(84(72,73)74)36-22-34(82(66,67)68)24-44(46(36)38)86(78,79)80/h3-24H,1-2H3,(H,54,60)(H,55,61)(H,56,58)(H,57,59)(H2,52,53,62)(H,63,64,65)(H,66,67,68)(H,69,70,71)(H,72,73,74)(H,75,76,77)(H,78,79,80)
FIAFUQMPZJWCLV-UHFFFAOYSA-N
null
null
C51H40N6O23S6
1297.30
null
null
null
1,297.3
null
null
null
null
null
null
CHEMBL265502
CHEMBL265502
CHEMBL265502
Farma [OTHER] | FARMA-939 [RESEARCH_CODE] | Fourneau [OTHER] | Metaret [OTHER] | Naganol [OTHER] | NSC-34936 [RESEARCH_CODE] | Suramin [OTHER] | Suramine [OTHER]
null
null
null
Homo sapiens
null
null
9,606
null
B
Binding
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Ability to destroy fluid-phase human complement 1 in the presence of complement 4 with appropriate serial twofold dilutions of the test compound using C1 assay
CHEMBL1121398
Default value - Target has yet to be curated
U
null
1
CHEMBL612545
null
null
null
null
Unchecked
false
UNCHECKED
null
null
null
null
null
0
null
null
null
null
null
null
null
Carcinoma, Non-Small-Cell Lung
non-small cell lung carcinoma
2.0
1
Conrow RB, Bauman N, Brockman JA, Bernstein S.
10.1021/jm00177a006
null
240
3
J Med Chem
null
7,365,741
1
Synthetic modulators of the complement system. 1. Synthesis and biological activity of 5,5',5''-[1,3,6-naphthalenetriyltris(sulfonylimino)]-tris[1,3-benzenedisulfonic acid] hexasodium salt.
23
1,980
null
34,396
CHEMBL706266
The ability to inhibit late component of human complement (C3-C9) using C-late assay
B
BAO_0000019
assay format
Cc1ccc(C(=O)Nc2ccc(S(=O)(=O)O)c3cc(S(=O)(=O)O)cc(S(=O)(=O)O)c23)cc1NC(=O)c1cccc(NC(=O)Nc2cccc(C(=O)Nc3cc(C(=O)Nc4ccc(S(=O)(=O)O)c5cc(S(=O)(=O)O)cc(S(=O)(=O)O)c45)ccc3C)c2)c1
null
CHEMBL1121398
J Med Chem
1,980
CHEMBL265502
SURAMIN
null
0
http://www.openphacts.org/units/MicrogramPerMilliliter
143,085
=
1
0
=
ED50
ug ml-1
50
CHEMBL612545
null
Unchecked
null
null
ED50
ug ml-1
UO_0000274
50.0
null
null
null
null
null
0
2
null
null
0
3.0
Small molecule
1
false
false
0
SURAMIN
0
MOL
false
false
null
1,997
false
Cc1ccc(C(=O)Nc2ccc(S(=O)(=O)O)c3cc(S(=O)(=O)O)cc(S(=O)(=O)O)c23)cc1NC(=O)c1cccc(NC(=O)Nc2cccc(C(=O)Nc3cc(C(=O)Nc4ccc(S(=O)(=O)O)c5cc(S(=O)(=O)O)cc(S(=O)(=O)O)c45)ccc3C)c2)c1
RDKit 2D 86 93 0 0 0 0 0 0 0 0999 V2000 -2.4083 -0.0667 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 2.8000 -1.2792 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -2.2167 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 1.3917 0.7458 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 -1.4708 -1.7000 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 0.9500 -1.2667 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -0.6000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.8833 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 -0.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.8833 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8167 -0.2125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8167 0.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -1.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4125 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -0.6000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7667 -0.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8750 -1.2917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 0.4625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7167 -0.0917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 1.7750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.3875 1.8208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 0.2000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.2500 -0.3542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.0125 2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4125 -0.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -1.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 2.0083 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.8625 2.1083 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.2542 1.7083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3333 1.8333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7292 0.8625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 1.0208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3333 1.2708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 1.1208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -1.5167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 0.4750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.9667 1.0750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -2.7542 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.0000 -1.9750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.5042 -1.5500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.8625 2.0500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9083 2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8208 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2375 0.6458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.4792 1.7833 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.4500 1.7833 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.9833 -0.0667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.8833 -0.0667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.0292 -0.8125 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.5417 -1.7667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.7375 1.1833 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.8083 -2.2167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.8958 -2.2167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.0792 0.3250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.7458 -2.1667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.6542 -0.8042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.2292 -1.7042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.2083 -1.2250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.7667 0.4083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8208 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7417 1.9583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 2.0875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.0125 2.6000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 1.2958 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.3042 -0.3917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.3875 1.3000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -4.2833 0.1958 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.4000 1.7750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4458 1.7583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9458 2.0333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9292 2.0500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.2958 1.2708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 1.1583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.2958 1.8333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 1.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8625 2.5708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9083 2.6208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4000 2.8458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3625 2.8583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9292 2.5708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9458 2.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 2.6333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7542 2.4958 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 7 1 0 3 14 1 0 4 13 1 0 5 16 1 0 6 15 1 0 7 10 1 0 8 1 1 0 9 8 1 0 10 18 1 0 11 9 2 0 12 10 2 0 13 47 2 0 14 11 1 0 15 28 2 0 16 19 1 0 17 9 1 0 18 26 1 0 19 8 2 0 20 7 2 0 21 25 1 0 22 34 1 0 23 44 1 0 24 31 1 0 25 17 1 0 26 22 1 0 27 49 1 0 28 12 1 0 29 16 2 0 30 23 1 0 31 33 1 0 32 30 1 0 33 36 1 0 34 37 2 0 35 21 1 0 36 35 2 0 37 32 1 0 38 2 1 0 39 1 1 0 40 4 1 0 41 3 1 0 42 5 1 0 43 6 1 0 44 71 2 0 45 24 1 0 46 63 1 0 47 62 1 0 48 27 1 0 49 73 1 0 50 1 2 0 51 1 2 0 52 2 2 0 53 2 2 0 54 4 2 0 55 3 2 0 56 3 2 0 57 4 2 0 58 5 2 0 59 6 2 0 60 6 2 0 61 5 2 0 62 18 2 0 63 17 2 0 64 32 2 0 65 77 1 0 66 27 2 0 67 23 2 0 68 22 2 0 69 24 2 0 70 21 2 0 71 74 1 0 72 45 1 0 73 72 2 0 74 48 1 0 75 35 1 0 76 78 2 0 77 75 2 0 78 64 1 0 79 81 2 0 80 45 2 0 81 83 1 0 82 80 1 0 83 74 2 0 84 82 2 0 85 65 1 0 86 64 1 0 11 29 1 0 14 46 2 0 33 65 2 0 73 84 1 0 44 79 1 0 34 76 1 0 12 13 1 0 20 15 1 0 M END > <chembl_id> CHEMBL265502 > <chembl_pref_name> SURAMIN
InChI=1S/C51H40N6O23S6/c1-25-9-11-29(49(60)54-37-13-15-41(83(69,70)71)35-21-33(81(63,64)65)23-43(45(35)37)85(75,76)77)19-39(25)56-47(58)27-5-3-7-31(17-27)52-51(62)53-32-8-4-6-28(18-32)48(59)57-40-20-30(12-10-26(40)2)50(61)55-38-14-16-42(84(72,73)74)36-22-34(82(66,67)68)24-44(46(36)38)86(78,79)80/h3-24H,1-2H3,(H,54,60)(H,55,61)(H,56,58)(H,57,59)(H2,52,53,62)(H,63,64,65)(H,66,67,68)(H,69,70,71)(H,72,73,74)(H,75,76,77)(H,78,79,80)
FIAFUQMPZJWCLV-UHFFFAOYSA-N
null
null
C51H40N6O23S6
1297.30
null
null
null
1,297.3
null
null
null
null
null
null
CHEMBL265502
CHEMBL265502
CHEMBL265502
Farma [OTHER] | FARMA-939 [RESEARCH_CODE] | Fourneau [OTHER] | Metaret [OTHER] | Naganol [OTHER] | NSC-34936 [RESEARCH_CODE] | Suramin [OTHER] | Suramine [OTHER]
null
null
null
Homo sapiens
null
null
9,606
null
B
Binding
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
The ability to inhibit late component of human complement (C3-C9) using C-late assay
CHEMBL1121398
Default value - Target has yet to be curated
U
null
1
CHEMBL612545
null
null
null
null
Unchecked
false
UNCHECKED
null
null
null
null
null
0
null
null
null
null
null
null
null
Carcinoma, Non-Small-Cell Lung
non-small cell lung carcinoma
2.0
1
Conrow RB, Bauman N, Brockman JA, Bernstein S.
10.1021/jm00177a006
null
240
3
J Med Chem
null
7,365,741
1
Synthetic modulators of the complement system. 1. Synthesis and biological activity of 5,5',5''-[1,3,6-naphthalenetriyltris(sulfonylimino)]-tris[1,3-benzenedisulfonic acid] hexasodium salt.
23
1,980
null
34,397
CHEMBL657541
Inhibition of the complement alternative pathway by Mercaptan-treated human erythrocytes lyse in autologous serum via the alternative pathway activated by cobra venom factor in the presence of appropriate serial twofold dilutions of the test compound
B
BAO_0000366
cell-free format
Cc1ccc(C(=O)Nc2ccc(S(=O)(=O)O)c3cc(S(=O)(=O)O)cc(S(=O)(=O)O)c23)cc1NC(=O)c1cccc(NC(=O)Nc2cccc(C(=O)Nc3cc(C(=O)Nc4ccc(S(=O)(=O)O)c5cc(S(=O)(=O)O)cc(S(=O)(=O)O)c45)ccc3C)c2)c1
null
CHEMBL1121398
J Med Chem
1,980
CHEMBL265502
SURAMIN
null
0
http://www.openphacts.org/units/MicrogramPerMilliliter
143,085
=
1
0
=
ED50
ug ml-1
167
CHEMBL612546
null
Molecular identity unknown
null
null
ED50
ug ml-1
UO_0000274
167.0
null
null
null
null
null
0
2
null
null
0
3.0
Small molecule
1
false
false
0
SURAMIN
0
MOL
false
false
null
1,997
false
Cc1ccc(C(=O)Nc2ccc(S(=O)(=O)O)c3cc(S(=O)(=O)O)cc(S(=O)(=O)O)c23)cc1NC(=O)c1cccc(NC(=O)Nc2cccc(C(=O)Nc3cc(C(=O)Nc4ccc(S(=O)(=O)O)c5cc(S(=O)(=O)O)cc(S(=O)(=O)O)c45)ccc3C)c2)c1
RDKit 2D 86 93 0 0 0 0 0 0 0 0999 V2000 -2.4083 -0.0667 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 2.8000 -1.2792 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -2.2167 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 1.3917 0.7458 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 -1.4708 -1.7000 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 0.9500 -1.2667 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -0.6000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.8833 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 -0.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.8833 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8167 -0.2125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8167 0.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -1.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4125 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -0.6000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7667 -0.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8750 -1.2917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 0.4625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7167 -0.0917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 1.7750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.3875 1.8208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 0.2000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.2500 -0.3542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.0125 2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4125 -0.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -1.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 2.0083 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.8625 2.1083 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.2542 1.7083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3333 1.8333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7292 0.8625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 1.0208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3333 1.2708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 1.1208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -1.5167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 0.4750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.9667 1.0750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -2.7542 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.0000 -1.9750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.5042 -1.5500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.8625 2.0500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9083 2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8208 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2375 0.6458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.4792 1.7833 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.4500 1.7833 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.9833 -0.0667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.8833 -0.0667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.0292 -0.8125 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.5417 -1.7667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.7375 1.1833 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.8083 -2.2167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.8958 -2.2167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.0792 0.3250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.7458 -2.1667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.6542 -0.8042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.2292 -1.7042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.2083 -1.2250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.7667 0.4083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8208 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7417 1.9583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 2.0875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.0125 2.6000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 1.2958 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.3042 -0.3917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.3875 1.3000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -4.2833 0.1958 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.4000 1.7750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4458 1.7583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9458 2.0333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9292 2.0500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.2958 1.2708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 1.1583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.2958 1.8333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 1.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8625 2.5708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9083 2.6208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4000 2.8458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3625 2.8583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9292 2.5708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9458 2.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 2.6333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7542 2.4958 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 7 1 0 3 14 1 0 4 13 1 0 5 16 1 0 6 15 1 0 7 10 1 0 8 1 1 0 9 8 1 0 10 18 1 0 11 9 2 0 12 10 2 0 13 47 2 0 14 11 1 0 15 28 2 0 16 19 1 0 17 9 1 0 18 26 1 0 19 8 2 0 20 7 2 0 21 25 1 0 22 34 1 0 23 44 1 0 24 31 1 0 25 17 1 0 26 22 1 0 27 49 1 0 28 12 1 0 29 16 2 0 30 23 1 0 31 33 1 0 32 30 1 0 33 36 1 0 34 37 2 0 35 21 1 0 36 35 2 0 37 32 1 0 38 2 1 0 39 1 1 0 40 4 1 0 41 3 1 0 42 5 1 0 43 6 1 0 44 71 2 0 45 24 1 0 46 63 1 0 47 62 1 0 48 27 1 0 49 73 1 0 50 1 2 0 51 1 2 0 52 2 2 0 53 2 2 0 54 4 2 0 55 3 2 0 56 3 2 0 57 4 2 0 58 5 2 0 59 6 2 0 60 6 2 0 61 5 2 0 62 18 2 0 63 17 2 0 64 32 2 0 65 77 1 0 66 27 2 0 67 23 2 0 68 22 2 0 69 24 2 0 70 21 2 0 71 74 1 0 72 45 1 0 73 72 2 0 74 48 1 0 75 35 1 0 76 78 2 0 77 75 2 0 78 64 1 0 79 81 2 0 80 45 2 0 81 83 1 0 82 80 1 0 83 74 2 0 84 82 2 0 85 65 1 0 86 64 1 0 11 29 1 0 14 46 2 0 33 65 2 0 73 84 1 0 44 79 1 0 34 76 1 0 12 13 1 0 20 15 1 0 M END > <chembl_id> CHEMBL265502 > <chembl_pref_name> SURAMIN
InChI=1S/C51H40N6O23S6/c1-25-9-11-29(49(60)54-37-13-15-41(83(69,70)71)35-21-33(81(63,64)65)23-43(45(35)37)85(75,76)77)19-39(25)56-47(58)27-5-3-7-31(17-27)52-51(62)53-32-8-4-6-28(18-32)48(59)57-40-20-30(12-10-26(40)2)50(61)55-38-14-16-42(84(72,73)74)36-22-34(82(66,67)68)24-44(46(36)38)86(78,79)80/h3-24H,1-2H3,(H,54,60)(H,55,61)(H,56,58)(H,57,59)(H2,52,53,62)(H,63,64,65)(H,66,67,68)(H,69,70,71)(H,72,73,74)(H,75,76,77)(H,78,79,80)
FIAFUQMPZJWCLV-UHFFFAOYSA-N
null
null
C51H40N6O23S6
1297.30
null
null
null
1,297.3
null
null
null
null
null
null
CHEMBL265502
CHEMBL265502
CHEMBL265502
Farma [OTHER] | FARMA-939 [RESEARCH_CODE] | Fourneau [OTHER] | Metaret [OTHER] | Naganol [OTHER] | NSC-34936 [RESEARCH_CODE] | Suramin [OTHER] | Suramine [OTHER]
null
null
null
Homo sapiens
null
null
9,606
Serum
B
Binding
BAO_0000366
cell-free format
null
Target assigned is molecular non-protein target
3
Inhibition of the complement alternative pathway by Mercaptan-treated human erythrocytes lyse in autologous serum via the alternative pathway activated by cobra venom factor in the presence of appropriate serial twofold dilutions of the test compound
CHEMBL1121398
Molecular target other than protein assigned
M
null
1
CHEMBL612546
CHEMBL3638229
null
null
null
Molecular identity unknown
false
UNKNOWN
null
null
null
null
null
0
null
null
null
null
null
null
null
Carcinoma, Non-Small-Cell Lung
non-small cell lung carcinoma
2.0
1
Conrow RB, Bauman N, Brockman JA, Bernstein S.
10.1021/jm00177a006
null
240
3
J Med Chem
null
7,365,741
1
Synthetic modulators of the complement system. 1. Synthesis and biological activity of 5,5',5''-[1,3,6-naphthalenetriyltris(sulfonylimino)]-tris[1,3-benzenedisulfonic acid] hexasodium salt.
23
1,980
null
34,398
CHEMBL694631
Evaluated in vitro for complement activity using guinea pig serum was determined by cap 50 assay
F
BAO_0000218
organism-based format
Cc1ccc(C(=O)Nc2ccc(S(=O)(=O)O)c3cc(S(=O)(=O)O)cc(S(=O)(=O)O)c23)cc1NC(=O)c1cccc(NC(=O)Nc2cccc(C(=O)Nc3cc(C(=O)Nc4ccc(S(=O)(=O)O)c5cc(S(=O)(=O)O)cc(S(=O)(=O)O)c45)ccc3C)c2)c1
null
CHEMBL1121398
J Med Chem
1,980
CHEMBL265502
SURAMIN
null
0
http://www.openphacts.org/units/MicrogramPerMilliliter
143,085
=
1
0
=
ED50
ug ml-1
603
CHEMBL369
Cavia porcellus
Cavia porcellus
10141
null
ED50
ug ml-1
UO_0000274
603.0
null
null
null
null
null
0
2
null
null
0
3.0
Small molecule
1
false
false
0
SURAMIN
0
MOL
false
false
null
1,997
false
Cc1ccc(C(=O)Nc2ccc(S(=O)(=O)O)c3cc(S(=O)(=O)O)cc(S(=O)(=O)O)c23)cc1NC(=O)c1cccc(NC(=O)Nc2cccc(C(=O)Nc3cc(C(=O)Nc4ccc(S(=O)(=O)O)c5cc(S(=O)(=O)O)cc(S(=O)(=O)O)c45)ccc3C)c2)c1
RDKit 2D 86 93 0 0 0 0 0 0 0 0999 V2000 -2.4083 -0.0667 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 2.8000 -1.2792 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -2.2167 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 1.3917 0.7458 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 -1.4708 -1.7000 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 0.9500 -1.2667 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -0.6000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.8833 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 -0.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.8833 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8167 -0.2125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8167 0.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -1.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4125 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -0.6000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7667 -0.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8750 -1.2917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 0.4625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7167 -0.0917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 1.7750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.3875 1.8208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 0.2000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.2500 -0.3542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.0125 2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4125 -0.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -1.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 2.0083 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.8625 2.1083 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.2542 1.7083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3333 1.8333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7292 0.8625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 1.0208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3333 1.2708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 1.1208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -1.5167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 0.4750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.9667 1.0750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -2.7542 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.0000 -1.9750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.5042 -1.5500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.8625 2.0500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9083 2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8208 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2375 0.6458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.4792 1.7833 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.4500 1.7833 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.9833 -0.0667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.8833 -0.0667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.0292 -0.8125 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.5417 -1.7667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.7375 1.1833 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.8083 -2.2167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.8958 -2.2167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.0792 0.3250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.7458 -2.1667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.6542 -0.8042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.2292 -1.7042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.2083 -1.2250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.7667 0.4083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8208 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7417 1.9583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 2.0875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.0125 2.6000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 1.2958 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.3042 -0.3917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.3875 1.3000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -4.2833 0.1958 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.4000 1.7750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4458 1.7583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9458 2.0333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9292 2.0500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.2958 1.2708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 1.1583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.2958 1.8333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 1.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8625 2.5708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9083 2.6208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4000 2.8458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3625 2.8583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9292 2.5708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9458 2.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 2.6333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7542 2.4958 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 7 1 0 3 14 1 0 4 13 1 0 5 16 1 0 6 15 1 0 7 10 1 0 8 1 1 0 9 8 1 0 10 18 1 0 11 9 2 0 12 10 2 0 13 47 2 0 14 11 1 0 15 28 2 0 16 19 1 0 17 9 1 0 18 26 1 0 19 8 2 0 20 7 2 0 21 25 1 0 22 34 1 0 23 44 1 0 24 31 1 0 25 17 1 0 26 22 1 0 27 49 1 0 28 12 1 0 29 16 2 0 30 23 1 0 31 33 1 0 32 30 1 0 33 36 1 0 34 37 2 0 35 21 1 0 36 35 2 0 37 32 1 0 38 2 1 0 39 1 1 0 40 4 1 0 41 3 1 0 42 5 1 0 43 6 1 0 44 71 2 0 45 24 1 0 46 63 1 0 47 62 1 0 48 27 1 0 49 73 1 0 50 1 2 0 51 1 2 0 52 2 2 0 53 2 2 0 54 4 2 0 55 3 2 0 56 3 2 0 57 4 2 0 58 5 2 0 59 6 2 0 60 6 2 0 61 5 2 0 62 18 2 0 63 17 2 0 64 32 2 0 65 77 1 0 66 27 2 0 67 23 2 0 68 22 2 0 69 24 2 0 70 21 2 0 71 74 1 0 72 45 1 0 73 72 2 0 74 48 1 0 75 35 1 0 76 78 2 0 77 75 2 0 78 64 1 0 79 81 2 0 80 45 2 0 81 83 1 0 82 80 1 0 83 74 2 0 84 82 2 0 85 65 1 0 86 64 1 0 11 29 1 0 14 46 2 0 33 65 2 0 73 84 1 0 44 79 1 0 34 76 1 0 12 13 1 0 20 15 1 0 M END > <chembl_id> CHEMBL265502 > <chembl_pref_name> SURAMIN
InChI=1S/C51H40N6O23S6/c1-25-9-11-29(49(60)54-37-13-15-41(83(69,70)71)35-21-33(81(63,64)65)23-43(45(35)37)85(75,76)77)19-39(25)56-47(58)27-5-3-7-31(17-27)52-51(62)53-32-8-4-6-28(18-32)48(59)57-40-20-30(12-10-26(40)2)50(61)55-38-14-16-42(84(72,73)74)36-22-34(82(66,67)68)24-44(46(36)38)86(78,79)80/h3-24H,1-2H3,(H,54,60)(H,55,61)(H,56,58)(H,57,59)(H2,52,53,62)(H,63,64,65)(H,66,67,68)(H,69,70,71)(H,72,73,74)(H,75,76,77)(H,78,79,80)
FIAFUQMPZJWCLV-UHFFFAOYSA-N
null
null
C51H40N6O23S6
1297.30
null
null
null
1,297.3
null
null
null
null
null
null
CHEMBL265502
CHEMBL265502
CHEMBL265502
Farma [OTHER] | FARMA-939 [RESEARCH_CODE] | Fourneau [OTHER] | Metaret [OTHER] | Naganol [OTHER] | NSC-34936 [RESEARCH_CODE] | Suramin [OTHER] | Suramine [OTHER]
null
null
null
Cavia porcellus
null
null
10,141
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Evaluated in vitro for complement activity using guinea pig serum was determined by cap 50 assay
CHEMBL1121398
Non-molecular target assigned
N
null
1
CHEMBL369
null
null
null
Cavia porcellus
Cavia porcellus
false
ORGANISM
10,141
null
null
null
null
0
null
null
null
null
null
null
null
Carcinoma, Non-Small-Cell Lung
non-small cell lung carcinoma
2.0
1
Conrow RB, Bauman N, Brockman JA, Bernstein S.
10.1021/jm00177a006
null
240
3
J Med Chem
null
7,365,741
1
Synthetic modulators of the complement system. 1. Synthesis and biological activity of 5,5',5''-[1,3,6-naphthalenetriyltris(sulfonylimino)]-tris[1,3-benzenedisulfonic acid] hexasodium salt.
23
1,980
null
34,399
CHEMBL685960
Evaluated in vivo after intraperitoneal administration by guinea pig assay
F
BAO_0000218
organism-based format
Cc1ccc(C(=O)Nc2ccc(S(=O)(=O)O)c3cc(S(=O)(=O)O)cc(S(=O)(=O)O)c23)cc1NC(=O)c1cccc(NC(=O)Nc2cccc(C(=O)Nc3cc(C(=O)Nc4ccc(S(=O)(=O)O)c5cc(S(=O)(=O)O)cc(S(=O)(=O)O)c45)ccc3C)c2)c1
null
CHEMBL1121398
J Med Chem
1,980
CHEMBL265502
SURAMIN
null
0
http://qudt.org/vocab/unit#Percent
143,085
=
1
1
=
Inhibition
%
44
CHEMBL369
Cavia porcellus
Cavia porcellus
10141
null
Inhibition
%
UO_0000187
44.0
null
null
null
null
null
0
2
null
null
0
3.0
Small molecule
1
false
false
0
SURAMIN
0
MOL
false
false
null
1,997
false
Cc1ccc(C(=O)Nc2ccc(S(=O)(=O)O)c3cc(S(=O)(=O)O)cc(S(=O)(=O)O)c23)cc1NC(=O)c1cccc(NC(=O)Nc2cccc(C(=O)Nc3cc(C(=O)Nc4ccc(S(=O)(=O)O)c5cc(S(=O)(=O)O)cc(S(=O)(=O)O)c45)ccc3C)c2)c1
RDKit 2D 86 93 0 0 0 0 0 0 0 0999 V2000 -2.4083 -0.0667 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 2.8000 -1.2792 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -2.2167 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 1.3917 0.7458 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 -1.4708 -1.7000 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 0.9500 -1.2667 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -0.6000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.8833 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 -0.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.8833 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8167 -0.2125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8167 0.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -1.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4125 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -0.6000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7667 -0.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8750 -1.2917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 0.4625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7167 -0.0917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 1.7750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.3875 1.8208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 0.2000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.2500 -0.3542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.0125 2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4125 -0.4375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 -1.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 2.0083 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.8625 2.1083 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.2542 1.7083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3333 1.8333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7292 0.8625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 1.0208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.3333 1.2708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 1.1208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -1.5167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.4083 0.4750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.9667 1.0750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.3500 -2.7542 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.0000 -1.9750 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.5042 -1.5500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.8625 2.0500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9083 2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8208 -1.4167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2375 0.6458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.4792 1.7833 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.4500 1.7833 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.9833 -0.0667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.8833 -0.0667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.0292 -0.8125 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.5417 -1.7667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.7375 1.1833 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.8083 -2.2167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.8958 -2.2167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.0792 0.3250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.7458 -2.1667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.6542 -0.8042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.2292 -1.7042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.2083 -1.2250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.7667 0.4083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8208 -0.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7417 1.9583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 2.0875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.0125 2.6000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.3375 1.2958 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.3042 -0.3917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.3875 1.3000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -4.2833 0.1958 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.4000 1.7750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4458 1.7583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9458 2.0333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9292 2.0500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.2958 1.2708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 1.1583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.2958 1.8333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 1.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8625 2.5708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9083 2.6208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.4000 2.8458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3625 2.8583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9292 2.5708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9458 2.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8125 2.6333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.7542 2.4958 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 7 1 0 3 14 1 0 4 13 1 0 5 16 1 0 6 15 1 0 7 10 1 0 8 1 1 0 9 8 1 0 10 18 1 0 11 9 2 0 12 10 2 0 13 47 2 0 14 11 1 0 15 28 2 0 16 19 1 0 17 9 1 0 18 26 1 0 19 8 2 0 20 7 2 0 21 25 1 0 22 34 1 0 23 44 1 0 24 31 1 0 25 17 1 0 26 22 1 0 27 49 1 0 28 12 1 0 29 16 2 0 30 23 1 0 31 33 1 0 32 30 1 0 33 36 1 0 34 37 2 0 35 21 1 0 36 35 2 0 37 32 1 0 38 2 1 0 39 1 1 0 40 4 1 0 41 3 1 0 42 5 1 0 43 6 1 0 44 71 2 0 45 24 1 0 46 63 1 0 47 62 1 0 48 27 1 0 49 73 1 0 50 1 2 0 51 1 2 0 52 2 2 0 53 2 2 0 54 4 2 0 55 3 2 0 56 3 2 0 57 4 2 0 58 5 2 0 59 6 2 0 60 6 2 0 61 5 2 0 62 18 2 0 63 17 2 0 64 32 2 0 65 77 1 0 66 27 2 0 67 23 2 0 68 22 2 0 69 24 2 0 70 21 2 0 71 74 1 0 72 45 1 0 73 72 2 0 74 48 1 0 75 35 1 0 76 78 2 0 77 75 2 0 78 64 1 0 79 81 2 0 80 45 2 0 81 83 1 0 82 80 1 0 83 74 2 0 84 82 2 0 85 65 1 0 86 64 1 0 11 29 1 0 14 46 2 0 33 65 2 0 73 84 1 0 44 79 1 0 34 76 1 0 12 13 1 0 20 15 1 0 M END > <chembl_id> CHEMBL265502 > <chembl_pref_name> SURAMIN
InChI=1S/C51H40N6O23S6/c1-25-9-11-29(49(60)54-37-13-15-41(83(69,70)71)35-21-33(81(63,64)65)23-43(45(35)37)85(75,76)77)19-39(25)56-47(58)27-5-3-7-31(17-27)52-51(62)53-32-8-4-6-28(18-32)48(59)57-40-20-30(12-10-26(40)2)50(61)55-38-14-16-42(84(72,73)74)36-22-34(82(66,67)68)24-44(46(36)38)86(78,79)80/h3-24H,1-2H3,(H,54,60)(H,55,61)(H,56,58)(H,57,59)(H2,52,53,62)(H,63,64,65)(H,66,67,68)(H,69,70,71)(H,72,73,74)(H,75,76,77)(H,78,79,80)
FIAFUQMPZJWCLV-UHFFFAOYSA-N
null
null
C51H40N6O23S6
1297.30
null
null
null
1,297.3
null
null
null
null
null
null
CHEMBL265502
CHEMBL265502
CHEMBL265502
Farma [OTHER] | FARMA-939 [RESEARCH_CODE] | Fourneau [OTHER] | Metaret [OTHER] | Naganol [OTHER] | NSC-34936 [RESEARCH_CODE] | Suramin [OTHER] | Suramine [OTHER]
null
null
null
Cavia porcellus
null
null
10,141
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Evaluated in vivo after intraperitoneal administration by guinea pig assay
CHEMBL1121398
Non-molecular target assigned
N
null
1
CHEMBL369
null
null
null
Cavia porcellus
Cavia porcellus
false
ORGANISM
10,141
null
null
null
null
0
null
null
null
null
null
null
null
Carcinoma, Non-Small-Cell Lung
non-small cell lung carcinoma
2.0
1
Conrow RB, Bauman N, Brockman JA, Bernstein S.
10.1021/jm00177a006
null
240
3
J Med Chem
null
7,365,741
1
Synthetic modulators of the complement system. 1. Synthesis and biological activity of 5,5',5''-[1,3,6-naphthalenetriyltris(sulfonylimino)]-tris[1,3-benzenedisulfonic acid] hexasodium salt.
23
1,980
null
34,400
CHEMBL778496
The percent fall in systolic blood pressure at 1.5 / 4 hr after peroral administration of 40 mg/kg in conscious renal hypertensive rats (RHR).
F
BAO_0000218
organism-based format
O=C(Nc1ccccc1)NC1CCN(CCCC(=O)c2ccccc2)CC1
null
CHEMBL1121617
J Med Chem
1,980
CHEMBL354681
null
null
0
null
334,500
=
1
0
=
Activity
null
39
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Activity
null
null
39.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(Nc1ccccc1)NC1CCN(CCCC(=O)c2ccccc2)CC1
RDKit 2D 27 29 0 0 0 0 0 0 0 0999 V2000 6.5417 -2.0042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4167 -1.5292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.1500 -1.9875 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.2292 -1.4875 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.7167 -0.3917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.2542 -2.5292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.1667 -0.2417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.2667 -0.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3125 -0.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3417 -2.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6292 -1.5000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.7042 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.7375 -2.0417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.4625 -2.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8167 -1.5417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5000 -1.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.9042 -1.0417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7292 -0.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3667 0.5458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1667 -3.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.0542 -2.4875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.9250 0.9083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2875 0.1333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.3667 -2.9917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.4792 -3.5417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3792 0.7083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.0792 -3.5292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 13 1 0 3 1 1 0 4 1 1 0 5 17 1 0 6 1 2 0 7 5 2 0 8 5 1 0 9 11 1 0 10 11 1 0 11 4 1 0 12 9 1 0 13 10 1 0 14 3 1 0 15 2 1 0 16 15 1 0 17 16 1 0 18 8 1 0 19 8 2 0 20 14 2 0 21 14 1 0 22 19 1 0 23 18 2 0 24 21 2 0 25 20 1 0 26 22 2 0 27 24 1 0 2 12 1 0 27 25 2 0 26 23 1 0 M END > <chembl_id> CHEMBL354681 > <chembl_pref_name> None
InChI=1S/C22H27N3O2/c26-21(18-8-3-1-4-9-18)12-7-15-25-16-13-20(14-17-25)24-22(27)23-19-10-5-2-6-11-19/h1-6,8-11,20H,7,12-17H2,(H2,23,24,27)
DEWQQKPKUSHDOB-UHFFFAOYSA-N
3.94
2
C22H27N3O2
365.48
3
2
27
365.48
-1.38
0
61.44
0.73
N
7
CHEMBL354681
CHEMBL354681
CHEMBL354681
null
null
null
null
Rattus norvegicus
null
null
10,116
Artery
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
The percent fall in systolic blood pressure at 1.5 / 4 hr after peroral administration of 40 mg/kg in conscious renal hypertensive rats (RHR).
CHEMBL1121617
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638216
null
DOSE=40.0 mg/kg | ROUTE=None None
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The synthesis of a series of 1-aralkyl-4-ureidopiperidines is reported. These compounds are related to the benzamidopiperidines exemplified by indoramin. Some of the ureidopiperidines are more potent antihypertensive agents than their benzamidopiperidine counterparts. Two examples, 1-(2-thenoyl)-3-[1-[2-(3-indolyl)ethyl]piperid-4-yl]urea and 1-(2-thenoyl)-3-[1-[4-(4-fluorophenyl)-4-oxobutyl]piperid-4-yl]urea (19 and 58), emerged as the most potent antihypertensive agents in this series.
Archibald JL, Beardsley DR, Bisset GM, Fairbrother P, Jackson JL, Opalko A, Ward TJ.
10.1021/jm00182a009
null
857
8
J Med Chem
null
7,401,114
1
Antihypertensive ureidopiperidines.
23
1,980
null
35,607
CHEMBL782626
Percent inhibition of PCA reaction in anesthetized rats at 11.7 mg/kg peroral administration for 3 hr
F
BAO_0000218
organism-based format
Cn1c(=O)c2nc[nH]c2n(C)c1=O.O
null
CHEMBL1121553
J Med Chem
1,980
CHEMBL1355736
THEOPHYLLINE
null
0
http://qudt.org/vocab/unit#Percent
22,463
=
1
1
=
Inhibition
%
25.1
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Inhibition
%
UO_0000187
25.1
null
null
null
null
1
0
2
1,976
null
0
4.0
Protein
0
true
true
0
THEOPHYLLINE
0
MOL
true
false
null
null
false
Cn1c(=O)c2nc[nH]c2n(C)c1=O.O
RDKit 2D 14 14 0 0 0 0 0 0 0 0999 V2000 8.9134 -7.3176 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -6.5370 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.4046 -6.1103 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9775 -5.2865 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.9775 -6.1103 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4046 -5.2865 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -4.8746 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.2137 -6.3752 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.2137 -5.0314 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.6992 -5.6984 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2419 -6.5370 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -4.0310 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -7.3756 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2419 -4.8746 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 2 1 0 4 5 1 0 5 2 1 0 6 3 2 0 7 4 1 0 8 3 1 0 9 6 1 0 10 8 1 0 11 5 2 0 12 7 2 0 13 2 1 0 14 4 1 0 6 7 1 0 9 10 2 0 M END > <chembl_id> CHEMBL1355736 > <chembl_pref_name> THEOPHYLLINE
InChI=1S/C7H8N4O2.H2O/c1-10-5-4(8-3-9-5)6(12)11(2)7(10)13;/h3H,1-2H3,(H,8,9);1H2
INQSMEFCAIHTJG-UHFFFAOYSA-N
-1.04
2
C7H10N4O3
198.18
5
1
13
180.17
-0.75
0
72.68
0.56
N
0
CHEMBL190
CHEMBL1355736
CHEMBL190
Accurbron [TRADE_NAME] | Aerolate [TRADE_NAME] | Aerolate iii [TRADE_NAME] | Aerolate jr [TRADE_NAME] | Aerolate sr [TRADE_NAME] | Aquaphyllin [TRADE_NAME] | Bronkodyl [TRADE_NAME] | Duraphyl [TRADE_NAME] | Elixicon [TRADE_NAME] | Elixomin [TRADE_NAME] | Elixophyllin [TRADE_NAME] | Elixophyllin sr [TRADE_NAME] | Labid [TRADE_NAME] | Lanophyllin [TRADE_NAME] | Lasma [TRADE_NAME] | NSC-757346 [RESEARCH_CODE] | Nuelin [TRADE_NAME] | Nuelin sa [TRADE_NAME] | Nuelin sa-250 [TRADE_NAME] | Pro-vent [TRADE_NAME] | Quibron-t [TRADE_NAME] | Quibron-t/sr [TRADE_NAME] | Slo-bid [TRADE_NAME] | Slo-phyllin [TRADE_NAME] | Somophyllin-crt [TRADE_NAME] | Somophyllin-t [TRADE_NAME] | Sustaire [TRADE_NAME] | Theo-24 [TRADE_NAME] | Theobid [TRADE_NAME] | Theobid jr. [TRADE_NAME] | Theochron [TRADE_NAME] | Theocin [TRADE_NAME] | Theoclear-100 [TRADE_NAME] | Theoclear-200 [TRADE_NAME] | Theoclear-80 [TRADE_NAME] | Theoclear l.a.-130 [TRADE_NAME] | Theoclear l.a.-260 [TRADE_NAME] | Theo-dur [TRADE_NAME] | Theograd [TRADE_NAME] | Theolair [TRADE_NAME] | Theolair-sr [TRADE_NAME] | Theolixir [TRADE_NAME] | Theophyl [TRADE_NAME] | Theophyl-225 [TRADE_NAME] | Theophylline [ATC] | Theophylline [BNF] | Theophylline [FDA] | Theophylline [MERCK_INDEX] | Theophylline [OTHER] | Theophylline [TRADE_NAME] | Theophylline 0.04% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.08% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.16% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.2% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.32% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.4% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline and dextrose 5% in plastic container [TRADE_NAME] | Theophylline component of dicurin procaine [TRADE_NAME] | Theophylline component of mersalyl- [TRADE_NAME] | Theophylline in dextrose 5% in plastic container [TRADE_NAME] | Theophylline monohydrate [OTHER] | Theophylline-sr [TRADE_NAME] | Theophyl-sr [TRADE_NAME] | Theovent [TRADE_NAME] | T-phyl [TRADE_NAME] | Uni-dur [TRADE_NAME] | Uniphyl [TRADE_NAME] | Uniphyllin continus [TRADE_NAME]
DailyMed:theophylline
null
null
Rattus norvegicus
null
null
10,116
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Percent inhibition of PCA reaction in anesthetized rats at 11.7 mg/kg peroral administration for 3 hr
CHEMBL1121553
Non-molecular target assigned
N
null
1
CHEMBL376
null
null
DOSE=11.7 mg/kg | ROUTE=None None
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
Phosphodiesterase 4 inhibitor | Phosphodiesterase 3 inhibitor | Adenosine receptor antagonist
INHIBITOR | ANTAGONIST
1
1
null
null
null
Pulmonary Disease, Chronic Obstructive | Lung Diseases, Obstructive | Renal Insufficiency, Chronic | Leukemia, Myeloid, Acute | Leukemia | Hypertension, Pulmonary | Prostatic Neoplasms | Carcinoma, Non-Small-Cell Lung | Kidney Diseases | Altitude Sickness | Virus Diseases | Respiratory Insufficiency | Apnea | Depressive Disorder, Major | Pseudohypoparathyroidism | Depressive Disorder | Bronchitis, Chronic | Asthma | Hernias, Diaphragmatic, Congenital | Lung Neoplasms | Severe Acute Respiratory Syndrome
chronic obstructive pulmonary disease | Airway obstruction | chronic kidney disease | acute myeloid leukemia | leukemia | pulmonary arterial hypertension | prostate carcinoma | non-small cell lung carcinoma | kidney disease | altitude sickness | viral disease | respiratory failure | Apnea | major depressive disorder | Albright hereditary osteodystrophy | depressive disorder | chronic bronchitis | asthma | pseudohypoparathyroidism type 1A | pseudohypoparathyroidism | congenital heart disease | lung cancer | COVID-19
4.0
23
The synthesis of a series of substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones is described. Several members of the series exhibit enhanced antiallergic and bronchodilator activity and reduced side effects as compared to theophylline. Structure-activity relationships and metabolic considerations are discussed for the series. Analogues substituted with a 4-(4-chlorobenzyl) moiety, such as 33 and 40, shown an optimal balance of antiallergic and bronchodilator activity and are of particular interest. Compound 33 is significantly more potent than theophylline against both metacholine- and antigen-induced bronchospasms, does not affect spontaneous motor activity, and shows minimal cardiovascular effects in the rat.
Temple DL, Yevich JP, Catt JD, Owens D, Hanning C, Covington RR, Seidehamel RJ, Dungan KW.
10.1021/jm00185a008
null
1188
11
J Med Chem
null
6,161,252
1
Substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones.
23
1,980
null
35,608
CHEMBL783956
Percent inhibition of PCA reaction in anesthetized rats at 47.6 mg/kg oral administration for 15 min
F
BAO_0000218
organism-based format
Cn1c(=O)c2nc[nH]c2n(C)c1=O.O
null
CHEMBL1121553
J Med Chem
1,980
CHEMBL1355736
THEOPHYLLINE
null
0
http://qudt.org/vocab/unit#Percent
22,463
=
1
1
=
Inhibition
%
51.9
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Inhibition
%
UO_0000187
51.9
null
null
null
null
1
0
2
1,976
null
0
4.0
Protein
0
true
true
0
THEOPHYLLINE
0
MOL
true
false
null
null
false
Cn1c(=O)c2nc[nH]c2n(C)c1=O.O
RDKit 2D 14 14 0 0 0 0 0 0 0 0999 V2000 8.9134 -7.3176 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -6.5370 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.4046 -6.1103 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9775 -5.2865 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.9775 -6.1103 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4046 -5.2865 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -4.8746 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.2137 -6.3752 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.2137 -5.0314 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.6992 -5.6984 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2419 -6.5370 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -4.0310 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -7.3756 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2419 -4.8746 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 2 1 0 4 5 1 0 5 2 1 0 6 3 2 0 7 4 1 0 8 3 1 0 9 6 1 0 10 8 1 0 11 5 2 0 12 7 2 0 13 2 1 0 14 4 1 0 6 7 1 0 9 10 2 0 M END > <chembl_id> CHEMBL1355736 > <chembl_pref_name> THEOPHYLLINE
InChI=1S/C7H8N4O2.H2O/c1-10-5-4(8-3-9-5)6(12)11(2)7(10)13;/h3H,1-2H3,(H,8,9);1H2
INQSMEFCAIHTJG-UHFFFAOYSA-N
-1.04
2
C7H10N4O3
198.18
5
1
13
180.17
-0.75
0
72.68
0.56
N
0
CHEMBL190
CHEMBL1355736
CHEMBL190
Accurbron [TRADE_NAME] | Aerolate [TRADE_NAME] | Aerolate iii [TRADE_NAME] | Aerolate jr [TRADE_NAME] | Aerolate sr [TRADE_NAME] | Aquaphyllin [TRADE_NAME] | Bronkodyl [TRADE_NAME] | Duraphyl [TRADE_NAME] | Elixicon [TRADE_NAME] | Elixomin [TRADE_NAME] | Elixophyllin [TRADE_NAME] | Elixophyllin sr [TRADE_NAME] | Labid [TRADE_NAME] | Lanophyllin [TRADE_NAME] | Lasma [TRADE_NAME] | NSC-757346 [RESEARCH_CODE] | Nuelin [TRADE_NAME] | Nuelin sa [TRADE_NAME] | Nuelin sa-250 [TRADE_NAME] | Pro-vent [TRADE_NAME] | Quibron-t [TRADE_NAME] | Quibron-t/sr [TRADE_NAME] | Slo-bid [TRADE_NAME] | Slo-phyllin [TRADE_NAME] | Somophyllin-crt [TRADE_NAME] | Somophyllin-t [TRADE_NAME] | Sustaire [TRADE_NAME] | Theo-24 [TRADE_NAME] | Theobid [TRADE_NAME] | Theobid jr. [TRADE_NAME] | Theochron [TRADE_NAME] | Theocin [TRADE_NAME] | Theoclear-100 [TRADE_NAME] | Theoclear-200 [TRADE_NAME] | Theoclear-80 [TRADE_NAME] | Theoclear l.a.-130 [TRADE_NAME] | Theoclear l.a.-260 [TRADE_NAME] | Theo-dur [TRADE_NAME] | Theograd [TRADE_NAME] | Theolair [TRADE_NAME] | Theolair-sr [TRADE_NAME] | Theolixir [TRADE_NAME] | Theophyl [TRADE_NAME] | Theophyl-225 [TRADE_NAME] | Theophylline [ATC] | Theophylline [BNF] | Theophylline [FDA] | Theophylline [MERCK_INDEX] | Theophylline [OTHER] | Theophylline [TRADE_NAME] | Theophylline 0.04% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.08% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.16% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.2% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.32% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.4% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline and dextrose 5% in plastic container [TRADE_NAME] | Theophylline component of dicurin procaine [TRADE_NAME] | Theophylline component of mersalyl- [TRADE_NAME] | Theophylline in dextrose 5% in plastic container [TRADE_NAME] | Theophylline monohydrate [OTHER] | Theophylline-sr [TRADE_NAME] | Theophyl-sr [TRADE_NAME] | Theovent [TRADE_NAME] | T-phyl [TRADE_NAME] | Uni-dur [TRADE_NAME] | Uniphyl [TRADE_NAME] | Uniphyllin continus [TRADE_NAME]
DailyMed:theophylline
null
null
Rattus norvegicus
null
null
10,116
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Percent inhibition of PCA reaction in anesthetized rats at 47.6 mg/kg oral administration for 15 min
CHEMBL1121553
Non-molecular target assigned
N
null
1
CHEMBL376
null
null
DOSE=47.6 mg/kg | ROUTE=None None
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
Phosphodiesterase 4 inhibitor | Phosphodiesterase 3 inhibitor | Adenosine receptor antagonist
INHIBITOR | ANTAGONIST
1
1
null
null
null
Pulmonary Disease, Chronic Obstructive | Lung Diseases, Obstructive | Renal Insufficiency, Chronic | Leukemia, Myeloid, Acute | Leukemia | Hypertension, Pulmonary | Prostatic Neoplasms | Carcinoma, Non-Small-Cell Lung | Kidney Diseases | Altitude Sickness | Virus Diseases | Respiratory Insufficiency | Apnea | Depressive Disorder, Major | Pseudohypoparathyroidism | Depressive Disorder | Bronchitis, Chronic | Asthma | Hernias, Diaphragmatic, Congenital | Lung Neoplasms | Severe Acute Respiratory Syndrome
chronic obstructive pulmonary disease | Airway obstruction | chronic kidney disease | acute myeloid leukemia | leukemia | pulmonary arterial hypertension | prostate carcinoma | non-small cell lung carcinoma | kidney disease | altitude sickness | viral disease | respiratory failure | Apnea | major depressive disorder | Albright hereditary osteodystrophy | depressive disorder | chronic bronchitis | asthma | pseudohypoparathyroidism type 1A | pseudohypoparathyroidism | congenital heart disease | lung cancer | COVID-19
4.0
23
The synthesis of a series of substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones is described. Several members of the series exhibit enhanced antiallergic and bronchodilator activity and reduced side effects as compared to theophylline. Structure-activity relationships and metabolic considerations are discussed for the series. Analogues substituted with a 4-(4-chlorobenzyl) moiety, such as 33 and 40, shown an optimal balance of antiallergic and bronchodilator activity and are of particular interest. Compound 33 is significantly more potent than theophylline against both metacholine- and antigen-induced bronchospasms, does not affect spontaneous motor activity, and shows minimal cardiovascular effects in the rat.
Temple DL, Yevich JP, Catt JD, Owens D, Hanning C, Covington RR, Seidehamel RJ, Dungan KW.
10.1021/jm00185a008
null
1188
11
J Med Chem
null
6,161,252
1
Substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones.
23
1,980
null
35,609
CHEMBL782624
Percent inhibition of PCA reaction in anesthetized rats at 47.6 mg/kg oral administration for 3 hr
F
BAO_0000218
organism-based format
Cn1c(=O)c2nc[nH]c2n(C)c1=O.O
null
CHEMBL1121553
J Med Chem
1,980
CHEMBL1355736
THEOPHYLLINE
null
0
http://qudt.org/vocab/unit#Percent
22,463
=
1
1
=
Inhibition
%
52.5
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Inhibition
%
UO_0000187
52.5
null
null
null
null
1
0
2
1,976
null
0
4.0
Protein
0
true
true
0
THEOPHYLLINE
0
MOL
true
false
null
null
false
Cn1c(=O)c2nc[nH]c2n(C)c1=O.O
RDKit 2D 14 14 0 0 0 0 0 0 0 0999 V2000 8.9134 -7.3176 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -6.5370 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.4046 -6.1103 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9775 -5.2865 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.9775 -6.1103 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4046 -5.2865 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -4.8746 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.2137 -6.3752 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.2137 -5.0314 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.6992 -5.6984 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2419 -6.5370 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -4.0310 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -7.3756 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2419 -4.8746 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 2 1 0 4 5 1 0 5 2 1 0 6 3 2 0 7 4 1 0 8 3 1 0 9 6 1 0 10 8 1 0 11 5 2 0 12 7 2 0 13 2 1 0 14 4 1 0 6 7 1 0 9 10 2 0 M END > <chembl_id> CHEMBL1355736 > <chembl_pref_name> THEOPHYLLINE
InChI=1S/C7H8N4O2.H2O/c1-10-5-4(8-3-9-5)6(12)11(2)7(10)13;/h3H,1-2H3,(H,8,9);1H2
INQSMEFCAIHTJG-UHFFFAOYSA-N
-1.04
2
C7H10N4O3
198.18
5
1
13
180.17
-0.75
0
72.68
0.56
N
0
CHEMBL190
CHEMBL1355736
CHEMBL190
Accurbron [TRADE_NAME] | Aerolate [TRADE_NAME] | Aerolate iii [TRADE_NAME] | Aerolate jr [TRADE_NAME] | Aerolate sr [TRADE_NAME] | Aquaphyllin [TRADE_NAME] | Bronkodyl [TRADE_NAME] | Duraphyl [TRADE_NAME] | Elixicon [TRADE_NAME] | Elixomin [TRADE_NAME] | Elixophyllin [TRADE_NAME] | Elixophyllin sr [TRADE_NAME] | Labid [TRADE_NAME] | Lanophyllin [TRADE_NAME] | Lasma [TRADE_NAME] | NSC-757346 [RESEARCH_CODE] | Nuelin [TRADE_NAME] | Nuelin sa [TRADE_NAME] | Nuelin sa-250 [TRADE_NAME] | Pro-vent [TRADE_NAME] | Quibron-t [TRADE_NAME] | Quibron-t/sr [TRADE_NAME] | Slo-bid [TRADE_NAME] | Slo-phyllin [TRADE_NAME] | Somophyllin-crt [TRADE_NAME] | Somophyllin-t [TRADE_NAME] | Sustaire [TRADE_NAME] | Theo-24 [TRADE_NAME] | Theobid [TRADE_NAME] | Theobid jr. [TRADE_NAME] | Theochron [TRADE_NAME] | Theocin [TRADE_NAME] | Theoclear-100 [TRADE_NAME] | Theoclear-200 [TRADE_NAME] | Theoclear-80 [TRADE_NAME] | Theoclear l.a.-130 [TRADE_NAME] | Theoclear l.a.-260 [TRADE_NAME] | Theo-dur [TRADE_NAME] | Theograd [TRADE_NAME] | Theolair [TRADE_NAME] | Theolair-sr [TRADE_NAME] | Theolixir [TRADE_NAME] | Theophyl [TRADE_NAME] | Theophyl-225 [TRADE_NAME] | Theophylline [ATC] | Theophylline [BNF] | Theophylline [FDA] | Theophylline [MERCK_INDEX] | Theophylline [OTHER] | Theophylline [TRADE_NAME] | Theophylline 0.04% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.08% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.16% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.2% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.32% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.4% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline and dextrose 5% in plastic container [TRADE_NAME] | Theophylline component of dicurin procaine [TRADE_NAME] | Theophylline component of mersalyl- [TRADE_NAME] | Theophylline in dextrose 5% in plastic container [TRADE_NAME] | Theophylline monohydrate [OTHER] | Theophylline-sr [TRADE_NAME] | Theophyl-sr [TRADE_NAME] | Theovent [TRADE_NAME] | T-phyl [TRADE_NAME] | Uni-dur [TRADE_NAME] | Uniphyl [TRADE_NAME] | Uniphyllin continus [TRADE_NAME]
DailyMed:theophylline
null
null
Rattus norvegicus
null
null
10,116
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Percent inhibition of PCA reaction in anesthetized rats at 47.6 mg/kg oral administration for 3 hr
CHEMBL1121553
Non-molecular target assigned
N
null
1
CHEMBL376
null
null
DOSE=47.6 mg/kg | ROUTE=None None
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
Phosphodiesterase 4 inhibitor | Phosphodiesterase 3 inhibitor | Adenosine receptor antagonist
INHIBITOR | ANTAGONIST
1
1
null
null
null
Pulmonary Disease, Chronic Obstructive | Lung Diseases, Obstructive | Renal Insufficiency, Chronic | Leukemia, Myeloid, Acute | Leukemia | Hypertension, Pulmonary | Prostatic Neoplasms | Carcinoma, Non-Small-Cell Lung | Kidney Diseases | Altitude Sickness | Virus Diseases | Respiratory Insufficiency | Apnea | Depressive Disorder, Major | Pseudohypoparathyroidism | Depressive Disorder | Bronchitis, Chronic | Asthma | Hernias, Diaphragmatic, Congenital | Lung Neoplasms | Severe Acute Respiratory Syndrome
chronic obstructive pulmonary disease | Airway obstruction | chronic kidney disease | acute myeloid leukemia | leukemia | pulmonary arterial hypertension | prostate carcinoma | non-small cell lung carcinoma | kidney disease | altitude sickness | viral disease | respiratory failure | Apnea | major depressive disorder | Albright hereditary osteodystrophy | depressive disorder | chronic bronchitis | asthma | pseudohypoparathyroidism type 1A | pseudohypoparathyroidism | congenital heart disease | lung cancer | COVID-19
4.0
23
The synthesis of a series of substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones is described. Several members of the series exhibit enhanced antiallergic and bronchodilator activity and reduced side effects as compared to theophylline. Structure-activity relationships and metabolic considerations are discussed for the series. Analogues substituted with a 4-(4-chlorobenzyl) moiety, such as 33 and 40, shown an optimal balance of antiallergic and bronchodilator activity and are of particular interest. Compound 33 is significantly more potent than theophylline against both metacholine- and antigen-induced bronchospasms, does not affect spontaneous motor activity, and shows minimal cardiovascular effects in the rat.
Temple DL, Yevich JP, Catt JD, Owens D, Hanning C, Covington RR, Seidehamel RJ, Dungan KW.
10.1021/jm00185a008
null
1188
11
J Med Chem
null
6,161,252
1
Substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones.
23
1,980
null
35,610
CHEMBL782625
Percent inhibition of PCA reaction in anesthetized rats at 47.6 mg/kg oral administration for 6 hr
F
BAO_0000218
organism-based format
Cn1c(=O)c2nc[nH]c2n(C)c1=O.O
null
CHEMBL1121553
J Med Chem
1,980
CHEMBL1355736
THEOPHYLLINE
null
0
http://qudt.org/vocab/unit#Percent
22,463
=
1
1
=
Inhibition
%
13
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Inhibition
%
UO_0000187
13.0
null
null
null
null
1
0
2
1,976
null
0
4.0
Protein
0
true
true
0
THEOPHYLLINE
0
MOL
true
false
null
null
false
Cn1c(=O)c2nc[nH]c2n(C)c1=O.O
RDKit 2D 14 14 0 0 0 0 0 0 0 0999 V2000 8.9134 -7.3176 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -6.5370 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.4046 -6.1103 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9775 -5.2865 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.9775 -6.1103 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4046 -5.2865 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -4.8746 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.2137 -6.3752 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.2137 -5.0314 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.6992 -5.6984 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2419 -6.5370 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -4.0310 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -7.3756 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2419 -4.8746 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 2 1 0 4 5 1 0 5 2 1 0 6 3 2 0 7 4 1 0 8 3 1 0 9 6 1 0 10 8 1 0 11 5 2 0 12 7 2 0 13 2 1 0 14 4 1 0 6 7 1 0 9 10 2 0 M END > <chembl_id> CHEMBL1355736 > <chembl_pref_name> THEOPHYLLINE
InChI=1S/C7H8N4O2.H2O/c1-10-5-4(8-3-9-5)6(12)11(2)7(10)13;/h3H,1-2H3,(H,8,9);1H2
INQSMEFCAIHTJG-UHFFFAOYSA-N
-1.04
2
C7H10N4O3
198.18
5
1
13
180.17
-0.75
0
72.68
0.56
N
0
CHEMBL190
CHEMBL1355736
CHEMBL190
Accurbron [TRADE_NAME] | Aerolate [TRADE_NAME] | Aerolate iii [TRADE_NAME] | Aerolate jr [TRADE_NAME] | Aerolate sr [TRADE_NAME] | Aquaphyllin [TRADE_NAME] | Bronkodyl [TRADE_NAME] | Duraphyl [TRADE_NAME] | Elixicon [TRADE_NAME] | Elixomin [TRADE_NAME] | Elixophyllin [TRADE_NAME] | Elixophyllin sr [TRADE_NAME] | Labid [TRADE_NAME] | Lanophyllin [TRADE_NAME] | Lasma [TRADE_NAME] | NSC-757346 [RESEARCH_CODE] | Nuelin [TRADE_NAME] | Nuelin sa [TRADE_NAME] | Nuelin sa-250 [TRADE_NAME] | Pro-vent [TRADE_NAME] | Quibron-t [TRADE_NAME] | Quibron-t/sr [TRADE_NAME] | Slo-bid [TRADE_NAME] | Slo-phyllin [TRADE_NAME] | Somophyllin-crt [TRADE_NAME] | Somophyllin-t [TRADE_NAME] | Sustaire [TRADE_NAME] | Theo-24 [TRADE_NAME] | Theobid [TRADE_NAME] | Theobid jr. [TRADE_NAME] | Theochron [TRADE_NAME] | Theocin [TRADE_NAME] | Theoclear-100 [TRADE_NAME] | Theoclear-200 [TRADE_NAME] | Theoclear-80 [TRADE_NAME] | Theoclear l.a.-130 [TRADE_NAME] | Theoclear l.a.-260 [TRADE_NAME] | Theo-dur [TRADE_NAME] | Theograd [TRADE_NAME] | Theolair [TRADE_NAME] | Theolair-sr [TRADE_NAME] | Theolixir [TRADE_NAME] | Theophyl [TRADE_NAME] | Theophyl-225 [TRADE_NAME] | Theophylline [ATC] | Theophylline [BNF] | Theophylline [FDA] | Theophylline [MERCK_INDEX] | Theophylline [OTHER] | Theophylline [TRADE_NAME] | Theophylline 0.04% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.08% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.16% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.2% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.32% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.4% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline and dextrose 5% in plastic container [TRADE_NAME] | Theophylline component of dicurin procaine [TRADE_NAME] | Theophylline component of mersalyl- [TRADE_NAME] | Theophylline in dextrose 5% in plastic container [TRADE_NAME] | Theophylline monohydrate [OTHER] | Theophylline-sr [TRADE_NAME] | Theophyl-sr [TRADE_NAME] | Theovent [TRADE_NAME] | T-phyl [TRADE_NAME] | Uni-dur [TRADE_NAME] | Uniphyl [TRADE_NAME] | Uniphyllin continus [TRADE_NAME]
DailyMed:theophylline
null
null
Rattus norvegicus
null
null
10,116
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Percent inhibition of PCA reaction in anesthetized rats at 47.6 mg/kg oral administration for 6 hr
CHEMBL1121553
Non-molecular target assigned
N
null
1
CHEMBL376
null
null
DOSE=47.6 mg/kg | ROUTE=None None
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
Phosphodiesterase 4 inhibitor | Phosphodiesterase 3 inhibitor | Adenosine receptor antagonist
INHIBITOR | ANTAGONIST
1
1
null
null
null
Pulmonary Disease, Chronic Obstructive | Lung Diseases, Obstructive | Renal Insufficiency, Chronic | Leukemia, Myeloid, Acute | Leukemia | Hypertension, Pulmonary | Prostatic Neoplasms | Carcinoma, Non-Small-Cell Lung | Kidney Diseases | Altitude Sickness | Virus Diseases | Respiratory Insufficiency | Apnea | Depressive Disorder, Major | Pseudohypoparathyroidism | Depressive Disorder | Bronchitis, Chronic | Asthma | Hernias, Diaphragmatic, Congenital | Lung Neoplasms | Severe Acute Respiratory Syndrome
chronic obstructive pulmonary disease | Airway obstruction | chronic kidney disease | acute myeloid leukemia | leukemia | pulmonary arterial hypertension | prostate carcinoma | non-small cell lung carcinoma | kidney disease | altitude sickness | viral disease | respiratory failure | Apnea | major depressive disorder | Albright hereditary osteodystrophy | depressive disorder | chronic bronchitis | asthma | pseudohypoparathyroidism type 1A | pseudohypoparathyroidism | congenital heart disease | lung cancer | COVID-19
4.0
23
The synthesis of a series of substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones is described. Several members of the series exhibit enhanced antiallergic and bronchodilator activity and reduced side effects as compared to theophylline. Structure-activity relationships and metabolic considerations are discussed for the series. Analogues substituted with a 4-(4-chlorobenzyl) moiety, such as 33 and 40, shown an optimal balance of antiallergic and bronchodilator activity and are of particular interest. Compound 33 is significantly more potent than theophylline against both metacholine- and antigen-induced bronchospasms, does not affect spontaneous motor activity, and shows minimal cardiovascular effects in the rat.
Temple DL, Yevich JP, Catt JD, Owens D, Hanning C, Covington RR, Seidehamel RJ, Dungan KW.
10.1021/jm00185a008
null
1188
11
J Med Chem
null
6,161,252
1
Substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones.
23
1,980
null
35,611
CHEMBL782623
Percent inhibition of PCA reaction in anesthetized rats at 47.6 mg/kg oral administration for 24 hr r
F
BAO_0000218
organism-based format
Cn1c(=O)c2nc[nH]c2n(C)c1=O.O
null
CHEMBL1121553
J Med Chem
1,980
CHEMBL1355736
THEOPHYLLINE
null
0
http://qudt.org/vocab/unit#Percent
22,463
=
1
1
=
Inhibition
%
0
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Inhibition
%
UO_0000187
0.0
null
null
null
null
1
0
2
1,976
null
0
4.0
Protein
0
true
true
0
THEOPHYLLINE
0
MOL
true
false
null
null
false
Cn1c(=O)c2nc[nH]c2n(C)c1=O.O
RDKit 2D 14 14 0 0 0 0 0 0 0 0999 V2000 8.9134 -7.3176 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -6.5370 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.4046 -6.1103 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9775 -5.2865 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.9775 -6.1103 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4046 -5.2865 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -4.8746 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.2137 -6.3752 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.2137 -5.0314 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.6992 -5.6984 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2419 -6.5370 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -4.0310 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -7.3756 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2419 -4.8746 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 2 1 0 4 5 1 0 5 2 1 0 6 3 2 0 7 4 1 0 8 3 1 0 9 6 1 0 10 8 1 0 11 5 2 0 12 7 2 0 13 2 1 0 14 4 1 0 6 7 1 0 9 10 2 0 M END > <chembl_id> CHEMBL1355736 > <chembl_pref_name> THEOPHYLLINE
InChI=1S/C7H8N4O2.H2O/c1-10-5-4(8-3-9-5)6(12)11(2)7(10)13;/h3H,1-2H3,(H,8,9);1H2
INQSMEFCAIHTJG-UHFFFAOYSA-N
-1.04
2
C7H10N4O3
198.18
5
1
13
180.17
-0.75
0
72.68
0.56
N
0
CHEMBL190
CHEMBL1355736
CHEMBL190
Accurbron [TRADE_NAME] | Aerolate [TRADE_NAME] | Aerolate iii [TRADE_NAME] | Aerolate jr [TRADE_NAME] | Aerolate sr [TRADE_NAME] | Aquaphyllin [TRADE_NAME] | Bronkodyl [TRADE_NAME] | Duraphyl [TRADE_NAME] | Elixicon [TRADE_NAME] | Elixomin [TRADE_NAME] | Elixophyllin [TRADE_NAME] | Elixophyllin sr [TRADE_NAME] | Labid [TRADE_NAME] | Lanophyllin [TRADE_NAME] | Lasma [TRADE_NAME] | NSC-757346 [RESEARCH_CODE] | Nuelin [TRADE_NAME] | Nuelin sa [TRADE_NAME] | Nuelin sa-250 [TRADE_NAME] | Pro-vent [TRADE_NAME] | Quibron-t [TRADE_NAME] | Quibron-t/sr [TRADE_NAME] | Slo-bid [TRADE_NAME] | Slo-phyllin [TRADE_NAME] | Somophyllin-crt [TRADE_NAME] | Somophyllin-t [TRADE_NAME] | Sustaire [TRADE_NAME] | Theo-24 [TRADE_NAME] | Theobid [TRADE_NAME] | Theobid jr. [TRADE_NAME] | Theochron [TRADE_NAME] | Theocin [TRADE_NAME] | Theoclear-100 [TRADE_NAME] | Theoclear-200 [TRADE_NAME] | Theoclear-80 [TRADE_NAME] | Theoclear l.a.-130 [TRADE_NAME] | Theoclear l.a.-260 [TRADE_NAME] | Theo-dur [TRADE_NAME] | Theograd [TRADE_NAME] | Theolair [TRADE_NAME] | Theolair-sr [TRADE_NAME] | Theolixir [TRADE_NAME] | Theophyl [TRADE_NAME] | Theophyl-225 [TRADE_NAME] | Theophylline [ATC] | Theophylline [BNF] | Theophylline [FDA] | Theophylline [MERCK_INDEX] | Theophylline [OTHER] | Theophylline [TRADE_NAME] | Theophylline 0.04% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.08% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.16% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.2% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.32% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.4% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline and dextrose 5% in plastic container [TRADE_NAME] | Theophylline component of dicurin procaine [TRADE_NAME] | Theophylline component of mersalyl- [TRADE_NAME] | Theophylline in dextrose 5% in plastic container [TRADE_NAME] | Theophylline monohydrate [OTHER] | Theophylline-sr [TRADE_NAME] | Theophyl-sr [TRADE_NAME] | Theovent [TRADE_NAME] | T-phyl [TRADE_NAME] | Uni-dur [TRADE_NAME] | Uniphyl [TRADE_NAME] | Uniphyllin continus [TRADE_NAME]
DailyMed:theophylline
null
null
Rattus norvegicus
null
null
10,116
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Percent inhibition of PCA reaction in anesthetized rats at 47.6 mg/kg oral administration for 24 hr r
CHEMBL1121553
Non-molecular target assigned
N
null
1
CHEMBL376
null
null
DOSE=47.6 mg/kg | ROUTE=None None
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
Phosphodiesterase 4 inhibitor | Phosphodiesterase 3 inhibitor | Adenosine receptor antagonist
INHIBITOR | ANTAGONIST
1
1
null
null
null
Pulmonary Disease, Chronic Obstructive | Lung Diseases, Obstructive | Renal Insufficiency, Chronic | Leukemia, Myeloid, Acute | Leukemia | Hypertension, Pulmonary | Prostatic Neoplasms | Carcinoma, Non-Small-Cell Lung | Kidney Diseases | Altitude Sickness | Virus Diseases | Respiratory Insufficiency | Apnea | Depressive Disorder, Major | Pseudohypoparathyroidism | Depressive Disorder | Bronchitis, Chronic | Asthma | Hernias, Diaphragmatic, Congenital | Lung Neoplasms | Severe Acute Respiratory Syndrome
chronic obstructive pulmonary disease | Airway obstruction | chronic kidney disease | acute myeloid leukemia | leukemia | pulmonary arterial hypertension | prostate carcinoma | non-small cell lung carcinoma | kidney disease | altitude sickness | viral disease | respiratory failure | Apnea | major depressive disorder | Albright hereditary osteodystrophy | depressive disorder | chronic bronchitis | asthma | pseudohypoparathyroidism type 1A | pseudohypoparathyroidism | congenital heart disease | lung cancer | COVID-19
4.0
23
The synthesis of a series of substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones is described. Several members of the series exhibit enhanced antiallergic and bronchodilator activity and reduced side effects as compared to theophylline. Structure-activity relationships and metabolic considerations are discussed for the series. Analogues substituted with a 4-(4-chlorobenzyl) moiety, such as 33 and 40, shown an optimal balance of antiallergic and bronchodilator activity and are of particular interest. Compound 33 is significantly more potent than theophylline against both metacholine- and antigen-induced bronchospasms, does not affect spontaneous motor activity, and shows minimal cardiovascular effects in the rat.
Temple DL, Yevich JP, Catt JD, Owens D, Hanning C, Covington RR, Seidehamel RJ, Dungan KW.
10.1021/jm00185a008
null
1188
11
J Med Chem
null
6,161,252
1
Substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones.
23
1,980
null
35,612
CHEMBL760588
Relative inhibition of rat lung phosphodiesterase cGMP and cAMP activity
B
BAO_0000019
assay format
Cn1c(=O)c2nc[nH]c2n(C)c1=O.O
null
CHEMBL1121553
J Med Chem
1,980
CHEMBL1355736
THEOPHYLLINE
null
0
null
22,463
=
1
0
=
Ratio
null
2.6
CHEMBL612545
null
Unchecked
null
null
Ratio
null
null
2.6
null
null
null
null
1
0
2
1,976
null
0
4.0
Protein
0
true
true
0
THEOPHYLLINE
0
MOL
true
false
null
null
false
Cn1c(=O)c2nc[nH]c2n(C)c1=O.O
RDKit 2D 14 14 0 0 0 0 0 0 0 0999 V2000 8.9134 -7.3176 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -6.5370 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.4046 -6.1103 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9775 -5.2865 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.9775 -6.1103 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4046 -5.2865 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -4.8746 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.2137 -6.3752 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.2137 -5.0314 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.6992 -5.6984 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2419 -6.5370 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -4.0310 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6984 -7.3756 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2419 -4.8746 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 2 1 0 4 5 1 0 5 2 1 0 6 3 2 0 7 4 1 0 8 3 1 0 9 6 1 0 10 8 1 0 11 5 2 0 12 7 2 0 13 2 1 0 14 4 1 0 6 7 1 0 9 10 2 0 M END > <chembl_id> CHEMBL1355736 > <chembl_pref_name> THEOPHYLLINE
InChI=1S/C7H8N4O2.H2O/c1-10-5-4(8-3-9-5)6(12)11(2)7(10)13;/h3H,1-2H3,(H,8,9);1H2
INQSMEFCAIHTJG-UHFFFAOYSA-N
-1.04
2
C7H10N4O3
198.18
5
1
13
180.17
-0.75
0
72.68
0.56
N
0
CHEMBL190
CHEMBL1355736
CHEMBL190
Accurbron [TRADE_NAME] | Aerolate [TRADE_NAME] | Aerolate iii [TRADE_NAME] | Aerolate jr [TRADE_NAME] | Aerolate sr [TRADE_NAME] | Aquaphyllin [TRADE_NAME] | Bronkodyl [TRADE_NAME] | Duraphyl [TRADE_NAME] | Elixicon [TRADE_NAME] | Elixomin [TRADE_NAME] | Elixophyllin [TRADE_NAME] | Elixophyllin sr [TRADE_NAME] | Labid [TRADE_NAME] | Lanophyllin [TRADE_NAME] | Lasma [TRADE_NAME] | NSC-757346 [RESEARCH_CODE] | Nuelin [TRADE_NAME] | Nuelin sa [TRADE_NAME] | Nuelin sa-250 [TRADE_NAME] | Pro-vent [TRADE_NAME] | Quibron-t [TRADE_NAME] | Quibron-t/sr [TRADE_NAME] | Slo-bid [TRADE_NAME] | Slo-phyllin [TRADE_NAME] | Somophyllin-crt [TRADE_NAME] | Somophyllin-t [TRADE_NAME] | Sustaire [TRADE_NAME] | Theo-24 [TRADE_NAME] | Theobid [TRADE_NAME] | Theobid jr. [TRADE_NAME] | Theochron [TRADE_NAME] | Theocin [TRADE_NAME] | Theoclear-100 [TRADE_NAME] | Theoclear-200 [TRADE_NAME] | Theoclear-80 [TRADE_NAME] | Theoclear l.a.-130 [TRADE_NAME] | Theoclear l.a.-260 [TRADE_NAME] | Theo-dur [TRADE_NAME] | Theograd [TRADE_NAME] | Theolair [TRADE_NAME] | Theolair-sr [TRADE_NAME] | Theolixir [TRADE_NAME] | Theophyl [TRADE_NAME] | Theophyl-225 [TRADE_NAME] | Theophylline [ATC] | Theophylline [BNF] | Theophylline [FDA] | Theophylline [MERCK_INDEX] | Theophylline [OTHER] | Theophylline [TRADE_NAME] | Theophylline 0.04% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.08% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.16% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.2% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.32% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline 0.4% and dextrose 5% in plastic container [TRADE_NAME] | Theophylline and dextrose 5% in plastic container [TRADE_NAME] | Theophylline component of dicurin procaine [TRADE_NAME] | Theophylline component of mersalyl- [TRADE_NAME] | Theophylline in dextrose 5% in plastic container [TRADE_NAME] | Theophylline monohydrate [OTHER] | Theophylline-sr [TRADE_NAME] | Theophyl-sr [TRADE_NAME] | Theovent [TRADE_NAME] | T-phyl [TRADE_NAME] | Uni-dur [TRADE_NAME] | Uniphyl [TRADE_NAME] | Uniphyllin continus [TRADE_NAME]
DailyMed:theophylline
null
null
Rattus norvegicus
null
null
10,116
null
B
Binding
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Relative inhibition of rat lung phosphodiesterase cGMP and cAMP activity
CHEMBL1121553
Default value - Target has yet to be curated
U
null
1
CHEMBL612545
null
null
null
null
Unchecked
false
UNCHECKED
null
null
null
null
null
0
Phosphodiesterase 4 inhibitor | Phosphodiesterase 3 inhibitor | Adenosine receptor antagonist
INHIBITOR | ANTAGONIST
1
1
null
null
null
Pulmonary Disease, Chronic Obstructive | Lung Diseases, Obstructive | Renal Insufficiency, Chronic | Leukemia, Myeloid, Acute | Leukemia | Hypertension, Pulmonary | Prostatic Neoplasms | Carcinoma, Non-Small-Cell Lung | Kidney Diseases | Altitude Sickness | Virus Diseases | Respiratory Insufficiency | Apnea | Depressive Disorder, Major | Pseudohypoparathyroidism | Depressive Disorder | Bronchitis, Chronic | Asthma | Hernias, Diaphragmatic, Congenital | Lung Neoplasms | Severe Acute Respiratory Syndrome
chronic obstructive pulmonary disease | Airway obstruction | chronic kidney disease | acute myeloid leukemia | leukemia | pulmonary arterial hypertension | prostate carcinoma | non-small cell lung carcinoma | kidney disease | altitude sickness | viral disease | respiratory failure | Apnea | major depressive disorder | Albright hereditary osteodystrophy | depressive disorder | chronic bronchitis | asthma | pseudohypoparathyroidism type 1A | pseudohypoparathyroidism | congenital heart disease | lung cancer | COVID-19
4.0
23
The synthesis of a series of substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones is described. Several members of the series exhibit enhanced antiallergic and bronchodilator activity and reduced side effects as compared to theophylline. Structure-activity relationships and metabolic considerations are discussed for the series. Analogues substituted with a 4-(4-chlorobenzyl) moiety, such as 33 and 40, shown an optimal balance of antiallergic and bronchodilator activity and are of particular interest. Compound 33 is significantly more potent than theophylline against both metacholine- and antigen-induced bronchospasms, does not affect spontaneous motor activity, and shows minimal cardiovascular effects in the rat.
Temple DL, Yevich JP, Catt JD, Owens D, Hanning C, Covington RR, Seidehamel RJ, Dungan KW.
10.1021/jm00185a008
null
1188
11
J Med Chem
null
6,161,252
1
Substituted 6,7-dihydroimidazo[1,2-a]purin-9(4H)-ones.
23
1,980
null
35,613
CHEMBL775944
Decrease in mean arterial blood pressure in response to intravenous administration at 2 uM/kg of the compound
F
BAO_0000218
organism-based format
CN(C)C1=Nc2ccccc2CN1
null
CHEMBL1121579
J Med Chem
1,980
CHEMBL270409
null
null
0
http://qudt.org/vocab/unit#Percent
30,838
=
1
0
=
Decrease in blood pressure
%
0
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Decrease in blood pressure
%
UO_0000187
0.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CN(C)C1=Nc2ccccc2CN1
RDKit 2D 13 14 0 0 0 0 0 0 0 0999 V2000 -4.1777 -7.0576 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.1789 -7.8843 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4645 -8.2970 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4663 -6.6451 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7515 -7.0539 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7527 -7.8864 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0363 -8.3014 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.3141 -7.8885 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3129 -7.0560 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.0339 -6.6364 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6013 -8.3027 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.1138 -7.8925 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6036 -9.1272 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 6 2 0 1 2 2 0 5 4 2 0 4 1 1 0 5 10 1 0 6 7 1 0 7 8 2 0 8 9 1 0 9 10 1 0 5 6 1 0 8 11 1 0 11 12 1 0 2 3 1 0 11 13 1 0 M END > <chembl_id> CHEMBL270409 > <chembl_pref_name> None
InChI=1S/C10H13N3/c1-13(2)10-11-7-8-5-3-4-6-9(8)12-10/h3-6H,7H2,1-2H3,(H,11,12)
MNTBAXGKERZVOZ-UHFFFAOYSA-N
1.34
1
C10H13N3
175.24
3
1
13
175.24
-0.21
0
27.63
0.64
Y
0
CHEMBL270409
CHEMBL270409
CHEMBL270409
null
null
null
null
Rattus norvegicus
null
null
10,116
Artery
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Decrease in mean arterial blood pressure in response to intravenous administration at 2 uM/kg of the compound
CHEMBL1121579
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638216
null
null
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Based on the known biological activity of a variety of guanidine-containing agents, several N-substituted 3,4-dihydroquinazolines were synthesized. These compounds can be considered to be rigid analogues of phenylguanidines. In anesthetized rats the compounds decreased blood pressure and were antagonists of the pressor response to norepinephrine.
Grosso JA, Nichols DE, Nichols MB, Yim GK.
10.1021/jm00185a026
null
1261
11
J Med Chem
null
7,452,680
1
Synthesis and adrenergic blocking effects of 2-(alkylamino)-3,4-dihydroquinazolines.
23
1,980
null
35,614
CHEMBL775946
Decrease in mean arterial blood pressure in response to intravenous administration at 4 uM/kg of the compound
F
BAO_0000218
organism-based format
CN(C)C1=Nc2ccccc2CN1
null
CHEMBL1121579
J Med Chem
1,980
CHEMBL270409
null
null
0
http://qudt.org/vocab/unit#Percent
30,838
=
1
0
=
Decrease in blood pressure
%
0
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Decrease in blood pressure
%
UO_0000187
0.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CN(C)C1=Nc2ccccc2CN1
RDKit 2D 13 14 0 0 0 0 0 0 0 0999 V2000 -4.1777 -7.0576 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.1789 -7.8843 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4645 -8.2970 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4663 -6.6451 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7515 -7.0539 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7527 -7.8864 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0363 -8.3014 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.3141 -7.8885 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3129 -7.0560 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.0339 -6.6364 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6013 -8.3027 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.1138 -7.8925 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6036 -9.1272 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 6 2 0 1 2 2 0 5 4 2 0 4 1 1 0 5 10 1 0 6 7 1 0 7 8 2 0 8 9 1 0 9 10 1 0 5 6 1 0 8 11 1 0 11 12 1 0 2 3 1 0 11 13 1 0 M END > <chembl_id> CHEMBL270409 > <chembl_pref_name> None
InChI=1S/C10H13N3/c1-13(2)10-11-7-8-5-3-4-6-9(8)12-10/h3-6H,7H2,1-2H3,(H,11,12)
MNTBAXGKERZVOZ-UHFFFAOYSA-N
1.34
1
C10H13N3
175.24
3
1
13
175.24
-0.21
0
27.63
0.64
Y
0
CHEMBL270409
CHEMBL270409
CHEMBL270409
null
null
null
null
Rattus norvegicus
null
null
10,116
Artery
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Decrease in mean arterial blood pressure in response to intravenous administration at 4 uM/kg of the compound
CHEMBL1121579
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638216
null
null
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Based on the known biological activity of a variety of guanidine-containing agents, several N-substituted 3,4-dihydroquinazolines were synthesized. These compounds can be considered to be rigid analogues of phenylguanidines. In anesthetized rats the compounds decreased blood pressure and were antagonists of the pressor response to norepinephrine.
Grosso JA, Nichols DE, Nichols MB, Yim GK.
10.1021/jm00185a026
null
1261
11
J Med Chem
null
7,452,680
1
Synthesis and adrenergic blocking effects of 2-(alkylamino)-3,4-dihydroquinazolines.
23
1,980
null
35,615
CHEMBL775949
Decrease in mean arterial blood pressure in response to intravenous administration at 8 uM/kg of the compound
F
BAO_0000218
organism-based format
CN(C)C1=Nc2ccccc2CN1
null
CHEMBL1121579
J Med Chem
1,980
CHEMBL270409
null
null
0
http://qudt.org/vocab/unit#Percent
30,838
=
1
0
=
Decrease in blood pressure
%
5.67
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Decrease in blood pressure
%
UO_0000187
5.67
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CN(C)C1=Nc2ccccc2CN1
RDKit 2D 13 14 0 0 0 0 0 0 0 0999 V2000 -4.1777 -7.0576 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.1789 -7.8843 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4645 -8.2970 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4663 -6.6451 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7515 -7.0539 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7527 -7.8864 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0363 -8.3014 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.3141 -7.8885 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3129 -7.0560 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.0339 -6.6364 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6013 -8.3027 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.1138 -7.8925 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6036 -9.1272 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 6 2 0 1 2 2 0 5 4 2 0 4 1 1 0 5 10 1 0 6 7 1 0 7 8 2 0 8 9 1 0 9 10 1 0 5 6 1 0 8 11 1 0 11 12 1 0 2 3 1 0 11 13 1 0 M END > <chembl_id> CHEMBL270409 > <chembl_pref_name> None
InChI=1S/C10H13N3/c1-13(2)10-11-7-8-5-3-4-6-9(8)12-10/h3-6H,7H2,1-2H3,(H,11,12)
MNTBAXGKERZVOZ-UHFFFAOYSA-N
1.34
1
C10H13N3
175.24
3
1
13
175.24
-0.21
0
27.63
0.64
Y
0
CHEMBL270409
CHEMBL270409
CHEMBL270409
null
null
null
null
Rattus norvegicus
null
null
10,116
Artery
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Decrease in mean arterial blood pressure in response to intravenous administration at 8 uM/kg of the compound
CHEMBL1121579
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638216
null
null
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Based on the known biological activity of a variety of guanidine-containing agents, several N-substituted 3,4-dihydroquinazolines were synthesized. These compounds can be considered to be rigid analogues of phenylguanidines. In anesthetized rats the compounds decreased blood pressure and were antagonists of the pressor response to norepinephrine.
Grosso JA, Nichols DE, Nichols MB, Yim GK.
10.1021/jm00185a026
null
1261
11
J Med Chem
null
7,452,680
1
Synthesis and adrenergic blocking effects of 2-(alkylamino)-3,4-dihydroquinazolines.
23
1,980
null
35,616
CHEMBL777707
Decrease in mean arterial blood pressure in response to intravenous administration at 16 uM/kg of the compound
F
BAO_0000218
organism-based format
CN(C)C1=Nc2ccccc2CN1
null
CHEMBL1121579
J Med Chem
1,980
CHEMBL270409
null
null
0
http://qudt.org/vocab/unit#Percent
30,838
=
1
0
=
Decrease in blood pressure
%
7.3
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Decrease in blood pressure
%
UO_0000187
7.3
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CN(C)C1=Nc2ccccc2CN1
RDKit 2D 13 14 0 0 0 0 0 0 0 0999 V2000 -4.1777 -7.0576 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.1789 -7.8843 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4645 -8.2970 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4663 -6.6451 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7515 -7.0539 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7527 -7.8864 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0363 -8.3014 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.3141 -7.8885 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3129 -7.0560 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.0339 -6.6364 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6013 -8.3027 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.1138 -7.8925 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6036 -9.1272 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 6 2 0 1 2 2 0 5 4 2 0 4 1 1 0 5 10 1 0 6 7 1 0 7 8 2 0 8 9 1 0 9 10 1 0 5 6 1 0 8 11 1 0 11 12 1 0 2 3 1 0 11 13 1 0 M END > <chembl_id> CHEMBL270409 > <chembl_pref_name> None
InChI=1S/C10H13N3/c1-13(2)10-11-7-8-5-3-4-6-9(8)12-10/h3-6H,7H2,1-2H3,(H,11,12)
MNTBAXGKERZVOZ-UHFFFAOYSA-N
1.34
1
C10H13N3
175.24
3
1
13
175.24
-0.21
0
27.63
0.64
Y
0
CHEMBL270409
CHEMBL270409
CHEMBL270409
null
null
null
null
Rattus norvegicus
null
null
10,116
Artery
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Decrease in mean arterial blood pressure in response to intravenous administration at 16 uM/kg of the compound
CHEMBL1121579
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638216
null
null
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Based on the known biological activity of a variety of guanidine-containing agents, several N-substituted 3,4-dihydroquinazolines were synthesized. These compounds can be considered to be rigid analogues of phenylguanidines. In anesthetized rats the compounds decreased blood pressure and were antagonists of the pressor response to norepinephrine.
Grosso JA, Nichols DE, Nichols MB, Yim GK.
10.1021/jm00185a026
null
1261
11
J Med Chem
null
7,452,680
1
Synthesis and adrenergic blocking effects of 2-(alkylamino)-3,4-dihydroquinazolines.
23
1,980
null
35,617
CHEMBL882050
Decrease in mean arterial blood pressure in response to intravenous administration at 32 uM/kg of the compound
F
BAO_0000218
organism-based format
CN(C)C1=Nc2ccccc2CN1
null
CHEMBL1121579
J Med Chem
1,980
CHEMBL270409
null
null
0
http://qudt.org/vocab/unit#Percent
30,838
=
1
0
=
Decrease in blood pressure
%
12.3
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Decrease in blood pressure
%
UO_0000187
12.3
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CN(C)C1=Nc2ccccc2CN1
RDKit 2D 13 14 0 0 0 0 0 0 0 0999 V2000 -4.1777 -7.0576 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.1789 -7.8843 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4645 -8.2970 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4663 -6.6451 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7515 -7.0539 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7527 -7.8864 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0363 -8.3014 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.3141 -7.8885 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3129 -7.0560 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.0339 -6.6364 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6013 -8.3027 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.1138 -7.8925 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6036 -9.1272 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 6 2 0 1 2 2 0 5 4 2 0 4 1 1 0 5 10 1 0 6 7 1 0 7 8 2 0 8 9 1 0 9 10 1 0 5 6 1 0 8 11 1 0 11 12 1 0 2 3 1 0 11 13 1 0 M END > <chembl_id> CHEMBL270409 > <chembl_pref_name> None
InChI=1S/C10H13N3/c1-13(2)10-11-7-8-5-3-4-6-9(8)12-10/h3-6H,7H2,1-2H3,(H,11,12)
MNTBAXGKERZVOZ-UHFFFAOYSA-N
1.34
1
C10H13N3
175.24
3
1
13
175.24
-0.21
0
27.63
0.64
Y
0
CHEMBL270409
CHEMBL270409
CHEMBL270409
null
null
null
null
Rattus norvegicus
null
null
10,116
Artery
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Decrease in mean arterial blood pressure in response to intravenous administration at 32 uM/kg of the compound
CHEMBL1121579
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638216
null
null
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Based on the known biological activity of a variety of guanidine-containing agents, several N-substituted 3,4-dihydroquinazolines were synthesized. These compounds can be considered to be rigid analogues of phenylguanidines. In anesthetized rats the compounds decreased blood pressure and were antagonists of the pressor response to norepinephrine.
Grosso JA, Nichols DE, Nichols MB, Yim GK.
10.1021/jm00185a026
null
1261
11
J Med Chem
null
7,452,680
1
Synthesis and adrenergic blocking effects of 2-(alkylamino)-3,4-dihydroquinazolines.
23
1,980
null
35,618
CHEMBL775948
Decrease in mean arterial blood pressure in response to intravenous administration at 64 uM/kg of the compound.
F
BAO_0000218
organism-based format
CN(C)C1=Nc2ccccc2CN1
null
CHEMBL1121579
J Med Chem
1,980
CHEMBL270409
null
null
0
http://qudt.org/vocab/unit#Percent
30,838
=
1
0
=
Decrease in blood pressure
%
24.7
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Decrease in blood pressure
%
UO_0000187
24.7
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CN(C)C1=Nc2ccccc2CN1
RDKit 2D 13 14 0 0 0 0 0 0 0 0999 V2000 -4.1777 -7.0576 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.1789 -7.8843 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4645 -8.2970 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4663 -6.6451 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7515 -7.0539 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7527 -7.8864 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0363 -8.3014 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.3141 -7.8885 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3129 -7.0560 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.0339 -6.6364 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6013 -8.3027 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.1138 -7.8925 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6036 -9.1272 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 6 2 0 1 2 2 0 5 4 2 0 4 1 1 0 5 10 1 0 6 7 1 0 7 8 2 0 8 9 1 0 9 10 1 0 5 6 1 0 8 11 1 0 11 12 1 0 2 3 1 0 11 13 1 0 M END > <chembl_id> CHEMBL270409 > <chembl_pref_name> None
InChI=1S/C10H13N3/c1-13(2)10-11-7-8-5-3-4-6-9(8)12-10/h3-6H,7H2,1-2H3,(H,11,12)
MNTBAXGKERZVOZ-UHFFFAOYSA-N
1.34
1
C10H13N3
175.24
3
1
13
175.24
-0.21
0
27.63
0.64
Y
0
CHEMBL270409
CHEMBL270409
CHEMBL270409
null
null
null
null
Rattus norvegicus
null
null
10,116
Artery
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Decrease in mean arterial blood pressure in response to intravenous administration at 64 uM/kg of the compound.
CHEMBL1121579
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638216
null
null
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Based on the known biological activity of a variety of guanidine-containing agents, several N-substituted 3,4-dihydroquinazolines were synthesized. These compounds can be considered to be rigid analogues of phenylguanidines. In anesthetized rats the compounds decreased blood pressure and were antagonists of the pressor response to norepinephrine.
Grosso JA, Nichols DE, Nichols MB, Yim GK.
10.1021/jm00185a026
null
1261
11
J Med Chem
null
7,452,680
1
Synthesis and adrenergic blocking effects of 2-(alkylamino)-3,4-dihydroquinazolines.
23
1,980
null
35,619
CHEMBL774154
Antagonist effect to pressor response of 0.3 ug/kg of norepinephrine intravenously in rats at the dose 32 uM/kg
F
BAO_0000218
organism-based format
CN(C)C1=Nc2ccccc2CN1
null
CHEMBL1121579
J Med Chem
1,980
CHEMBL270409
null
null
0
http://qudt.org/vocab/unit#Percent
30,838
=
1
0
=
Block
%
10
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Block
%
UO_0000187
10.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CN(C)C1=Nc2ccccc2CN1
RDKit 2D 13 14 0 0 0 0 0 0 0 0999 V2000 -4.1777 -7.0576 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.1789 -7.8843 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4645 -8.2970 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4663 -6.6451 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7515 -7.0539 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.7527 -7.8864 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0363 -8.3014 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.3141 -7.8885 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3129 -7.0560 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.0339 -6.6364 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6013 -8.3027 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.1138 -7.8925 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6036 -9.1272 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 6 2 0 1 2 2 0 5 4 2 0 4 1 1 0 5 10 1 0 6 7 1 0 7 8 2 0 8 9 1 0 9 10 1 0 5 6 1 0 8 11 1 0 11 12 1 0 2 3 1 0 11 13 1 0 M END > <chembl_id> CHEMBL270409 > <chembl_pref_name> None
InChI=1S/C10H13N3/c1-13(2)10-11-7-8-5-3-4-6-9(8)12-10/h3-6H,7H2,1-2H3,(H,11,12)
MNTBAXGKERZVOZ-UHFFFAOYSA-N
1.34
1
C10H13N3
175.24
3
1
13
175.24
-0.21
0
27.63
0.64
Y
0
CHEMBL270409
CHEMBL270409
CHEMBL270409
null
null
null
null
Rattus norvegicus
null
null
10,116
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Antagonist effect to pressor response of 0.3 ug/kg of norepinephrine intravenously in rats at the dose 32 uM/kg
CHEMBL1121579
Non-molecular target assigned
N
null
1
CHEMBL376
null
null
null
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Based on the known biological activity of a variety of guanidine-containing agents, several N-substituted 3,4-dihydroquinazolines were synthesized. These compounds can be considered to be rigid analogues of phenylguanidines. In anesthetized rats the compounds decreased blood pressure and were antagonists of the pressor response to norepinephrine.
Grosso JA, Nichols DE, Nichols MB, Yim GK.
10.1021/jm00185a026
null
1261
11
J Med Chem
null
7,452,680
1
Synthesis and adrenergic blocking effects of 2-(alkylamino)-3,4-dihydroquinazolines.
23
1,980
null
35,620
CHEMBL773605
Lowest active dose which cured rats with Entamoeba histolytica cecal infection was measured
F
BAO_0000218
organism-based format
CN1CCN(c2nc3ccc(N)cc3nc2N2CCN(C)CC2)CC1
null
CHEMBL1121391
J Med Chem
1,980
CHEMBL417733
null
null
0
null
110,548
=
1
0
=
Dose
mg kg-1 day-1
50
CHEMBL612853
Entamoeba histolytica
Entamoeba histolytica
5759
null
Dose
mg kg-1 day-1
UO_0000311
50.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CN1CCN(c2nc3ccc(N)cc3nc2N2CCN(C)CC2)CC1
RDKit 2D 25 28 0 0 0 0 0 0 0 0999 V2000 5.6917 -5.1292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.6917 -4.3000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9792 -5.5417 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.9750 -3.8917 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.4042 -3.8792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.4125 -5.5375 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.2667 -5.1292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2667 -4.3042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.8250 -3.0542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 7.8375 -6.3542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5500 -5.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.3917 -3.0542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4125 -6.3625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1167 -4.2917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1167 -5.1167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5500 -3.8917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8375 -5.1375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1250 -6.7667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.8292 -3.8792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.8375 -5.5292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.1042 -2.6417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1167 -5.5500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.8375 -4.3125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.5542 -6.7667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.5417 -2.6417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 2 0 4 2 2 0 5 2 1 0 6 1 1 0 7 3 1 0 8 7 1 0 9 19 1 0 10 20 1 0 11 7 2 0 12 5 1 0 13 6 1 0 14 5 1 0 15 6 1 0 16 8 2 0 17 11 1 0 18 13 1 0 19 14 1 0 20 15 1 0 21 12 1 0 22 17 1 0 23 17 2 0 24 10 1 0 25 9 1 0 18 10 1 0 4 8 1 0 9 21 1 0 23 16 1 0 M END > <chembl_id> CHEMBL417733 > <chembl_pref_name> None
InChI=1S/C18H27N7/c1-22-5-9-24(10-6-22)17-18(25-11-7-23(2)8-12-25)21-16-13-14(19)3-4-15(16)20-17/h3-4,13H,5-12,19H2,1-2H3
DYJCLTDKKIKWJG-UHFFFAOYSA-N
0.72
2
C18H27N7
341.46
7
1
25
341.46
-0.89
0
64.76
0.81
N
2
CHEMBL417733
CHEMBL417733
CHEMBL417733
null
null
null
null
Entamoeba histolytica
null
null
5,759
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Lowest active dose which cured rats with Entamoeba histolytica cecal infection was measured
CHEMBL1121391
Non-molecular target assigned
N
null
1
CHEMBL612853
null
null
null
Entamoeba histolytica
Entamoeba histolytica
false
ORGANISM
5,759
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of amidines and sulfonamides of 5- and 6-amino-2,3-bis(4-alkyl-1-piperazinyl)quinoxalines was synthesized and tested against cecal and hepatic forms of Entamoeba histolytica infections in rats and hamsters, respectively. Four compounds (5, 6, 8, and 9) were found to have acceptable activity against infections in both species but were too toxic to be considered for use in man.
Fabio PF, Lang SA, Lin YI, Tomcufcik AS.
10.1021/jm00176a017
null
201
2
J Med Chem
null
7,359,534
1
Antiamebic amidines and sulfonamides of 5- and 6-amino-2,3-bis(4-alkyl-1-piperazinyl)quinoxalines.
23
1,980
null
35,622
CHEMBL778496
The percent fall in systolic blood pressure at 1.5 / 4 hr after peroral administration of 40 mg/kg in conscious renal hypertensive rats (RHR).
F
BAO_0000218
organism-based format
Cc1cccc(NC(=O)NC2CCN(CCc3c[nH]c4ccccc34)CC2)c1
null
CHEMBL1121617
J Med Chem
1,980
CHEMBL169389
null
null
0
null
334,455
=
1
0
=
Activity
null
14
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Activity
null
null
14.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
Cc1cccc(NC(=O)NC2CCN(CCc3c[nH]c4ccccc34)CC2)c1
RDKit 2D 28 31 0 0 0 0 0 0 0 0999 V2000 3.4417 -1.6292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.1583 -0.6792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.1833 -0.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.6708 -0.3250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3708 -1.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3292 -1.1542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.0417 -1.6125 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.9708 -1.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.1292 -1.1167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.1542 -2.1542 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.4167 -0.6625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.3542 -2.1250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.7292 -1.1750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2417 -1.6542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2167 -0.6167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5292 -1.1292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.6417 -1.6667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.6167 -0.6292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9500 -2.1042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.2625 -2.6167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0708 -1.7667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.3750 -3.1625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0625 -2.6500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.2708 -1.7667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9750 -3.1500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.8625 -2.6042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3708 -2.2792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9708 -2.2875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 4 1 0 3 11 1 0 4 3 2 0 5 3 1 0 6 18 1 0 7 1 1 0 8 5 2 0 9 1 1 0 10 1 2 0 11 13 1 0 12 7 1 0 13 6 1 0 14 16 1 0 15 16 1 0 16 9 1 0 17 14 1 0 18 15 1 0 19 12 1 0 20 19 2 0 21 5 1 0 22 23 1 0 23 12 2 0 24 8 1 0 25 22 2 0 26 20 1 0 27 21 2 0 28 27 1 0 6 17 1 0 25 20 1 0 8 2 1 0 28 24 2 0 M END > <chembl_id> CHEMBL169389 > <chembl_pref_name> None
InChI=1S/C23H28N4O/c1-17-5-4-6-20(15-17)26-23(28)25-19-10-13-27(14-11-19)12-9-18-16-24-22-8-3-2-7-21(18)22/h2-8,15-16,19,24H,9-14H2,1H3,(H2,25,26,28)
WXBRFAULXRFZPT-UHFFFAOYSA-N
4.3
3
C23H28N4O
376.50
2
3
28
376.5
-1.53
0
60.16
0.62
N
5
CHEMBL169389
CHEMBL169389
CHEMBL169389
null
null
null
null
Rattus norvegicus
null
null
10,116
Artery
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
The percent fall in systolic blood pressure at 1.5 / 4 hr after peroral administration of 40 mg/kg in conscious renal hypertensive rats (RHR).
CHEMBL1121617
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638216
null
DOSE=40.0 mg/kg | ROUTE=None None
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The synthesis of a series of 1-aralkyl-4-ureidopiperidines is reported. These compounds are related to the benzamidopiperidines exemplified by indoramin. Some of the ureidopiperidines are more potent antihypertensive agents than their benzamidopiperidine counterparts. Two examples, 1-(2-thenoyl)-3-[1-[2-(3-indolyl)ethyl]piperid-4-yl]urea and 1-(2-thenoyl)-3-[1-[4-(4-fluorophenyl)-4-oxobutyl]piperid-4-yl]urea (19 and 58), emerged as the most potent antihypertensive agents in this series.
Archibald JL, Beardsley DR, Bisset GM, Fairbrother P, Jackson JL, Opalko A, Ward TJ.
10.1021/jm00182a009
null
857
8
J Med Chem
null
7,401,114
1
Antihypertensive ureidopiperidines.
23
1,980
null
35,623
CHEMBL792281
Starting systolic blood pressure at dose of 50 mg/kg in rat
F
BAO_0000218
organism-based format
O=C(NC(=O)c1cccs1)NC1CCN(CCCC(=O)c2ccc(F)cc2)CC1
null
CHEMBL1121617
J Med Chem
1,980
CHEMBL353005
null
null
0
null
334,496
=
1
0
=
SP
mmHg
179
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
SP
mmHg
UO_0000272
179.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(NC(=O)c1cccs1)NC1CCN(CCCC(=O)c2ccc(F)cc2)CC1
RDKit 2D 29 31 0 0 0 0 0 0 0 0999 V2000 6.2417 -1.5125 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.6417 -1.4542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4875 -2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.0792 -2.1167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.5292 -1.7125 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 3.6042 -0.7167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4000 -0.9000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.6875 -1.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.2917 -1.9375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.9292 -2.1125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.1292 -2.5500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 7.3375 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.0625 -2.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.9417 -2.6042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0917 -1.4917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.5167 -2.1792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.5667 -2.5917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4417 -1.3292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5542 -0.2875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.7917 -0.8375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8417 -1.2625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9542 -0.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4000 -3.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8042 -3.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7625 -2.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -3.7917 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 3.0042 -0.6542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.6500 -1.1375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0500 -1.0750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 1 0 4 3 1 0 5 4 1 0 6 22 1 0 7 2 1 0 8 29 1 0 9 2 2 0 10 8 1 0 11 3 2 0 12 4 2 0 13 5 1 0 14 12 1 0 15 8 2 0 16 10 1 0 17 10 2 0 18 20 1 0 19 20 1 0 20 7 1 0 21 18 1 0 22 19 1 0 23 24 2 0 24 17 1 0 25 16 2 0 26 23 1 0 27 6 1 0 28 27 1 0 29 28 1 0 13 14 2 0 6 21 1 0 23 25 1 0 M END > <chembl_id> CHEMBL353005 > <chembl_pref_name> None
InChI=1S/C21H24FN3O3S/c22-16-7-5-15(6-8-16)18(26)3-1-11-25-12-9-17(10-13-25)23-21(28)24-20(27)19-4-2-14-29-19/h2,4-8,14,17H,1,3,9-13H2,(H2,23,24,27,28)
NSMREXXYHJWAAO-UHFFFAOYSA-N
3.45
2
C21H24FN3O3S
417.51
5
2
29
417.51
-1.99
0
78.51
0.68
N
7
CHEMBL353005
CHEMBL353005
CHEMBL353005
null
null
null
null
Rattus norvegicus
null
null
10,116
Artery
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Starting systolic blood pressure at dose of 50 mg/kg in rat
CHEMBL1121617
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638216
null
DOSE=50.0 mg/kg
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The synthesis of a series of 1-aralkyl-4-ureidopiperidines is reported. These compounds are related to the benzamidopiperidines exemplified by indoramin. Some of the ureidopiperidines are more potent antihypertensive agents than their benzamidopiperidine counterparts. Two examples, 1-(2-thenoyl)-3-[1-[2-(3-indolyl)ethyl]piperid-4-yl]urea and 1-(2-thenoyl)-3-[1-[4-(4-fluorophenyl)-4-oxobutyl]piperid-4-yl]urea (19 and 58), emerged as the most potent antihypertensive agents in this series.
Archibald JL, Beardsley DR, Bisset GM, Fairbrother P, Jackson JL, Opalko A, Ward TJ.
10.1021/jm00182a009
null
857
8
J Med Chem
null
7,401,114
1
Antihypertensive ureidopiperidines.
23
1,980
null
35,624
CHEMBL782993
The percent fall in systolic blood pressure at 1.5 / 4 h after peroral administration of 50 mg/kg in DOCA/saline hypertensive rats at 2 hr
F
BAO_0000218
organism-based format
O=C(NC(=O)c1cccs1)NC1CCN(CCCC(=O)c2ccc(F)cc2)CC1
null
CHEMBL1121617
J Med Chem
1,980
CHEMBL353005
null
null
0
http://qudt.org/vocab/unit#Percent
334,496
=
1
0
=
Fall
%
49
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Fall
%
UO_0000187
49.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(NC(=O)c1cccs1)NC1CCN(CCCC(=O)c2ccc(F)cc2)CC1
RDKit 2D 29 31 0 0 0 0 0 0 0 0999 V2000 6.2417 -1.5125 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.6417 -1.4542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4875 -2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.0792 -2.1167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.5292 -1.7125 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 3.6042 -0.7167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4000 -0.9000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.6875 -1.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.2917 -1.9375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.9292 -2.1125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.1292 -2.5500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 7.3375 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.0625 -2.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.9417 -2.6042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0917 -1.4917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.5167 -2.1792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.5667 -2.5917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4417 -1.3292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5542 -0.2875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.7917 -0.8375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8417 -1.2625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9542 -0.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4000 -3.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8042 -3.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7625 -2.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -3.7917 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 3.0042 -0.6542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.6500 -1.1375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0500 -1.0750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 1 0 4 3 1 0 5 4 1 0 6 22 1 0 7 2 1 0 8 29 1 0 9 2 2 0 10 8 1 0 11 3 2 0 12 4 2 0 13 5 1 0 14 12 1 0 15 8 2 0 16 10 1 0 17 10 2 0 18 20 1 0 19 20 1 0 20 7 1 0 21 18 1 0 22 19 1 0 23 24 2 0 24 17 1 0 25 16 2 0 26 23 1 0 27 6 1 0 28 27 1 0 29 28 1 0 13 14 2 0 6 21 1 0 23 25 1 0 M END > <chembl_id> CHEMBL353005 > <chembl_pref_name> None
InChI=1S/C21H24FN3O3S/c22-16-7-5-15(6-8-16)18(26)3-1-11-25-12-9-17(10-13-25)23-21(28)24-20(27)19-4-2-14-29-19/h2,4-8,14,17H,1,3,9-13H2,(H2,23,24,27,28)
NSMREXXYHJWAAO-UHFFFAOYSA-N
3.45
2
C21H24FN3O3S
417.51
5
2
29
417.51
-1.99
0
78.51
0.68
N
7
CHEMBL353005
CHEMBL353005
CHEMBL353005
null
null
null
null
Rattus norvegicus
null
null
10,116
Artery
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
The percent fall in systolic blood pressure at 1.5 / 4 h after peroral administration of 50 mg/kg in DOCA/saline hypertensive rats at 2 hr
CHEMBL1121617
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638216
null
DOSE=50.0 mg/kg | ROUTE=None None
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The synthesis of a series of 1-aralkyl-4-ureidopiperidines is reported. These compounds are related to the benzamidopiperidines exemplified by indoramin. Some of the ureidopiperidines are more potent antihypertensive agents than their benzamidopiperidine counterparts. Two examples, 1-(2-thenoyl)-3-[1-[2-(3-indolyl)ethyl]piperid-4-yl]urea and 1-(2-thenoyl)-3-[1-[4-(4-fluorophenyl)-4-oxobutyl]piperid-4-yl]urea (19 and 58), emerged as the most potent antihypertensive agents in this series.
Archibald JL, Beardsley DR, Bisset GM, Fairbrother P, Jackson JL, Opalko A, Ward TJ.
10.1021/jm00182a009
null
857
8
J Med Chem
null
7,401,114
1
Antihypertensive ureidopiperidines.
23
1,980
null
35,625
CHEMBL787703
The percent fall in systolic blood pressure at 1.5 / 4 hr after peroral administration of 50 mg/kg in DOCA/saline hypertensive rats at 6 hr
F
BAO_0000218
organism-based format
O=C(NC(=O)c1cccs1)NC1CCN(CCCC(=O)c2ccc(F)cc2)CC1
null
CHEMBL1121617
J Med Chem
1,980
CHEMBL353005
null
null
0
http://qudt.org/vocab/unit#Percent
334,496
=
1
0
=
Fall
%
45
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Fall
%
UO_0000187
45.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(NC(=O)c1cccs1)NC1CCN(CCCC(=O)c2ccc(F)cc2)CC1
RDKit 2D 29 31 0 0 0 0 0 0 0 0999 V2000 6.2417 -1.5125 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.6417 -1.4542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4875 -2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.0792 -2.1167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.5292 -1.7125 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 3.6042 -0.7167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4000 -0.9000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.6875 -1.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.2917 -1.9375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.9292 -2.1125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.1292 -2.5500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 7.3375 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.0625 -2.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.9417 -2.6042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0917 -1.4917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.5167 -2.1792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.5667 -2.5917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4417 -1.3292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5542 -0.2875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.7917 -0.8375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8417 -1.2625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9542 -0.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4000 -3.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8042 -3.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7625 -2.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -3.7917 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 3.0042 -0.6542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.6500 -1.1375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0500 -1.0750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 1 0 4 3 1 0 5 4 1 0 6 22 1 0 7 2 1 0 8 29 1 0 9 2 2 0 10 8 1 0 11 3 2 0 12 4 2 0 13 5 1 0 14 12 1 0 15 8 2 0 16 10 1 0 17 10 2 0 18 20 1 0 19 20 1 0 20 7 1 0 21 18 1 0 22 19 1 0 23 24 2 0 24 17 1 0 25 16 2 0 26 23 1 0 27 6 1 0 28 27 1 0 29 28 1 0 13 14 2 0 6 21 1 0 23 25 1 0 M END > <chembl_id> CHEMBL353005 > <chembl_pref_name> None
InChI=1S/C21H24FN3O3S/c22-16-7-5-15(6-8-16)18(26)3-1-11-25-12-9-17(10-13-25)23-21(28)24-20(27)19-4-2-14-29-19/h2,4-8,14,17H,1,3,9-13H2,(H2,23,24,27,28)
NSMREXXYHJWAAO-UHFFFAOYSA-N
3.45
2
C21H24FN3O3S
417.51
5
2
29
417.51
-1.99
0
78.51
0.68
N
7
CHEMBL353005
CHEMBL353005
CHEMBL353005
null
null
null
null
Rattus norvegicus
null
null
10,116
Artery
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
The percent fall in systolic blood pressure at 1.5 / 4 hr after peroral administration of 50 mg/kg in DOCA/saline hypertensive rats at 6 hr
CHEMBL1121617
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638216
null
DOSE=50.0 mg/kg | ROUTE=None None
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The synthesis of a series of 1-aralkyl-4-ureidopiperidines is reported. These compounds are related to the benzamidopiperidines exemplified by indoramin. Some of the ureidopiperidines are more potent antihypertensive agents than their benzamidopiperidine counterparts. Two examples, 1-(2-thenoyl)-3-[1-[2-(3-indolyl)ethyl]piperid-4-yl]urea and 1-(2-thenoyl)-3-[1-[4-(4-fluorophenyl)-4-oxobutyl]piperid-4-yl]urea (19 and 58), emerged as the most potent antihypertensive agents in this series.
Archibald JL, Beardsley DR, Bisset GM, Fairbrother P, Jackson JL, Opalko A, Ward TJ.
10.1021/jm00182a009
null
857
8
J Med Chem
null
7,401,114
1
Antihypertensive ureidopiperidines.
23
1,980
null
35,626
CHEMBL782991
The percent fall in systolic blood pressure at 1.5 / 4 hr after peroral administration of 50 mg/kg in DOCA/saline hypertensive rats at 24 hr
F
BAO_0000218
organism-based format
O=C(NC(=O)c1cccs1)NC1CCN(CCCC(=O)c2ccc(F)cc2)CC1
null
CHEMBL1121617
J Med Chem
1,980
CHEMBL353005
null
null
0
http://qudt.org/vocab/unit#Percent
334,496
=
1
0
=
Fall
%
21
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Fall
%
UO_0000187
21.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(NC(=O)c1cccs1)NC1CCN(CCCC(=O)c2ccc(F)cc2)CC1
RDKit 2D 29 31 0 0 0 0 0 0 0 0999 V2000 6.2417 -1.5125 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.6417 -1.4542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4875 -2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.0792 -2.1167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.5292 -1.7125 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 3.6042 -0.7167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4000 -0.9000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.6875 -1.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.2917 -1.9375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.9292 -2.1125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.1292 -2.5500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 7.3375 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.0625 -2.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.9417 -2.6042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0917 -1.4917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.5167 -2.1792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.5667 -2.5917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4417 -1.3292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5542 -0.2875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.7917 -0.8375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8417 -1.2625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9542 -0.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4000 -3.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8042 -3.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7625 -2.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -3.7917 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 3.0042 -0.6542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.6500 -1.1375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0500 -1.0750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 1 0 4 3 1 0 5 4 1 0 6 22 1 0 7 2 1 0 8 29 1 0 9 2 2 0 10 8 1 0 11 3 2 0 12 4 2 0 13 5 1 0 14 12 1 0 15 8 2 0 16 10 1 0 17 10 2 0 18 20 1 0 19 20 1 0 20 7 1 0 21 18 1 0 22 19 1 0 23 24 2 0 24 17 1 0 25 16 2 0 26 23 1 0 27 6 1 0 28 27 1 0 29 28 1 0 13 14 2 0 6 21 1 0 23 25 1 0 M END > <chembl_id> CHEMBL353005 > <chembl_pref_name> None
InChI=1S/C21H24FN3O3S/c22-16-7-5-15(6-8-16)18(26)3-1-11-25-12-9-17(10-13-25)23-21(28)24-20(27)19-4-2-14-29-19/h2,4-8,14,17H,1,3,9-13H2,(H2,23,24,27,28)
NSMREXXYHJWAAO-UHFFFAOYSA-N
3.45
2
C21H24FN3O3S
417.51
5
2
29
417.51
-1.99
0
78.51
0.68
N
7
CHEMBL353005
CHEMBL353005
CHEMBL353005
null
null
null
null
Rattus norvegicus
null
null
10,116
Artery
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
The percent fall in systolic blood pressure at 1.5 / 4 hr after peroral administration of 50 mg/kg in DOCA/saline hypertensive rats at 24 hr
CHEMBL1121617
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638216
null
DOSE=50.0 mg/kg | ROUTE=None None
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The synthesis of a series of 1-aralkyl-4-ureidopiperidines is reported. These compounds are related to the benzamidopiperidines exemplified by indoramin. Some of the ureidopiperidines are more potent antihypertensive agents than their benzamidopiperidine counterparts. Two examples, 1-(2-thenoyl)-3-[1-[2-(3-indolyl)ethyl]piperid-4-yl]urea and 1-(2-thenoyl)-3-[1-[4-(4-fluorophenyl)-4-oxobutyl]piperid-4-yl]urea (19 and 58), emerged as the most potent antihypertensive agents in this series.
Archibald JL, Beardsley DR, Bisset GM, Fairbrother P, Jackson JL, Opalko A, Ward TJ.
10.1021/jm00182a009
null
857
8
J Med Chem
null
7,401,114
1
Antihypertensive ureidopiperidines.
23
1,980
null
35,627
CHEMBL792280
Starting systolic blood pressure at dose of 25 mg/kg
F
BAO_0000218
organism-based format
O=C(NC(=O)c1cccs1)NC1CCN(CCCC(=O)c2ccc(F)cc2)CC1
null
CHEMBL1121617
J Med Chem
1,980
CHEMBL353005
null
null
0
null
334,496
=
1
0
=
SP
mmHg
174
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
SP
mmHg
UO_0000272
174.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(NC(=O)c1cccs1)NC1CCN(CCCC(=O)c2ccc(F)cc2)CC1
RDKit 2D 29 31 0 0 0 0 0 0 0 0999 V2000 6.2417 -1.5125 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.6417 -1.4542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4875 -2.0625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.0792 -2.1167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.5292 -1.7125 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 3.6042 -0.7167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4000 -0.9000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.6875 -1.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.2917 -1.9375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.9292 -2.1125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.1292 -2.5500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 7.3375 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.0625 -2.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.9417 -2.6042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0917 -1.4917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.5167 -2.1792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.5667 -2.5917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4417 -1.3292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5542 -0.2875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.7917 -0.8375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8417 -1.2625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9542 -0.2292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4000 -3.2167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8042 -3.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.7625 -2.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -3.7917 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 3.0042 -0.6542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.6500 -1.1375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0500 -1.0750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 1 0 4 3 1 0 5 4 1 0 6 22 1 0 7 2 1 0 8 29 1 0 9 2 2 0 10 8 1 0 11 3 2 0 12 4 2 0 13 5 1 0 14 12 1 0 15 8 2 0 16 10 1 0 17 10 2 0 18 20 1 0 19 20 1 0 20 7 1 0 21 18 1 0 22 19 1 0 23 24 2 0 24 17 1 0 25 16 2 0 26 23 1 0 27 6 1 0 28 27 1 0 29 28 1 0 13 14 2 0 6 21 1 0 23 25 1 0 M END > <chembl_id> CHEMBL353005 > <chembl_pref_name> None
InChI=1S/C21H24FN3O3S/c22-16-7-5-15(6-8-16)18(26)3-1-11-25-12-9-17(10-13-25)23-21(28)24-20(27)19-4-2-14-29-19/h2,4-8,14,17H,1,3,9-13H2,(H2,23,24,27,28)
NSMREXXYHJWAAO-UHFFFAOYSA-N
3.45
2
C21H24FN3O3S
417.51
5
2
29
417.51
-1.99
0
78.51
0.68
N
7
CHEMBL353005
CHEMBL353005
CHEMBL353005
null
null
null
null
Rattus norvegicus
null
null
10,116
Artery
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Starting systolic blood pressure at dose of 25 mg/kg
CHEMBL1121617
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638216
null
DOSE=25.0 mg/kg
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The synthesis of a series of 1-aralkyl-4-ureidopiperidines is reported. These compounds are related to the benzamidopiperidines exemplified by indoramin. Some of the ureidopiperidines are more potent antihypertensive agents than their benzamidopiperidine counterparts. Two examples, 1-(2-thenoyl)-3-[1-[2-(3-indolyl)ethyl]piperid-4-yl]urea and 1-(2-thenoyl)-3-[1-[4-(4-fluorophenyl)-4-oxobutyl]piperid-4-yl]urea (19 and 58), emerged as the most potent antihypertensive agents in this series.
Archibald JL, Beardsley DR, Bisset GM, Fairbrother P, Jackson JL, Opalko A, Ward TJ.
10.1021/jm00182a009
null
857
8
J Med Chem
null
7,401,114
1
Antihypertensive ureidopiperidines.
23
1,980
null
33,154
CHEMBL663829
Saluretic property was estimated by the excretion of Na+ in dog administered intravenously; microequiv of Na+/min at 5 mg/kg iv stat, 0-99
A
BAO_0000218
organism-based format
CN(C)Cc1cc(C(C)(C)C)cc(I)c1O
null
CHEMBL1122081
J Med Chem
1,982
CHEMBL163066
null
null
0
null
321,226
=
1
0
=
Saluretic potency
u equiv min-1
0
CHEMBL373
Canis lupus familiaris
Canis familiaris
9615
null
Saluretic potency
u equiv min-1
null
0.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CN(C)Cc1cc(C(C)(C)C)cc(I)c1O
RDKit 2D 16 16 0 0 0 0 0 0 0 0999 V2000 3.5542 -1.3375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0292 -2.2417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0292 -1.0375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5167 -1.3375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5542 -1.9417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5167 -1.9417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0667 -1.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0292 -2.8417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0667 -0.4292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.9917 -1.0417 0.0000 I 0 0 0 0 0 0 0 0 0 0 0 0 3.0292 -0.4375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.5542 -3.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.0292 -3.4417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5167 -3.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.5792 -0.1250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5417 -0.1375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 5 2 0 3 1 2 0 4 3 1 0 5 1 1 0 6 2 1 0 7 1 1 0 8 2 1 0 9 7 1 0 10 4 1 0 11 3 1 0 12 8 1 0 13 8 1 0 14 8 1 0 15 9 1 0 16 9 1 0 4 6 2 0 M END > <chembl_id> CHEMBL163066 > <chembl_pref_name> None
InChI=1S/C13H20INO/c1-13(2,3)10-6-9(8-15(4)5)12(16)11(14)7-10/h6-7,16H,8H2,1-5H3
XCTGWUBSZMSEJY-UHFFFAOYSA-N
3.36
1
C13H20INO
333.21
2
1
16
333.21
-0.75
0
23.47
0.84
N
2
CHEMBL163066
CHEMBL163066
CHEMBL163066
null
null
null
null
Canis lupus familiaris
null
null
9,615
null
A
ADME
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Saluretic property was estimated by the excretion of Na+ in dog administered intravenously; microequiv of Na+/min at 5 mg/kg iv stat, 0-99
CHEMBL1122081
Non-molecular target assigned
N
null
1
CHEMBL373
null
null
DOSE=5.0 mg/kg | ROUTE=None None
Canis lupus familiaris
Canis familiaris
false
ORGANISM
9,615
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of oxygen and/or nitrogen substituted 2-(aminomethyl)phenols was synthesized and tested orally in rats for saluretic and diuretic effects. Intravenous dog data are included as supplementary material to demonstrate diuretic responses, or lack thereof, in a second species. In general, substitution on nitrogen with groups other than lower alkyl or substitution on nitrogen and/or oxygen with groups resistant to hydrolysis substantially diminished or ablated saluretic effects.
Stokker GE, Deana AA, deSolms SJ, Schultz EM, Smith RL, Cragoe EJ, Baer JE, Russo HF, Watson LS.
10.1021/jm00348a024
null
735
6
J Med Chem
null
7,097,728
1
2-(Aminomethyl)phenols, a new class of saluretic agents. 4. Effects of oxygen and/or nitrogen substitution.
25
1,982
null
33,156
CHEMBL788494
Percent inhibition of rat passive cutaneous anaphylaxis model after intravenous administration of the 0.5 mg/kg
F
BAO_0000218
organism-based format
O=c1c2ccccc2nc2ccc(-c3nn[nH]n3)cn12
null
CHEMBL1122082
J Med Chem
1,982
CHEMBL163354
null
null
0
http://qudt.org/vocab/unit#Percent
321,565
=
1
1
=
Inhibition
%
68
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Inhibition
%
UO_0000187
68.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=c1c2ccccc2nc2ccc(-c3nn[nH]n3)cn12
RDKit 2D 20 23 0 0 0 0 0 0 0 0999 V2000 1.2667 -0.7500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.7417 -1.0542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2667 -0.1542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3042 -0.7417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7792 -1.0500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.7417 0.1458 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.8250 -1.0417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.2250 -0.7542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3625 -0.7792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.7750 -1.2167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.9125 -1.6417 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 3.5000 -1.7417 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.2250 -0.1542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3042 -0.1542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7792 0.1458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.7375 -1.6542 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.2958 -1.0542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.2958 0.1458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.8208 -0.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.8208 -0.1542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 1 0 4 5 2 0 5 1 1 0 6 3 2 0 7 4 1 0 8 2 1 0 9 7 1 0 10 9 2 0 11 7 2 0 12 11 1 0 13 6 1 0 14 4 1 0 15 3 1 0 16 2 2 0 17 8 2 0 18 13 2 0 19 17 1 0 20 18 1 0 15 14 2 0 13 8 1 0 12 10 1 0 19 20 2 0 M END > <chembl_id> CHEMBL163354 > <chembl_pref_name> None
InChI=1S/C13H8N6O/c20-13-9-3-1-2-4-10(9)14-11-6-5-8(7-19(11)13)12-15-17-18-16-12/h1-7H,(H,15,16,17,18)
VDTILFANVMDZEW-UHFFFAOYSA-N
1.03
4
C13H8N6O
264.25
6
1
20
264.25
-1.78
0
88.83
0.52
N
1
CHEMBL163354
CHEMBL163354
CHEMBL163354
null
null
null
null
Rattus norvegicus
null
null
10,116
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Percent inhibition of rat passive cutaneous anaphylaxis model after intravenous administration of the 0.5 mg/kg
CHEMBL1122082
Non-molecular target assigned
N
null
1
CHEMBL376
null
null
DOSE=0.5 mg/kg | ROUTE=None None
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Several known antiallergic agents, including cromolyn sodium and a series of pyrido[2,1-b]quinazolines, inhibit human alkaline phosphatase (ALP), a membranal enzyme associated with calcium uptake in certain tissues. A comparison of ALP and rat passive cutaneous anaphylaxis (PCA) inhibition indicates that PCA inhibition may be associated with drug-ALP interaction, since ALP inhibition potency parallels PCA inhibitory activity. The unpredictability of the PCA test toward clinical efficacy could in part be related to the uncompetitive nature of these inhibitors. The results also suggest that alkaline phosphatase may be a component of membranal calcium channels.
Schwender CF, Sunday BR, Decker VL.
10.1021/jm00348a025
null
742
6
J Med Chem
null
6,808,133
1
Alkaline phosphatase inhibition by a series of pyrido[2,1-b]quinazolines: A possible relationship with cromolyn-like antiallergy activity.
25
1,982
null
33,159
CHEMBL634600
Solubility ratio ([HbS+drug (5 mM)]/[HbS-drug])
A
BAO_0000019
assay format
O=C(O)C(CCOc1ccc(Br)cc1)C(=O)O
null
CHEMBL1122711
J Med Chem
1,984
CHEMBL368988
null
null
0
null
347,488
=
1
0
=
Solubility ratio
null
1.057
CHEMBL612558
null
ADMET
null
null
Solubility ratio
null
null
1.057
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)C(CCOc1ccc(Br)cc1)C(=O)O
RDKit 2D 17 17 0 0 0 0 0 0 0 0999 V2000 3.3792 -0.7167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 -0.7167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.9625 -0.0042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -0.0167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.6292 -1.4292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.3750 0.7125 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.6167 0.0083 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.7458 -2.1792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9042 -2.1667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.9750 -1.4417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5708 -2.1792 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 -0.3333 -1.4625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3250 -2.8917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.4875 -1.4542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5042 -2.8875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7375 -2.1667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.1500 -1.4500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 1 0 4 3 2 0 5 2 2 0 6 3 1 0 7 2 1 0 8 13 1 0 9 16 1 0 10 1 1 0 11 8 1 0 12 14 1 0 13 15 2 0 14 9 2 0 15 9 1 0 16 17 1 0 17 10 1 0 8 12 2 0 M END > <chembl_id> CHEMBL368988 > <chembl_pref_name> None
InChI=1S/C11H11BrO5/c12-7-1-3-8(4-2-7)17-6-5-9(10(13)14)11(15)16/h1-4,9H,5-6H2,(H,13,14)(H,15,16)
WKNLVAFBHNNWQX-UHFFFAOYSA-N
2
1
C11H11BrO5
303.11
3
2
17
303.11
-0.24
0
83.83
0.79
N
6
CHEMBL368988
CHEMBL368988
CHEMBL368988
null
null
null
null
Homo sapiens
null
null
9,606
null
A
ADME
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Solubility ratio ([HbS+drug (5 mM)]/[HbS-drug])
CHEMBL1122711
Default value - Target has yet to be curated
U
null
1
CHEMBL612558
null
null
null
null
ADMET
false
ADMET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
In this paper we further establish the activity of two classes of small molecules, benzyloxy and phenoxy acids, as potent inhibitors of hemoglobin S (HbS) gelation. Structural modifications with a large number of each class confirm our earlier work that the highest activity is observed with compounds that contain dihalogenated aromatic rings with attached polar side chains. We have also found a halogenated aromatic malonic acid derivative to be quite active. Compounds reported in this paper are compared with other antigelling agents studied in our laboratory. Comments are made concerning the antigelling activity and binding sites of four derivatives and their effect on the allosteric mechanism of hemoglobin (Hb) function.
Abraham DJ, Kennedy PE, Mehanna AS, Patwa DC, Williams FL.
10.1021/jm00374a006
null
967
8
J Med Chem
null
6,747,995
1
Design, synthesis, and testing of potential antisickling agents. 4. Structure-activity relationships of benzyloxy and phenoxy acids.
27
1,984
null
33,160
CHEMBL633104
Solubility ratio ([HbS+drug (10 mM)]/[HbS-drug])
A
BAO_0000019
assay format
O=C(O)C(CCOc1ccc(Br)cc1)C(=O)O
null
CHEMBL1122711
J Med Chem
1,984
CHEMBL368988
null
null
0
null
347,488
=
1
0
=
Solubility ratio
null
1.134
CHEMBL612558
null
ADMET
null
null
Solubility ratio
null
null
1.134
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)C(CCOc1ccc(Br)cc1)C(=O)O
RDKit 2D 17 17 0 0 0 0 0 0 0 0999 V2000 3.3792 -0.7167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 -0.7167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.9625 -0.0042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -0.0167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.6292 -1.4292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.3750 0.7125 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.6167 0.0083 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.7458 -2.1792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9042 -2.1667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.9750 -1.4417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5708 -2.1792 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 -0.3333 -1.4625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3250 -2.8917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.4875 -1.4542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5042 -2.8875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7375 -2.1667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.1500 -1.4500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 1 0 4 3 2 0 5 2 2 0 6 3 1 0 7 2 1 0 8 13 1 0 9 16 1 0 10 1 1 0 11 8 1 0 12 14 1 0 13 15 2 0 14 9 2 0 15 9 1 0 16 17 1 0 17 10 1 0 8 12 2 0 M END > <chembl_id> CHEMBL368988 > <chembl_pref_name> None
InChI=1S/C11H11BrO5/c12-7-1-3-8(4-2-7)17-6-5-9(10(13)14)11(15)16/h1-4,9H,5-6H2,(H,13,14)(H,15,16)
WKNLVAFBHNNWQX-UHFFFAOYSA-N
2
1
C11H11BrO5
303.11
3
2
17
303.11
-0.24
0
83.83
0.79
N
6
CHEMBL368988
CHEMBL368988
CHEMBL368988
null
null
null
null
Homo sapiens
null
null
9,606
null
A
ADME
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Solubility ratio ([HbS+drug (10 mM)]/[HbS-drug])
CHEMBL1122711
Default value - Target has yet to be curated
U
null
1
CHEMBL612558
null
null
null
null
ADMET
false
ADMET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
In this paper we further establish the activity of two classes of small molecules, benzyloxy and phenoxy acids, as potent inhibitors of hemoglobin S (HbS) gelation. Structural modifications with a large number of each class confirm our earlier work that the highest activity is observed with compounds that contain dihalogenated aromatic rings with attached polar side chains. We have also found a halogenated aromatic malonic acid derivative to be quite active. Compounds reported in this paper are compared with other antigelling agents studied in our laboratory. Comments are made concerning the antigelling activity and binding sites of four derivatives and their effect on the allosteric mechanism of hemoglobin (Hb) function.
Abraham DJ, Kennedy PE, Mehanna AS, Patwa DC, Williams FL.
10.1021/jm00374a006
null
967
8
J Med Chem
null
6,747,995
1
Design, synthesis, and testing of potential antisickling agents. 4. Structure-activity relationships of benzyloxy and phenoxy acids.
27
1,984
null
33,161
CHEMBL633105
Solubility ratio ([HbS+drug (20 mM)]/[HbS-drug]
A
BAO_0000019
assay format
O=C(O)C(CCOc1ccc(Br)cc1)C(=O)O
null
CHEMBL1122711
J Med Chem
1,984
CHEMBL368988
null
null
0
null
347,488
=
1
0
=
Solubility ratio
null
1.323
CHEMBL612558
null
ADMET
null
null
Solubility ratio
null
null
1.323
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)C(CCOc1ccc(Br)cc1)C(=O)O
RDKit 2D 17 17 0 0 0 0 0 0 0 0999 V2000 3.3792 -0.7167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 -0.7167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.9625 -0.0042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -0.0167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.6292 -1.4292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.3750 0.7125 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.6167 0.0083 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.7458 -2.1792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9042 -2.1667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.9750 -1.4417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5708 -2.1792 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 -0.3333 -1.4625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3250 -2.8917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.4875 -1.4542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5042 -2.8875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7375 -2.1667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.1500 -1.4500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 1 0 4 3 2 0 5 2 2 0 6 3 1 0 7 2 1 0 8 13 1 0 9 16 1 0 10 1 1 0 11 8 1 0 12 14 1 0 13 15 2 0 14 9 2 0 15 9 1 0 16 17 1 0 17 10 1 0 8 12 2 0 M END > <chembl_id> CHEMBL368988 > <chembl_pref_name> None
InChI=1S/C11H11BrO5/c12-7-1-3-8(4-2-7)17-6-5-9(10(13)14)11(15)16/h1-4,9H,5-6H2,(H,13,14)(H,15,16)
WKNLVAFBHNNWQX-UHFFFAOYSA-N
2
1
C11H11BrO5
303.11
3
2
17
303.11
-0.24
0
83.83
0.79
N
6
CHEMBL368988
CHEMBL368988
CHEMBL368988
null
null
null
null
Homo sapiens
null
null
9,606
null
A
ADME
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Solubility ratio ([HbS+drug (20 mM)]/[HbS-drug]
CHEMBL1122711
Default value - Target has yet to be curated
U
null
1
CHEMBL612558
null
null
null
null
ADMET
false
ADMET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
In this paper we further establish the activity of two classes of small molecules, benzyloxy and phenoxy acids, as potent inhibitors of hemoglobin S (HbS) gelation. Structural modifications with a large number of each class confirm our earlier work that the highest activity is observed with compounds that contain dihalogenated aromatic rings with attached polar side chains. We have also found a halogenated aromatic malonic acid derivative to be quite active. Compounds reported in this paper are compared with other antigelling agents studied in our laboratory. Comments are made concerning the antigelling activity and binding sites of four derivatives and their effect on the allosteric mechanism of hemoglobin (Hb) function.
Abraham DJ, Kennedy PE, Mehanna AS, Patwa DC, Williams FL.
10.1021/jm00374a006
null
967
8
J Med Chem
null
6,747,995
1
Design, synthesis, and testing of potential antisickling agents. 4. Structure-activity relationships of benzyloxy and phenoxy acids.
27
1,984
null
33,162
CHEMBL634599
Solubility ratio ([HbS+drug (40 mM)]/[HbS-drug])
A
BAO_0000019
assay format
O=C(O)C(CCOc1ccc(Br)cc1)C(=O)O
null
CHEMBL1122711
J Med Chem
1,984
CHEMBL368988
null
null
0
null
347,488
=
1
0
=
Solubility ratio
null
1.36
CHEMBL612558
null
ADMET
null
null
Solubility ratio
null
null
1.36
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)C(CCOc1ccc(Br)cc1)C(=O)O
RDKit 2D 17 17 0 0 0 0 0 0 0 0999 V2000 3.3792 -0.7167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 -0.7167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.9625 -0.0042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.1417 -0.0167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.6292 -1.4292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.3750 0.7125 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.6167 0.0083 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.7458 -2.1792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9042 -2.1667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.9750 -1.4417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5708 -2.1792 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 -0.3333 -1.4625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3250 -2.8917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.4875 -1.4542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.5042 -2.8875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7375 -2.1667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.1500 -1.4500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 1 1 0 4 3 2 0 5 2 2 0 6 3 1 0 7 2 1 0 8 13 1 0 9 16 1 0 10 1 1 0 11 8 1 0 12 14 1 0 13 15 2 0 14 9 2 0 15 9 1 0 16 17 1 0 17 10 1 0 8 12 2 0 M END > <chembl_id> CHEMBL368988 > <chembl_pref_name> None
InChI=1S/C11H11BrO5/c12-7-1-3-8(4-2-7)17-6-5-9(10(13)14)11(15)16/h1-4,9H,5-6H2,(H,13,14)(H,15,16)
WKNLVAFBHNNWQX-UHFFFAOYSA-N
2
1
C11H11BrO5
303.11
3
2
17
303.11
-0.24
0
83.83
0.79
N
6
CHEMBL368988
CHEMBL368988
CHEMBL368988
null
null
null
null
Homo sapiens
null
null
9,606
null
A
ADME
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Solubility ratio ([HbS+drug (40 mM)]/[HbS-drug])
CHEMBL1122711
Default value - Target has yet to be curated
U
null
1
CHEMBL612558
null
null
null
null
ADMET
false
ADMET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
In this paper we further establish the activity of two classes of small molecules, benzyloxy and phenoxy acids, as potent inhibitors of hemoglobin S (HbS) gelation. Structural modifications with a large number of each class confirm our earlier work that the highest activity is observed with compounds that contain dihalogenated aromatic rings with attached polar side chains. We have also found a halogenated aromatic malonic acid derivative to be quite active. Compounds reported in this paper are compared with other antigelling agents studied in our laboratory. Comments are made concerning the antigelling activity and binding sites of four derivatives and their effect on the allosteric mechanism of hemoglobin (Hb) function.
Abraham DJ, Kennedy PE, Mehanna AS, Patwa DC, Williams FL.
10.1021/jm00374a006
null
967
8
J Med Chem
null
6,747,995
1
Design, synthesis, and testing of potential antisickling agents. 4. Structure-activity relationships of benzyloxy and phenoxy acids.
27
1,984
null
33,165
CHEMBL634600
Solubility ratio ([HbS+drug (5 mM)]/[HbS-drug])
A
BAO_0000019
assay format
O=C(O)COCc1ccc(Br)cc1
null
CHEMBL1122711
J Med Chem
1,984
CHEMBL9256
null
null
0
null
347,497
=
1
0
=
Solubility ratio
null
1.059
CHEMBL612558
null
ADMET
null
null
Solubility ratio
null
null
1.059
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)COCc1ccc(Br)cc1
RDKit 2D 13 13 0 0 0 0 0 0 0 0999 V2000 6.1792 -1.4125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.8167 -0.9292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.2500 -1.5167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3542 -2.0292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 6.7792 -1.3375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.4500 -1.5167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4625 -1.5292 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 3.5542 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5417 -2.0375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1500 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1500 -2.0375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.9417 -1.9625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0500 -1.5125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 2 0 3 9 1 0 4 12 1 0 5 1 1 0 6 13 1 0 7 3 1 0 8 10 1 0 9 11 2 0 10 6 2 0 11 6 1 0 12 1 1 0 13 4 1 0 3 8 2 0 M END > <chembl_id> CHEMBL9256 > <chembl_pref_name> None
InChI=1S/C9H9BrO3/c10-8-3-1-7(2-4-8)5-13-6-9(11)12/h1-4H,5-6H2,(H,11,12)
ZIEXYIQTFZVRBI-UHFFFAOYSA-N
2.05
1
C9H9BrO3
245.07
2
1
13
245.07
-0.62
0
46.53
0.88
N
4
CHEMBL9256
CHEMBL9256
CHEMBL9256
null
null
null
null
Homo sapiens
null
null
9,606
null
A
ADME
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Solubility ratio ([HbS+drug (5 mM)]/[HbS-drug])
CHEMBL1122711
Default value - Target has yet to be curated
U
null
1
CHEMBL612558
null
null
null
null
ADMET
false
ADMET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
In this paper we further establish the activity of two classes of small molecules, benzyloxy and phenoxy acids, as potent inhibitors of hemoglobin S (HbS) gelation. Structural modifications with a large number of each class confirm our earlier work that the highest activity is observed with compounds that contain dihalogenated aromatic rings with attached polar side chains. We have also found a halogenated aromatic malonic acid derivative to be quite active. Compounds reported in this paper are compared with other antigelling agents studied in our laboratory. Comments are made concerning the antigelling activity and binding sites of four derivatives and their effect on the allosteric mechanism of hemoglobin (Hb) function.
Abraham DJ, Kennedy PE, Mehanna AS, Patwa DC, Williams FL.
10.1021/jm00374a006
null
967
8
J Med Chem
null
6,747,995
1
Design, synthesis, and testing of potential antisickling agents. 4. Structure-activity relationships of benzyloxy and phenoxy acids.
27
1,984
null
33,166
CHEMBL633104
Solubility ratio ([HbS+drug (10 mM)]/[HbS-drug])
A
BAO_0000019
assay format
O=C(O)COCc1ccc(Br)cc1
null
CHEMBL1122711
J Med Chem
1,984
CHEMBL9256
null
null
0
null
347,497
=
1
0
=
Solubility ratio
null
1.118
CHEMBL612558
null
ADMET
null
null
Solubility ratio
null
null
1.118
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)COCc1ccc(Br)cc1
RDKit 2D 13 13 0 0 0 0 0 0 0 0999 V2000 6.1792 -1.4125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.8167 -0.9292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.2500 -1.5167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3542 -2.0292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 6.7792 -1.3375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.4500 -1.5167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4625 -1.5292 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 3.5542 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5417 -2.0375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1500 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1500 -2.0375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.9417 -1.9625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0500 -1.5125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 2 0 3 9 1 0 4 12 1 0 5 1 1 0 6 13 1 0 7 3 1 0 8 10 1 0 9 11 2 0 10 6 2 0 11 6 1 0 12 1 1 0 13 4 1 0 3 8 2 0 M END > <chembl_id> CHEMBL9256 > <chembl_pref_name> None
InChI=1S/C9H9BrO3/c10-8-3-1-7(2-4-8)5-13-6-9(11)12/h1-4H,5-6H2,(H,11,12)
ZIEXYIQTFZVRBI-UHFFFAOYSA-N
2.05
1
C9H9BrO3
245.07
2
1
13
245.07
-0.62
0
46.53
0.88
N
4
CHEMBL9256
CHEMBL9256
CHEMBL9256
null
null
null
null
Homo sapiens
null
null
9,606
null
A
ADME
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Solubility ratio ([HbS+drug (10 mM)]/[HbS-drug])
CHEMBL1122711
Default value - Target has yet to be curated
U
null
1
CHEMBL612558
null
null
null
null
ADMET
false
ADMET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
In this paper we further establish the activity of two classes of small molecules, benzyloxy and phenoxy acids, as potent inhibitors of hemoglobin S (HbS) gelation. Structural modifications with a large number of each class confirm our earlier work that the highest activity is observed with compounds that contain dihalogenated aromatic rings with attached polar side chains. We have also found a halogenated aromatic malonic acid derivative to be quite active. Compounds reported in this paper are compared with other antigelling agents studied in our laboratory. Comments are made concerning the antigelling activity and binding sites of four derivatives and their effect on the allosteric mechanism of hemoglobin (Hb) function.
Abraham DJ, Kennedy PE, Mehanna AS, Patwa DC, Williams FL.
10.1021/jm00374a006
null
967
8
J Med Chem
null
6,747,995
1
Design, synthesis, and testing of potential antisickling agents. 4. Structure-activity relationships of benzyloxy and phenoxy acids.
27
1,984
null
33,167
CHEMBL633105
Solubility ratio ([HbS+drug (20 mM)]/[HbS-drug]
A
BAO_0000019
assay format
O=C(O)COCc1ccc(Br)cc1
null
CHEMBL1122711
J Med Chem
1,984
CHEMBL9256
null
null
0
null
347,497
=
1
0
=
Solubility ratio
null
1.233
CHEMBL612558
null
ADMET
null
null
Solubility ratio
null
null
1.233
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)COCc1ccc(Br)cc1
RDKit 2D 13 13 0 0 0 0 0 0 0 0999 V2000 6.1792 -1.4125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.8167 -0.9292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.2500 -1.5167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3542 -2.0292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 6.7792 -1.3375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.4500 -1.5167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4625 -1.5292 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 3.5542 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5417 -2.0375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1500 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1500 -2.0375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.9417 -1.9625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0500 -1.5125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 2 0 3 9 1 0 4 12 1 0 5 1 1 0 6 13 1 0 7 3 1 0 8 10 1 0 9 11 2 0 10 6 2 0 11 6 1 0 12 1 1 0 13 4 1 0 3 8 2 0 M END > <chembl_id> CHEMBL9256 > <chembl_pref_name> None
InChI=1S/C9H9BrO3/c10-8-3-1-7(2-4-8)5-13-6-9(11)12/h1-4H,5-6H2,(H,11,12)
ZIEXYIQTFZVRBI-UHFFFAOYSA-N
2.05
1
C9H9BrO3
245.07
2
1
13
245.07
-0.62
0
46.53
0.88
N
4
CHEMBL9256
CHEMBL9256
CHEMBL9256
null
null
null
null
Homo sapiens
null
null
9,606
null
A
ADME
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Solubility ratio ([HbS+drug (20 mM)]/[HbS-drug]
CHEMBL1122711
Default value - Target has yet to be curated
U
null
1
CHEMBL612558
null
null
null
null
ADMET
false
ADMET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
In this paper we further establish the activity of two classes of small molecules, benzyloxy and phenoxy acids, as potent inhibitors of hemoglobin S (HbS) gelation. Structural modifications with a large number of each class confirm our earlier work that the highest activity is observed with compounds that contain dihalogenated aromatic rings with attached polar side chains. We have also found a halogenated aromatic malonic acid derivative to be quite active. Compounds reported in this paper are compared with other antigelling agents studied in our laboratory. Comments are made concerning the antigelling activity and binding sites of four derivatives and their effect on the allosteric mechanism of hemoglobin (Hb) function.
Abraham DJ, Kennedy PE, Mehanna AS, Patwa DC, Williams FL.
10.1021/jm00374a006
null
967
8
J Med Chem
null
6,747,995
1
Design, synthesis, and testing of potential antisickling agents. 4. Structure-activity relationships of benzyloxy and phenoxy acids.
27
1,984
null
33,168
CHEMBL634599
Solubility ratio ([HbS+drug (40 mM)]/[HbS-drug])
A
BAO_0000019
assay format
O=C(O)COCc1ccc(Br)cc1
null
CHEMBL1122711
J Med Chem
1,984
CHEMBL9256
null
null
0
null
347,497
=
1
0
=
Solubility ratio
null
1.398
CHEMBL612558
null
ADMET
null
null
Solubility ratio
null
null
1.398
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
O=C(O)COCc1ccc(Br)cc1
RDKit 2D 13 13 0 0 0 0 0 0 0 0999 V2000 6.1792 -1.4125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.8167 -0.9292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.2500 -1.5167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.3542 -2.0292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 6.7792 -1.3375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.4500 -1.5167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4625 -1.5292 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 3.5542 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5417 -2.0375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1500 -1.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1500 -2.0375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.9417 -1.9625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.0500 -1.5125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 2 0 3 9 1 0 4 12 1 0 5 1 1 0 6 13 1 0 7 3 1 0 8 10 1 0 9 11 2 0 10 6 2 0 11 6 1 0 12 1 1 0 13 4 1 0 3 8 2 0 M END > <chembl_id> CHEMBL9256 > <chembl_pref_name> None
InChI=1S/C9H9BrO3/c10-8-3-1-7(2-4-8)5-13-6-9(11)12/h1-4H,5-6H2,(H,11,12)
ZIEXYIQTFZVRBI-UHFFFAOYSA-N
2.05
1
C9H9BrO3
245.07
2
1
13
245.07
-0.62
0
46.53
0.88
N
4
CHEMBL9256
CHEMBL9256
CHEMBL9256
null
null
null
null
Homo sapiens
null
null
9,606
null
A
ADME
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Solubility ratio ([HbS+drug (40 mM)]/[HbS-drug])
CHEMBL1122711
Default value - Target has yet to be curated
U
null
1
CHEMBL612558
null
null
null
null
ADMET
false
ADMET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
In this paper we further establish the activity of two classes of small molecules, benzyloxy and phenoxy acids, as potent inhibitors of hemoglobin S (HbS) gelation. Structural modifications with a large number of each class confirm our earlier work that the highest activity is observed with compounds that contain dihalogenated aromatic rings with attached polar side chains. We have also found a halogenated aromatic malonic acid derivative to be quite active. Compounds reported in this paper are compared with other antigelling agents studied in our laboratory. Comments are made concerning the antigelling activity and binding sites of four derivatives and their effect on the allosteric mechanism of hemoglobin (Hb) function.
Abraham DJ, Kennedy PE, Mehanna AS, Patwa DC, Williams FL.
10.1021/jm00374a006
null
967
8
J Med Chem
null
6,747,995
1
Design, synthesis, and testing of potential antisickling agents. 4. Structure-activity relationships of benzyloxy and phenoxy acids.
27
1,984
null
33,171
CHEMBL634600
Solubility ratio ([HbS+drug (5 mM)]/[HbS-drug])
A
BAO_0000019
assay format
COc1cc(OCC(=O)O)cc(OC)c1OC
null
CHEMBL1122711
J Med Chem
1,984
CHEMBL176835
null
null
0
null
347,503
=
1
0
=
Solubility ratio
null
0.987
CHEMBL612558
null
ADMET
null
null
Solubility ratio
null
null
0.987
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
COc1cc(OCC(=O)O)cc(OC)c1OC
RDKit 2D 17 17 0 0 0 0 0 0 0 0999 V2000 2.0917 -3.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 -2.5625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 -3.7917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5167 -3.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 -2.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5167 -2.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -0.9042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -0.0792 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2417 -2.1417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2417 -1.3167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3667 -3.8042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.3667 -2.1417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 -4.6167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6750 -1.3167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.6417 -3.4000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6542 -2.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5167 -5.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 2 0 3 1 1 0 4 3 2 0 5 2 1 0 6 4 1 0 7 10 1 0 8 7 2 0 9 6 1 0 10 9 1 0 11 1 1 0 12 2 1 0 13 3 1 0 14 7 1 0 15 11 1 0 16 12 1 0 17 13 1 0 6 5 2 0 M END > <chembl_id> CHEMBL176835 > <chembl_pref_name> None
InChI=1S/C11H14O6/c1-14-8-4-7(17-6-10(12)13)5-9(15-2)11(8)16-3/h4-5H,6H2,1-3H3,(H,12,13)
DUUIKSNOGTVREZ-UHFFFAOYSA-N
1.18
1
C11H14O6
242.23
5
1
17
242.23
-0.07
0
74.22
0.81
N
6
CHEMBL176835
CHEMBL176835
CHEMBL176835
null
null
null
null
Homo sapiens
null
null
9,606
null
A
ADME
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Solubility ratio ([HbS+drug (5 mM)]/[HbS-drug])
CHEMBL1122711
Default value - Target has yet to be curated
U
null
1
CHEMBL612558
null
null
null
null
ADMET
false
ADMET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
In this paper we further establish the activity of two classes of small molecules, benzyloxy and phenoxy acids, as potent inhibitors of hemoglobin S (HbS) gelation. Structural modifications with a large number of each class confirm our earlier work that the highest activity is observed with compounds that contain dihalogenated aromatic rings with attached polar side chains. We have also found a halogenated aromatic malonic acid derivative to be quite active. Compounds reported in this paper are compared with other antigelling agents studied in our laboratory. Comments are made concerning the antigelling activity and binding sites of four derivatives and their effect on the allosteric mechanism of hemoglobin (Hb) function.
Abraham DJ, Kennedy PE, Mehanna AS, Patwa DC, Williams FL.
10.1021/jm00374a006
null
967
8
J Med Chem
null
6,747,995
1
Design, synthesis, and testing of potential antisickling agents. 4. Structure-activity relationships of benzyloxy and phenoxy acids.
27
1,984
null
33,172
CHEMBL633104
Solubility ratio ([HbS+drug (10 mM)]/[HbS-drug])
A
BAO_0000019
assay format
COc1cc(OCC(=O)O)cc(OC)c1OC
null
CHEMBL1122711
J Med Chem
1,984
CHEMBL176835
null
null
0
null
347,503
=
1
0
=
Solubility ratio
null
1.013
CHEMBL612558
null
ADMET
null
null
Solubility ratio
null
null
1.013
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
COc1cc(OCC(=O)O)cc(OC)c1OC
RDKit 2D 17 17 0 0 0 0 0 0 0 0999 V2000 2.0917 -3.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 -2.5625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 -3.7917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5167 -3.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 -2.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5167 -2.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -0.9042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -0.0792 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2417 -2.1417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2417 -1.3167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3667 -3.8042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.3667 -2.1417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 -4.6167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6750 -1.3167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.6417 -3.4000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6542 -2.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5167 -5.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 2 0 3 1 1 0 4 3 2 0 5 2 1 0 6 4 1 0 7 10 1 0 8 7 2 0 9 6 1 0 10 9 1 0 11 1 1 0 12 2 1 0 13 3 1 0 14 7 1 0 15 11 1 0 16 12 1 0 17 13 1 0 6 5 2 0 M END > <chembl_id> CHEMBL176835 > <chembl_pref_name> None
InChI=1S/C11H14O6/c1-14-8-4-7(17-6-10(12)13)5-9(15-2)11(8)16-3/h4-5H,6H2,1-3H3,(H,12,13)
DUUIKSNOGTVREZ-UHFFFAOYSA-N
1.18
1
C11H14O6
242.23
5
1
17
242.23
-0.07
0
74.22
0.81
N
6
CHEMBL176835
CHEMBL176835
CHEMBL176835
null
null
null
null
Homo sapiens
null
null
9,606
null
A
ADME
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Solubility ratio ([HbS+drug (10 mM)]/[HbS-drug])
CHEMBL1122711
Default value - Target has yet to be curated
U
null
1
CHEMBL612558
null
null
null
null
ADMET
false
ADMET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
In this paper we further establish the activity of two classes of small molecules, benzyloxy and phenoxy acids, as potent inhibitors of hemoglobin S (HbS) gelation. Structural modifications with a large number of each class confirm our earlier work that the highest activity is observed with compounds that contain dihalogenated aromatic rings with attached polar side chains. We have also found a halogenated aromatic malonic acid derivative to be quite active. Compounds reported in this paper are compared with other antigelling agents studied in our laboratory. Comments are made concerning the antigelling activity and binding sites of four derivatives and their effect on the allosteric mechanism of hemoglobin (Hb) function.
Abraham DJ, Kennedy PE, Mehanna AS, Patwa DC, Williams FL.
10.1021/jm00374a006
null
967
8
J Med Chem
null
6,747,995
1
Design, synthesis, and testing of potential antisickling agents. 4. Structure-activity relationships of benzyloxy and phenoxy acids.
27
1,984
null
33,173
CHEMBL633105
Solubility ratio ([HbS+drug (20 mM)]/[HbS-drug]
A
BAO_0000019
assay format
COc1cc(OCC(=O)O)cc(OC)c1OC
null
CHEMBL1122711
J Med Chem
1,984
CHEMBL176835
null
null
0
null
347,503
=
1
0
=
Solubility ratio
null
1.015
CHEMBL612558
null
ADMET
null
null
Solubility ratio
null
null
1.015
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
COc1cc(OCC(=O)O)cc(OC)c1OC
RDKit 2D 17 17 0 0 0 0 0 0 0 0999 V2000 2.0917 -3.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 -2.5625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 -3.7917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5167 -3.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 -2.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5167 -2.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -0.9042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -0.0792 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2417 -2.1417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2417 -1.3167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3667 -3.8042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.3667 -2.1417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 -4.6167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6750 -1.3167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.6417 -3.4000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6542 -2.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5167 -5.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 2 0 3 1 1 0 4 3 2 0 5 2 1 0 6 4 1 0 7 10 1 0 8 7 2 0 9 6 1 0 10 9 1 0 11 1 1 0 12 2 1 0 13 3 1 0 14 7 1 0 15 11 1 0 16 12 1 0 17 13 1 0 6 5 2 0 M END > <chembl_id> CHEMBL176835 > <chembl_pref_name> None
InChI=1S/C11H14O6/c1-14-8-4-7(17-6-10(12)13)5-9(15-2)11(8)16-3/h4-5H,6H2,1-3H3,(H,12,13)
DUUIKSNOGTVREZ-UHFFFAOYSA-N
1.18
1
C11H14O6
242.23
5
1
17
242.23
-0.07
0
74.22
0.81
N
6
CHEMBL176835
CHEMBL176835
CHEMBL176835
null
null
null
null
Homo sapiens
null
null
9,606
null
A
ADME
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Solubility ratio ([HbS+drug (20 mM)]/[HbS-drug]
CHEMBL1122711
Default value - Target has yet to be curated
U
null
1
CHEMBL612558
null
null
null
null
ADMET
false
ADMET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
In this paper we further establish the activity of two classes of small molecules, benzyloxy and phenoxy acids, as potent inhibitors of hemoglobin S (HbS) gelation. Structural modifications with a large number of each class confirm our earlier work that the highest activity is observed with compounds that contain dihalogenated aromatic rings with attached polar side chains. We have also found a halogenated aromatic malonic acid derivative to be quite active. Compounds reported in this paper are compared with other antigelling agents studied in our laboratory. Comments are made concerning the antigelling activity and binding sites of four derivatives and their effect on the allosteric mechanism of hemoglobin (Hb) function.
Abraham DJ, Kennedy PE, Mehanna AS, Patwa DC, Williams FL.
10.1021/jm00374a006
null
967
8
J Med Chem
null
6,747,995
1
Design, synthesis, and testing of potential antisickling agents. 4. Structure-activity relationships of benzyloxy and phenoxy acids.
27
1,984
null
33,174
CHEMBL634599
Solubility ratio ([HbS+drug (40 mM)]/[HbS-drug])
A
BAO_0000019
assay format
COc1cc(OCC(=O)O)cc(OC)c1OC
null
CHEMBL1122711
J Med Chem
1,984
CHEMBL176835
null
null
0
null
347,503
=
1
0
=
Solubility ratio
null
1.047
CHEMBL612558
null
ADMET
null
null
Solubility ratio
null
null
1.047
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
COc1cc(OCC(=O)O)cc(OC)c1OC
RDKit 2D 17 17 0 0 0 0 0 0 0 0999 V2000 2.0917 -3.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 -2.5625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 -3.7917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5167 -3.3792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 -2.1417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5167 -2.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -0.9042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -0.0792 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2417 -2.1417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2417 -1.3167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3667 -3.8042 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.3667 -2.1417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.8042 -4.6167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.6750 -1.3167 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.6417 -3.4000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6542 -2.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5167 -5.0292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 2 0 3 1 1 0 4 3 2 0 5 2 1 0 6 4 1 0 7 10 1 0 8 7 2 0 9 6 1 0 10 9 1 0 11 1 1 0 12 2 1 0 13 3 1 0 14 7 1 0 15 11 1 0 16 12 1 0 17 13 1 0 6 5 2 0 M END > <chembl_id> CHEMBL176835 > <chembl_pref_name> None
InChI=1S/C11H14O6/c1-14-8-4-7(17-6-10(12)13)5-9(15-2)11(8)16-3/h4-5H,6H2,1-3H3,(H,12,13)
DUUIKSNOGTVREZ-UHFFFAOYSA-N
1.18
1
C11H14O6
242.23
5
1
17
242.23
-0.07
0
74.22
0.81
N
6
CHEMBL176835
CHEMBL176835
CHEMBL176835
null
null
null
null
Homo sapiens
null
null
9,606
null
A
ADME
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Solubility ratio ([HbS+drug (40 mM)]/[HbS-drug])
CHEMBL1122711
Default value - Target has yet to be curated
U
null
1
CHEMBL612558
null
null
null
null
ADMET
false
ADMET
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
In this paper we further establish the activity of two classes of small molecules, benzyloxy and phenoxy acids, as potent inhibitors of hemoglobin S (HbS) gelation. Structural modifications with a large number of each class confirm our earlier work that the highest activity is observed with compounds that contain dihalogenated aromatic rings with attached polar side chains. We have also found a halogenated aromatic malonic acid derivative to be quite active. Compounds reported in this paper are compared with other antigelling agents studied in our laboratory. Comments are made concerning the antigelling activity and binding sites of four derivatives and their effect on the allosteric mechanism of hemoglobin (Hb) function.
Abraham DJ, Kennedy PE, Mehanna AS, Patwa DC, Williams FL.
10.1021/jm00374a006
null
967
8
J Med Chem
null
6,747,995
1
Design, synthesis, and testing of potential antisickling agents. 4. Structure-activity relationships of benzyloxy and phenoxy acids.
27
1,984
null
33,177
CHEMBL688000
Lowest concentration necessary to induce DNA gyrase-mediated cleavage of DNA
B
BAO_0000223
protein complex format
CCNCC1CCN(c2c(F)cc3c(=O)c(C(=O)O)cn(-c4nccs4)c3c2F)C1
null
CHEMBL1124223
J Med Chem
1,988
CHEMBL6299
null
null
0
http://www.openphacts.org/units/MicrogramPerMilliliter
227
=
1
0
=
Concentration
ug ml-1
10
CHEMBL2094139
Escherichia coli
DNA gyrase
562
null
Concentration
ug ml-1
UO_0000274
10.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCNCC1CCN(c2c(F)cc3c(=O)c(C(=O)O)cn(-c4nccs4)c3c2F)C1
RDKit 2D 30 33 0 0 0 0 0 0 0 0999 V2000 4.7042 -3.9167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4125 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9875 -3.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9875 -2.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.4167 -3.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -3.9250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6917 -2.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -3.5125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8417 -3.9250 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.7042 -4.7417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -2.6875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -2.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.1250 -2.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0292 -5.2292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.3667 -5.2250 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 1.0917 -3.5917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7542 -4.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6917 -1.4417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2917 -6.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.1167 -6.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2750 -4.7500 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 6.1167 -1.4292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.5417 -4.2042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8417 -2.2750 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 6.8417 -2.6667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.9500 -4.9167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7708 -4.7792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.2833 -4.1167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5875 -4.6917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0708 -5.3667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 5 2 0 3 1 1 0 4 3 1 0 5 1 1 0 6 3 2 0 7 2 1 0 8 6 1 0 9 8 1 0 10 1 1 0 11 8 2 0 12 4 2 0 13 2 1 0 14 10 2 0 15 10 1 0 16 9 1 0 17 9 1 0 18 7 2 0 19 14 1 0 20 15 1 0 21 6 1 0 22 13 2 0 23 16 1 0 24 11 1 0 25 13 1 0 26 17 1 0 27 28 1 0 28 23 1 0 29 27 1 0 30 29 1 0 19 20 2 0 4 7 1 0 12 11 1 0 23 26 1 0 M END > <chembl_id> CHEMBL6299 > <chembl_pref_name> None
InChI=1S/C20H20F2N4O3S/c1-2-23-8-11-3-5-25(9-11)17-14(21)7-12-16(15(17)22)26(20-24-4-6-30-20)10-13(18(12)27)19(28)29/h4,6-7,10-11,23H,2-3,5,8-9H2,1H3,(H,28,29)
MAVIDMIMQVTJOW-UHFFFAOYSA-N
2.86
3
C20H20F2N4O3S
434.47
7
2
30
434.47
-1.16
0
87.46
0.62
N
6
CHEMBL6299
CHEMBL6299
CHEMBL6299
null
null
null
null
Escherichia coli
null
null
562
null
B
Binding
BAO_0000223
protein complex format
null
Direct protein complex subunits assigned
7
Lowest concentration necessary to induce DNA gyrase-mediated cleavage of DNA
CHEMBL1124223
Direct protein target assigned
D
null
1
CHEMBL2094139
null
null
null
Escherichia coli
DNA gyrase
false
PROTEIN COMPLEX
562
P0AES6
DNA gyrase subunit B
PROTEIN
123
2
null
null
null
null
null
null
null
null
null
null
null
A series of 18 1-substituted 7-[3-[(ethylamino)methyl]-1- pyrrolidinyl]-6,8-difluoro-1,4-dihydro-4-oxo-3-quinoline- carboxylic acids (N1 analogues of CI-934) were synthesized and evaluated for antibacterial activity and DNA-gyrase inhibition. Correlations between the inhibition of DNA gyrase and antibacterial potency were established. A quantitative structure-activity relationship (QSAR) was derived by using the antibacterial potency for each of 11 strains of bacteria and the Gram-negative mean. The equations indicated that antibacterial potency was strongly dependent on STERIMOL length and width and the level of unsaturation of the N1 substituent. Some strains also showed a dependence on the presence of heteroatoms (O, N, S) in the N1 group. No significant correlations between gyrase inhibition and combinations of these parameters were found. These QSAR results are discussed in conjunction with the conformational analyses from molecular modeling studies. The substituent that most enhanced the activity of the quinolone in all regards was the cyclopropyl group. This analogue, 1-cyclopropyl-7-[3-[(ethylamino)-methyl]-1-pyrrolidinyl]-6, 8-difluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid (PD 117558), demonstrated outstanding broad spectrum activity both in vitro and in vivo when compared to relevant standards.
Domagala JM, Heifetz CL, Hutt MP, Mich TF, Nichols JB, Solomon M, Worth DF.
10.1021/jm00400a017
null
991
5
J Med Chem
null
2,834,557
1
1-Substituted 7-[3-[(ethylamino)methyl]-1-pyrrolidinyl]-6,8- difluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acids. New quantitative structure-activity relationships at N1 for the quinolone antibacterials.
31
1,988
null
33,178
CHEMBL689081
Concentration required for 50% inhibition of gyrase.
B
BAO_0000223
protein complex format
CCNCC1CCN(c2c(F)cc3c(=O)c(C(=O)O)cn(-c4nccs4)c3c2F)C1
null
CHEMBL1124223
J Med Chem
1,988
CHEMBL6299
null
null
0
http://www.openphacts.org/units/MicrogramPerMilliliter
227
=
1
0
=
Concentration
ug ml-1
30
CHEMBL2094139
Escherichia coli
DNA gyrase
562
null
Concentration
ug ml-1
UO_0000274
30.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCNCC1CCN(c2c(F)cc3c(=O)c(C(=O)O)cn(-c4nccs4)c3c2F)C1
RDKit 2D 30 33 0 0 0 0 0 0 0 0999 V2000 4.7042 -3.9167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4125 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9875 -3.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9875 -2.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.4167 -3.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -3.9250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6917 -2.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -3.5125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8417 -3.9250 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.7042 -4.7417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -2.6875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -2.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.1250 -2.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0292 -5.2292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.3667 -5.2250 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 1.0917 -3.5917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7542 -4.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6917 -1.4417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2917 -6.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.1167 -6.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2750 -4.7500 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 6.1167 -1.4292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.5417 -4.2042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8417 -2.2750 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 6.8417 -2.6667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.9500 -4.9167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7708 -4.7792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.2833 -4.1167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5875 -4.6917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0708 -5.3667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 5 2 0 3 1 1 0 4 3 1 0 5 1 1 0 6 3 2 0 7 2 1 0 8 6 1 0 9 8 1 0 10 1 1 0 11 8 2 0 12 4 2 0 13 2 1 0 14 10 2 0 15 10 1 0 16 9 1 0 17 9 1 0 18 7 2 0 19 14 1 0 20 15 1 0 21 6 1 0 22 13 2 0 23 16 1 0 24 11 1 0 25 13 1 0 26 17 1 0 27 28 1 0 28 23 1 0 29 27 1 0 30 29 1 0 19 20 2 0 4 7 1 0 12 11 1 0 23 26 1 0 M END > <chembl_id> CHEMBL6299 > <chembl_pref_name> None
InChI=1S/C20H20F2N4O3S/c1-2-23-8-11-3-5-25(9-11)17-14(21)7-12-16(15(17)22)26(20-24-4-6-30-20)10-13(18(12)27)19(28)29/h4,6-7,10-11,23H,2-3,5,8-9H2,1H3,(H,28,29)
MAVIDMIMQVTJOW-UHFFFAOYSA-N
2.86
3
C20H20F2N4O3S
434.47
7
2
30
434.47
-1.16
0
87.46
0.62
N
6
CHEMBL6299
CHEMBL6299
CHEMBL6299
null
null
null
null
Escherichia coli
null
null
562
null
B
Binding
BAO_0000223
protein complex format
null
Direct protein complex subunits assigned
7
Concentration required for 50% inhibition of gyrase.
CHEMBL1124223
Direct protein target assigned
D
null
1
CHEMBL2094139
null
null
null
Escherichia coli
DNA gyrase
false
PROTEIN COMPLEX
562
P0AES6
DNA gyrase subunit B
PROTEIN
123
2
null
null
null
null
null
null
null
null
null
null
null
A series of 18 1-substituted 7-[3-[(ethylamino)methyl]-1- pyrrolidinyl]-6,8-difluoro-1,4-dihydro-4-oxo-3-quinoline- carboxylic acids (N1 analogues of CI-934) were synthesized and evaluated for antibacterial activity and DNA-gyrase inhibition. Correlations between the inhibition of DNA gyrase and antibacterial potency were established. A quantitative structure-activity relationship (QSAR) was derived by using the antibacterial potency for each of 11 strains of bacteria and the Gram-negative mean. The equations indicated that antibacterial potency was strongly dependent on STERIMOL length and width and the level of unsaturation of the N1 substituent. Some strains also showed a dependence on the presence of heteroatoms (O, N, S) in the N1 group. No significant correlations between gyrase inhibition and combinations of these parameters were found. These QSAR results are discussed in conjunction with the conformational analyses from molecular modeling studies. The substituent that most enhanced the activity of the quinolone in all regards was the cyclopropyl group. This analogue, 1-cyclopropyl-7-[3-[(ethylamino)-methyl]-1-pyrrolidinyl]-6, 8-difluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid (PD 117558), demonstrated outstanding broad spectrum activity both in vitro and in vivo when compared to relevant standards.
Domagala JM, Heifetz CL, Hutt MP, Mich TF, Nichols JB, Solomon M, Worth DF.
10.1021/jm00400a017
null
991
5
J Med Chem
null
2,834,557
1
1-Substituted 7-[3-[(ethylamino)methyl]-1-pyrrolidinyl]-6,8- difluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acids. New quantitative structure-activity relationships at N1 for the quinolone antibacterials.
31
1,988
null
33,179
CHEMBL677348
Minimum inhibitory concentration against Escherichia coli (H560)
F
BAO_0000218
organism-based format
CCNCC1CCN(c2c(F)cc3c(=O)c(C(=O)O)cn(-c4nccs4)c3c2F)C1
null
CHEMBL1124223
J Med Chem
1,988
CHEMBL6299
null
null
0
http://www.openphacts.org/units/MicrogramPerMilliliter
227
=
1
1
=
MIC
ug.mL-1
3.1
CHEMBL354
Escherichia coli
Escherichia coli
562
null
MIC
ug ml-1
UO_0000274
3.1
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCNCC1CCN(c2c(F)cc3c(=O)c(C(=O)O)cn(-c4nccs4)c3c2F)C1
RDKit 2D 30 33 0 0 0 0 0 0 0 0999 V2000 4.7042 -3.9167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4125 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9875 -3.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9875 -2.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.4167 -3.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -3.9250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6917 -2.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -3.5125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8417 -3.9250 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.7042 -4.7417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -2.6875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -2.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.1250 -2.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0292 -5.2292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.3667 -5.2250 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 1.0917 -3.5917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7542 -4.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6917 -1.4417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2917 -6.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.1167 -6.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2750 -4.7500 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 6.1167 -1.4292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.5417 -4.2042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8417 -2.2750 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 6.8417 -2.6667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.9500 -4.9167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7708 -4.7792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.2833 -4.1167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5875 -4.6917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0708 -5.3667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 5 2 0 3 1 1 0 4 3 1 0 5 1 1 0 6 3 2 0 7 2 1 0 8 6 1 0 9 8 1 0 10 1 1 0 11 8 2 0 12 4 2 0 13 2 1 0 14 10 2 0 15 10 1 0 16 9 1 0 17 9 1 0 18 7 2 0 19 14 1 0 20 15 1 0 21 6 1 0 22 13 2 0 23 16 1 0 24 11 1 0 25 13 1 0 26 17 1 0 27 28 1 0 28 23 1 0 29 27 1 0 30 29 1 0 19 20 2 0 4 7 1 0 12 11 1 0 23 26 1 0 M END > <chembl_id> CHEMBL6299 > <chembl_pref_name> None
InChI=1S/C20H20F2N4O3S/c1-2-23-8-11-3-5-25(9-11)17-14(21)7-12-16(15(17)22)26(20-24-4-6-30-20)10-13(18(12)27)19(28)29/h4,6-7,10-11,23H,2-3,5,8-9H2,1H3,(H,28,29)
MAVIDMIMQVTJOW-UHFFFAOYSA-N
2.86
3
C20H20F2N4O3S
434.47
7
2
30
434.47
-1.16
0
87.46
0.62
N
6
CHEMBL6299
CHEMBL6299
CHEMBL6299
null
null
null
null
Escherichia coli
null
null
562
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Minimum inhibitory concentration against Escherichia coli (H560)
CHEMBL1124223
Non-molecular target assigned
N
null
1
CHEMBL354
null
null
null
Escherichia coli
Escherichia coli
false
ORGANISM
562
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of 18 1-substituted 7-[3-[(ethylamino)methyl]-1- pyrrolidinyl]-6,8-difluoro-1,4-dihydro-4-oxo-3-quinoline- carboxylic acids (N1 analogues of CI-934) were synthesized and evaluated for antibacterial activity and DNA-gyrase inhibition. Correlations between the inhibition of DNA gyrase and antibacterial potency were established. A quantitative structure-activity relationship (QSAR) was derived by using the antibacterial potency for each of 11 strains of bacteria and the Gram-negative mean. The equations indicated that antibacterial potency was strongly dependent on STERIMOL length and width and the level of unsaturation of the N1 substituent. Some strains also showed a dependence on the presence of heteroatoms (O, N, S) in the N1 group. No significant correlations between gyrase inhibition and combinations of these parameters were found. These QSAR results are discussed in conjunction with the conformational analyses from molecular modeling studies. The substituent that most enhanced the activity of the quinolone in all regards was the cyclopropyl group. This analogue, 1-cyclopropyl-7-[3-[(ethylamino)-methyl]-1-pyrrolidinyl]-6, 8-difluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid (PD 117558), demonstrated outstanding broad spectrum activity both in vitro and in vivo when compared to relevant standards.
Domagala JM, Heifetz CL, Hutt MP, Mich TF, Nichols JB, Solomon M, Worth DF.
10.1021/jm00400a017
null
991
5
J Med Chem
null
2,834,557
1
1-Substituted 7-[3-[(ethylamino)methyl]-1-pyrrolidinyl]-6,8- difluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acids. New quantitative structure-activity relationships at N1 for the quinolone antibacterials.
31
1,988
null
33,180
CHEMBL677349
Minimum inhibitory concentration against Escherichia coli (vogel)
F
BAO_0000218
organism-based format
CCNCC1CCN(c2c(F)cc3c(=O)c(C(=O)O)cn(-c4nccs4)c3c2F)C1
null
CHEMBL1124223
J Med Chem
1,988
CHEMBL6299
null
null
0
http://www.openphacts.org/units/MicrogramPerMilliliter
227
=
1
1
=
MIC
ug.mL-1
1.6
CHEMBL354
Escherichia coli
Escherichia coli
562
null
MIC
ug ml-1
UO_0000274
1.6
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCNCC1CCN(c2c(F)cc3c(=O)c(C(=O)O)cn(-c4nccs4)c3c2F)C1
RDKit 2D 30 33 0 0 0 0 0 0 0 0999 V2000 4.7042 -3.9167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4125 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9875 -3.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9875 -2.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.4167 -3.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -3.9250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6917 -2.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -3.5125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8417 -3.9250 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.7042 -4.7417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -2.6875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -2.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.1250 -2.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0292 -5.2292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.3667 -5.2250 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 1.0917 -3.5917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7542 -4.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6917 -1.4417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2917 -6.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.1167 -6.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2750 -4.7500 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 6.1167 -1.4292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.5417 -4.2042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8417 -2.2750 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 6.8417 -2.6667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.9500 -4.9167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7708 -4.7792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.2833 -4.1167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5875 -4.6917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0708 -5.3667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 5 2 0 3 1 1 0 4 3 1 0 5 1 1 0 6 3 2 0 7 2 1 0 8 6 1 0 9 8 1 0 10 1 1 0 11 8 2 0 12 4 2 0 13 2 1 0 14 10 2 0 15 10 1 0 16 9 1 0 17 9 1 0 18 7 2 0 19 14 1 0 20 15 1 0 21 6 1 0 22 13 2 0 23 16 1 0 24 11 1 0 25 13 1 0 26 17 1 0 27 28 1 0 28 23 1 0 29 27 1 0 30 29 1 0 19 20 2 0 4 7 1 0 12 11 1 0 23 26 1 0 M END > <chembl_id> CHEMBL6299 > <chembl_pref_name> None
InChI=1S/C20H20F2N4O3S/c1-2-23-8-11-3-5-25(9-11)17-14(21)7-12-16(15(17)22)26(20-24-4-6-30-20)10-13(18(12)27)19(28)29/h4,6-7,10-11,23H,2-3,5,8-9H2,1H3,(H,28,29)
MAVIDMIMQVTJOW-UHFFFAOYSA-N
2.86
3
C20H20F2N4O3S
434.47
7
2
30
434.47
-1.16
0
87.46
0.62
N
6
CHEMBL6299
CHEMBL6299
CHEMBL6299
null
null
null
null
Escherichia coli
null
null
562
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Minimum inhibitory concentration against Escherichia coli (vogel)
CHEMBL1124223
Non-molecular target assigned
N
null
1
CHEMBL354
null
null
null
Escherichia coli
Escherichia coli
false
ORGANISM
562
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of 18 1-substituted 7-[3-[(ethylamino)methyl]-1- pyrrolidinyl]-6,8-difluoro-1,4-dihydro-4-oxo-3-quinoline- carboxylic acids (N1 analogues of CI-934) were synthesized and evaluated for antibacterial activity and DNA-gyrase inhibition. Correlations between the inhibition of DNA gyrase and antibacterial potency were established. A quantitative structure-activity relationship (QSAR) was derived by using the antibacterial potency for each of 11 strains of bacteria and the Gram-negative mean. The equations indicated that antibacterial potency was strongly dependent on STERIMOL length and width and the level of unsaturation of the N1 substituent. Some strains also showed a dependence on the presence of heteroatoms (O, N, S) in the N1 group. No significant correlations between gyrase inhibition and combinations of these parameters were found. These QSAR results are discussed in conjunction with the conformational analyses from molecular modeling studies. The substituent that most enhanced the activity of the quinolone in all regards was the cyclopropyl group. This analogue, 1-cyclopropyl-7-[3-[(ethylamino)-methyl]-1-pyrrolidinyl]-6, 8-difluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid (PD 117558), demonstrated outstanding broad spectrum activity both in vitro and in vivo when compared to relevant standards.
Domagala JM, Heifetz CL, Hutt MP, Mich TF, Nichols JB, Solomon M, Worth DF.
10.1021/jm00400a017
null
991
5
J Med Chem
null
2,834,557
1
1-Substituted 7-[3-[(ethylamino)methyl]-1-pyrrolidinyl]-6,8- difluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acids. New quantitative structure-activity relationships at N1 for the quinolone antibacterials.
31
1,988
null
33,181
CHEMBL700973
Minimum inhibitory concentration against Klebsiella pneumoniae (MGH-2)
F
BAO_0000218
organism-based format
CCNCC1CCN(c2c(F)cc3c(=O)c(C(=O)O)cn(-c4nccs4)c3c2F)C1
null
CHEMBL1124223
J Med Chem
1,988
CHEMBL6299
null
null
0
http://www.openphacts.org/units/MicrogramPerMilliliter
227
=
1
1
=
MIC
ug.mL-1
3.1
CHEMBL350
Klebsiella pneumoniae
Klebsiella pneumoniae
573
null
MIC
ug ml-1
UO_0000274
3.1
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCNCC1CCN(c2c(F)cc3c(=O)c(C(=O)O)cn(-c4nccs4)c3c2F)C1
RDKit 2D 30 33 0 0 0 0 0 0 0 0999 V2000 4.7042 -3.9167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4125 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9875 -3.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9875 -2.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.4167 -3.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -3.9250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6917 -2.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -3.5125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8417 -3.9250 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.7042 -4.7417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -2.6875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -2.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.1250 -2.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0292 -5.2292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.3667 -5.2250 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 1.0917 -3.5917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7542 -4.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6917 -1.4417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2917 -6.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.1167 -6.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2750 -4.7500 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 6.1167 -1.4292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.5417 -4.2042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8417 -2.2750 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 6.8417 -2.6667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.9500 -4.9167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7708 -4.7792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.2833 -4.1167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5875 -4.6917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0708 -5.3667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 5 2 0 3 1 1 0 4 3 1 0 5 1 1 0 6 3 2 0 7 2 1 0 8 6 1 0 9 8 1 0 10 1 1 0 11 8 2 0 12 4 2 0 13 2 1 0 14 10 2 0 15 10 1 0 16 9 1 0 17 9 1 0 18 7 2 0 19 14 1 0 20 15 1 0 21 6 1 0 22 13 2 0 23 16 1 0 24 11 1 0 25 13 1 0 26 17 1 0 27 28 1 0 28 23 1 0 29 27 1 0 30 29 1 0 19 20 2 0 4 7 1 0 12 11 1 0 23 26 1 0 M END > <chembl_id> CHEMBL6299 > <chembl_pref_name> None
InChI=1S/C20H20F2N4O3S/c1-2-23-8-11-3-5-25(9-11)17-14(21)7-12-16(15(17)22)26(20-24-4-6-30-20)10-13(18(12)27)19(28)29/h4,6-7,10-11,23H,2-3,5,8-9H2,1H3,(H,28,29)
MAVIDMIMQVTJOW-UHFFFAOYSA-N
2.86
3
C20H20F2N4O3S
434.47
7
2
30
434.47
-1.16
0
87.46
0.62
N
6
CHEMBL6299
CHEMBL6299
CHEMBL6299
null
null
null
null
Klebsiella pneumoniae
null
null
573
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Minimum inhibitory concentration against Klebsiella pneumoniae (MGH-2)
CHEMBL1124223
Non-molecular target assigned
N
null
1
CHEMBL350
null
null
null
Klebsiella pneumoniae
Klebsiella pneumoniae
false
ORGANISM
573
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of 18 1-substituted 7-[3-[(ethylamino)methyl]-1- pyrrolidinyl]-6,8-difluoro-1,4-dihydro-4-oxo-3-quinoline- carboxylic acids (N1 analogues of CI-934) were synthesized and evaluated for antibacterial activity and DNA-gyrase inhibition. Correlations between the inhibition of DNA gyrase and antibacterial potency were established. A quantitative structure-activity relationship (QSAR) was derived by using the antibacterial potency for each of 11 strains of bacteria and the Gram-negative mean. The equations indicated that antibacterial potency was strongly dependent on STERIMOL length and width and the level of unsaturation of the N1 substituent. Some strains also showed a dependence on the presence of heteroatoms (O, N, S) in the N1 group. No significant correlations between gyrase inhibition and combinations of these parameters were found. These QSAR results are discussed in conjunction with the conformational analyses from molecular modeling studies. The substituent that most enhanced the activity of the quinolone in all regards was the cyclopropyl group. This analogue, 1-cyclopropyl-7-[3-[(ethylamino)-methyl]-1-pyrrolidinyl]-6, 8-difluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid (PD 117558), demonstrated outstanding broad spectrum activity both in vitro and in vivo when compared to relevant standards.
Domagala JM, Heifetz CL, Hutt MP, Mich TF, Nichols JB, Solomon M, Worth DF.
10.1021/jm00400a017
null
991
5
J Med Chem
null
2,834,557
1
1-Substituted 7-[3-[(ethylamino)methyl]-1-pyrrolidinyl]-6,8- difluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acids. New quantitative structure-activity relationships at N1 for the quinolone antibacterials.
31
1,988
null
33,182
CHEMBL772086
Minimum inhibitory concentration against Providencia rettgeri. (M1771)
F
BAO_0000218
organism-based format
CCNCC1CCN(c2c(F)cc3c(=O)c(C(=O)O)cn(-c4nccs4)c3c2F)C1
null
CHEMBL1124223
J Med Chem
1,988
CHEMBL6299
null
null
0
http://www.openphacts.org/units/MicrogramPerMilliliter
227
=
1
1
=
MIC
ug.mL-1
12.5
CHEMBL612537
Providencia rettgeri
Providencia rettgeri
587
null
MIC
ug ml-1
UO_0000274
12.5
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCNCC1CCN(c2c(F)cc3c(=O)c(C(=O)O)cn(-c4nccs4)c3c2F)C1
RDKit 2D 30 33 0 0 0 0 0 0 0 0999 V2000 4.7042 -3.9167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4125 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9875 -3.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9875 -2.6792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.4167 -3.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -3.9250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6917 -2.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -3.5125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8417 -3.9250 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.7042 -4.7417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5542 -2.6875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2667 -2.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.1250 -2.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0292 -5.2292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.3667 -5.2250 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 1.0917 -3.5917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7542 -4.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.6917 -1.4417 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2917 -6.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.1167 -6.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2750 -4.7500 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 6.1167 -1.4292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.5417 -4.2042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8417 -2.2750 0.0000 F 0 0 0 0 0 0 0 0 0 0 0 0 6.8417 -2.6667 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.9500 -4.9167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7708 -4.7792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.2833 -4.1167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.5875 -4.6917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0708 -5.3667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 5 2 0 3 1 1 0 4 3 1 0 5 1 1 0 6 3 2 0 7 2 1 0 8 6 1 0 9 8 1 0 10 1 1 0 11 8 2 0 12 4 2 0 13 2 1 0 14 10 2 0 15 10 1 0 16 9 1 0 17 9 1 0 18 7 2 0 19 14 1 0 20 15 1 0 21 6 1 0 22 13 2 0 23 16 1 0 24 11 1 0 25 13 1 0 26 17 1 0 27 28 1 0 28 23 1 0 29 27 1 0 30 29 1 0 19 20 2 0 4 7 1 0 12 11 1 0 23 26 1 0 M END > <chembl_id> CHEMBL6299 > <chembl_pref_name> None
InChI=1S/C20H20F2N4O3S/c1-2-23-8-11-3-5-25(9-11)17-14(21)7-12-16(15(17)22)26(20-24-4-6-30-20)10-13(18(12)27)19(28)29/h4,6-7,10-11,23H,2-3,5,8-9H2,1H3,(H,28,29)
MAVIDMIMQVTJOW-UHFFFAOYSA-N
2.86
3
C20H20F2N4O3S
434.47
7
2
30
434.47
-1.16
0
87.46
0.62
N
6
CHEMBL6299
CHEMBL6299
CHEMBL6299
null
null
null
null
Providencia rettgeri
null
null
587
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Minimum inhibitory concentration against Providencia rettgeri. (M1771)
CHEMBL1124223
Non-molecular target assigned
N
null
1
CHEMBL612537
null
null
null
Providencia rettgeri
Providencia rettgeri
false
ORGANISM
587
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of 18 1-substituted 7-[3-[(ethylamino)methyl]-1- pyrrolidinyl]-6,8-difluoro-1,4-dihydro-4-oxo-3-quinoline- carboxylic acids (N1 analogues of CI-934) were synthesized and evaluated for antibacterial activity and DNA-gyrase inhibition. Correlations between the inhibition of DNA gyrase and antibacterial potency were established. A quantitative structure-activity relationship (QSAR) was derived by using the antibacterial potency for each of 11 strains of bacteria and the Gram-negative mean. The equations indicated that antibacterial potency was strongly dependent on STERIMOL length and width and the level of unsaturation of the N1 substituent. Some strains also showed a dependence on the presence of heteroatoms (O, N, S) in the N1 group. No significant correlations between gyrase inhibition and combinations of these parameters were found. These QSAR results are discussed in conjunction with the conformational analyses from molecular modeling studies. The substituent that most enhanced the activity of the quinolone in all regards was the cyclopropyl group. This analogue, 1-cyclopropyl-7-[3-[(ethylamino)-methyl]-1-pyrrolidinyl]-6, 8-difluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid (PD 117558), demonstrated outstanding broad spectrum activity both in vitro and in vivo when compared to relevant standards.
Domagala JM, Heifetz CL, Hutt MP, Mich TF, Nichols JB, Solomon M, Worth DF.
10.1021/jm00400a017
null
991
5
J Med Chem
null
2,834,557
1
1-Substituted 7-[3-[(ethylamino)methyl]-1-pyrrolidinyl]-6,8- difluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acids. New quantitative structure-activity relationships at N1 for the quinolone antibacterials.
31
1,988
null
38,115
CHEMBL796079
Negative logarithm of the concentration of compound required to reduce the response of EC50 dose of ANG II to the response to half the EC50 dose
F
BAO_0000218
organism-based format
CC[C@H](C)[C@H](NC(=O)[C@H](Cc1ccc(O)cc1)N(C)C(=O)[C@@H](NC(=O)[C@H](CCCN=C(N)N)NC(=O)C(C)(C)NC)C(C)C)C(=O)N[C@@H](Cc1c[nH]cn1)C(=O)N1CCC[C@H]1C(=O)N[C@@H](Cc1ccccc1)C(=O)O
null
CHEMBL1124158
J Med Chem
1,988
CHEMBL262226
null
6
0
http://www.openphacts.org/units/Nanomolar
48,159
=
1
1
=
Kd
nM
1,000
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
pA2
null
UO_0000065
6.0
null
null
null
null
-1
0
-1
null
PEPTIDE1{[Me_Aib].R.V.[meY].I.H.P.F}$$$$
-1
null
Protein
0
false
false
0
null
-1
BOTH
false
false
null
null
false
CC[C@H](C)[C@H](NC(=O)[C@H](Cc1ccc(O)cc1)N(C)C(=O)[C@@H](NC(=O)[C@H](CCCN=C(N)N)NC(=O)C(C)(C)NC)C(C)C)C(=O)N[C@@H](Cc1c[nH]cn1)C(=O)N1CCC[C@H]1C(=O)N[C@@H](Cc1ccccc1)C(=O)O
RDKit 2D 75 78 0 0 1 0 0 0 0 0999 V2000 5.1833 -12.0167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.0083 -2.9917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.1833 -10.5125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8917 -3.7542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2917 -3.7458 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.5500 -12.4042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.1875 -7.5083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8875 -5.2542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.6083 -2.9833 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.4833 -9.7625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.3083 -3.7375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5917 -3.0000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9708 -12.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.9083 -3.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4833 -8.2625 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -3.8958 -0.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.2458 -10.9333 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.1875 -6.0083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -5.2000 -1.4750 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 11.4375 -9.2792 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.8250 -10.4583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -11.7042 -3.7042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3000 -11.4500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.7792 -10.5167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.0833 -9.7708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.2208 -8.2875 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -3.8875 0.7708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -5.2083 -2.9750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 10.6875 -7.9792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0042 -1.7917 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -12.7417 -3.1000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 10.4333 -10.3917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1417 -9.9125 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.9333 -3.1583 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.5958 -1.5000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.6500 -13.2000 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.1458 -8.1083 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -3.9125 -4.9292 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -2.8583 -1.3375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 0.5208 -8.9875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4375 -11.0708 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -10.4042 -2.9583 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -11.7083 -4.9042 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.3167 -5.2375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.5833 1.5167 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 6.3958 -12.8708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4875 -5.2583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8958 -0.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0625 -12.6250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 6.5000 0.7417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9000 -8.5125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.2875 -4.9458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.1917 -1.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9000 0.7500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.2000 1.4958 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4917 -0.7583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4375 -14.3042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.5375 1.3375 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 5.9375 -14.3000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.9250 1.3750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8792 1.9708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -6.5042 -3.7208 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -9.1042 -3.7125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.5750 2.7167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.4875 -3.7583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.3583 -5.8333 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.2833 -5.8458 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.5250 -5.8583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.0208 -9.5083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.2042 -7.0417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -7.8042 -2.9667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.5250 -3.1583 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.6292 -6.5708 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.4458 -9.0375 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.7500 -7.5667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 5 1 0 3 1 1 0 4 8 1 0 5 12 1 0 13 6 1 1 7 15 1 0 18 8 1 1 11 9 1 6 10 3 1 0 11 2 1 0 12 4 1 0 13 1 1 0 14 9 1 0 10 15 1 1 16 19 1 0 17 6 1 0 18 7 1 0 19 28 1 0 20 32 1 0 21 17 1 6 22 42 2 0 23 21 1 0 24 10 1 0 25 24 1 0 26 25 1 0 27 16 1 0 28 14 1 0 29 26 2 0 30 2 2 0 31 22 1 0 32 25 2 0 33 3 2 0 34 4 2 0 12 35 1 1 36 6 2 0 37 7 2 0 38 14 2 0 39 16 2 0 40 21 1 0 41 23 2 0 42 63 1 0 43 22 1 0 44 11 1 0 45 27 1 0 46 1 1 0 47 18 1 0 48 35 1 0 49 23 1 0 50 56 1 0 51 40 1 0 52 5 1 0 53 48 1 0 54 48 2 0 55 54 1 0 56 53 2 0 57 13 1 0 58 50 1 0 59 46 1 0 60 27 1 0 61 27 1 0 28 62 1 6 63 71 1 0 64 45 1 0 65 47 1 0 66 44 1 0 67 44 1 0 47 68 1 6 69 51 1 0 70 51 2 0 71 62 1 0 72 65 1 0 73 70 1 0 74 69 2 0 75 74 1 0 57 59 1 0 29 20 1 0 75 73 2 0 50 55 2 0 M END > <chembl_id> CHEMBL262226 > <chembl_pref_name> None
InChI=1S/C52H77N13O10/c1-9-31(4)42(46(70)59-37(27-34-28-56-29-58-34)47(71)65-24-14-18-39(65)44(68)60-38(49(73)74)25-32-15-11-10-12-16-32)63-45(69)40(26-33-19-21-35(66)22-20-33)64(8)48(72)41(30(2)3)62-43(67)36(17-13-23-57-51(53)54)61-50(75)52(5,6)55-7/h10-12,15-16,19-22,28-31,36-42,55,66H,9,13-14,17-18,23-27H2,1-8H3,(H,56,58)(H,59,70)(H,60,68)(H,61,75)(H,62,67)(H,63,69)(H,73,74)(H4,53,54,57)/t31-,36-,37-,38-,39-,40-,41-,42-/m0/s1
OQIKRTPSWNAWRM-DDLCQNJHSA-N
null
null
C52H77N13O10
1044.27
null
null
null
1,044.27
null
null
null
null
null
null
CHEMBL262226
CHEMBL262226
CHEMBL262226
null
null
null
null
Rattus norvegicus
null
null
10,116
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Negative logarithm of the concentration of compound required to reduce the response of EC50 dose of ANG II to the response to half the EC50 dose
CHEMBL1124158
Non-molecular target assigned
N
null
1
CHEMBL376
null
null
null
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Analogues of the competitive angiotensin antagonist [Sar1,Tyr(ME)4]angiotensin II (sarmesin) with modifications at the N-terminus have been prepared by the solid-phase method and purified by reversed-phase HPLC. Substitution of the Sar1 residue of sarmesin with N,N-dimethyl-Gly, N-ethyl-Gly, aminoisobutyric, (methylamino)isobutyric, aminocaproic, and oxamic acids gave analogues that had the following respective antagonist activities (pA2) in the rat isolated uterus assay: less than 6, 6.9, 5.5, 6.0, less than 6, and 5.3. The additional substitution of Ile for Phe at the C-terminus of the latter four peptides gave pA2 values of 7.1, 5.1, less than 5, and 5. Substitution of the Arg2 residue of sarmesin with Nle or Sar abolished antagonist activity. These data emphasize the stringent and discriminating structural requirements in the N-terminal domain of sarmesin that endow this analogue with its antagonist properties and suggest the presence of defined steric constraints in this region of the molecule during receptor blockade.
Matsoukas J, Cordopatis P, Belte U, Goghari MH, Ganter RC, Franklin KJ, Moore GJ.
10.1021/jm00402a028
null
1418
7
J Med Chem
null
2,455,051
1
Importance of the N-terminal domain of the type II angiotensin antagonist sarmesin for receptor blockade.
31
1,988
null
38,118
CHEMBL630713
Compound (1 mM) was evaluated in vitro for the effect on rate of aging(rate constant) of Soman-inhibited rat erythrocyte AChE and first order rate constant was determined
A
BAO_0000218
organism-based format
C[N+](C)(C)CCCCl.[Br-]
null
CHEMBL1123058
J Med Chem
1,985
CHEMBL15795
null
null
0
null
17,688
=
1
0
=
Rate constant
null
0.0359
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Rate constant
null
null
0.0359
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
C[N+](C)(C)CCCCl.[Br-]
RDKit 2D 9 7 0 0 0 0 0 0 0 0999 V2000 4.7125 -1.9667 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 3.1667 -2.5542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.3125 -2.5542 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 1.7417 -2.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4542 -2.9667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8792 -2.9667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.1667 -1.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3792 -3.3500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0292 -2.9667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 9 1 0 4 5 1 0 5 2 1 0 6 2 1 0 7 2 1 0 8 2 1 0 9 4 1 0 M CHG 2 1 -1 2 1 M END > <chembl_id> CHEMBL15795 > <chembl_pref_name> None
InChI=1S/C6H15ClN.BrH/c1-8(2,3)6-4-5-7;/h4-6H2,1-3H3;1H/q+1;/p-1
XMRUUKXYPYSSLI-UHFFFAOYSA-M
1.32
0
C6H15BrClN
216.55
0
0
8
136.65
0.63
0
0
0.41
Y
3
CHEMBL1178211
CHEMBL15795
CHEMBL1178211
null
null
null
null
Rattus norvegicus
null
null
10,116
null
A
ADME
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Compound (1 mM) was evaluated in vitro for the effect on rate of aging(rate constant) of Soman-inhibited rat erythrocyte AChE and first order rate constant was determined
CHEMBL1123058
Non-molecular target assigned
N
null
1
CHEMBL376
null
null
null
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A number of compounds were synthesized and tested for their ability to realkylate the phosphonate anion of "aged", soman-inhibited acetylcholinesterase. None were found able to do so, but two of the compounds in particular, [2-(4-pyridyl)ethyl]diethylmethylammonium iodide (6) and its 2-isomer 7, proved able to slow the rate of aging significantly.
Gray AP, Platz RD, Chang TC, Leverone TR, Ferrick DA, Kramer DN.
10.1021/jm00379a020
null
111
1
J Med Chem
null
3,965,704
1
Synthesis of some quaternary ammonium alkylating agents and their effects on soman-inhibited acetylcholinesterase.
28
1,985
null
38,119
CHEMBL852817
Ratio of control/treated value of the compound
F
BAO_0000019
assay format
C[N+](C)(C)CCCCl.[Br-]
null
CHEMBL1123058
J Med Chem
1,985
CHEMBL15795
null
null
0
null
17,688
=
1
0
=
Ratio
null
1.19
CHEMBL612545
null
Unchecked
null
null
Ratio
null
null
1.19
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
C[N+](C)(C)CCCCl.[Br-]
RDKit 2D 9 7 0 0 0 0 0 0 0 0999 V2000 4.7125 -1.9667 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 3.1667 -2.5542 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.3125 -2.5542 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 1.7417 -2.5542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4542 -2.9667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.8792 -2.9667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.1667 -1.7292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3792 -3.3500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0292 -2.9667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 9 1 0 4 5 1 0 5 2 1 0 6 2 1 0 7 2 1 0 8 2 1 0 9 4 1 0 M CHG 2 1 -1 2 1 M END > <chembl_id> CHEMBL15795 > <chembl_pref_name> None
InChI=1S/C6H15ClN.BrH/c1-8(2,3)6-4-5-7;/h4-6H2,1-3H3;1H/q+1;/p-1
XMRUUKXYPYSSLI-UHFFFAOYSA-M
1.32
0
C6H15BrClN
216.55
0
0
8
136.65
0.63
0
0
0.41
Y
3
CHEMBL1178211
CHEMBL15795
CHEMBL1178211
null
null
null
null
null
null
null
null
null
F
Functional
BAO_0000019
assay format
null
Default value - Target unknown or has yet to be assigned
0
Ratio of control/treated value of the compound
CHEMBL1123058
Default value - Target has yet to be curated
U
null
1
CHEMBL612545
null
null
null
null
Unchecked
false
UNCHECKED
null
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A number of compounds were synthesized and tested for their ability to realkylate the phosphonate anion of "aged", soman-inhibited acetylcholinesterase. None were found able to do so, but two of the compounds in particular, [2-(4-pyridyl)ethyl]diethylmethylammonium iodide (6) and its 2-isomer 7, proved able to slow the rate of aging significantly.
Gray AP, Platz RD, Chang TC, Leverone TR, Ferrick DA, Kramer DN.
10.1021/jm00379a020
null
111
1
J Med Chem
null
3,965,704
1
Synthesis of some quaternary ammonium alkylating agents and their effects on soman-inhibited acetylcholinesterase.
28
1,985
null
38,120
CHEMBL758714
Inhibition against porcine pancreatic elastase
B
BAO_0000224
protein format
O=C(Nc1ccccc1)n1ccnc1
null
CHEMBL1122889
J Med Chem
1,985
CHEMBL294113
IMIDAZOLE-1-CARBOXYLIC ACID PHENYLAMIDE
null
0
null
113,308
=
1
0
=
Activity
null
null
CHEMBL2096984
Sus scrofa
Pancreatic elastase
9823
null
Activity
null
null
null
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
IMIDAZOLE-1-CARBOXYLIC ACID PHENYLAMIDE
-1
MOL
false
false
null
null
false
O=C(Nc1ccccc1)n1ccnc1
RDKit 2D 14 15 0 0 0 0 0 0 0 0999 V2000 8.9167 -8.3292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 8.9250 -7.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.5000 -9.6042 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 9.6417 -7.1000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 8.2417 -8.8042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.5750 -8.8250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.2125 -7.0875 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 9.3167 -9.6042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.6500 -6.2750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 10.3667 -5.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.9417 -5.8625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.9417 -5.0417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 10.3792 -5.0500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.6667 -4.6292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 5 2 0 4 2 1 0 5 1 1 0 6 1 1 0 7 2 2 0 8 6 2 0 9 4 1 0 10 9 2 0 11 9 1 0 12 11 2 0 13 10 1 0 14 12 1 0 3 8 1 0 13 14 2 0 M END > <chembl_id> CHEMBL294113 > <chembl_pref_name> IMIDAZOLE-1-CARBOXYLIC ACID PHENYLAMIDE
InChI=1S/C10H9N3O/c14-10(13-7-6-11-8-13)12-9-4-2-1-3-5-9/h1-8H,(H,12,14)
KPPADAGTNGHGBR-UHFFFAOYSA-N
1.96
2
C10H9N3O
187.20
3
1
14
187.2
-1.62
0
46.92
0.74
Y
1
CHEMBL294113
CHEMBL294113
CHEMBL294113
null
null
null
null
null
null
null
null
null
B
Binding
BAO_0000224
protein format
null
Multiple homologous protein targets may be assigned
4
Inhibition against porcine pancreatic elastase
CHEMBL1122889
Homologous protein target assigned
H
null
1
CHEMBL2096984
null
null
null
Sus scrofa
Pancreatic elastase
false
PROTEIN FAMILY
9,823
P08419
Chymotrypsin-like elastase family member 2A
PROTEIN
748
2
null
null
null
null
null
null
null
null
null
null
null
Several amino acid derived azolides (I) have been synthesized and investigated for their inhibitory activity toward human leukocyte elastase and porcine pancreatic elastase. The inhibitory activity was found to be dependent on the nature of the precursor amino acid ester. Thus, compounds derived from L-valine methyl ester 3, L-norvaline methyl ester 5, DL-norleucine methyl ester 9, and L-methionine methyl ester 10 were found to inhibit irreversibly both enzymes. Compound 10 was found to be a specific and selective inhibitor of human leukocyte elastase. In contrast to these, inhibitors derived from glycine methyl ester 1, D-valine methyl ester 4, and D-norvaline methyl ester 6 were found to be inactive. The results of the present study show that latent isocyanates derived from appropriate amino acids can serve as selective inhibitors of serine proteases and are of potential pharmacological value.
Groutas WC, Abrams WR, Theodorakis MC, Kasper AM, Rude SA, Badger RC, Ocain TD, Miller KE, Moi MK, Brubaker MJ.
10.1021/jm00380a010
null
204
2
J Med Chem
null
3,844,034
1
Amino acid derived latent isocyanates: irreversible inactivation of porcine pancreatic elastase and human leukocyte elastase.
28
1,985
null
38,121
CHEMBL705697
Inhibition of human leukocyte elastase
B
BAO_0000357
single protein format
O=C(Nc1ccccc1)n1ccnc1
null
CHEMBL1122889
J Med Chem
1,985
CHEMBL294113
IMIDAZOLE-1-CARBOXYLIC ACID PHENYLAMIDE
null
0
null
113,308
=
1
0
=
Activity
null
null
CHEMBL248
Homo sapiens
Neutrophil elastase
9606
null
Activity
null
null
null
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
IMIDAZOLE-1-CARBOXYLIC ACID PHENYLAMIDE
-1
MOL
false
false
null
null
false
O=C(Nc1ccccc1)n1ccnc1
RDKit 2D 14 15 0 0 0 0 0 0 0 0999 V2000 8.9167 -8.3292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 8.9250 -7.5042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.5000 -9.6042 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 9.6417 -7.1000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 8.2417 -8.8042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.5750 -8.8250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.2125 -7.0875 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 9.3167 -9.6042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.6500 -6.2750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 10.3667 -5.8750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.9417 -5.8625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.9417 -5.0417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 10.3792 -5.0500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 9.6667 -4.6292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 1 0 3 5 2 0 4 2 1 0 5 1 1 0 6 1 1 0 7 2 2 0 8 6 2 0 9 4 1 0 10 9 2 0 11 9 1 0 12 11 2 0 13 10 1 0 14 12 1 0 3 8 1 0 13 14 2 0 M END > <chembl_id> CHEMBL294113 > <chembl_pref_name> IMIDAZOLE-1-CARBOXYLIC ACID PHENYLAMIDE
InChI=1S/C10H9N3O/c14-10(13-7-6-11-8-13)12-9-4-2-1-3-5-9/h1-8H,(H,12,14)
KPPADAGTNGHGBR-UHFFFAOYSA-N
1.96
2
C10H9N3O
187.20
3
1
14
187.2
-1.62
0
46.92
0.74
Y
1
CHEMBL294113
CHEMBL294113
CHEMBL294113
null
null
null
null
null
null
null
null
null
B
Binding
BAO_0000357
single protein format
null
Homologous single protein target assigned
8
Inhibition of human leukocyte elastase
CHEMBL1122889
Homologous protein target assigned
H
null
1
CHEMBL248
null
null
null
Homo sapiens
Neutrophil elastase
false
SINGLE PROTEIN
9,606
P08246
Neutrophil elastase
PROTEIN
366
1
null
null
null
null
null
null
null
null
null
null
null
Several amino acid derived azolides (I) have been synthesized and investigated for their inhibitory activity toward human leukocyte elastase and porcine pancreatic elastase. The inhibitory activity was found to be dependent on the nature of the precursor amino acid ester. Thus, compounds derived from L-valine methyl ester 3, L-norvaline methyl ester 5, DL-norleucine methyl ester 9, and L-methionine methyl ester 10 were found to inhibit irreversibly both enzymes. Compound 10 was found to be a specific and selective inhibitor of human leukocyte elastase. In contrast to these, inhibitors derived from glycine methyl ester 1, D-valine methyl ester 4, and D-norvaline methyl ester 6 were found to be inactive. The results of the present study show that latent isocyanates derived from appropriate amino acids can serve as selective inhibitors of serine proteases and are of potential pharmacological value.
Groutas WC, Abrams WR, Theodorakis MC, Kasper AM, Rude SA, Badger RC, Ocain TD, Miller KE, Moi MK, Brubaker MJ.
10.1021/jm00380a010
null
204
2
J Med Chem
null
3,844,034
1
Amino acid derived latent isocyanates: irreversible inactivation of porcine pancreatic elastase and human leukocyte elastase.
28
1,985
null
38,122
CHEMBL785434
Effective dose against DOPA accumulation in rat brain limbic region after reserpine pretreatment by subcutaneous administration
F
BAO_0000218
organism-based format
CCCN(CCC)[C@H]1CCc2c(OC)cccc2[C@H]1C.Cl
null
CHEMBL1122913
J Med Chem
1,985
CHEMBL544195
null
null
0
null
5,909
=
1
1
=
ED50
mg.kg-1
1.7
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
ED50
mg kg-1
UO_0000308
1.7
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCN(CCC)[C@H]1CCc2c(OC)cccc2[C@H]1C.Cl
RDKit 2D 21 21 0 0 0 0 0 0 0 0999 V2000 3.8893 2.1804 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 1.0018 2.8580 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.2873 2.4455 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.2873 1.6205 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0018 1.2080 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7163 1.6205 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7163 2.4455 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4272 2.8581 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.1417 2.4456 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.1417 1.6206 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4272 1.2081 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.8561 2.8581 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.5706 2.4456 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.8561 3.6831 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.5706 4.0956 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.5706 4.9206 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.2851 2.8581 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.9996 2.4456 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0018 0.3830 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.7163 -0.0295 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4272 3.6831 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 3 1 0 2 7 2 0 4 5 1 0 5 6 2 0 6 7 1 0 3 8 1 0 3 4 2 0 11 4 1 0 8 9 1 0 9 10 1 0 10 11 1 0 9 12 1 6 12 13 1 0 12 14 1 0 14 15 1 0 15 16 1 0 13 17 1 0 17 18 1 0 5 19 1 0 19 20 1 0 8 21 1 6 M END > <chembl_id> CHEMBL544195 > <chembl_pref_name> None
InChI=1S/C18H29NO.ClH/c1-5-12-19(13-6-2)17-11-10-16-15(14(17)3)8-7-9-18(16)20-4;/h7-9,14,17H,5-6,10-13H2,1-4H3;1H/t14-,17+;/m1./s1
ADVQBNGWEGSMGY-CVLQQERVSA-N
4.24
1
C18H30ClNO
311.90
2
0
20
275.44
0.02
0
12.47
0.77
N
6
CHEMBL157937
CHEMBL544195
CHEMBL157937
null
null
null
null
Rattus norvegicus
null
null
10,116
Brain
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Effective dose against DOPA accumulation in rat brain limbic region after reserpine pretreatment by subcutaneous administration
CHEMBL1122913
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638188
null
null
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The enantiomers of cis-5-hydroxy-1-methyl-2-(di-n-propylamino)tetralin and its methyl ether have been synthesized. The compounds were tested for central dopamine (DA) receptor activity, by using biochemical and behavioral tests in rats. The (1R,2S)-(-) enantiomers of 1 and 2 are characterized as centrally acting DA-receptor agonists while the corresponding (1S,2R)-(+) enantiomers are characterized as centrally acting DA-receptor antagonists. Compounds (+)-1 and (+)-2 differ from classical neuroleptics in being able to increase DA synthesis rate in a wide dose range without reducing locomotor activity, suggesting a pronounced selectivity for DA autoreceptors. Also the (-) enantiomers seem to act preferentially on DA autoreceptors.
Johansson AM, Arvidsson LE, Hacksell U, Nilsson JL, Svensson K, Hjorth S, Clark D, Carlsson A, Sanchez D, Andersson B.
10.1021/jm00146a012
null
1049
8
J Med Chem
null
3,927,002
1
Novel dopamine receptor agonists and antagonists with preferential action on autoreceptors.
28
1,985
null
38,123
CHEMBL785439
Effective dose against DOPA accumulation in rat brain striatal region after reserpine pretreatment by subcutaneous administration
F
BAO_0000218
organism-based format
CCCN(CCC)[C@H]1CCc2c(OC)cccc2[C@H]1C.Cl
null
CHEMBL1122913
J Med Chem
1,985
CHEMBL544195
null
null
0
null
5,909
=
1
1
=
ED50
mg.kg-1
1.8
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
ED50
mg kg-1
UO_0000308
1.8
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCN(CCC)[C@H]1CCc2c(OC)cccc2[C@H]1C.Cl
RDKit 2D 21 21 0 0 0 0 0 0 0 0999 V2000 3.8893 2.1804 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 1.0018 2.8580 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.2873 2.4455 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.2873 1.6205 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0018 1.2080 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7163 1.6205 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7163 2.4455 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4272 2.8581 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.1417 2.4456 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.1417 1.6206 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4272 1.2081 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.8561 2.8581 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.5706 2.4456 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.8561 3.6831 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.5706 4.0956 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.5706 4.9206 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.2851 2.8581 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.9996 2.4456 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0018 0.3830 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.7163 -0.0295 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4272 3.6831 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 3 1 0 2 7 2 0 4 5 1 0 5 6 2 0 6 7 1 0 3 8 1 0 3 4 2 0 11 4 1 0 8 9 1 0 9 10 1 0 10 11 1 0 9 12 1 6 12 13 1 0 12 14 1 0 14 15 1 0 15 16 1 0 13 17 1 0 17 18 1 0 5 19 1 0 19 20 1 0 8 21 1 6 M END > <chembl_id> CHEMBL544195 > <chembl_pref_name> None
InChI=1S/C18H29NO.ClH/c1-5-12-19(13-6-2)17-11-10-16-15(14(17)3)8-7-9-18(16)20-4;/h7-9,14,17H,5-6,10-13H2,1-4H3;1H/t14-,17+;/m1./s1
ADVQBNGWEGSMGY-CVLQQERVSA-N
4.24
1
C18H30ClNO
311.90
2
0
20
275.44
0.02
0
12.47
0.77
N
6
CHEMBL157937
CHEMBL544195
CHEMBL157937
null
null
null
null
Rattus norvegicus
null
null
10,116
Brain
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Effective dose against DOPA accumulation in rat brain striatal region after reserpine pretreatment by subcutaneous administration
CHEMBL1122913
Non-molecular target assigned
N
null
1
CHEMBL376
CHEMBL3638188
null
null
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The enantiomers of cis-5-hydroxy-1-methyl-2-(di-n-propylamino)tetralin and its methyl ether have been synthesized. The compounds were tested for central dopamine (DA) receptor activity, by using biochemical and behavioral tests in rats. The (1R,2S)-(-) enantiomers of 1 and 2 are characterized as centrally acting DA-receptor agonists while the corresponding (1S,2R)-(+) enantiomers are characterized as centrally acting DA-receptor antagonists. Compounds (+)-1 and (+)-2 differ from classical neuroleptics in being able to increase DA synthesis rate in a wide dose range without reducing locomotor activity, suggesting a pronounced selectivity for DA autoreceptors. Also the (-) enantiomers seem to act preferentially on DA autoreceptors.
Johansson AM, Arvidsson LE, Hacksell U, Nilsson JL, Svensson K, Hjorth S, Clark D, Carlsson A, Sanchez D, Andersson B.
10.1021/jm00146a012
null
1049
8
J Med Chem
null
3,927,002
1
Novel dopamine receptor agonists and antagonists with preferential action on autoreceptors.
28
1,985
null
38,126
CHEMBL773735
Locomotor activity after reserpine pretreatment in rat
F
BAO_0000218
organism-based format
CCCN(CCC)[C@H]1CCc2c(OC)cccc2[C@H]1C.Cl
null
CHEMBL1122913
J Med Chem
1,985
CHEMBL544195
null
null
0
null
5,909
=
1
0
=
Accumulated counts/30 min
null
8
CHEMBL376
Rattus norvegicus
Rattus norvegicus
10116
null
Accumulated counts/30 min
null
null
8.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCN(CCC)[C@H]1CCc2c(OC)cccc2[C@H]1C.Cl
RDKit 2D 21 21 0 0 0 0 0 0 0 0999 V2000 3.8893 2.1804 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 1.0018 2.8580 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.2873 2.4455 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.2873 1.6205 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0018 1.2080 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7163 1.6205 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7163 2.4455 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4272 2.8581 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.1417 2.4456 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.1417 1.6206 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4272 1.2081 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.8561 2.8581 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.5706 2.4456 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.8561 3.6831 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.5706 4.0956 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.5706 4.9206 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.2851 2.8581 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.9996 2.4456 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0018 0.3830 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 1.7163 -0.0295 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4272 3.6831 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 3 1 0 2 7 2 0 4 5 1 0 5 6 2 0 6 7 1 0 3 8 1 0 3 4 2 0 11 4 1 0 8 9 1 0 9 10 1 0 10 11 1 0 9 12 1 6 12 13 1 0 12 14 1 0 14 15 1 0 15 16 1 0 13 17 1 0 17 18 1 0 5 19 1 0 19 20 1 0 8 21 1 6 M END > <chembl_id> CHEMBL544195 > <chembl_pref_name> None
InChI=1S/C18H29NO.ClH/c1-5-12-19(13-6-2)17-11-10-16-15(14(17)3)8-7-9-18(16)20-4;/h7-9,14,17H,5-6,10-13H2,1-4H3;1H/t14-,17+;/m1./s1
ADVQBNGWEGSMGY-CVLQQERVSA-N
4.24
1
C18H30ClNO
311.90
2
0
20
275.44
0.02
0
12.47
0.77
N
6
CHEMBL157937
CHEMBL544195
CHEMBL157937
null
null
null
null
Rattus norvegicus
null
null
10,116
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Locomotor activity after reserpine pretreatment in rat
CHEMBL1122913
Non-molecular target assigned
N
null
1
CHEMBL376
null
null
null
Rattus norvegicus
Rattus norvegicus
false
ORGANISM
10,116
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
The enantiomers of cis-5-hydroxy-1-methyl-2-(di-n-propylamino)tetralin and its methyl ether have been synthesized. The compounds were tested for central dopamine (DA) receptor activity, by using biochemical and behavioral tests in rats. The (1R,2S)-(-) enantiomers of 1 and 2 are characterized as centrally acting DA-receptor agonists while the corresponding (1S,2R)-(+) enantiomers are characterized as centrally acting DA-receptor antagonists. Compounds (+)-1 and (+)-2 differ from classical neuroleptics in being able to increase DA synthesis rate in a wide dose range without reducing locomotor activity, suggesting a pronounced selectivity for DA autoreceptors. Also the (-) enantiomers seem to act preferentially on DA autoreceptors.
Johansson AM, Arvidsson LE, Hacksell U, Nilsson JL, Svensson K, Hjorth S, Clark D, Carlsson A, Sanchez D, Andersson B.
10.1021/jm00146a012
null
1049
8
J Med Chem
null
3,927,002
1
Novel dopamine receptor agonists and antagonists with preferential action on autoreceptors.
28
1,985
null
38,129
CHEMBL706332
Tested in vitro against murine L1210 leukemia.
F
BAO_0000219
cell-based format
CCCCCCNc1ccc2c3c(nn2CCN(CC)CC)-c2ccccc2C(=O)c13.Cl
null
CHEMBL1123657
J Med Chem
1,987
CHEMBL542321
null
5.7
0
http://www.openphacts.org/units/Nanomolar
35,153
=
1
1
=
IC50
nM
2,000
CHEMBL386
Mus musculus
L1210
10090
null
IC50
M
UO_0000065
0.000002
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCCCCNc1ccc2c3c(nn2CCN(CC)CC)-c2ccccc2C(=O)c13.Cl
RDKit 2D 32 34 0 0 0 0 0 0 0 0999 V2000 5.4623 0.0000 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 1.0815 0.6692 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.3637 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.7762 1.5264 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.3637 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0488 1.5264 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.0815 -0.9808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3488 0.6692 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7940 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7940 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.5262 2.1992 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3488 -0.9808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0613 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0829 -1.8058 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.0613 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.1822 2.9491 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3488 -1.8058 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.6596 3.6219 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.5085 0.6692 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5085 -0.9808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4810 3.5449 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3155 4.3718 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0633 -2.2183 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0633 -3.0433 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4922 -4.6933 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.7778 -4.2808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.7778 -3.4558 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2230 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2230 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7929 5.0446 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 4.2178 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4922 -5.5183 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 3 1 0 2 4 2 0 3 5 2 0 4 6 1 0 5 7 1 0 3 8 1 0 6 8 1 0 2 9 1 0 7 10 1 0 9 10 1 0 6 11 1 0 5 12 1 0 8 13 2 0 7 14 2 0 12 15 2 0 13 15 1 0 11 16 1 0 12 17 1 0 16 18 1 0 9 19 2 0 10 20 2 0 18 21 1 0 18 22 1 0 17 23 1 0 23 24 1 0 25 26 1 0 24 27 1 0 26 27 1 0 20 28 1 0 19 29 1 0 28 29 2 0 22 30 1 0 21 31 1 0 25 32 1 0 M END > <chembl_id> CHEMBL542321 > <chembl_pref_name> None
InChI=1S/C26H34N4O.ClH/c1-4-7-8-11-16-27-21-14-15-22-24-23(21)26(31)20-13-10-9-12-19(20)25(24)28-30(22)18-17-29(5-2)6-3;/h9-10,12-15,27H,4-8,11,16-18H2,1-3H3;1H
KJLHRQLQYPIDIX-UHFFFAOYSA-N
5.58
3
C26H35ClN4O
455.05
5
1
31
418.59
-0.89
1
50.16
0.32
N
11
CHEMBL1191248
CHEMBL542321
CHEMBL1191248
null
null
null
L1210
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000219
cell-based format
CHEMBL3308391
Target assigned is non-molecular
1
Tested in vitro against murine L1210 leukemia.
CHEMBL1123657
Non-molecular target assigned
N
null
1
CHEMBL386
null
null
null
Mus musculus
L1210
false
CELL-LINE
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Chromophore modification of the anthracenediones related to mitoxantrone in an attempt to provide agents with diminished or no cardiotoxicity has resulted in a novel class of DNA binders, the anthrapyrazoles. Their synthesis was carried out by a two-stage condensation sequence starting from requisite 1,4- or 1,5-dichloro-9,10-anthracenedione precursors. Reaction with a monoalkylhydrazine gave a chloroanthrapyrazole intermediate whose subsequent condensation with primary or secondary alkylamines provided the target "two-armed" anthrapyrazoles. A-ring 7,10-dihydroxy anthrapyrazoles were derived from amine condensation with intermediate 5-chloro-7,10-dihydroxyanthrapyrazoles or, alternatively, from intermediate 5-chloro-7,10-bis(benzyloxy)anthrapyrazoles followed by hydrogenolysis of the benzyl protecting groups to provide the target compounds. Potent in vitro activity was demonstrated against murine L1210 leukemia in vitro (IC50 = 10(-7)-10(-8) M) as well as against P388 leukemia in vivo over a wide range of structural variants. In general, activity against the P388 line was maximized by basic side chains at N-2 and C-5, two to three carbon spacers between proximal and distal nitrogens of the side chain, and A-ring hydroxylation. Besides having curative activity against the P388 line, the more active compounds were curative against murine B-16 melanoma in vivo. On the basis of their exceptional in vivo anticancer activity, A-ring dihydroxy compounds 71 and 74 reported in this study have been selected for development toward clinical trials.
Showalter HD, Johnson JL, Hoftiezer JM, Turner WR, Werbel LM, Leopold WR, Shillis JL, Jackson RC, Elslager EF.
10.1021/jm00384a021
null
121
1
J Med Chem
null
3,806,589
1
Anthrapyrazole anticancer agents. Synthesis and structure-activity relationships against murine leukemias.
30
1,987
null
38,130
CHEMBL758597
Optimal dose per injection in mg/kg required to inhibit growth of P388 leukemia cells in mice
F
BAO_0000218
organism-based format
CCCCCCNc1ccc2c3c(nn2CCN(CC)CC)-c2ccccc2C(=O)c13.Cl
null
CHEMBL1123657
J Med Chem
1,987
CHEMBL542321
null
null
0
null
35,153
=
1
1
=
DOSE
mg.kg-1
200
CHEMBL389
Mus musculus
P388
10090
null
Dose
mg kg-1
UO_0000308
200.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCCCCNc1ccc2c3c(nn2CCN(CC)CC)-c2ccccc2C(=O)c13.Cl
RDKit 2D 32 34 0 0 0 0 0 0 0 0999 V2000 5.4623 0.0000 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 1.0815 0.6692 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.3637 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.7762 1.5264 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.3637 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0488 1.5264 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.0815 -0.9808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3488 0.6692 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7940 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7940 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.5262 2.1992 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3488 -0.9808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0613 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0829 -1.8058 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.0613 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.1822 2.9491 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3488 -1.8058 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.6596 3.6219 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.5085 0.6692 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5085 -0.9808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4810 3.5449 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3155 4.3718 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0633 -2.2183 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0633 -3.0433 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4922 -4.6933 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.7778 -4.2808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.7778 -3.4558 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2230 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2230 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7929 5.0446 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 4.2178 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4922 -5.5183 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 3 1 0 2 4 2 0 3 5 2 0 4 6 1 0 5 7 1 0 3 8 1 0 6 8 1 0 2 9 1 0 7 10 1 0 9 10 1 0 6 11 1 0 5 12 1 0 8 13 2 0 7 14 2 0 12 15 2 0 13 15 1 0 11 16 1 0 12 17 1 0 16 18 1 0 9 19 2 0 10 20 2 0 18 21 1 0 18 22 1 0 17 23 1 0 23 24 1 0 25 26 1 0 24 27 1 0 26 27 1 0 20 28 1 0 19 29 1 0 28 29 2 0 22 30 1 0 21 31 1 0 25 32 1 0 M END > <chembl_id> CHEMBL542321 > <chembl_pref_name> None
InChI=1S/C26H34N4O.ClH/c1-4-7-8-11-16-27-21-14-15-22-24-23(21)26(31)20-13-10-9-12-19(20)25(24)28-30(22)18-17-29(5-2)6-3;/h9-10,12-15,27H,4-8,11,16-18H2,1-3H3;1H
KJLHRQLQYPIDIX-UHFFFAOYSA-N
5.58
3
C26H35ClN4O
455.05
5
1
31
418.59
-0.89
1
50.16
0.32
N
11
CHEMBL1191248
CHEMBL542321
CHEMBL1191248
null
null
null
P388
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000218
organism-based format
CHEMBL3308401
Target assigned is non-molecular
1
Optimal dose per injection in mg/kg required to inhibit growth of P388 leukemia cells in mice
CHEMBL1123657
Non-molecular target assigned
N
null
1
CHEMBL389
null
null
null
Mus musculus
P388
false
CELL-LINE
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Chromophore modification of the anthracenediones related to mitoxantrone in an attempt to provide agents with diminished or no cardiotoxicity has resulted in a novel class of DNA binders, the anthrapyrazoles. Their synthesis was carried out by a two-stage condensation sequence starting from requisite 1,4- or 1,5-dichloro-9,10-anthracenedione precursors. Reaction with a monoalkylhydrazine gave a chloroanthrapyrazole intermediate whose subsequent condensation with primary or secondary alkylamines provided the target "two-armed" anthrapyrazoles. A-ring 7,10-dihydroxy anthrapyrazoles were derived from amine condensation with intermediate 5-chloro-7,10-dihydroxyanthrapyrazoles or, alternatively, from intermediate 5-chloro-7,10-bis(benzyloxy)anthrapyrazoles followed by hydrogenolysis of the benzyl protecting groups to provide the target compounds. Potent in vitro activity was demonstrated against murine L1210 leukemia in vitro (IC50 = 10(-7)-10(-8) M) as well as against P388 leukemia in vivo over a wide range of structural variants. In general, activity against the P388 line was maximized by basic side chains at N-2 and C-5, two to three carbon spacers between proximal and distal nitrogens of the side chain, and A-ring hydroxylation. Besides having curative activity against the P388 line, the more active compounds were curative against murine B-16 melanoma in vivo. On the basis of their exceptional in vivo anticancer activity, A-ring dihydroxy compounds 71 and 74 reported in this study have been selected for development toward clinical trials.
Showalter HD, Johnson JL, Hoftiezer JM, Turner WR, Werbel LM, Leopold WR, Shillis JL, Jackson RC, Elslager EF.
10.1021/jm00384a021
null
121
1
J Med Chem
null
3,806,589
1
Anthrapyrazole anticancer agents. Synthesis and structure-activity relationships against murine leukemias.
30
1,987
null
38,131
CHEMBL762168
Activity against P388 leukemia cells in mice, by intraperitoneal dosing and net log tumor cell kill was reported
F
BAO_0000219
cell-based format
CCCCCCNc1ccc2c3c(nn2CCN(CC)CC)-c2ccccc2C(=O)c13.Cl
null
CHEMBL1123657
J Med Chem
1,987
CHEMBL542321
null
null
0
null
35,153
=
1
0
=
Activity
null
-1.4
CHEMBL389
Mus musculus
P388
10090
null
Activity
null
null
-1.4
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCCCCNc1ccc2c3c(nn2CCN(CC)CC)-c2ccccc2C(=O)c13.Cl
RDKit 2D 32 34 0 0 0 0 0 0 0 0999 V2000 5.4623 0.0000 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 1.0815 0.6692 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.3637 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.7762 1.5264 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.3637 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0488 1.5264 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.0815 -0.9808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3488 0.6692 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7940 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7940 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.5262 2.1992 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3488 -0.9808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0613 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0829 -1.8058 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.0613 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.1822 2.9491 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3488 -1.8058 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.6596 3.6219 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.5085 0.6692 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5085 -0.9808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4810 3.5449 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3155 4.3718 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0633 -2.2183 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0633 -3.0433 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4922 -4.6933 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.7778 -4.2808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.7778 -3.4558 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2230 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2230 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7929 5.0446 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 4.2178 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4922 -5.5183 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 3 1 0 2 4 2 0 3 5 2 0 4 6 1 0 5 7 1 0 3 8 1 0 6 8 1 0 2 9 1 0 7 10 1 0 9 10 1 0 6 11 1 0 5 12 1 0 8 13 2 0 7 14 2 0 12 15 2 0 13 15 1 0 11 16 1 0 12 17 1 0 16 18 1 0 9 19 2 0 10 20 2 0 18 21 1 0 18 22 1 0 17 23 1 0 23 24 1 0 25 26 1 0 24 27 1 0 26 27 1 0 20 28 1 0 19 29 1 0 28 29 2 0 22 30 1 0 21 31 1 0 25 32 1 0 M END > <chembl_id> CHEMBL542321 > <chembl_pref_name> None
InChI=1S/C26H34N4O.ClH/c1-4-7-8-11-16-27-21-14-15-22-24-23(21)26(31)20-13-10-9-12-19(20)25(24)28-30(22)18-17-29(5-2)6-3;/h9-10,12-15,27H,4-8,11,16-18H2,1-3H3;1H
KJLHRQLQYPIDIX-UHFFFAOYSA-N
5.58
3
C26H35ClN4O
455.05
5
1
31
418.59
-0.89
1
50.16
0.32
N
11
CHEMBL1191248
CHEMBL542321
CHEMBL1191248
null
null
null
P388
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000219
cell-based format
CHEMBL3308401
Target assigned is non-molecular
1
Activity against P388 leukemia cells in mice, by intraperitoneal dosing and net log tumor cell kill was reported
CHEMBL1123657
Non-molecular target assigned
N
null
1
CHEMBL389
null
null
null
Mus musculus
P388
false
CELL-LINE
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Chromophore modification of the anthracenediones related to mitoxantrone in an attempt to provide agents with diminished or no cardiotoxicity has resulted in a novel class of DNA binders, the anthrapyrazoles. Their synthesis was carried out by a two-stage condensation sequence starting from requisite 1,4- or 1,5-dichloro-9,10-anthracenedione precursors. Reaction with a monoalkylhydrazine gave a chloroanthrapyrazole intermediate whose subsequent condensation with primary or secondary alkylamines provided the target "two-armed" anthrapyrazoles. A-ring 7,10-dihydroxy anthrapyrazoles were derived from amine condensation with intermediate 5-chloro-7,10-dihydroxyanthrapyrazoles or, alternatively, from intermediate 5-chloro-7,10-bis(benzyloxy)anthrapyrazoles followed by hydrogenolysis of the benzyl protecting groups to provide the target compounds. Potent in vitro activity was demonstrated against murine L1210 leukemia in vitro (IC50 = 10(-7)-10(-8) M) as well as against P388 leukemia in vivo over a wide range of structural variants. In general, activity against the P388 line was maximized by basic side chains at N-2 and C-5, two to three carbon spacers between proximal and distal nitrogens of the side chain, and A-ring hydroxylation. Besides having curative activity against the P388 line, the more active compounds were curative against murine B-16 melanoma in vivo. On the basis of their exceptional in vivo anticancer activity, A-ring dihydroxy compounds 71 and 74 reported in this study have been selected for development toward clinical trials.
Showalter HD, Johnson JL, Hoftiezer JM, Turner WR, Werbel LM, Leopold WR, Shillis JL, Jackson RC, Elslager EF.
10.1021/jm00384a021
null
121
1
J Med Chem
null
3,806,589
1
Anthrapyrazole anticancer agents. Synthesis and structure-activity relationships against murine leukemias.
30
1,987
null
38,132
CHEMBL759554
Inhibition of P388 leukemia cells in mice, measured as percent treated to the control values with the number of 30 day survivors
F
BAO_0000219
cell-based format
CCCCCCNc1ccc2c3c(nn2CCN(CC)CC)-c2ccccc2C(=O)c13.Cl
null
CHEMBL1123657
J Med Chem
1,987
CHEMBL542321
null
null
0
http://qudt.org/vocab/unit#Percent
35,153
=
1
0
=
T/C
%
110
CHEMBL389
Mus musculus
P388
10090
null
T/C
%
UO_0000187
110.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
CCCCCCNc1ccc2c3c(nn2CCN(CC)CC)-c2ccccc2C(=O)c13.Cl
RDKit 2D 32 34 0 0 0 0 0 0 0 0999 V2000 5.4623 0.0000 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 1.0815 0.6692 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.3637 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.7762 1.5264 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.3637 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0488 1.5264 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.0815 -0.9808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3488 0.6692 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7940 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.7940 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.5262 2.1992 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3488 -0.9808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0613 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.0829 -1.8058 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.0613 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.1822 2.9491 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3488 -1.8058 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.6596 3.6219 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.5085 0.6692 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.5085 -0.9808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4810 3.5449 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.3155 4.3718 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0633 -2.2183 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.0633 -3.0433 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4922 -4.6933 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.7778 -4.2808 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.7778 -3.4558 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2230 -0.5683 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.2230 0.2567 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7929 5.0446 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.9583 4.2178 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.4922 -5.5183 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 3 1 0 2 4 2 0 3 5 2 0 4 6 1 0 5 7 1 0 3 8 1 0 6 8 1 0 2 9 1 0 7 10 1 0 9 10 1 0 6 11 1 0 5 12 1 0 8 13 2 0 7 14 2 0 12 15 2 0 13 15 1 0 11 16 1 0 12 17 1 0 16 18 1 0 9 19 2 0 10 20 2 0 18 21 1 0 18 22 1 0 17 23 1 0 23 24 1 0 25 26 1 0 24 27 1 0 26 27 1 0 20 28 1 0 19 29 1 0 28 29 2 0 22 30 1 0 21 31 1 0 25 32 1 0 M END > <chembl_id> CHEMBL542321 > <chembl_pref_name> None
InChI=1S/C26H34N4O.ClH/c1-4-7-8-11-16-27-21-14-15-22-24-23(21)26(31)20-13-10-9-12-19(20)25(24)28-30(22)18-17-29(5-2)6-3;/h9-10,12-15,27H,4-8,11,16-18H2,1-3H3;1H
KJLHRQLQYPIDIX-UHFFFAOYSA-N
5.58
3
C26H35ClN4O
455.05
5
1
31
418.59
-0.89
1
50.16
0.32
N
11
CHEMBL1191248
CHEMBL542321
CHEMBL1191248
null
null
null
P388
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000219
cell-based format
CHEMBL3308401
Target assigned is non-molecular
1
Inhibition of P388 leukemia cells in mice, measured as percent treated to the control values with the number of 30 day survivors
CHEMBL1123657
Non-molecular target assigned
N
null
1
CHEMBL389
null
null
null
Mus musculus
P388
false
CELL-LINE
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Chromophore modification of the anthracenediones related to mitoxantrone in an attempt to provide agents with diminished or no cardiotoxicity has resulted in a novel class of DNA binders, the anthrapyrazoles. Their synthesis was carried out by a two-stage condensation sequence starting from requisite 1,4- or 1,5-dichloro-9,10-anthracenedione precursors. Reaction with a monoalkylhydrazine gave a chloroanthrapyrazole intermediate whose subsequent condensation with primary or secondary alkylamines provided the target "two-armed" anthrapyrazoles. A-ring 7,10-dihydroxy anthrapyrazoles were derived from amine condensation with intermediate 5-chloro-7,10-dihydroxyanthrapyrazoles or, alternatively, from intermediate 5-chloro-7,10-bis(benzyloxy)anthrapyrazoles followed by hydrogenolysis of the benzyl protecting groups to provide the target compounds. Potent in vitro activity was demonstrated against murine L1210 leukemia in vitro (IC50 = 10(-7)-10(-8) M) as well as against P388 leukemia in vivo over a wide range of structural variants. In general, activity against the P388 line was maximized by basic side chains at N-2 and C-5, two to three carbon spacers between proximal and distal nitrogens of the side chain, and A-ring hydroxylation. Besides having curative activity against the P388 line, the more active compounds were curative against murine B-16 melanoma in vivo. On the basis of their exceptional in vivo anticancer activity, A-ring dihydroxy compounds 71 and 74 reported in this study have been selected for development toward clinical trials.
Showalter HD, Johnson JL, Hoftiezer JM, Turner WR, Werbel LM, Leopold WR, Shillis JL, Jackson RC, Elslager EF.
10.1021/jm00384a021
null
121
1
J Med Chem
null
3,806,589
1
Anthrapyrazole anticancer agents. Synthesis and structure-activity relationships against murine leukemias.
30
1,987
null
38,133
CHEMBL706332
Tested in vitro against murine L1210 leukemia.
F
BAO_0000219
cell-based format
Br.CCN(CC)CCn1nc2c3c(c(NCCNC)ccc31)C(=O)c1c(O)ccc(O)c1-2
null
CHEMBL1123657
J Med Chem
1,987
CHEMBL543035
null
5.13
0
http://www.openphacts.org/units/Nanomolar
35,168
=
1
1
=
IC50
nM
7,400
CHEMBL386
Mus musculus
L1210
10090
null
IC50
M
UO_0000065
0.0000074
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
Br.CCN(CC)CCn1nc2c3c(c(NCCNC)ccc31)C(=O)c1c(O)ccc(O)c1-2
RDKit 2D 32 34 0 0 0 0 0 0 0 0999 V2000 8.5875 -2.1500 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 3.4500 -2.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9542 -2.6667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.4417 -1.8042 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.9500 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9542 -3.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.9500 -3.2625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.4542 -3.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4500 -1.8000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.4542 -2.3750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9667 -1.4917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4667 -3.5417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4417 -2.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4417 -3.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -2.6625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.4542 -4.1250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.9667 -3.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.9500 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.9500 -3.2625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9625 -0.8917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4667 -4.1250 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4792 -0.5875 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.4417 -4.1500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.4417 -1.7875 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.7792 -5.5500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4750 0.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.0042 -0.8875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0417 -4.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 -5.1250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9417 -6.1292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 0.3083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.0042 -1.4875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 2 1 0 4 2 2 0 5 2 1 0 6 3 2 0 7 5 1 0 8 7 1 0 9 4 1 0 10 3 1 0 11 9 1 0 12 6 1 0 13 5 2 0 14 7 2 0 15 10 2 0 16 8 2 0 17 15 1 0 18 13 1 0 19 18 2 0 20 11 1 0 21 12 1 0 22 20 1 0 23 14 1 0 24 13 1 0 25 29 1 0 26 22 1 0 27 22 1 0 28 21 1 0 29 28 1 0 30 25 1 0 31 26 1 0 32 27 1 0 9 10 1 0 6 8 1 0 14 19 1 0 12 17 2 0 M END > <chembl_id> CHEMBL543035 > <chembl_pref_name> None
InChI=1S/C23H29N5O3.BrH/c1-4-27(5-2)12-13-28-15-7-6-14(25-11-10-24-3)18-19(15)22(26-28)20-16(29)8-9-17(30)21(20)23(18)31;/h6-9,24-25,29-30H,4-5,10-13H2,1-3H3;1H
COCDUXBIESOLCR-UHFFFAOYSA-N
2.63
3
C23H30BrN5O3
504.43
8
4
31
423.52
-0.47
0
102.65
0.24
N
9
CHEMBL1191878
CHEMBL543035
CHEMBL1191878
null
null
null
L1210
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000219
cell-based format
CHEMBL3308391
Target assigned is non-molecular
1
Tested in vitro against murine L1210 leukemia.
CHEMBL1123657
Non-molecular target assigned
N
null
1
CHEMBL386
null
null
null
Mus musculus
L1210
false
CELL-LINE
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Chromophore modification of the anthracenediones related to mitoxantrone in an attempt to provide agents with diminished or no cardiotoxicity has resulted in a novel class of DNA binders, the anthrapyrazoles. Their synthesis was carried out by a two-stage condensation sequence starting from requisite 1,4- or 1,5-dichloro-9,10-anthracenedione precursors. Reaction with a monoalkylhydrazine gave a chloroanthrapyrazole intermediate whose subsequent condensation with primary or secondary alkylamines provided the target "two-armed" anthrapyrazoles. A-ring 7,10-dihydroxy anthrapyrazoles were derived from amine condensation with intermediate 5-chloro-7,10-dihydroxyanthrapyrazoles or, alternatively, from intermediate 5-chloro-7,10-bis(benzyloxy)anthrapyrazoles followed by hydrogenolysis of the benzyl protecting groups to provide the target compounds. Potent in vitro activity was demonstrated against murine L1210 leukemia in vitro (IC50 = 10(-7)-10(-8) M) as well as against P388 leukemia in vivo over a wide range of structural variants. In general, activity against the P388 line was maximized by basic side chains at N-2 and C-5, two to three carbon spacers between proximal and distal nitrogens of the side chain, and A-ring hydroxylation. Besides having curative activity against the P388 line, the more active compounds were curative against murine B-16 melanoma in vivo. On the basis of their exceptional in vivo anticancer activity, A-ring dihydroxy compounds 71 and 74 reported in this study have been selected for development toward clinical trials.
Showalter HD, Johnson JL, Hoftiezer JM, Turner WR, Werbel LM, Leopold WR, Shillis JL, Jackson RC, Elslager EF.
10.1021/jm00384a021
null
121
1
J Med Chem
null
3,806,589
1
Anthrapyrazole anticancer agents. Synthesis and structure-activity relationships against murine leukemias.
30
1,987
null
38,134
CHEMBL758597
Optimal dose per injection in mg/kg required to inhibit growth of P388 leukemia cells in mice
F
BAO_0000218
organism-based format
Br.CCN(CC)CCn1nc2c3c(c(NCCNC)ccc31)C(=O)c1c(O)ccc(O)c1-2
null
CHEMBL1123657
J Med Chem
1,987
CHEMBL543035
null
null
0
null
35,168
=
1
1
=
DOSE
mg.kg-1
25
CHEMBL389
Mus musculus
P388
10090
null
Dose
mg kg-1
UO_0000308
25.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
Br.CCN(CC)CCn1nc2c3c(c(NCCNC)ccc31)C(=O)c1c(O)ccc(O)c1-2
RDKit 2D 32 34 0 0 0 0 0 0 0 0999 V2000 8.5875 -2.1500 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 3.4500 -2.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9542 -2.6667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.4417 -1.8042 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.9500 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9542 -3.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.9500 -3.2625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.4542 -3.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4500 -1.8000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.4542 -2.3750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9667 -1.4917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4667 -3.5417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4417 -2.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4417 -3.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -2.6625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.4542 -4.1250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.9667 -3.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.9500 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.9500 -3.2625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9625 -0.8917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4667 -4.1250 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4792 -0.5875 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.4417 -4.1500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.4417 -1.7875 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.7792 -5.5500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4750 0.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.0042 -0.8875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0417 -4.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 -5.1250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9417 -6.1292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 0.3083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.0042 -1.4875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 2 1 0 4 2 2 0 5 2 1 0 6 3 2 0 7 5 1 0 8 7 1 0 9 4 1 0 10 3 1 0 11 9 1 0 12 6 1 0 13 5 2 0 14 7 2 0 15 10 2 0 16 8 2 0 17 15 1 0 18 13 1 0 19 18 2 0 20 11 1 0 21 12 1 0 22 20 1 0 23 14 1 0 24 13 1 0 25 29 1 0 26 22 1 0 27 22 1 0 28 21 1 0 29 28 1 0 30 25 1 0 31 26 1 0 32 27 1 0 9 10 1 0 6 8 1 0 14 19 1 0 12 17 2 0 M END > <chembl_id> CHEMBL543035 > <chembl_pref_name> None
InChI=1S/C23H29N5O3.BrH/c1-4-27(5-2)12-13-28-15-7-6-14(25-11-10-24-3)18-19(15)22(26-28)20-16(29)8-9-17(30)21(20)23(18)31;/h6-9,24-25,29-30H,4-5,10-13H2,1-3H3;1H
COCDUXBIESOLCR-UHFFFAOYSA-N
2.63
3
C23H30BrN5O3
504.43
8
4
31
423.52
-0.47
0
102.65
0.24
N
9
CHEMBL1191878
CHEMBL543035
CHEMBL1191878
null
null
null
P388
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000218
organism-based format
CHEMBL3308401
Target assigned is non-molecular
1
Optimal dose per injection in mg/kg required to inhibit growth of P388 leukemia cells in mice
CHEMBL1123657
Non-molecular target assigned
N
null
1
CHEMBL389
null
null
null
Mus musculus
P388
false
CELL-LINE
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Chromophore modification of the anthracenediones related to mitoxantrone in an attempt to provide agents with diminished or no cardiotoxicity has resulted in a novel class of DNA binders, the anthrapyrazoles. Their synthesis was carried out by a two-stage condensation sequence starting from requisite 1,4- or 1,5-dichloro-9,10-anthracenedione precursors. Reaction with a monoalkylhydrazine gave a chloroanthrapyrazole intermediate whose subsequent condensation with primary or secondary alkylamines provided the target "two-armed" anthrapyrazoles. A-ring 7,10-dihydroxy anthrapyrazoles were derived from amine condensation with intermediate 5-chloro-7,10-dihydroxyanthrapyrazoles or, alternatively, from intermediate 5-chloro-7,10-bis(benzyloxy)anthrapyrazoles followed by hydrogenolysis of the benzyl protecting groups to provide the target compounds. Potent in vitro activity was demonstrated against murine L1210 leukemia in vitro (IC50 = 10(-7)-10(-8) M) as well as against P388 leukemia in vivo over a wide range of structural variants. In general, activity against the P388 line was maximized by basic side chains at N-2 and C-5, two to three carbon spacers between proximal and distal nitrogens of the side chain, and A-ring hydroxylation. Besides having curative activity against the P388 line, the more active compounds were curative against murine B-16 melanoma in vivo. On the basis of their exceptional in vivo anticancer activity, A-ring dihydroxy compounds 71 and 74 reported in this study have been selected for development toward clinical trials.
Showalter HD, Johnson JL, Hoftiezer JM, Turner WR, Werbel LM, Leopold WR, Shillis JL, Jackson RC, Elslager EF.
10.1021/jm00384a021
null
121
1
J Med Chem
null
3,806,589
1
Anthrapyrazole anticancer agents. Synthesis and structure-activity relationships against murine leukemias.
30
1,987
null
38,136
CHEMBL759554
Inhibition of P388 leukemia cells in mice, measured as percent treated to the control values with the number of 30 day survivors
F
BAO_0000219
cell-based format
Br.CCN(CC)CCn1nc2c3c(c(NCCNC)ccc31)C(=O)c1c(O)ccc(O)c1-2
null
CHEMBL1123657
J Med Chem
1,987
CHEMBL543035
null
null
0
http://qudt.org/vocab/unit#Percent
35,168
=
1
0
=
T/C
%
219
CHEMBL389
Mus musculus
P388
10090
null
T/C
%
UO_0000187
219.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
Br.CCN(CC)CCn1nc2c3c(c(NCCNC)ccc31)C(=O)c1c(O)ccc(O)c1-2
RDKit 2D 32 34 0 0 0 0 0 0 0 0999 V2000 8.5875 -2.1500 0.0000 Br 0 0 0 0 0 0 0 0 0 0 0 0 3.4500 -2.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9542 -2.6667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.4417 -1.8042 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.9500 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9542 -3.2542 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.9500 -3.2625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.4542 -3.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4500 -1.8000 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 4.4542 -2.3750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9667 -1.4917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4667 -3.5417 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4417 -2.3875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.4417 -3.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 -2.6625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.4542 -4.1250 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 4.9667 -3.2500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.9500 -2.6750 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.9500 -3.2625 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9625 -0.8917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.4667 -4.1250 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4792 -0.5875 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.4417 -4.1500 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.4417 -1.7875 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 3.7792 -5.5500 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4750 0.0125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.0042 -0.8875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.0417 -4.5500 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.2042 -5.1250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.9417 -6.1292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.9542 0.3083 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.0042 -1.4875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3 2 1 0 4 2 2 0 5 2 1 0 6 3 2 0 7 5 1 0 8 7 1 0 9 4 1 0 10 3 1 0 11 9 1 0 12 6 1 0 13 5 2 0 14 7 2 0 15 10 2 0 16 8 2 0 17 15 1 0 18 13 1 0 19 18 2 0 20 11 1 0 21 12 1 0 22 20 1 0 23 14 1 0 24 13 1 0 25 29 1 0 26 22 1 0 27 22 1 0 28 21 1 0 29 28 1 0 30 25 1 0 31 26 1 0 32 27 1 0 9 10 1 0 6 8 1 0 14 19 1 0 12 17 2 0 M END > <chembl_id> CHEMBL543035 > <chembl_pref_name> None
InChI=1S/C23H29N5O3.BrH/c1-4-27(5-2)12-13-28-15-7-6-14(25-11-10-24-3)18-19(15)22(26-28)20-16(29)8-9-17(30)21(20)23(18)31;/h6-9,24-25,29-30H,4-5,10-13H2,1-3H3;1H
COCDUXBIESOLCR-UHFFFAOYSA-N
2.63
3
C23H30BrN5O3
504.43
8
4
31
423.52
-0.47
0
102.65
0.24
N
9
CHEMBL1191878
CHEMBL543035
CHEMBL1191878
null
null
null
P388
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000219
cell-based format
CHEMBL3308401
Target assigned is non-molecular
1
Inhibition of P388 leukemia cells in mice, measured as percent treated to the control values with the number of 30 day survivors
CHEMBL1123657
Non-molecular target assigned
N
null
1
CHEMBL389
null
null
null
Mus musculus
P388
false
CELL-LINE
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Chromophore modification of the anthracenediones related to mitoxantrone in an attempt to provide agents with diminished or no cardiotoxicity has resulted in a novel class of DNA binders, the anthrapyrazoles. Their synthesis was carried out by a two-stage condensation sequence starting from requisite 1,4- or 1,5-dichloro-9,10-anthracenedione precursors. Reaction with a monoalkylhydrazine gave a chloroanthrapyrazole intermediate whose subsequent condensation with primary or secondary alkylamines provided the target "two-armed" anthrapyrazoles. A-ring 7,10-dihydroxy anthrapyrazoles were derived from amine condensation with intermediate 5-chloro-7,10-dihydroxyanthrapyrazoles or, alternatively, from intermediate 5-chloro-7,10-bis(benzyloxy)anthrapyrazoles followed by hydrogenolysis of the benzyl protecting groups to provide the target compounds. Potent in vitro activity was demonstrated against murine L1210 leukemia in vitro (IC50 = 10(-7)-10(-8) M) as well as against P388 leukemia in vivo over a wide range of structural variants. In general, activity against the P388 line was maximized by basic side chains at N-2 and C-5, two to three carbon spacers between proximal and distal nitrogens of the side chain, and A-ring hydroxylation. Besides having curative activity against the P388 line, the more active compounds were curative against murine B-16 melanoma in vivo. On the basis of their exceptional in vivo anticancer activity, A-ring dihydroxy compounds 71 and 74 reported in this study have been selected for development toward clinical trials.
Showalter HD, Johnson JL, Hoftiezer JM, Turner WR, Werbel LM, Leopold WR, Shillis JL, Jackson RC, Elslager EF.
10.1021/jm00384a021
null
121
1
J Med Chem
null
3,806,589
1
Anthrapyrazole anticancer agents. Synthesis and structure-activity relationships against murine leukemias.
30
1,987
null
38,137
CHEMBL706332
Tested in vitro against murine L1210 leukemia.
F
BAO_0000219
cell-based format
Cl.O=C1c2c(NCCNCCO)cccc2-c2nn(CCNCCO)c3cccc1c23
null
CHEMBL1123657
J Med Chem
1,987
CHEMBL545155
null
6.41
0
http://www.openphacts.org/units/Nanomolar
35,158
=
1
1
=
IC50
nM
390
CHEMBL386
Mus musculus
L1210
10090
null
IC50
M
UO_0000065
3.9E-7
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
Cl.O=C1c2c(NCCNCCO)cccc2-c2nn(CCNCCO)c3cccc1c23
RDKit 2D 31 33 0 0 0 0 0 0 0 0999 V2000 5.0455 0.0000 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 0.6648 0.9829 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.3594 1.8400 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.0531 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6648 -0.6671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4656 1.8400 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0531 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7656 0.9829 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 -0.6671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6661 -1.4921 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.9430 2.5129 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 -1.4921 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.7656 -0.6671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 0.9829 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.2418 3.1087 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.6628 -3.1421 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.4781 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4781 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.3619 3.6276 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.0517 -5.2046 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.8062 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.7644 2.4359 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8062 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 -1.9046 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 -2.7296 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6628 -3.9671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.0632 3.0318 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0517 -4.3796 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.5405 3.7046 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 3 2 0 2 4 1 0 3 6 1 0 5 7 1 0 4 8 2 0 5 8 1 0 2 9 1 0 7 9 1 0 4 10 1 0 6 10 1 0 7 11 2 0 5 12 2 0 6 13 1 0 11 14 1 0 8 15 1 0 9 16 2 0 10 19 2 0 15 20 2 0 19 20 1 0 16 23 1 0 13 24 1 0 17 24 1 0 11 25 1 0 23 25 2 0 14 26 1 0 18 27 1 0 26 27 1 0 18 28 1 0 17 29 1 0 22 30 1 0 28 30 1 0 21 31 1 0 29 31 1 0 M END > <chembl_id> CHEMBL545155 > <chembl_pref_name> None
InChI=1S/C22H27N5O3.ClH/c28-13-10-23-7-8-25-17-5-1-3-15-19(17)22(30)16-4-2-6-18-20(16)21(15)26-27(18)12-9-24-11-14-29;/h1-6,23-25,28-29H,7-14H2;1H
HRMOIPHLLBLBBJ-UHFFFAOYSA-N
0.82
3
C22H28ClN5O3
445.95
8
5
30
409.49
-0.66
0
111.44
0.23
N
11
CHEMBL1193703
CHEMBL545155
CHEMBL1193703
null
null
null
L1210
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000219
cell-based format
CHEMBL3308391
Target assigned is non-molecular
1
Tested in vitro against murine L1210 leukemia.
CHEMBL1123657
Non-molecular target assigned
N
null
1
CHEMBL386
null
null
null
Mus musculus
L1210
false
CELL-LINE
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Chromophore modification of the anthracenediones related to mitoxantrone in an attempt to provide agents with diminished or no cardiotoxicity has resulted in a novel class of DNA binders, the anthrapyrazoles. Their synthesis was carried out by a two-stage condensation sequence starting from requisite 1,4- or 1,5-dichloro-9,10-anthracenedione precursors. Reaction with a monoalkylhydrazine gave a chloroanthrapyrazole intermediate whose subsequent condensation with primary or secondary alkylamines provided the target "two-armed" anthrapyrazoles. A-ring 7,10-dihydroxy anthrapyrazoles were derived from amine condensation with intermediate 5-chloro-7,10-dihydroxyanthrapyrazoles or, alternatively, from intermediate 5-chloro-7,10-bis(benzyloxy)anthrapyrazoles followed by hydrogenolysis of the benzyl protecting groups to provide the target compounds. Potent in vitro activity was demonstrated against murine L1210 leukemia in vitro (IC50 = 10(-7)-10(-8) M) as well as against P388 leukemia in vivo over a wide range of structural variants. In general, activity against the P388 line was maximized by basic side chains at N-2 and C-5, two to three carbon spacers between proximal and distal nitrogens of the side chain, and A-ring hydroxylation. Besides having curative activity against the P388 line, the more active compounds were curative against murine B-16 melanoma in vivo. On the basis of their exceptional in vivo anticancer activity, A-ring dihydroxy compounds 71 and 74 reported in this study have been selected for development toward clinical trials.
Showalter HD, Johnson JL, Hoftiezer JM, Turner WR, Werbel LM, Leopold WR, Shillis JL, Jackson RC, Elslager EF.
10.1021/jm00384a021
null
121
1
J Med Chem
null
3,806,589
1
Anthrapyrazole anticancer agents. Synthesis and structure-activity relationships against murine leukemias.
30
1,987
null
38,138
CHEMBL758597
Optimal dose per injection in mg/kg required to inhibit growth of P388 leukemia cells in mice
F
BAO_0000218
organism-based format
Cl.O=C1c2c(NCCNCCO)cccc2-c2nn(CCNCCO)c3cccc1c23
null
CHEMBL1123657
J Med Chem
1,987
CHEMBL545155
null
null
0
null
35,158
=
1
1
=
DOSE
mg.kg-1
12.5
CHEMBL389
Mus musculus
P388
10090
null
Dose
mg kg-1
UO_0000308
12.5
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
Cl.O=C1c2c(NCCNCCO)cccc2-c2nn(CCNCCO)c3cccc1c23
RDKit 2D 31 33 0 0 0 0 0 0 0 0999 V2000 5.0455 0.0000 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 0.6648 0.9829 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.3594 1.8400 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.0531 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6648 -0.6671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4656 1.8400 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0531 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7656 0.9829 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 -0.6671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6661 -1.4921 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.9430 2.5129 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 -1.4921 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.7656 -0.6671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 0.9829 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.2418 3.1087 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.6628 -3.1421 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.4781 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4781 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.3619 3.6276 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.0517 -5.2046 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.8062 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.7644 2.4359 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8062 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 -1.9046 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 -2.7296 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6628 -3.9671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.0632 3.0318 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0517 -4.3796 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.5405 3.7046 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 3 2 0 2 4 1 0 3 6 1 0 5 7 1 0 4 8 2 0 5 8 1 0 2 9 1 0 7 9 1 0 4 10 1 0 6 10 1 0 7 11 2 0 5 12 2 0 6 13 1 0 11 14 1 0 8 15 1 0 9 16 2 0 10 19 2 0 15 20 2 0 19 20 1 0 16 23 1 0 13 24 1 0 17 24 1 0 11 25 1 0 23 25 2 0 14 26 1 0 18 27 1 0 26 27 1 0 18 28 1 0 17 29 1 0 22 30 1 0 28 30 1 0 21 31 1 0 29 31 1 0 M END > <chembl_id> CHEMBL545155 > <chembl_pref_name> None
InChI=1S/C22H27N5O3.ClH/c28-13-10-23-7-8-25-17-5-1-3-15-19(17)22(30)16-4-2-6-18-20(16)21(15)26-27(18)12-9-24-11-14-29;/h1-6,23-25,28-29H,7-14H2;1H
HRMOIPHLLBLBBJ-UHFFFAOYSA-N
0.82
3
C22H28ClN5O3
445.95
8
5
30
409.49
-0.66
0
111.44
0.23
N
11
CHEMBL1193703
CHEMBL545155
CHEMBL1193703
null
null
null
P388
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000218
organism-based format
CHEMBL3308401
Target assigned is non-molecular
1
Optimal dose per injection in mg/kg required to inhibit growth of P388 leukemia cells in mice
CHEMBL1123657
Non-molecular target assigned
N
null
1
CHEMBL389
null
null
null
Mus musculus
P388
false
CELL-LINE
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Chromophore modification of the anthracenediones related to mitoxantrone in an attempt to provide agents with diminished or no cardiotoxicity has resulted in a novel class of DNA binders, the anthrapyrazoles. Their synthesis was carried out by a two-stage condensation sequence starting from requisite 1,4- or 1,5-dichloro-9,10-anthracenedione precursors. Reaction with a monoalkylhydrazine gave a chloroanthrapyrazole intermediate whose subsequent condensation with primary or secondary alkylamines provided the target "two-armed" anthrapyrazoles. A-ring 7,10-dihydroxy anthrapyrazoles were derived from amine condensation with intermediate 5-chloro-7,10-dihydroxyanthrapyrazoles or, alternatively, from intermediate 5-chloro-7,10-bis(benzyloxy)anthrapyrazoles followed by hydrogenolysis of the benzyl protecting groups to provide the target compounds. Potent in vitro activity was demonstrated against murine L1210 leukemia in vitro (IC50 = 10(-7)-10(-8) M) as well as against P388 leukemia in vivo over a wide range of structural variants. In general, activity against the P388 line was maximized by basic side chains at N-2 and C-5, two to three carbon spacers between proximal and distal nitrogens of the side chain, and A-ring hydroxylation. Besides having curative activity against the P388 line, the more active compounds were curative against murine B-16 melanoma in vivo. On the basis of their exceptional in vivo anticancer activity, A-ring dihydroxy compounds 71 and 74 reported in this study have been selected for development toward clinical trials.
Showalter HD, Johnson JL, Hoftiezer JM, Turner WR, Werbel LM, Leopold WR, Shillis JL, Jackson RC, Elslager EF.
10.1021/jm00384a021
null
121
1
J Med Chem
null
3,806,589
1
Anthrapyrazole anticancer agents. Synthesis and structure-activity relationships against murine leukemias.
30
1,987
null
38,139
CHEMBL762168
Activity against P388 leukemia cells in mice, by intraperitoneal dosing and net log tumor cell kill was reported
F
BAO_0000219
cell-based format
Cl.O=C1c2c(NCCNCCO)cccc2-c2nn(CCNCCO)c3cccc1c23
null
CHEMBL1123657
J Med Chem
1,987
CHEMBL545155
null
null
0
null
35,158
=
1
0
=
Activity
null
-0.3
CHEMBL389
Mus musculus
P388
10090
null
Activity
null
null
-0.3
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
Cl.O=C1c2c(NCCNCCO)cccc2-c2nn(CCNCCO)c3cccc1c23
RDKit 2D 31 33 0 0 0 0 0 0 0 0999 V2000 5.0455 0.0000 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 0.6648 0.9829 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.3594 1.8400 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.0531 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6648 -0.6671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4656 1.8400 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0531 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7656 0.9829 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 -0.6671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6661 -1.4921 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.9430 2.5129 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 -1.4921 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.7656 -0.6671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 0.9829 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.2418 3.1087 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.6628 -3.1421 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.4781 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4781 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.3619 3.6276 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.0517 -5.2046 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.8062 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.7644 2.4359 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8062 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 -1.9046 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 -2.7296 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6628 -3.9671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.0632 3.0318 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0517 -4.3796 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.5405 3.7046 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 3 2 0 2 4 1 0 3 6 1 0 5 7 1 0 4 8 2 0 5 8 1 0 2 9 1 0 7 9 1 0 4 10 1 0 6 10 1 0 7 11 2 0 5 12 2 0 6 13 1 0 11 14 1 0 8 15 1 0 9 16 2 0 10 19 2 0 15 20 2 0 19 20 1 0 16 23 1 0 13 24 1 0 17 24 1 0 11 25 1 0 23 25 2 0 14 26 1 0 18 27 1 0 26 27 1 0 18 28 1 0 17 29 1 0 22 30 1 0 28 30 1 0 21 31 1 0 29 31 1 0 M END > <chembl_id> CHEMBL545155 > <chembl_pref_name> None
InChI=1S/C22H27N5O3.ClH/c28-13-10-23-7-8-25-17-5-1-3-15-19(17)22(30)16-4-2-6-18-20(16)21(15)26-27(18)12-9-24-11-14-29;/h1-6,23-25,28-29H,7-14H2;1H
HRMOIPHLLBLBBJ-UHFFFAOYSA-N
0.82
3
C22H28ClN5O3
445.95
8
5
30
409.49
-0.66
0
111.44
0.23
N
11
CHEMBL1193703
CHEMBL545155
CHEMBL1193703
null
null
null
P388
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000219
cell-based format
CHEMBL3308401
Target assigned is non-molecular
1
Activity against P388 leukemia cells in mice, by intraperitoneal dosing and net log tumor cell kill was reported
CHEMBL1123657
Non-molecular target assigned
N
null
1
CHEMBL389
null
null
null
Mus musculus
P388
false
CELL-LINE
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Chromophore modification of the anthracenediones related to mitoxantrone in an attempt to provide agents with diminished or no cardiotoxicity has resulted in a novel class of DNA binders, the anthrapyrazoles. Their synthesis was carried out by a two-stage condensation sequence starting from requisite 1,4- or 1,5-dichloro-9,10-anthracenedione precursors. Reaction with a monoalkylhydrazine gave a chloroanthrapyrazole intermediate whose subsequent condensation with primary or secondary alkylamines provided the target "two-armed" anthrapyrazoles. A-ring 7,10-dihydroxy anthrapyrazoles were derived from amine condensation with intermediate 5-chloro-7,10-dihydroxyanthrapyrazoles or, alternatively, from intermediate 5-chloro-7,10-bis(benzyloxy)anthrapyrazoles followed by hydrogenolysis of the benzyl protecting groups to provide the target compounds. Potent in vitro activity was demonstrated against murine L1210 leukemia in vitro (IC50 = 10(-7)-10(-8) M) as well as against P388 leukemia in vivo over a wide range of structural variants. In general, activity against the P388 line was maximized by basic side chains at N-2 and C-5, two to three carbon spacers between proximal and distal nitrogens of the side chain, and A-ring hydroxylation. Besides having curative activity against the P388 line, the more active compounds were curative against murine B-16 melanoma in vivo. On the basis of their exceptional in vivo anticancer activity, A-ring dihydroxy compounds 71 and 74 reported in this study have been selected for development toward clinical trials.
Showalter HD, Johnson JL, Hoftiezer JM, Turner WR, Werbel LM, Leopold WR, Shillis JL, Jackson RC, Elslager EF.
10.1021/jm00384a021
null
121
1
J Med Chem
null
3,806,589
1
Anthrapyrazole anticancer agents. Synthesis and structure-activity relationships against murine leukemias.
30
1,987
null
38,140
CHEMBL759554
Inhibition of P388 leukemia cells in mice, measured as percent treated to the control values with the number of 30 day survivors
F
BAO_0000219
cell-based format
Cl.O=C1c2c(NCCNCCO)cccc2-c2nn(CCNCCO)c3cccc1c23
null
CHEMBL1123657
J Med Chem
1,987
CHEMBL545155
null
null
0
http://qudt.org/vocab/unit#Percent
35,158
=
1
0
=
T/C
%
133
CHEMBL389
Mus musculus
P388
10090
null
T/C
%
UO_0000187
133.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
Cl.O=C1c2c(NCCNCCO)cccc2-c2nn(CCNCCO)c3cccc1c23
RDKit 2D 31 33 0 0 0 0 0 0 0 0999 V2000 5.0455 0.0000 0.0000 Cl 0 0 0 0 0 0 0 0 0 0 0 0 0.6648 0.9829 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.3594 1.8400 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.0531 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6648 -0.6671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.4656 1.8400 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0531 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.7656 0.9829 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 -0.6671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6661 -1.4921 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.9430 2.5129 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 -1.4921 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.7656 -0.6671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.0917 0.9829 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.2418 3.1087 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.6628 -3.1421 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 -1.4781 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.4781 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -4.3619 3.6276 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 -0.0517 -5.2046 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.8062 0.5704 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -1.7644 2.4359 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.8062 -0.2546 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 -1.9046 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.3773 -2.7296 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 0.6628 -3.9671 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.0632 3.0318 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.0517 -4.3796 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.5405 3.7046 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 3 2 0 2 4 1 0 3 6 1 0 5 7 1 0 4 8 2 0 5 8 1 0 2 9 1 0 7 9 1 0 4 10 1 0 6 10 1 0 7 11 2 0 5 12 2 0 6 13 1 0 11 14 1 0 8 15 1 0 9 16 2 0 10 19 2 0 15 20 2 0 19 20 1 0 16 23 1 0 13 24 1 0 17 24 1 0 11 25 1 0 23 25 2 0 14 26 1 0 18 27 1 0 26 27 1 0 18 28 1 0 17 29 1 0 22 30 1 0 28 30 1 0 21 31 1 0 29 31 1 0 M END > <chembl_id> CHEMBL545155 > <chembl_pref_name> None
InChI=1S/C22H27N5O3.ClH/c28-13-10-23-7-8-25-17-5-1-3-15-19(17)22(30)16-4-2-6-18-20(16)21(15)26-27(18)12-9-24-11-14-29;/h1-6,23-25,28-29H,7-14H2;1H
HRMOIPHLLBLBBJ-UHFFFAOYSA-N
0.82
3
C22H28ClN5O3
445.95
8
5
30
409.49
-0.66
0
111.44
0.23
N
11
CHEMBL1193703
CHEMBL545155
CHEMBL1193703
null
null
null
P388
Mus musculus
null
null
10,090
null
F
Functional
BAO_0000219
cell-based format
CHEMBL3308401
Target assigned is non-molecular
1
Inhibition of P388 leukemia cells in mice, measured as percent treated to the control values with the number of 30 day survivors
CHEMBL1123657
Non-molecular target assigned
N
null
1
CHEMBL389
null
null
null
Mus musculus
P388
false
CELL-LINE
10,090
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
Chromophore modification of the anthracenediones related to mitoxantrone in an attempt to provide agents with diminished or no cardiotoxicity has resulted in a novel class of DNA binders, the anthrapyrazoles. Their synthesis was carried out by a two-stage condensation sequence starting from requisite 1,4- or 1,5-dichloro-9,10-anthracenedione precursors. Reaction with a monoalkylhydrazine gave a chloroanthrapyrazole intermediate whose subsequent condensation with primary or secondary alkylamines provided the target "two-armed" anthrapyrazoles. A-ring 7,10-dihydroxy anthrapyrazoles were derived from amine condensation with intermediate 5-chloro-7,10-dihydroxyanthrapyrazoles or, alternatively, from intermediate 5-chloro-7,10-bis(benzyloxy)anthrapyrazoles followed by hydrogenolysis of the benzyl protecting groups to provide the target compounds. Potent in vitro activity was demonstrated against murine L1210 leukemia in vitro (IC50 = 10(-7)-10(-8) M) as well as against P388 leukemia in vivo over a wide range of structural variants. In general, activity against the P388 line was maximized by basic side chains at N-2 and C-5, two to three carbon spacers between proximal and distal nitrogens of the side chain, and A-ring hydroxylation. Besides having curative activity against the P388 line, the more active compounds were curative against murine B-16 melanoma in vivo. On the basis of their exceptional in vivo anticancer activity, A-ring dihydroxy compounds 71 and 74 reported in this study have been selected for development toward clinical trials.
Showalter HD, Johnson JL, Hoftiezer JM, Turner WR, Werbel LM, Leopold WR, Shillis JL, Jackson RC, Elslager EF.
10.1021/jm00384a021
null
121
1
J Med Chem
null
3,806,589
1
Anthrapyrazole anticancer agents. Synthesis and structure-activity relationships against murine leukemias.
30
1,987
null
38,141
CHEMBL740648
Nematocidal activity against Nematospiroides dubius induced necropsy in mouse, oral administration 200 mg/kg
F
BAO_0000218
organism-based format
COc1ccc(N/C(=N/c2cccc(C3CN4CCSC4=N3)c2)SC)cc1
null
CHEMBL1123619
J Med Chem
1,987
CHEMBL54651
null
null
0
http://qudt.org/vocab/unit#Percent
91,483
=
1
0
=
Reduction
%
0
CHEMBL612662
Heligmosomoides polygyrus
Heligmosomoides polygyrus
6339
null
Reduction
%
UO_0000187
0.0
null
null
null
null
-1
0
-1
null
null
-1
null
Small molecule
0
false
false
0
null
-1
MOL
false
false
null
null
false
COc1ccc(N/C(=N/c2cccc(C3CN4CCSC4=N3)c2)SC)cc1
RDKit 2D 27 30 0 0 0 0 0 0 0 0999 V2000 1.0667 -2.8125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 1.6917 -3.1750 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 1.0667 -2.0917 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 5.4292 -3.1917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3167 -2.8167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2.3167 -2.1000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.0542 -2.8292 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 0.4417 -3.1750 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 4.8042 -2.8250 0.0000 N 0 0 0 0 0 0 0 0 0 0 0 0 2.9375 -3.1792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5542 -2.8250 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1750 -3.1875 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 5.4292 -3.9125 0.0000 S 0 0 0 0 0 0 0 0 0 0 0 0 6.6792 -3.1917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.1708 -2.0917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.1708 -2.8167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.9292 -3.9167 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 6.6750 -3.9125 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.3042 -2.8292 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.9292 -3.1917 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 7.3000 -4.2792 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.5542 -4.2792 0.0000 O 0 0 0 0 0 0 0 0 0 0 0 0 2.9292 -3.9000 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 3.5500 -4.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.1750 -3.9042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 4.8000 -4.2667 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 8.5542 -5.0042 0.0000 C 0 0 0 0 0 0 0 0 0 0 0 0 2 1 2 0 3 1 1 0 4 9 2 0 5 2 1 0 6 3 1 0 7 4 1 0 8 1 1 0 9 12 1 0 10 5 1 0 11 10 2 0 12 11 1 0 13 4 1 0 14 7 1 0 15 3 1 0 16 8 1 0 17 20 1 0 18 14 2 0 19 14 1 0 20 19 2 0 21 18 1 0 22 17 1 0 23 10 1 0 24 23 2 0 25 24 1 0 26 13 1 0 27 22 1 0 15 16 1 0 5 6 1 0 12 25 2 0 21 17 2 0 M END > <chembl_id> CHEMBL54651 > <chembl_pref_name> None
InChI=1S/C20H22N4OS2/c1-25-17-8-6-15(7-9-17)21-19(26-2)22-16-5-3-4-14(12-16)18-13-24-10-11-27-20(24)23-18/h3-9,12,18H,10-11,13H2,1-2H3,(H,21,22)
COEWCKOZENJWDU-UHFFFAOYSA-N
4.62
2
C20H22N4OS2
398.56
6
1
27
398.56
-0.95
0
49.22
0.6
N
4
CHEMBL54651
CHEMBL54651
CHEMBL54651
null
null
null
null
Heligmosomoides polygyrus
null
null
6,339
null
F
Functional
BAO_0000218
organism-based format
null
Target assigned is non-molecular
1
Nematocidal activity against Nematospiroides dubius induced necropsy in mouse, oral administration 200 mg/kg
CHEMBL1123619
Non-molecular target assigned
N
null
1
CHEMBL612662
null
null
DOSE=200.0 mg/kg | ROUTE=None None
Heligmosomoides polygyrus
Heligmosomoides polygyrus
false
ORGANISM
6,339
null
null
null
null
0
null
null
null
null
null
null
null
null
null
null
null
A series of isothiourea derivatives of 6-phenyl-2,3,5,6-tetrahydroimidazo[2,1-b]thiazole (tetramisole) is described. The compounds are prepared by the S-alkylation of the thioureas that were obtained either by the reaction of an amine with 6-(3-isothiocyanatophenyl)-2,3,5,6-tetrahydroimidazo[2,1-b] thiazole or by the reaction of an isothiocyanate with 6-(3-aminophenyl)-2,3,5,6-tetrahydroimidazo[2,1-b]thiazole. These derivatives have an improved spectrum of activity over tetramisole and are active against nematodes, cestodes, and trematodes. The structure-activity relationships are discussed.
Brewer MD, Dorgan RJ, Manger BR, Mamalis P, Webster RA.
10.1021/jm00393a028
null
1848
10
J Med Chem
null
3,116,256
1
Isothiourea derivatives of 6-phenyl-2,3,5,6-tetrahydroimidazo[2,1-b]thiazole with broad-spectrum anthelmintic activity.
30
1,987