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11 values
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244
10.1021_acs.orglett.3c02241
c1(C#CCS(=O)(=O)CC(O)c2ccc(OC)cc2)ccccc1
11
11
[0.63165376 0.365625 0.87059808 0.45546875]
[0.1211315 0.45625 0.61174173 0.49375 ]
1H NMR
400 MHz
CDCl3
7.47 (d, J = 6.4 Hz, 2H), 7.38-7.31 (m, 5H), 6.89 (d, J = 8.8 Hz, 2H), 5.34 (dd, J = 10.4, 1.6 Hz, 1H), 4.35 (d, J = 16.8 Hz, 1H), 4.11(d, J =16.8 Hz, 1H), 3.79 (s, 3H), 3.77-3.73 (m, 1H), 3.28 (d, J =14.8 Hz, 1H)
null
[('d', ['6.4Hz'], '2H', 7.47, 7.47), ('m', [], '5H', 7.38, 7.31), ('d', ['8.8Hz'], '2H', 6.89, 6.89), ('dd', ['10.4Hz', '1.6Hz'], '1H', 5.34, 5.34), ('d', ['16.8Hz'], '1H', 4.35, 4.35), ('d', ['16.8Hz'], '1H', 4.11, 4.11), ('s', [], '3H', 3.79, 3.79), ('m', [], '1H', 3.77, 3.73), ('d', ['14.8Hz'], '1H', 3.28, 3.28)]
18
10
17
10.1021_acs.orglett.3c02241
C(#CCS(=O)(=O)CC(O)(c1ccccc1)c1ccccc1)c1ccccc1
12
12
[0.70466452 0.34296875 0.86727941 0.4140625 ]
[0.12057839 0.46015625 0.87944787 0.49921875]
1H NMR
400 MHz
CDCl3
7.53-7.49 (m, 6H), 7.41-7.36 (m, 7H), 7.34-7.30 (m, 2H), 5.00 (s, 1H), 4.27 (s, 2H), 3.48 (s, 2H)
null
[('m', [], '6H', 7.53, 7.49), ('m', [], '7H', 7.41, 7.36), ('m', [], '2H', 7.34, 7.3), ('s', [], '1H', 5.0, 5.0), ('s', [], '2H', 4.27, 4.27), ('s', [], '2H', 3.48, 3.48)]
20
9
20
10.1021_acs.orglett.3c02241
C#CCS(=O)(=O)CCO
13
13
[0.77103795 0.34453125 0.86174829 0.40390625]
[0.12071667 0.41054687 0.64271599 0.42460938]
1H NMR
400 MHz
CDCl3
4.12 (q, J = 4.4 Hz, 2H), 3.99 (d, J = 2.8 Hz, 2H), 3.42 (t, J = 5.4 Hz, 2H), 2.77 (bs, 1H), 2.54 (t, J = 2.4 Hz, 1H)
null
[('q', ['4.4Hz'], '2H', 4.12, 4.12), ('d', ['2.8Hz'], '2H', 3.99, 3.99), ('t', ['5.4Hz'], '2H', 3.42, 3.42), ('brs', [], '1H', 2.77, 2.77), ('t', ['2.4Hz'], '1H', 2.54, 2.54)]
8
5
8
10.1021_acs.orglett.3c02241
C#CCS(=O)(=O)CCO
13
13
[0.77103795 0.34453125 0.86174829 0.40390625]
[0.12071667 0.41054687 0.64271599 0.42460938]
13C NMR
100 MHz
CDCl3
76.7 (C), 71.7 (CH), 56.5 (CH2), 53.6 (CH2), 47.1 (CH2)
null
[(76.7, None, None), (71.7, None, None), (56.5, None, None), (53.6, None, None), (47.1, None, None)]
5
5
5
10.1021_acs.orglett.3c02241
C(=CN(C(=O)OC(C)(C)C)c1ccccc1C#CCS(=O)(=O)CCO)C(=O)OCC
15
15
[0.69692096 0.4125 0.86949186 0.50625 ]
[0.12057839 0.51015625 0.43474593 0.52421875]
1H NMR
400 MHz
CDCl3
8.41 (d, J = 14.0 Hz, 1H), 7.59 (dd, J = 7.6, 1.2 Hz, 1H), 7.46 (td, J = 7.6, 1.6 Hz, 1H), 7.39 (td, J = 7.6, 1.2 Hz, 1H), 7.19 (dd, J = 8.0, 0.8 Hz, 1H), 4.63 (d, J = 14.0 Hz, 1H), 4.22-4.06 (m, 5H), 3.47-3.41 (m, 1H), 3.24-3.18 (m, 2H), 1.39 (s, 9H), 1.22 (t, J = 7.2 Hz, 3H)
null
[('d', ['14.0Hz'], '1H', 8.41, 8.41), ('dd', ['7.6Hz', '1.2Hz'], '1H', 7.59, 7.59), ('td', ['7.6Hz', '1.6Hz'], '1H', 7.46, 7.46), ('td', ['7.6Hz', '1.2Hz'], '1H', 7.39, 7.39), ('dd', ['8.0Hz', '0.8Hz'], '1H', 7.19, 7.19), ('d', ['14.0Hz'], '1H', 4.63, 4.63), ('m', [], '5H', 4.22, 4.06), ('m', [], '1H', 3.47, 3.41), ('m...
27
13
26
10.1021_acs.orglett.3c02241
C(=Cc1ccccc1C#CCS(=O)(=O)CCO)C(=O)OCC
16
16
[0.71572676 0.09628906 0.86617319 0.18105469]
[0.11891905 0.18144531 0.88166032 0.275 ]
1H NMR
400 MHz
CDCl3
8.24 (d, J = 16.4 Hz, 1H), 7.65 (dd, J = 8.8, 1.6 Hz, 1H), 7.52 (td, J = 5.2, 1.6 Hz, 1H), 7.40-7.32 (m, 2H), 6.51 (d, J = 16.0 Hz, 1H), 4.31 (s, 2H), 4.27 (q, J = 7.2 Hz, 2H), 4.19 (t, J = 5.2 Hz, 2H), 3.45 (t, J = 5.6 Hz, 2H), 1.33 (t, J = 7.2 Hz, 3H)
null
[('d', ['16.4Hz'], '1H', 8.24, 8.24), ('dd', ['8.8Hz', '1.6Hz'], '1H', 7.65, 7.65), ('td', ['5.2Hz', '1.6Hz'], '1H', 7.52, 7.52), ('m', [], '2H', 7.4, 7.32), ('d', ['16.0Hz'], '1H', 6.51, 6.51), ('s', [], '2H', 4.31, 4.31), ('q', ['7.2Hz'], '2H', 4.27, 4.27), ('t', ['5.2Hz'], '2H', 4.19, 4.19), ('t', ['5.6Hz'], '2H', 3...
18
12
17
10.1021_acs.orglett.3c02241
C(=Cc1ccccc1C#CCS(=O)(=O)CCO)C(=O)OCC
16
16
[0.71572676 0.09628906 0.86617319 0.18105469]
[0.11891905 0.18144531 0.88166032 0.275 ]
13C NMR
100 MHz
CDCl3
168.2 (C), 142.8 (CH), 136.3 (C), 133.2 (CH), 130.3 (CH), 129.6 (CH), 125.9 (CH), 123.0 (C), 119.5 (CH), 84.6 (C), 83.9 (C), 61.4 (CH2), 56.6 (CH2), 54.6 (CH2), 48.3 (CH2), 14.3 (CH3)
null
[(168.2, None, None), (142.8, None, None), (136.3, None, None), (133.2, None, None), (130.3, None, None), (129.6, None, None), (125.9, None, None), (123.0, None, None), (119.5, None, None), (84.6, None, None), (83.9, None, None), (61.4, None, None), (56.6, None, None), (54.6, None, None), (48.3, None, None), (14.3, Non...
16
16
16
10.1021_acs.orglett.3c02241
C=CS(=O)(=O)CC(=O)Cc1ccc(C)cc1
18
18
[0.67922138 0.290625 0.86838564 0.35234375]
[0.12154633 0.35957031 0.61837907 0.37441406]
1H NMR
500 MHz
CDCl3
7.16 (d, J = 8.0 Hz, 2H), 7.09 (d, J = 8.0 Hz, 2H), 6.74 (dd, J = 16.5, 10.0 Hz, 1H), 6.43 (d, J = 17.0 Hz, 1H), 6.17 (d, J = 10.0 Hz, 1H), 4.06 (s, 2H), 3.91 (s, 2H), 2.34 (s, 3H)
null
[('d', ['8.0Hz'], '2H', 7.16, 7.16), ('d', ['8.0Hz'], '2H', 7.09, 7.09), ('dd', ['16.5Hz', '10.0Hz'], '1H', 6.74, 6.74), ('d', ['17.0Hz'], '1H', 6.43, 6.43), ('d', ['10.0Hz'], '1H', 6.17, 6.17), ('s', [], '2H', 4.06, 4.06), ('s', [], '2H', 3.91, 3.91), ('s', [], '3H', 2.34, 2.34)]
14
7
14
10.1021_acs.orglett.3c02241
O(C)CCS(=O)(=O)CC(=O)Cc1ccc(C)cc1
18
18
[0.63054753 0.75390625 0.86949186 0.82734375]
[0.12057839 0.8328125 0.78210018 0.8453125 ]
1H NMR
400 MHz
CDCl3
7.16 (d, J = 7.6 Hz, 2H), 7.08 (d, J = 8.0 Hz, 2H), 4.15 (s, 2H), 3.86 (s, 2H), 3.79 (t, J = 5.2 Hz, 2H), 3.39 (t, J = 5.2 Hz, 2H), 3.32 (s, 3H), 2.34 (s, 3H)
null
[('d', ['7.6Hz'], '2H', 7.16, 7.16), ('d', ['8.0Hz'], '2H', 7.08, 7.08), ('s', [], '2H', 4.15, 4.15), ('s', [], '2H', 3.86, 3.86), ('t', ['5.2Hz'], '2H', 3.79, 3.79), ('t', ['5.2Hz'], '2H', 3.39, 3.39), ('s', [], '3H', 3.32, 3.32), ('s', [], '3H', 2.34, 2.34)]
18
8
18
10.1021_acs.orglett.3c02241
c1(C2CCS(=O)(=O)CC2=O)ccccc1
19
19
[0.77988774 0.265625 0.86506696 0.34335938]
[0.1211315 0.38769531 0.88000098 0.4515625 ]
1H NMR
400 MHz
DMSO-d6
7.31-7.22 (m, 3H), 7.07 (d, J = 7.6 Hz, 2H), 4.40 (d, J = 13.6 Hz, 1H), 3.92-3.88 (m, 1H), 3.82-3.78 (m, 1H), 3.59-3.51 (m, 1H), 3.36-3.32 (m, 1H), 2.38-2.30 (m, 2H)
null
[('m', [], '3H', 7.31, 7.22), ('d', ['7.6Hz'], '2H', 7.07, 7.07), ('d', ['13.6Hz'], '1H', 4.4, 4.4), ('m', [], '1H', 3.92, 3.88), ('m', [], '1H', 3.82, 3.78), ('m', [], '1H', 3.59, 3.51), ('m', [], '1H', 3.36, 3.32), ('m', [], '2H', 2.38, 2.3)]
12
7
12
10.1021_acs.orglett.3c02241
O=C1CS(=O)(=O)CCC1c1cccc2ccccc12
23
23
[0.75721015 0.63203125 0.87004497 0.73984375]
[0.12002528 0.75585938 0.87944787 0.84375 ]
1H NMR
400 MHz
CD3CN
7.97-7.93 (m, 1H), 7.89 (d, J = 8.4 Hz, 1H), 7.85 (dd, J = 9.6, 3.6 Hz, 1H), 7.56-7.51(m, 3H), 7.41 (dd, J = 7.2, 0.4 Hz, 1H), 4.72 (d, J = 13.6 Hz, 2H), 4.02 (dd, J = 8.0, 4.4 Hz, 1H), 3.79-3.71 (m, 1H), 3.55 (dq, J = 14.4, 3.6 Hz, 1H), 2.63-2.57 (m, 2H)
null
[('m', [], '1H', 7.97, 7.93), ('d', ['8.4Hz'], '1H', 7.89, 7.89), ('dd', ['9.6Hz', '3.6Hz'], '1H', 7.85, 7.85), ('m', [], '3H', 7.56, 7.51), ('dd', ['7.2Hz', '0.4Hz'], '1H', 7.41, 7.41), ('d', ['13.6Hz'], '2H', 4.72, 4.72), ('dd', ['8.0Hz', '4.4Hz'], '1H', 4.02, 4.02), ('m', [], '1H', 3.79, 3.71), ('dq', ['14.4Hz', '3....
14
11
14
10.1021_acs.orglett.3c02241
O=C1CS(=O)(=O)CCC1c1c[nH]c2ccccc12
24
24
[0.73895746 0.2578125 0.85621717 0.36992188]
[0.1211315 0.38496094 0.88000098 0.49765625]
1H NMR
400 MHz
CD3CN
9.35 (bs, 1H), 7.42 (dt, J = 8.4, 0.8 Hz, 1H), 7.36 (dd, J = 8.0, 0.8 Hz, 1H), 7.19 (d, J = 2.0 Hz, 1H), 7.15 (ddd, J = 8.0, 6.8, 1.2 Hz, 1H), 7.04 (ddd, J = 8.0, 7.2, 1.2 Hz, 1H), 4.46 (d, J = 13.6 Hz, 1H), 4.18 (dd, J = 12.0, 5.6 Hz, 1H), 3.96 (dd, J = 13.2, 3.6 Hz, 1H), 3.65-3.57 (m, 1H), 3.45 (dq, J = 14.4, 4.0 Hz,...
null
[('brs', [], '1H', 9.35, 9.35), ('dt', ['8.4Hz', '0.8Hz'], '1H', 7.42, 7.42), ('dd', ['8.0Hz', '0.8Hz'], '1H', 7.36, 7.36), ('d', ['2.0Hz'], '1H', 7.19, 7.19), ('ddd', ['8.0Hz', '6.8Hz', '1.2Hz'], '1H', 7.15, 7.15), ('ddd', ['8.0Hz', '7.2Hz', '1.2Hz'], '1H', 7.04, 7.04), ('d', ['13.6Hz'], '1H', 4.46, 4.46), ('dd', ['12...
13
10
13
10.1021_acs.orglett.3c02241
O=C1CS(=O)(=O)CCC1c1c[nH]c2ccccc12
24
24
[0.73895746 0.2578125 0.85621717 0.36992188]
[0.1211315 0.38496094 0.88000098 0.49765625]
13C NMR
100 MHz
CD3CN
196.9 (C), 137.2 (C), 127.6 (C), 124.0 (CH), 122.6 (CH), 120.0 (CH), 119.6 (CH), 112.5 (CH), 111.5 (C), 66.5 (CH2), 51.6 (CH2), 47.9 (CH), 26.2 (CH2)
null
[(196.9, None, None), (137.2, None, None), (127.6, None, None), (124.0, None, None), (122.6, None, None), (120.0, None, None), (119.6, None, None), (112.5, None, None), (111.5, None, None), (66.5, None, None), (51.6, None, None), (47.9, None, None), (26.2, None, None)]
13
13
13
10.1021_acs.orglett.3c02241
c1(CC(=O)CS(=O)(=O)C=C(c2ccccc2)c2ccccc2)ccccc1
29
29
[0.72347033 0.70898438 0.88719144 0.77460938]
[0.1211315 0.77929688 0.69249606 0.79335937]
1H NMR
500 MHz
CDCl3
7.47-7.41 (m, 4H), 7.37-7.32 (m, 6H), 7.29-7.26 (m, 3H), 7.15 (d, J = 7.5 Hz, 2H), 6.83 (s, 1H), 3.90 (s, 2H), 3.86 (s, 2H)
null
[('m', [], '4H', 7.47, 7.41), ('m', [], '6H', 7.37, 7.32), ('m', [], '3H', 7.29, 7.26), ('d', ['7.5Hz'], '2H', 7.15, 7.15), ('s', [], '1H', 6.83, 6.83), ('s', [], '2H', 3.9, 3.9), ('s', [], '2H', 3.86, 3.86)]
20
9
20
10.1021_acs.orglett.3c02241
O(CC)CCS(=O)(=O)CC(C)=O
31
31
[0.7223641 0.30078125 0.87170431 0.3671875 ]
[0.12002528 0.38710937 0.88000098 0.42695312]
1H NMR
500 MHz
CD3CN
4.26 (s, 2H), 3.80 (t, J = 5.0 Hz, 2H), 3.51 (q, J = 14.0, 7.0 Hz, 2H), 3.35 (t, J = 5.5 Hz, 2H), 2.29 (s, 3H), 1.17 (t, J = 7.0 Hz, 3H)
null
[('s', [], '2H', 4.26, 4.26), ('t', ['5.0Hz'], '2H', 3.8, 3.8), ('q', ['14.0Hz', '7.0Hz'], '2H', 3.51, 3.51), ('t', ['5.5Hz'], '2H', 3.35, 3.35), ('s', [], '3H', 2.29, 2.29), ('t', ['7.0Hz'], '3H', 1.17, 1.17)]
14
6
14
10.1021_acs.orglett.3c02241
c1(C2CCS(=O)(=O)c3c2oc2ccccc32)ccccc1
35
35
[0.75112592 0.69453125 0.86838564 0.77265625]
[0.12002528 0.78125 0.87944787 0.8203125 ]
1H NMR
400 MHz
CDCl3
7.94-7.92 (m, 1H), 7.41-7.31 (m, 6H), 7.14 (d, J = 6.4 Hz, 2H), 4.38 (t, J = 6.4 Hz, 1H), 3.45-3.31 (m, 2H), 2.92-2.84 (m, 1H), 2.67-2.58 (m, 1H)
null
[('m', [], '1H', 7.94, 7.92), ('m', [], '6H', 7.41, 7.31), ('d', ['6.4Hz'], '2H', 7.14, 7.14), ('t', ['6.4Hz'], '1H', 4.38, 4.38), ('m', [], '2H', 3.45, 3.31), ('m', [], '1H', 2.92, 2.84), ('m', [], '1H', 2.67, 2.58)]
14
10
14
10.1021_acs.orglett.3c02241
O=S1(=O)CCc2c(oc3ccccc23)C1
36
36
[0.78431263 0.2890625 0.86838564 0.3921875 ]
[0.12168461 0.40820312 0.87944787 0.44804688]
1H NMR
500 MHz
CDCl3
7.46 (dd, J = 14.0, 8.0 Hz, 2H), 7.33 (t, J = 7.5 Hz, 1H), 7.28 (t, J = 7.5 Hz, 1H), 4.42 (s, 2H), 3.33 (t, J = 6.0 Hz, 2H), 3.22 (t, J = 6.0 Hz, 2H)
null
[('dd', ['14.0Hz', '8.0Hz'], '2H', 7.46, 7.46), ('t', ['7.5Hz'], '1H', 7.33, 7.33), ('t', ['7.5Hz'], '1H', 7.28, 7.28), ('s', [], '2H', 4.42, 4.42), ('t', ['6.0Hz'], '2H', 3.33, 3.33), ('t', ['6.0Hz'], '2H', 3.22, 3.22)]
10
7
10
10.1021_acs.orglett.3c02241
O=S1(=O)CCc2c(oc3ccccc23)C1
36
36
[0.78431263 0.2890625 0.86838564 0.3921875 ]
[0.12168461 0.40820312 0.87944787 0.44804688]
13C NMR
125 MHz
CDCl3
155.0 (C), 142.5 (C), 126.9 (C), 125.2 (CH), 123.3 (CH), 119.0 (CH), 111.7 (C), 111.5 (CH), 51.6 (CH2), 48.4 (CH2), 18.6 (CH2)
null
[(155.0, None, None), (142.5, None, None), (126.9, None, None), (125.2, None, None), (123.3, None, None), (119.0, None, None), (111.7, None, None), (111.5, None, None), (51.6, None, None), (48.4, None, None), (18.6, None, None)]
11
11
11
10.1021_acs.orglett.3c02241
C(=CCC(C(=O)O)c1ccccc1)c1ccccc1
38
38
[0.71240809 0.115625 0.87170431 0.1546875 ]
[0.1211315 0.16152344 0.43474593 0.17558594]
1H NMR
500 MHz
CDCl3
7.37-7.34 (m, 4H), 7.32-7.27 (m, 5H), 7.23-7.20 (m, 1H), 6.46 (d, J = 16.0 Hz, 1H), 6.12 (dt, J = 15.5, 7.0 Hz, 1H), 3.74 (t, J = 7.5 Hz, 1H), 3.00 (quint, J = 7.0 Hz, 1H), 2.71 (quint, J = 7.0 Hz, 1H)
null
[('m', [], '4H', 7.37, 7.34), ('m', [], '5H', 7.32, 7.27), ('m', [], '1H', 7.23, 7.2), ('d', ['16.0Hz'], '1H', 6.46, 6.46), ('dt', ['15.5Hz', '7.0Hz'], '1H', 6.12, 6.12), ('t', ['7.5Hz'], '1H', 3.74, 3.74), ('p', ['7.0Hz'], '1H', 3.0, 3.0), ('p', ['7.0Hz'], '1H', 2.71, 2.71)]
16
11
15
10.1039_d4cc03507k
C(c1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1)(F)(F)F
2
2
[0.15078323 0.44648438 0.26069481 0.52226565]
[0.14802163 0.56562504 0.84946742 0.85625003]
1H NMR
400 MHz
CDCl3
8.91 (s, 1H), 8.75 (d, J = 8.0 Hz, 1H), 8.61 (d, J = 12.0 Hz, 1H), 8.15 (d, J = 8.0 Hz, 1H), 7.84-7.80 (m, 1H), 7.74-7.69 (m, 5H), 7.53-7.41 (m, 7H), 2.59 (d, J = 4.0 Hz, 3H)
null
[('s', [], '1H', 8.91, 8.91), ('d', ['8.0Hz'], '1H', 8.75, 8.75), ('d', ['12.0Hz'], '1H', 8.61, 8.61), ('d', ['8.0Hz'], '1H', 8.15, 8.15), ('m', [], '1H', 7.84, 7.8), ('m', [], '5H', 7.74, 7.69), ('m', [], '7H', 7.53, 7.41), ('d', ['4.0Hz'], '3H', 2.59, 2.59)]
20
11
20
10.1039_d4cc03507k
C(c1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1)(F)(F)F
2
2
[0.15078323 0.44648438 0.26069481 0.52226565]
[0.14802163 0.56562504 0.84946742 0.85625003]
13C NMR
100 MHz
CDCl3
145.3 (d, J = 8.0 Hz, 1C), 136.0, 135.0, 133.8 (d, J = 10.0 Hz, 1C), 131.8 (d, J = 12.0 Hz, 1C), 131.6 (d, J = 3.0 Hz, 1C), 131.4 (d, J = 2.0 Hz, 1C), 131.0 (d, J = 10.0 Hz, 1C), 129.4 (d, J = 9.0 Hz, 1C), 129.2 (d, J = 5.0 Hz, 1C), 128.8 (d, J = 12.0 Hz, 1C), 128.0, 127.6 (d, J = 32.0 Hz, 1C), 125.5 (d, J = 10.0 Hz, 1...
null
[(145.3, 'd', 8.0), (136.0, None, None), (135.0, None, None), (133.8, 'd', 10.0), (131.8, 'd', 12.0), (131.6, 'd', 3.0), (131.4, 'd', 2.0), (131.0, 'd', 10.0), (129.4, 'd', 9.0), (129.2, 'd', 5.0), (128.8, 'd', 12.0), (128.0, None, None), (127.6, 'd', 32.0), (125.5, 'd', 10.0), (125.4, None, None), (124.5, None, None),...
28
20
20
10.1039_d4cc03507k
C(c1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1)(F)(F)F
2
2
[0.15078323 0.44648438 0.26069481 0.52226565]
[0.14802163 0.56562504 0.84946742 0.85625003]
19F NMR
376 MHz
CDCl3
-62.14
null
[(-62.14, None, None)]
3
1
1
10.1039_d4cc03507k
C(c1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1)(F)(F)F
2
2
[0.15078323 0.44648438 0.26069481 0.52226565]
[0.14802163 0.56562504 0.84946742 0.85625003]
31P NMR
162 MHz
CDCl3
30.26
null
[(30.26, None, None)]
1
1
1
10.1039_d4cc03507k
CC(=O)c1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1
3
3
[0.1502309 0.09511719 0.25406699 0.16933595]
[0.14857395 0.21484377 0.84891508 0.44960939]
1H NMR
400 MHz
CDCl3
9.28 (s, 1H), 8.83 (d, J = 8.0 Hz, 1H), 8.46 (d, J = 8.0 Hz, 1H), 8.14 (d, J = 8.0 Hz, 1H), 7.82 (t, J = 8.0 Hz, 1H), 7.76 (dd, J1 = 8.0 Hz, J2 = 4.0 Hz, 1H), 7.70 (dd, J1 = 12.0 Hz, J2 = 8.0 Hz, 5H), 7.49 (t, J = 8.0 Hz, 2H), 7.44-7.39 (m, 4H), 2.69 (s, 3H), 2.61 (d, J = 4.0 Hz, 3H)
null
[('s', [], '1H', 9.28, 9.28), ('d', ['8.0Hz'], '1H', 8.83, 8.83), ('d', ['8.0Hz'], '1H', 8.46, 8.46), ('d', ['8.0Hz'], '1H', 8.14, 8.14), ('t', ['8.0Hz'], '1H', 7.82, 7.82), ('dd', "['8.0Hz', '4.0Hz']", '1H', 7.76, 7.76), ('dd', "['12.0Hz', '8.0Hz']", '5H', 7.7, 7.7), ('t', ['8.0Hz'], '2H', 7.49, 7.49), ('m', [], '4H',...
23
12
23
10.1039_d4cc03507k
CC(=O)c1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1
3
3
[0.1502309 0.09511719 0.25406699 0.16933595]
[0.14857395 0.21484377 0.84891508 0.44960939]
13C NMR
100 MHz
CDCl3
198.0, 146.0, 136.4, 135.3, 135.0, 133.9, 132.1, 132.0, 131.6 (d, J = 3.0 Hz, 1C), 131.0 (d, J = 10.0 Hz, 1C), 129.5 (d, J = 9.0 Hz, 1C), 129.3, 129.0, 128.8, 127.8, 125.5, 124.8, 123.5, 123.2, 26.9, 21.8 (d, J = 8.0 Hz, 1C)
null
[(198.0, None, None), (146.0, None, None), (136.4, None, None), (135.3, None, None), (135.0, None, None), (133.9, None, None), (132.1, None, None), (132.0, None, None), (131.6, 'd', 3.0), (131.0, 'd', 10.0), (129.5, 'd', 9.0), (129.3, None, None), (129.0, None, None), (128.8, None, None), (127.8, None, None), (125.5, N...
29
21
21
10.1039_d4cc03507k
CC(=O)c1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1
3
3
[0.1502309 0.09511719 0.25406699 0.16933595]
[0.14857395 0.21484377 0.84891508 0.44960939]
31P NMR
162 MHz
CDCl3
29.79
null
[(29.79, None, None)]
1
1
1
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(c2c(C)c3c(c4c2ccc(F)c4)cccc3)=O)cc1
3
3
[0.15050707 0.46562503 0.24661065 0.53984378]
[0.1474693 0.58515629 0.85996147 0.87421879]
1H NMR
400 MHz
CDCl3
8.59 (d, J = 8.0 Hz, 1H), 8.54 (dd, J1 = 12.0 Hz, J2 = 8.0 Hz, 1H), 8.25 (d, J = 8.0 Hz, 1H), 8.11 (d, J = 8.0 Hz, 1H), 7.78-7.66 (m, 6H), 7.51-7.47 (m, 2H), 7.44-7.40 (m, 4H), 7.05-7.00 (m, 1H), 2.53 (d, J = 4.0 Hz, 3H)
null
[('d', ['8.0Hz'], '1H', 8.59, 8.59), ('dd', "['12.0Hz', '8.0Hz']", '1H', 8.54, 8.54), ('d', ['8.0Hz'], '1H', 8.25, 8.25), ('d', ['8.0Hz'], '1H', 8.11, 8.11), ('m', [], '6H', 7.78, 7.66), ('m', [], '2H', 7.51, 7.47), ('m', [], '4H', 7.44, 7.4), ('m', [], '1H', 7.05, 7.0), ('d', ['4.0Hz'], '3H', 2.53, 2.53)]
20
11
20
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(c2c(C)c3c(c4c2ccc(F)c4)cccc3)=O)cc1
3
3
[0.15050707 0.46562503 0.24661065 0.53984378]
[0.1474693 0.58515629 0.85996147 0.87421879]
19F NMR
376 MHz
CDCl3
-114.07
null
[(-114.07, None, None)]
1
1
1
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(c2c(C)c3c(c4c2ccc(F)c4)cccc3)=O)cc1
3
3
[0.15050707 0.46562503 0.24661065 0.53984378]
[0.1474693 0.58515629 0.85996147 0.87421879]
31P NMR
162 MHz
CDCl3
30.54
null
[(30.54, None, None)]
1
1
1
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(c2c(C)c3c(c4c2ccc(Br)c4)cccc3)=O)cc1
4
4
[0.15050707 0.09492188 0.25379082 0.16953125]
[0.1474693 0.21484377 0.84891508 0.4761719 ]
1H NMR
400 MHz
CDCl3
8.77 (s, 1H), 8.63 (d, J = 8.0 Hz, 1H), 8.36 (d, J = 12.0 Hz, 1H), 8.11 (d, J = 8.0 Hz, 1H), 7.77 (t, J = 8.0 Hz, 1H), 7.72-7.65 (m, 5H), 7.49 (t, J = 8.0 Hz, 2H), 7.43-7.40 (m, 4H), 7.34 (dd, J1 = 8.0 Hz, J2 = 4.0 Hz, 1H), 2.55 (s, 3H)
null
[('s', [], '1H', 8.77, 8.77), ('d', ['8.0Hz'], '1H', 8.63, 8.63), ('d', ['12.0Hz'], '1H', 8.36, 8.36), ('d', ['8.0Hz'], '1H', 8.11, 8.11), ('t', ['8.0Hz'], '1H', 7.77, 7.77), ('m', [], '5H', 7.72, 7.65), ('t', ['8.0Hz'], '2H', 7.49, 7.49), ('m', [], '4H', 7.43, 7.4), ('dd', "['8.0Hz', '4.0Hz']", '1H', 7.34, 7.34), ('s'...
20
11
20
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(c2c(C)c3c(c4c2ccc(Br)c4)cccc3)=O)cc1
4
4
[0.15050707 0.09492188 0.25379082 0.16953125]
[0.1474693 0.21484377 0.84891508 0.4761719 ]
13C NMR
100 MHz
CDCl3
143.3 (d, J = 8.0 Hz, 1C), 136.3, 135.3, 131.8 (d, J = 12.0 Hz, 1C), 131.5 (q, J = 2.0 Hz, 1C), 131.1, 131.0, 130.7 (d, J = 2.0 Hz, 1C), 130.4 (d, J = 10.0 Hz, 1C), 130.1 (d, J = 6.0 Hz, 1C), 128.9, 128.9, 128.7, 127.8, 125.3 (d, J = 13.0 Hz, 1C), 124.5, 123.0, 120.6, 21.5 (d, J = 7.0 Hz, 1C)
null
[(143.3, 'd', 8.0), (136.3, None, None), (135.3, None, None), (131.8, 'd', 12.0), (131.5, 'q', 2.0), (131.1, None, None), (131.0, None, None), (130.7, 'd', 2.0), (130.4, 'd', 10.0), (130.1, 'd', 6.0), (128.9, None, None), (128.9, None, None), (128.7, None, None), (127.8, None, None), (125.3, 'd', 13.0), (124.5, None, N...
27
19
19
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(c2c(C)c3c(c4c2ccc(Br)c4)cccc3)=O)cc1
4
4
[0.15050707 0.09492188 0.25379082 0.16953125]
[0.1474693 0.21484377 0.84891508 0.4761719 ]
31P NMR
162 MHz
CDCl3
30.09
null
[(30.09, None, None)]
1
1
1
10.1039_d4cc03507k
CCc1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1
4
4
[0.15050707 0.49296878 0.25241002 0.56796877]
[0.14691699 0.61171876 0.84836274 0.87656256]
1H NMR
400 MHz
CDCl3
8.75 (d, J = 8.0 Hz, 1H), 8.46 (s, 1H), 8.29 (d, J = 8.0 Hz, 1H), 8.11 (d, J = 8.0 Hz, 1H), 7.77-7.69 (m, 5H), 7.66-7.62 (m, 1H), 7.50-7.46 (m, 2H), 7.43-7.38 (m, 4H), 7.12 (dd, J1 = 8.0 Hz, J2 = 4.0 Hz, 1H), 2.81 (q, J = 8.0 Hz, 2H), 2.59 (d, J = 4.0 Hz, 3H), 1.31 (t, J = 8.0 Hz, 3H)
null
[('d', ['8.0Hz'], '1H', 8.75, 8.75), ('s', [], '1H', 8.46, 8.46), ('d', ['8.0Hz'], '1H', 8.29, 8.29), ('d', ['8.0Hz'], '1H', 8.11, 8.11), ('m', [], '5H', 7.77, 7.69), ('m', [], '1H', 7.66, 7.62), ('m', [], '2H', 7.5, 7.46), ('m', [], '4H', 7.43, 7.38), ('dd', "['8.0Hz', '4.0Hz']", '1H', 7.12, 7.12), ('q', ['8.0Hz'], '2...
25
13
25
10.1039_d4cc03507k
CCc1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1
4
4
[0.15050707 0.49296878 0.25241002 0.56796877]
[0.14691699 0.61171876 0.84836274 0.87656256]
31P NMR
162 MHz
CDCl3
30.48
null
[(30.48, None, None)]
1
1
1
10.1039_d4cc03507k
CC(C)(C)c1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1
5
5
[0.15133554 0.09497071 0.26069481 0.16953125]
[0.14802163 0.21328126 0.84946742 0.47734378]
1H NMR
400 MHz
CDCl3
8.78 (d, J = 8.0 Hz, 1H), 8.65 (s, 1H), 8.38 (d, J = 8.0 Hz, 1H), 8.11 (d, J = 8.0 Hz, 1H), 7.78-7.71 (m, 5H), 7.63 (t, J = 8.0 Hz, 1H), 7.51-7.48 (m, 2H), 7.44-7.40 (m, 4H), 7.36 (dd, J1 = 8.0 Hz, J2 = 4.0 Hz, 1H), 2.56 (d, J = 4.0 Hz, 3H), 1.42 (s, 9H)
null
[('d', ['8.0Hz'], '1H', 8.78, 8.78), ('s', [], '1H', 8.65, 8.65), ('d', ['8.0Hz'], '1H', 8.38, 8.38), ('d', ['8.0Hz'], '1H', 8.11, 8.11), ('m', [], '5H', 7.78, 7.71), ('t', ['8.0Hz'], '1H', 7.63, 7.63), ('m', [], '2H', 7.51, 7.48), ('m', [], '4H', 7.44, 7.4), ('dd', "['8.0Hz', '4.0Hz']", '1H', 7.36, 7.36), ('d', ['4.0H...
29
12
29
10.1039_d4cc03507k
CC(C)(C)c1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1
5
5
[0.15133554 0.09497071 0.26069481 0.16953125]
[0.14802163 0.21328126 0.84946742 0.47734378]
13C NMR
100 MHz
CDCl3
148.6, 141.8 (d, J = 9.0 Hz, 1C), 136.6, 135.6, 132.1 (d, J = 2.0 Hz, 1C), 131.7 (d, J = 13.0 Hz, 1C), 131.3 (d, J = 3.0 Hz, 1C), 131.1 (d, J = 10.0 Hz, 1C), 129.7 (d, J = 10.0 Hz, 1C), 129.4 (d, J = 9.0 Hz, 1C), 128.6 (d, J = 12.0 Hz, 1C), 128.4, 128.2 (d, J = 5.0 Hz, 1C), 126.8, 125.2, 124.3, 122.8, 118.2, 34.9, 31.3...
null
[(148.6, None, None), (141.8, 'd', 9.0), (136.6, None, None), (135.6, None, None), (132.1, 'd', 2.0), (131.7, 'd', 13.0), (131.3, 'd', 3.0), (131.1, 'd', 10.0), (129.7, 'd', 10.0), (129.4, 'd', 9.0), (128.6, 'd', 12.0), (128.4, None, None), (128.2, 'd', 5.0), (126.8, None, None), (125.2, None, None), (124.3, None, None...
31
21
21
10.1039_d4cc03507k
CC(C)(C)c1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1
5
5
[0.15133554 0.09497071 0.26069481 0.16953125]
[0.14802163 0.21328126 0.84946742 0.47734378]
31P NMR
162 MHz
CDCl3
31.02
null
[(31.02, None, None)]
1
1
1
10.1039_d4cc03507k
COc1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1
5
5
[0.15050707 0.49375002 0.26594183 0.56718753]
[0.14912627 0.58515629 0.65339395 0.59921877]
1H NMR
400 MHz
CDCl3
8.65 (d, J = 8.0 Hz, 1H), 8.37 (d, J = 12.0 Hz, 1H), 8.10 (d, J = 8.0 Hz, 1H), 8.02 (s, 1H), 7.76-7.69 (m, 5H), 7.64 (t, J = 8.0 Hz, 1H), 7.49-7.45 (m, 2H), 7.42-7.38 (m, 4H), 6.90 (dd, J1 = 12.0 Hz, J2 = 4.0 Hz, 1H), 3.94 (s, 3H), 2.54 (d, J = 4.0 Hz, 3H)
null
[('d', ['8.0Hz'], '1H', 8.65, 8.65), ('d', ['12.0Hz'], '1H', 8.37, 8.37), ('d', ['8.0Hz'], '1H', 8.1, 8.1), ('s', [], '1H', 8.02, 8.02), ('m', [], '5H', 7.76, 7.69), ('t', ['8.0Hz'], '1H', 7.64, 7.64), ('m', [], '2H', 7.49, 7.45), ('m', [], '4H', 7.42, 7.38), ('dd', "['12.0Hz', '4.0Hz']", '1H', 6.9, 6.9), ('s', [], '3H...
23
12
23
10.1039_d4cc03507k
COc1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1
5
5
[0.15050707 0.49375002 0.26594183 0.56718753]
[0.14912627 0.58515629 0.65339395 0.59921877]
13C NMR
100 MHz
CDCl3
157.5, 140.2 (d, J = 8.0 Hz, 1C), 136.8, 135.8, 131.9 (d, J = 12.0 Hz, 1C), 131.4 (d, J = 8.0 Hz, 1C), 131.2 (d, J = 2.0 Hz, 1C), 131.1 (d, J = 10.0 Hz, 1C), 130.1 (d, J = 6.0 Hz, 1C), 128.7 (d, J = 13.0 Hz, 1C), 128.2, 127.1, 126.4 (d, J = 10.0 Hz, 1C), 125.3, 124.4, 123.0, 115.2, 104.4, 55.3, 21.1 (d, J = 8.0 Hz, 1C)
null
[(157.5, None, None), (140.2, 'd', 8.0), (136.8, None, None), (135.8, None, None), (131.9, 'd', 12.0), (131.4, 'd', 8.0), (131.2, 'd', 2.0), (131.1, 'd', 10.0), (130.1, 'd', 6.0), (128.7, 'd', 13.0), (128.2, None, None), (127.1, None, None), (126.4, 'd', 10.0), (125.3, None, None), (124.4, None, None), (123.0, None, No...
28
20
20
10.1039_d4cc03507k
COc1ccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c2c1
5
5
[0.15050707 0.49375002 0.26594183 0.56718753]
[0.14912627 0.58515629 0.65339395 0.59921877]
31P NMR
162 MHz
CDCl3
30.41
null
[(30.41, None, None)]
1
1
1
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(c2c(C)c3c(c4c2cc(F)cc4)cccc3)=O)cc1
6
6
[0.15078323 0.09335938 0.26538952 0.15156251]
[0.14802163 0.19648438 0.84946742 0.45820313]
1H NMR
400 MHz
CDCl3
8.64 (t, J = 8.0 Hz, 2H), 8.24 (dd, J1 = 12.0 Hz, J2 = 4.0 Hz, 1H), 8.11 (d, J = 8.0 Hz, 1H), 7.78-7.70 (m, 5H), 7.64 (t, J = 8.0 Hz, 1H), 7.51 (t, J = 8.0 Hz, 2H), 7.45-7.42 (m, 4H), 7.29-7.26 (m, 1H), 2.57 (s, 3H)
null
[('t', ['8.0Hz'], '2H', 8.64, 8.64), ('dd', "['12.0Hz', '4.0Hz']", '1H', 8.24, 8.24), ('d', ['8.0Hz'], '1H', 8.11, 8.11), ('m', [], '5H', 7.78, 7.7), ('t', ['8.0Hz'], '1H', 7.64, 7.64), ('t', ['8.0Hz'], '2H', 7.51, 7.51), ('m', [], '4H', 7.45, 7.42), ('m', [], '1H', 7.29, 7.26), ('s', [], '3H', 2.57, 2.57)]
20
11
20
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(c2c(C)c3c(c4c2cc(F)cc4)cccc3)=O)cc1
6
6
[0.15078323 0.09335938 0.26538952 0.15156251]
[0.14802163 0.19648438 0.84946742 0.45820313]
13C NMR
100 MHz
CDCl3
161.7, 159.3, 144.2 (d, J = 8.0 Hz, 1C), 136.1, 135.1, 133.5, 131.6, 131.1 (d, J = 9.0 Hz, 1C), 129.0, 128.8 (d, J = 12.0 Hz, 1C), 126.9, 126.4, 125.4, 124.7 (d, J = 9.0 Hz, 1C), 122.8, 115.0 (d, J = 23.0 Hz, 1C), 113.7 (d, J = 7.0 Hz, 1C), 113.4 (d, J = 6.0 Hz, 1C), 21.6 (d, J = 8.0 Hz, 1C)
null
[(161.7, None, None), (159.3, None, None), (144.2, 'd', 8.0), (136.1, None, None), (135.1, None, None), (133.5, None, None), (131.6, None, None), (131.1, 'd', 9.0), (129.0, None, None), (128.8, 'd', 12.0), (126.9, None, None), (126.4, None, None), (125.4, None, None), (124.7, 'd', 9.0), (122.8, None, None), (115.0, 'd'...
27
19
19
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(c2c(C)c3c(c4c2cc(F)cc4)cccc3)=O)cc1
6
6
[0.15078323 0.09335938 0.26538952 0.15156251]
[0.14802163 0.19648438 0.84946742 0.45820313]
19F NMR
376 MHz
CDCl3
-113.16
null
[(-113.16, None, None)]
1
1
1
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(c2c(C)c3c(c4c2cc(F)cc4)cccc3)=O)cc1
6
6
[0.15078323 0.09335938 0.26538952 0.15156251]
[0.14802163 0.19648438 0.84946742 0.45820313]
31P NMR
162 MHz
CDCl3
30.68
null
[(30.68, None, None)]
1
1
1
10.1039_d4cc03507k
C(c1cccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c12)#N
9
9
[0.15064514 0.29003908 0.24509179 0.36425785]
[0.14898819 0.38164065 0.63295814 0.39492189]
1H NMR
400 MHz
CDCl3
9.68 (d, J = 8.0 Hz, 1H), 8.81 (d, J = 8.0 Hz, 1H), 8.13 (d, J = 8.0 Hz, 1H), 7.94 (d, J = 8.0 Hz, 1H), 7.87 (t, J = 8.0 Hz, 1H), 7.77 (t, J = 8.0 Hz, 1H), 7.69 (d, J = 8.0 Hz, 2H), 7.66 (d, J = 8.0 Hz, 2H), 7.50 (t, J = 8.0 Hz, 2H), 7.45-7.40 (m, 4H), 7.33 (t, J = 8.0 Hz, 1H), 2.48 (s, 3H)
null
[('d', ['8.0Hz'], '1H', 9.68, 9.68), ('d', ['8.0Hz'], '1H', 8.81, 8.81), ('d', ['8.0Hz'], '1H', 8.13, 8.13), ('d', ['8.0Hz'], '1H', 7.94, 7.94), ('t', ['8.0Hz'], '1H', 7.87, 7.87), ('t', ['8.0Hz'], '1H', 7.77, 7.77), ('d', ['8.0Hz'], '2H', 7.69, 7.69), ('d', ['8.0Hz'], '2H', 7.66, 7.66), ('t', ['8.0Hz'], '2H', 7.5, 7.5...
20
11
20
10.1039_d4cc03507k
C(c1cccc2c(P(c3ccccc3)(c3ccccc3)=O)c(C)c3ccccc3c12)#N
9
9
[0.15064514 0.29003908 0.24509179 0.36425785]
[0.14898819 0.38164065 0.63295814 0.39492189]
31P NMR
162 MHz
CDCl3
29.54
null
[(29.54, None, None)]
1
1
1
10.1039_d4cc03507k
Cc1ccc(P(=O)(c2ccc(C)cc2)c2c(C)c3ccccc3c3ccccc23)cc1
10
10
[0.15078323 0.19921877 0.2902439 0.28789064]
[0.14857395 0.29785158 0.57551694 0.31152344]
1H NMR
500 MHz
CDCl3
8.72 (d, J = 10.0 Hz, 1H), 8.64 (d, J = 5.0 Hz, 1H), 8.40 (d, J = 5.0 Hz, 1H), 8.13 (d, J = 5.0 Hz, 1H), 7.75 (t, J = 10.0 Hz, 1H), 7.64 (t, J = 10.0 Hz, 1H), 7.60 (d, J = 5.0 Hz, 2H), 7.57 (d, J = 10.0 Hz, 2H), 7.50 (t, J = 10.0 Hz, 1H), 7.25 (t, J = 10.0 Hz, 1H), 7.21-7.20 (m, 4H), 2.61 (s, 3H), 2.36 (s, 6H)
null
[('d', ['10.0Hz'], '1H', 8.72, 8.72), ('d', ['5.0Hz'], '1H', 8.64, 8.64), ('d', ['5.0Hz'], '1H', 8.4, 8.4), ('d', ['5.0Hz'], '1H', 8.13, 8.13), ('t', ['10.0Hz'], '1H', 7.75, 7.75), ('t', ['10.0Hz'], '1H', 7.64, 7.64), ('d', ['5.0Hz'], '2H', 7.6, 7.6), ('d', ['10.0Hz'], '2H', 7.57, 7.57), ('t', ['10.0Hz'], '1H', 7.5, 7....
25
12
25
10.1039_d4cc03507k
Cc1ccc(P(=O)(c2ccc(C)cc2)c2c(C)c3ccccc3c3ccccc23)cc1
10
10
[0.15078323 0.19921877 0.2902439 0.28789064]
[0.14857395 0.29785158 0.57551694 0.31152344]
13C NMR
125 MHz
CDCl3
142.9 (d, J = 7.5 Hz, 1C), 141.6 (d, J = 2.5 Hz, 1C), 133.5, 132.7, 131.9 (d, J = 6.3 Hz, 1C), 131.8, 131.6 (d, J = 12.5 Hz, 1C), 131.1 (d, J = 9.0 Hz, 1C), 129.6 (d, J = 8.8 Hz, 1C), 129.4 (d, J = 12.5 Hz, 1C), 129.0, 128.6 (d, J = 6.3 Hz, 1C), 128.5, 127.0, 125.9 (d, J = 20.0 Hz, 1C), 125.2 (d, J = 4.0 Hz, 1C), 122.9...
null
[(142.9, 'd', 7.5), (141.6, 'd', 2.5), (133.5, None, None), (132.7, None, None), (131.9, 'd', 6.3), (131.8, None, None), (131.6, 'd', 12.5), (131.1, 'd', 9.0), (129.6, 'd', 8.8), (129.4, 'd', 12.5), (129.0, None, None), (128.6, 'd', 6.3), (128.5, None, None), (127.0, None, None), (125.9, 'd', 20.0), (125.2, 'd', 4.0), ...
29
20
20
10.1039_d4cc03507k
Cc1ccc(P(=O)(c2ccc(C)cc2)c2c(C)c3ccccc3c3ccccc23)cc1
10
10
[0.15078323 0.19921877 0.2902439 0.28789064]
[0.14857395 0.29785158 0.57551694 0.31152344]
31P NMR
202 MHz
CDCl3
30.52
null
[(30.52, None, None)]
1
1
1
10.1039_d4cc03507k
Cc1cc(C)cc(P(=O)(c2cc(C)cc(C)c2)c2c(C)c3ccccc3c3ccccc23)c1
10
10
[0.15078323 0.63203129 0.30101414 0.72578129]
[0.1474693 0.77070317 0.84946742 0.89531253]
1H NMR
500 MHz
CDCl3
8.73 (d, J = 10.0 Hz, 1H), 8.64 (d, J = 10.0 Hz, 1H), 8.44 (d, J = 5.0 Hz, 1H), 8.13 (d, J = 10.0 Hz, 1H), 7.75 (t, J = 10.0 Hz, 1H), 7.64 (t, J = 10.0 Hz, 1H), 7.50 (d, J = 10.0 Hz, 1H), 7.30 (s, 2H), 7.28 (s, 2H), 7.24 (s, 1H), 7.08 (s, 2H), 2.59 (s, 3H), 2.25 (s, 12H)
null
[('d', ['10.0Hz'], '1H', 8.73, 8.73), ('d', ['10.0Hz'], '1H', 8.64, 8.64), ('d', ['5.0Hz'], '1H', 8.44, 8.44), ('d', ['10.0Hz'], '1H', 8.13, 8.13), ('t', ['10.0Hz'], '1H', 7.75, 7.75), ('t', ['10.0Hz'], '1H', 7.64, 7.64), ('d', ['10.0Hz'], '1H', 7.5, 7.5), ('s', [], '2H', 7.3, 7.3), ('s', [], '2H', 7.28, 7.28), ('s', [...
29
12
29
10.1039_d4cc03507k
Cc1cc(C)cc(P(=O)(c2cc(C)cc(C)c2)c2c(C)c3ccccc3c3ccccc23)c1
10
10
[0.15078323 0.63203129 0.30101414 0.72578129]
[0.1474693 0.77070317 0.84946742 0.89531253]
13C NMR
125 MHz
CDCl3
142.7 (d, J = 7.5 Hz, 1C), 138.2 (d, J = 12.5 Hz, 1C), 136.3, 135.5, 133.1 (d, J = 2.5 Hz, 1C), 132.1 (d, J = 10.0 Hz, 1C), 131.9, 131.7 (d, J = 13.8 Hz, 1C), 129.7 (d, J = 8.8 Hz, 1C), 128.7 (d, J = 8.8 Hz, 1C), 128.4, 127.0, 126.2, 126.0, 125.8, 125.3, 122.9, 122.5, 21.4 (d, J = 7.5 Hz, 1C), 21.3
null
[(142.7, 'd', 7.5), (138.2, 'd', 12.5), (136.3, None, None), (135.5, None, None), (133.1, 'd', 2.5), (132.1, 'd', 10.0), (131.9, None, None), (131.7, 'd', 13.8), (129.7, 'd', 8.8), (128.7, 'd', 8.8), (128.4, None, None), (127.0, None, None), (126.2, None, None), (126.0, None, None), (125.8, None, None), (125.3, None, N...
31
20
20
10.1039_d4cc03507k
Cc1cc(C)cc(P(=O)(c2cc(C)cc(C)c2)c2c(C)c3ccccc3c3ccccc23)c1
10
10
[0.15078323 0.63203129 0.30101414 0.72578129]
[0.1474693 0.77070317 0.84946742 0.89531253]
31P NMR
202 MHz
CDCl3
31.55
null
[(31.55, None, None)]
1
1
1
10.1039_d4cc03507k
Cc1cc2c(C)c(P(c3ccccc3)(c3ccccc3)=O)c3ccccc3c2cc1C
11
11
[0.15050707 0.22656252 0.26345641 0.29765626]
[0.14802163 0.33535158 0.84836274 0.59765629]
1H NMR
400 MHz
CDCl3
8.63 (d, J = 12.0 Hz, 1H), 8.47 (s, 1H), 8.31 (d, J = 8.0 Hz, 1H), 7.86 (s, 1H), 7.72 (d, J = 8.0 Hz, 2H), 7.69 (d, J = 8.0 Hz, 2H), 7.47 (t, J = 8.0 Hz, 3H), 7.41-7.38 (m, 4H), 7.19 (t, J = 8.0 Hz, 1H), 2.56 (s, 6H), 2.48 (s, 3H)
null
[('d', ['12.0Hz'], '1H', 8.63, 8.63), ('s', [], '1H', 8.47, 8.47), ('d', ['8.0Hz'], '1H', 8.31, 8.31), ('s', [], '1H', 7.86, 7.86), ('d', ['8.0Hz'], '2H', 7.72, 7.72), ('d', ['8.0Hz'], '2H', 7.69, 7.69), ('t', ['8.0Hz'], '3H', 7.47, 7.47), ('m', [], '4H', 7.41, 7.38), ('t', ['8.0Hz'], '1H', 7.19, 7.19), ('s', [], '6H',...
25
12
25
10.1039_d4cc03507k
Cc1cc2c(C)c(P(c3ccccc3)(c3ccccc3)=O)c3ccccc3c2cc1C
11
11
[0.15050707 0.22656252 0.26345641 0.29765626]
[0.14802163 0.33535158 0.84836274 0.59765629]
13C NMR
100 MHz
CDCl3
142.9 (d, J = 8.0 Hz, 1C), 138.3, 137.1, 136.4, 136.1, 131.5 (d, J = 10.0 Hz, 1C), 131.1 (d, J = 10.0 Hz, 1C), 131.1, 130.3 (d, J = 2.0 Hz, 1C), 130.1 (d, J = 13.0 Hz, 1C), 129.4 (d, J = 9.0 Hz, 1C), 128.6 (d, J = 12.0 Hz, 1C), 128.5, 125.8, 125.5, 125.3, 123.3, 122.4, 21.4 (d, J = 8.0 Hz, 1C), 20.5, 20.3
null
[(142.9, 'd', 8.0), (138.3, None, None), (137.1, None, None), (136.4, None, None), (136.1, None, None), (131.5, 'd', 10.0), (131.1, 'd', 10.0), (131.1, None, None), (130.3, 'd', 2.0), (130.1, 'd', 13.0), (129.4, 'd', 9.0), (128.6, 'd', 12.0), (128.5, None, None), (125.8, None, None), (125.5, None, None), (125.3, None, ...
29
21
21
10.1039_d4cc03507k
Cc1cc2c(C)c(P(c3ccccc3)(c3ccccc3)=O)c3ccccc3c2cc1C
11
11
[0.15050707 0.22656252 0.26345641 0.29765626]
[0.14802163 0.33535158 0.84836274 0.59765629]
31P NMR
162 MHz
CDCl3
29.90
null
[(29.9, None, None)]
1
1
1
10.1039_d4cc03507k
O(c1cc2c(C)c(P(c3ccccc3)(c3ccccc3)=O)c3ccccc3c2cc1OC)C
11
11
[0.15050707 0.61328125 0.28554919 0.68828128]
[0.14912627 0.7058594 0.68100998 0.71914064]
1H NMR
400 MHz
CDCl3
8.51 (d, J = 12.0 Hz, 1H), 8.31 (d, J = 12.0 Hz, 1H), 8.04 (s, 1H), 7.73 (d, J = 8.0 Hz, 2H), 7.70 (d, J = 8.0 Hz, 2H), 7.47 (t, J = 8.0 Hz, 3H), 7.42-7.39 (m, 5H), 7.18 (t, J = 8.0 Hz, 1H), 4.16 (s, 3H), 4.02 (s, 3H), 2.60 (s, 3H)
null
[('d', ['12.0Hz'], '1H', 8.51, 8.51), ('d', ['12.0Hz'], '1H', 8.31, 8.31), ('s', [], '1H', 8.04, 8.04), ('d', ['8.0Hz'], '2H', 7.73, 7.73), ('d', ['8.0Hz'], '2H', 7.7, 7.7), ('t', ['8.0Hz'], '3H', 7.47, 7.47), ('m', [], '5H', 7.42, 7.39), ('t', ['8.0Hz'], '1H', 7.18, 7.18), ('s', [], '3H', 4.16, 4.16), ('s', [], '3H', ...
25
12
25
10.1039_d4cc03507k
O(c1cc2c(C)c(P(c3ccccc3)(c3ccccc3)=O)c3ccccc3c2cc1OC)C
11
11
[0.15050707 0.61328125 0.28554919 0.68828128]
[0.14912627 0.7058594 0.68100998 0.71914064]
13C NMR
100 MHz
CDCl3
150.8, 149.4, 142.1 (d, J = 8.0 Hz, 1C), 137.1, 136.1, 131.4 (d, J = 10.0 Hz, 1C), 131.2 (d, J = 10.0 Hz, 1C), 129.1 (d, J = 9.0 Hz, 1C), 128.6 (d, J = 12.0 Hz, 1C), 127.3 (d, J = 2.0 Hz, 1C), 126.7 (d, J = 12.0 Hz, 1C), 125.7, 124.9, 123.6, 122.6, 122.2, 105.4, 103.3, 56.0, 55.9, 21.5 (d, J = 8.0 Hz, 1C)
null
[(150.8, None, None), (149.4, None, None), (142.1, 'd', 8.0), (137.1, None, None), (136.1, None, None), (131.4, 'd', 10.0), (131.2, 'd', 10.0), (129.1, 'd', 9.0), (128.6, 'd', 12.0), (127.3, 'd', 2.0), (126.7, 'd', 12.0), (125.7, None, None), (124.9, None, None), (123.6, None, None), (122.6, None, None), (122.2, None, ...
29
21
21
10.1039_d4cc03507k
O(c1cc2c(C)c(P(c3ccccc3)(c3ccccc3)=O)c3ccccc3c2cc1OC)C
11
11
[0.15050707 0.61328125 0.28554919 0.68828128]
[0.14912627 0.7058594 0.68100998 0.71914064]
31P NMR
162 MHz
CDCl3
30.26
null
[(30.26, None, None)]
1
1
1
10.1039_d4cc03507k
Cc1c(P(c2ccccc2)(c2ccccc2)=O)c2ccccc2c2cc(F)c(F)cc12
12
12
[0.15050707 0.61484381 0.26594183 0.68828128]
[0.14802163 0.73398443 0.84836274 0.91250001]
1H NMR
500 MHz
CDCl3
8.45-8.41 (m, 2H), 8.33 (d, J = 5.0 Hz, 1H), 7.88 (dd, J1 = 10.0 Hz, J2 = 5.0 Hz, 1H), 7.70 (dd, J1 = 10.0 Hz, J2 = 5.0 Hz, 4H), 7.51 (dd, J1 = 15.0 Hz, J2 = 5.0 Hz, 3H), 7.44-7.41 (m, 4H), 7.25 (d, J = 10.0 Hz, 1H), 2.55 (d, J = 5.0 Hz, 3H)
null
[('m', [], '2H', 8.45, 8.41), ('d', ['5.0Hz'], '1H', 8.33, 8.33), ('dd', "['10.0Hz', '5.0Hz']", '1H', 7.88, 7.88), ('dd', "['10.0Hz', '5.0Hz']", '4H', 7.7, 7.7), ('dd', "['15.0Hz', '5.0Hz']", '3H', 7.51, 7.51), ('m', [], '4H', 7.44, 7.41), ('d', ['10.0Hz'], '1H', 7.25, 7.25), ('d', ['5.0Hz'], '3H', 2.55, 2.55)]
19
10
19
10.1039_d4cc03507k
Cc1c(P(c2ccccc2)(c2ccccc2)=O)c2ccccc2c2cc(F)c(F)cc12
12
12
[0.15050707 0.61484381 0.26594183 0.68828128]
[0.14802163 0.73398443 0.84836274 0.91250001]
13C NMR
125 MHz
CDCl3
152.2 (d, J = 15.0 Hz, 1C), 151.0, 150.2, 141.8, 136.2, 135.4, 131.8 (d, J = 2.5 Hz, 1C), 131.7 (d, J = 2.5 Hz, 1C), 131.5 (d, J = 2.5 Hz, 1C), 131.1 (d, J = 9.0 Hz, 1C), 129.7, 128.8 (d, J = 12.5 Hz, 1C), 128.2 (d, J = 12.5 Hz, 1C), 126.5, 126.3, 122.7, 112.9 (d, J = 20.0 Hz, 1C), 110.6 (d, J = 17.5 Hz, 1C), 21.4 (d, ...
null
[(152.2, 'd', 15.0), (151.0, None, None), (150.2, None, None), (141.8, None, None), (136.2, None, None), (135.4, None, None), (131.8, 'd', 2.5), (131.7, 'd', 2.5), (131.5, 'd', 2.5), (131.1, 'd', 9.0), (129.7, None, None), (128.8, 'd', 12.5), (128.2, 'd', 12.5), (126.5, None, None), (126.3, None, None), (122.7, None, N...
27
19
19
10.1039_d4cc03507k
Cc1c(P(c2ccccc2)(c2ccccc2)=O)c2ccccc2c2cc(F)c(F)cc12
12
12
[0.15050707 0.61484381 0.26594183 0.68828128]
[0.14802163 0.73398443 0.84836274 0.91250001]
19F NMR
470 MHz
CDCl3
-133.96,-136.14
null
[(-133.96, None, None), (-136.14, None, None)]
2
2
2
10.1039_d4cc03507k
Cc1c(P(c2ccccc2)(c2ccccc2)=O)c2ccccc2c2cc(F)c(F)cc12
12
12
[0.15050707 0.61484381 0.26594183 0.68828128]
[0.14802163 0.73398443 0.84836274 0.91250001]
31P NMR
202 MHz
CDCl3
30.24
null
[(30.24, None, None)]
1
1
1
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(C2C(=C(C)C)c3ccccc3-c3ccccc32)=O)cc1
13
13
[0.15105939 0.59375004 0.24661065 0.65312503]
[0.14912627 0.66796882 0.75115454 0.68203126]
1H NMR
400 MHz
CDCl3
7.61-7.57 (m, 3H), 7.42 (t, J = 8.0 Hz, 1H), 7.32-7.22 (m, 8H), 7.20-7.11 (m, 5H), 7.01 (t, J = 8.0 Hz, 1H), 4.95 (d, J = 20.0 Hz, 1H), 1.94 (d, J = 8.0 Hz, 3H), 1.75 (d, J = 4.0 Hz, 3H)
null
[('m', [], '3H', 7.61, 7.57), ('t', ['8.0Hz'], '1H', 7.42, 7.42), ('m', [], '8H', 7.32, 7.22), ('m', [], '5H', 7.2, 7.11), ('t', ['8.0Hz'], '1H', 7.01, 7.01), ('d', ['20.0Hz'], '1H', 4.95, 4.95), ('d', ['8.0Hz'], '3H', 1.94, 1.94), ('d', ['4.0Hz'], '3H', 1.75, 1.75)]
25
13
25
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(C2C(=C(C)C)c3ccccc3-c3ccccc32)=O)cc1
13
13
[0.15105939 0.59375004 0.24661065 0.65312503]
[0.14912627 0.66796882 0.75115454 0.68203126]
13C NMR
100 MHz
CDCl3
135.6 (d, J = 4.0 Hz, 1C), 134.9 (d, J = 2.0 Hz, 1C), 133.9 (d, J = 3.0 Hz, 1C), 133.2 (d, J = 12.0 Hz, 1C), 132.1 (q, J = 9.0 Hz, 1C), 131.4 (d, J = 3.0 Hz, 1C), 131.1 (d, J = 9.0 Hz, 1C), 129.7 (d, J = 5.0 Hz, 1C), 129.6 (d, J = 1.0 Hz, 1C), 128.8, 127.8 (d, J = 3.0 Hz, 1C), 127.6 (d, J = 12.0 Hz, 1C), 127.5, 127.2 (...
null
[(135.6, 'd', 4.0), (134.9, 'd', 2.0), (133.9, 'd', 3.0), (133.2, 'd', 12.0), (132.1, 'q', 9.0), (131.4, 'd', 3.0), (131.1, 'd', 9.0), (129.7, 'd', 5.0), (129.6, 'd', 1.0), (128.8, None, None), (127.8, 'd', 3.0), (127.6, 'd', 12.0), (127.5, None, None), (127.2, 'd', 3.0), (126.6, None, None), (124.3, 'd', 7.0), (123.7,...
29
20
21
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(C2C(=C(C)C)c3ccccc3-c3ccccc32)=O)cc1
13
13
[0.15105939 0.59375004 0.24661065 0.65312503]
[0.14912627 0.66796882 0.75115454 0.68203126]
31P NMR
162 MHz
CDCl3
27.79
null
[(27.79, None, None)]
1
1
1
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(=O)/C=C(\C2=CCCCC2)c2ccccc2)cc1
14
14
[0.15078323 0.17177736 0.24578219 0.23984377]
[0.1474693 0.27968751 0.84891508 0.51250003]
1H NMR
400 MHz
CDCl3
7.87-7.82 (m, 4H), 7.47-7.39 (m, 8H), 7.36-7.34 (m, 3H), 6.39 (d, J = 20.0 Hz, 1H), 6.30 (s, 1H), 1.92 (d, J = 4.0 Hz, 2H), 1.50 (s, 2H), 1.18-1.13 (m, 2H), 1.08-1.04 (m, 2H)
null
[('m', [], '4H', 7.87, 7.82), ('m', [], '8H', 7.47, 7.39), ('m', [], '3H', 7.36, 7.34), ('d', ['20.0Hz'], '1H', 6.39, 6.39), ('s', [], '1H', 6.3, 6.3), ('d', ['4.0Hz'], '2H', 1.92, 1.92), ('s', [], '2H', 1.5, 1.5), ('m', [], '2H', 1.18, 1.13), ('m', [], '2H', 1.08, 1.04)]
25
12
25
10.1039_d4cc03507k
c1ccc(P(c2ccccc2)(=O)/C=C(\C2=CCCCC2)c2ccccc2)cc1
14
14
[0.15078323 0.17177736 0.24578219 0.23984377]
[0.1474693 0.27968751 0.84891508 0.51250003]
31P NMR
162 MHz
CDCl3
18.16
null
[(18.16, None, None)]
1
1
1
10.1039_d4cc03507k
O=P(C1C=CC=CC=1)(C1C=CC=CC=1)CC1C2C(=CC=CC=2)C2C(=CC=CC=2)C=1
14
14
[0.15050707 0.52890627 0.25434313 0.58828126]
[0.14691699 0.63203129 0.84836274 0.89296876]
1H NMR
400 MHz
CDCl3
8.66 (d, J = 8.0 Hz, 1H), 8.61 (d, J = 8.0 Hz, 1H), 8.01 (d, J = 8.0 Hz, 1H), 7.75-7.71 (m, 4H), 7.65 (d, J = 8.0 Hz, 1H), 7.59 (t, J = 8.0 Hz, 2H), 7.53-7.46 (m, 5H), 7.41-7.36 (m, 4H), 4.14 (d, J = 16.0 Hz, 2H)
null
[('d', ['8.0Hz'], '1H', 8.66, 8.66), ('d', ['8.0Hz'], '1H', 8.61, 8.61), ('d', ['8.0Hz'], '1H', 8.01, 8.01), ('m', [], '4H', 7.75, 7.71), ('d', ['8.0Hz'], '1H', 7.65, 7.65), ('t', ['8.0Hz'], '2H', 7.59, 7.59), ('m', [], '5H', 7.53, 7.46), ('m', [], '4H', 7.41, 7.36), ('d', ['16.0Hz'], '2H', 4.14, 4.14)]
21
13
21
10.1039_d4cc03507k
O=P(C1C=CC=CC=1)(C1C=CC=CC=1)CC1C2C(=CC=CC=2)C2C(=CC=CC=2)C=1
14
14
[0.15050707 0.52890627 0.25434313 0.58828126]
[0.14691699 0.63203129 0.84836274 0.89296876]
13C NMR
100 MHz
CDCl3
132.9, 131.9, 131.7 (d, J = 2.0 Hz, 1C), 131.2, 131.2 (d, J = 2.0 Hz, 1C), 131.1, 130.5 (d, J = 1.0 Hz, 1C), 129.8 (d, J = 2.0 Hz, 1C), 129.4 (d, J = 7.0 Hz, 1C), 128.4 (d, J = 12.0 Hz, 1C), 128.2 (d, J = 1.0 Hz, 1C), 126.5, 126.4, 126.3 (d, J = 8.0 Hz, 1C), 126.2, 125.0, 122.8, 122.3 (d, J = 1.0 Hz, 1C), 35.1 (d, J = ...
null
[(132.9, None, None), (131.9, None, None), (131.7, 'd', 2.0), (131.2, None, None), (131.2, 'd', 2.0), (131.1, None, None), (130.5, 'd', 1.0), (129.8, 'd', 2.0), (129.4, 'd', 7.0), (128.4, 'd', 12.0), (128.2, 'd', 1.0), (126.5, None, None), (126.4, None, None), (126.3, 'd', 8.0), (126.2, None, None), (125.0, None, None)...
27
19
19
10.1039_d4cc03507k
O=P(C1C=CC=CC=1)(C1C=CC=CC=1)CC1C2C(=CC=CC=2)C2C(=CC=CC=2)C=1
14
14
[0.15050707 0.52890627 0.25434313 0.58828126]
[0.14691699 0.63203129 0.84836274 0.89296876]
31P NMR
162 MHz
CDCl3
29.53
null
[(29.53, None, None)]
1
1
1
10.1039_d4cc03507k
CC(C)[P+]1(C(C)C)C(c2ccccc2)=C(C)Oc2c1cccc2.O=S(=O)(C(F)(F)F)[O-]
15
15
[0.14995474 0.35000001 0.28002599 0.39609377]
[0.14760739 0.40859376 0.68432387 0.44921879]
1H NMR
400 MHz
CDCl3
8.03 (t, J = 8.0 Hz, 1H), 7.81 (t, J = 8.0 Hz, 1H), 7.59 (t, J = 8.0 Hz, 1H), 7.55-7.47 (m, 3H), 7.40 (dd, J1 = 8.0 Hz, J2 = 4.0 Hz, 1H), 7.26 (d, J = 8.0 Hz, 2H), 3.24-3.11 (m, 2H), 2.17 (s, 3H), 1.32 (dd, J1 = 12.0 Hz, J2 = 4.0 Hz, 6H), 0.97 (dd, J1 = 12.0 Hz, J2 = 4.0 Hz, 6H)
null
[('t', ['8.0Hz'], '1H', 8.03, 8.03), ('t', ['8.0Hz'], '1H', 7.81, 7.81), ('t', ['8.0Hz'], '1H', 7.59, 7.59), ('m', [], '3H', 7.55, 7.47), ('dd', "['8.0Hz', '4.0Hz']", '1H', 7.4, 7.4), ('d', ['8.0Hz'], '2H', 7.26, 7.26), ('m', [], '2H', 3.24, 3.11), ('s', [], '3H', 2.17, 2.17), ('dd', "['12.0Hz', '4.0Hz']", '6H', 1.32, ...
26
10
26
10.1039_d4cc03507k
CC(C)[P+]1(C(C)C)C(c2ccccc2)=C(C)Oc2c1cccc2.O=S(=O)(C(F)(F)F)[O-]
15
15
[0.14995474 0.35000001 0.28002599 0.39609377]
[0.14760739 0.40859376 0.68432387 0.44921879]
19F NMR
376 MHz
CDCl3
-78.23
null
[(-78.23, None, None)]
3
1
1
10.1039_d4cc03507k
CC(C)[P+]1(C(C)C)C(c2ccccc2)=C(C)Oc2c1cccc2.O=S(=O)(C(F)(F)F)[O-]
15
15
[0.14995474 0.35000001 0.28002599 0.39609377]
[0.14760739 0.40859376 0.68432387 0.44921879]
31P NMR
162 MHz
CDCl3
11.88
null
[(11.88, None, None)]
1
1
1
10.1039_d4cc03507k
CC(C)[P+]1(C(C)C)C(c2ccccc2)=C(C)Oc2c1cc(C)c(C)c2.O=S(=O)(C(F)(F)F)[O-]
15
15
[0.1488501 0.76640628 0.29549095 0.81250007]
[0.14912627 0.82656251 0.7246432 0.86718757]
1H NMR
400 MHz
CDCl3
7.74 (d, J = 12.0 Hz, 1H), 7.55-7.47 (m, 3H), 7.25 (d, J = 8.0 Hz, 2H), 7.17 (d, J = 4.0 Hz, 1H), 3.22-3.09 (m, 2H), 2.40 (s, 3H), 2.39 (s, 3H), 2.14 (s, 3H), 1.32 (dd, J1 = 20.0 Hz, J2 = 8.0 Hz, 6H), 0.97 (dd, J1 = 20.0 Hz, J2 = 8.0 Hz, 6H)
null
[('d', ['12.0Hz'], '1H', 7.74, 7.74), ('m', [], '3H', 7.55, 7.47), ('d', ['8.0Hz'], '2H', 7.25, 7.25), ('d', ['4.0Hz'], '1H', 7.17, 7.17), ('m', [], '2H', 3.22, 3.09), ('s', [], '3H', 2.4, 2.4), ('s', [], '3H', 2.39, 2.39), ('s', [], '3H', 2.14, 2.14), ('dd', "['20.0Hz', '8.0Hz']", '6H', 1.32, 1.32), ('dd', "['20.0Hz',...
30
10
30
10.1039_d4cc03507k
CC(C)[P+]1(C(C)C)C(c2ccccc2)=C(C)Oc2c1cc(C)c(C)c2.O=S(=O)(C(F)(F)F)[O-]
15
15
[0.1488501 0.76640628 0.29549095 0.81250007]
[0.14912627 0.82656251 0.7246432 0.86718757]
13C NMR
100 MHz
CDCl3
167.6, 154.2, 147.3, 137.3 (d, J = 11.0 Hz, 1C), 131.3 (d, J = 5.0 Hz, 1C), 130.6 (d, J = 6.0 Hz, 1C), 130.3 (d, J = 3.0 Hz, 1C), 130.1 (d, J = 1.0 Hz, 1C), 129.9 (d, J = 2.0 Hz, 1C), 122.5, 119.5 (d, J = 6.0 Hz, 1C), 92.0 (d, J = 80.0 Hz, 1C), 88.1 (d, J = 76.0 Hz, 1C), 23.2 (d, J = 48.0 Hz, 1C), 20.5, 19.0, 15.5 (d, ...
null
[(167.6, None, None), (154.2, None, None), (147.3, None, None), (137.3, 'd', 11.0), (131.3, 'd', 5.0), (130.6, 'd', 6.0), (130.3, 'd', 3.0), (130.1, 'd', 1.0), (129.9, 'd', 2.0), (122.5, None, None), (119.5, 'd', 6.0), (92.0, 'd', 80.0), (88.1, 'd', 76.0), (23.2, 'd', 48.0), (20.5, None, None), (19.0, None, None), (15....
24
18
18
10.1039_d4cc03507k
CC(C)[P+]1(C(C)C)C(c2ccccc2)=C(C)Oc2c1cc(C)c(C)c2.O=S(=O)(C(F)(F)F)[O-]
15
15
[0.1488501 0.76640628 0.29549095 0.81250007]
[0.14912627 0.82656251 0.7246432 0.86718757]
19F NMR
376 MHz
CDCl3
-78.21
null
[(-78.21, None, None)]
3
1
1
10.1039_d4cc03507k
CC(C)[P+]1(C(C)C)C(c2ccccc2)=C(C)Oc2c1cc(C)c(C)c2.O=S(=O)(C(F)(F)F)[O-]
15
15
[0.1488501 0.76640628 0.29549095 0.81250007]
[0.14912627 0.82656251 0.7246432 0.86718757]
31P NMR
162 MHz
CDCl3
11.61
null
[(11.61, None, None)]
1
1
1
10.1039_d4cc03507k
CC(C)[P+]1(C(C)C)C(c2ccccc2)=C(C)Oc2c1cc1ccccc1c2.O=S(=O)(C(F)(F)F)[O-]
16
16
[0.14967859 0.36796878 0.31040356 0.41406254]
[0.1474693 0.42734377 0.7274048 0.46796879]
1H NMR
400 MHz
CDCl3
8.97 (d, J = 12.0 Hz, 1H), 8.39 (d, J = 8.0 Hz, 1H), 7.89 (d, J = 8.0 Hz, 1H), 7.81 (d, J = 4.0 Hz, 1H), 7.71 (t, J = 8.0 Hz, 1H), 7.61 (t, J = 8.0 Hz, 1H), 7.57-7.50 (m, 3H), 7.29 (d, J = 8.0 Hz, 2H), 3.44-3.35 (m, 2H), 2.22 (s, 3H), 1.37 (dd, J1 = 20.0 Hz, J2 = 8.0 Hz, 6H), 1.00 (dd, J1 = 20.0 Hz, J2 = 8.0 Hz, 6H)
null
[('d', ['12.0Hz'], '1H', 8.97, 8.97), ('d', ['8.0Hz'], '1H', 8.39, 8.39), ('d', ['8.0Hz'], '1H', 7.89, 7.89), ('d', ['4.0Hz'], '1H', 7.81, 7.81), ('t', ['8.0Hz'], '1H', 7.71, 7.71), ('t', ['8.0Hz'], '1H', 7.61, 7.61), ('m', [], '3H', 7.57, 7.5), ('d', ['8.0Hz'], '2H', 7.29, 7.29), ('m', [], '2H', 3.44, 3.35), ('s', [],...
28
12
28
10.1039_d4cc03507k
CC(C)[P+]1(C(C)C)C(c2ccccc2)=C(C)Oc2c1cc1ccccc1c2.O=S(=O)(C(F)(F)F)[O-]
16
16
[0.14967859 0.36796878 0.31040356 0.41406254]
[0.1474693 0.42734377 0.7274048 0.46796879]
19F NMR
376 MHz
CDCl3
-78.21
null
[(-78.21, None, None)]
3
1
1
10.1039_d4cc03507k
CC(C)[P+]1(C(C)C)C(c2ccccc2)=C(C)Oc2c1cc1ccccc1c2.O=S(=O)(C(F)(F)F)[O-]
16
16
[0.14967859 0.36796878 0.31040356 0.41406254]
[0.1474693 0.42734377 0.7274048 0.46796879]
31P NMR
162 MHz
CDCl3
12.38
null
[(12.38, None, None)]
1
1
1
10.1039_d4cc03507k
C1CCC([P+]2(C3CCCCC3)C(c3ccccc3)=C(C)Oc3c2cccc3)CC1.O=S(=O)(C(F)(F)F)[O-]
16
16
[0.14995474 0.81328128 0.27864519 0.86015628]
[0.1474693 0.87187503 0.69371329 0.91250001]
1H NMR
400 MHz
CDCl3
8.06 (t, J = 8.0 Hz, 1H), 7.79 (t, J = 8.0 Hz, 1H), 7.61 (t, J = 8.0 Hz, 1H), 7.56-7.49 (m, 3H), 7.38 (dd, J1 = 8.0 Hz, J2 = 4.0 Hz, 1H), 7.21 (d, J = 8.0 Hz, 2H), 2.77 (q, J = 8.0 Hz, 2H), 2.15 (s, 3H), 1.85-1.65 (m, 10H), 1.44-1.36 (m, 6H), 1.00-0.90 (m, 2H), 0.61-0.52 (m, 2H)
null
[('t', ['8.0Hz'], '1H', 8.06, 8.06), ('t', ['8.0Hz'], '1H', 7.79, 7.79), ('t', ['8.0Hz'], '1H', 7.61, 7.61), ('m', [], '3H', 7.56, 7.49), ('dd', "['8.0Hz', '4.0Hz']", '1H', 7.38, 7.38), ('d', ['8.0Hz'], '2H', 7.21, 7.21), ('q', ['8.0Hz'], '2H', 2.77, 2.77), ('s', [], '3H', 2.15, 2.15), ('m', [], '10H', 1.85, 1.65), ('m...
34
12
34
10.1039_d4cc03507k
C1CCC([P+]2(C3CCCCC3)C(c3ccccc3)=C(C)Oc3c2cccc3)CC1.O=S(=O)(C(F)(F)F)[O-]
16
16
[0.14995474 0.81328128 0.27864519 0.86015628]
[0.1474693 0.87187503 0.69371329 0.91250001]
19F NMR
376 MHz
CDCl3
-78.12
null
[(-78.12, None, None)]
3
1
1
10.1039_d4cc03507k
C1CCC([P+]2(C3CCCCC3)C(c3ccccc3)=C(C)Oc3c2cccc3)CC1.O=S(=O)(C(F)(F)F)[O-]
16
16
[0.14995474 0.81328128 0.27864519 0.86015628]
[0.1474693 0.87187503 0.69371329 0.91250001]
31P NMR
162 MHz
CDCl3
4.34
null
[(4.34, None, None)]
1
1
1
10.1039_d4cc03507k
C1CCC([P+]2(C3CCCCC3)C(c3ccccc3)=C(C)Oc3c2cc(C)c(C)c3)CC1.O=S(=O)(C(F)(F)F)[O-]
17
17
[0.14857395 0.39648441 0.29549095 0.44257813]
[0.14802163 0.45507816 0.73568959 0.49648439]
1H NMR
400 MHz
CDCl3
7.73 (d, J = 12.0 Hz, 1H), 7.55-7.50 (m, 3H), 7.21 (d, J = 8.0 Hz, 2H), 7.16 (d, J = 4.0 Hz, 1H), 2.79-2.71 (m, 2H), 2.42 (s, 3H), 2.38 (s, 3H), 2.12 (s, 3H), 1.87-1.85 (m, 4H), 1.70-1.67 (m, 6H), 1.48-1.35 (m, 6H), 1.03-0.94 (m, 2H), 0.63-0.57 (m, 2H)
null
[('d', ['12.0Hz'], '1H', 7.73, 7.73), ('m', [], '3H', 7.55, 7.5), ('d', ['8.0Hz'], '2H', 7.21, 7.21), ('d', ['4.0Hz'], '1H', 7.16, 7.16), ('m', [], '2H', 2.79, 2.71), ('s', [], '3H', 2.42, 2.42), ('s', [], '3H', 2.38, 2.38), ('s', [], '3H', 2.12, 2.12), ('m', [], '4H', 1.87, 1.85), ('m', [], '6H', 1.7, 1.67), ('m', [],...
38
12
38
10.1039_d4cc03507k
C1CCC([P+]2(C3CCCCC3)C(c3ccccc3)=C(C)Oc3c2cc(C)c(C)c3)CC1.O=S(=O)(C(F)(F)F)[O-]
17
17
[0.14857395 0.39648441 0.29549095 0.44257813]
[0.14802163 0.45507816 0.73568959 0.49648439]
19F NMR
376 MHz
CDCl3
-78.16
null
[(-78.16, None, None)]
3
1
1
10.1039_d4cc03507k
C1CCC([P+]2(C3CCCCC3)C(c3ccccc3)=C(C)Oc3c2cc(C)c(C)c3)CC1.O=S(=O)(C(F)(F)F)[O-]
17
17
[0.14857395 0.39648441 0.29549095 0.44257813]
[0.14802163 0.45507816 0.73568959 0.49648439]
31P NMR
162 MHz
CDCl3
4.15
null
[(4.15, None, None)]
1
1
1
10.1039_d4cc03507k
Cc1c(P(c2ccccc2)c2ccccc2)c2ccccc2c2ccccc12
18
18
[0.15078323 0.58515629 0.24550602 0.64375004]
[0.14802163 0.68671879 0.84946742 0.89453132]
1H NMR
400 MHz
CDCl3
8.80 (d, J = 8.0 Hz, 1H), 8.74 (d, J = 8.0 Hz, 1H), 8.45 (dd, J1 = 8.0 Hz, J2 = 4.0 Hz, 1H), 8.25 (d, J = 8.0 Hz, 1H), 7.77 (t, J = 8.0 Hz, 1H), 7.70 (t, J = 8.0 Hz, 1H), 7.55 (d, J = 8.0 Hz, 1H), 7.50 (t, J = 8.0 Hz, 4H), 7.31 (q, J = 8.0 Hz, 7H), 3.04 (s, 3H)
null
[('d', ['8.0Hz'], '1H', 8.8, 8.8), ('d', ['8.0Hz'], '1H', 8.74, 8.74), ('dd', "['8.0Hz', '4.0Hz']", '1H', 8.45, 8.45), ('d', ['8.0Hz'], '1H', 8.25, 8.25), ('t', ['8.0Hz'], '1H', 7.77, 7.77), ('t', ['8.0Hz'], '1H', 7.7, 7.7), ('d', ['8.0Hz'], '1H', 7.55, 7.55), ('t', ['8.0Hz'], '4H', 7.5, 7.5), ('q', ['8.0Hz'], '7H', 7....
21
12
21
10.1039_d4cc03507k
Cc1c(P(c2ccccc2)c2ccccc2)c2ccccc2c2ccccc12
18
18
[0.15078323 0.58515629 0.24550602 0.64375004]
[0.14802163 0.68671879 0.84946742 0.89453132]
13C NMR
100 MHz
CDCl3
144.1 (d, J = 20.0 Hz, 1C), 136.7 (d, J = 15.0 Hz, 1C), 133.4 (d, J = 10.0 Hz, 1C), 131.9 (d, J = 5.0 Hz, 1C), 131.5, 131.4, 131.2, 130.1 (d, J = 3.0 Hz, 1C), 129.6 (d, J = 18.0 Hz, 1C), 129.0 (d, J = 17.0 Hz, 1C), 128.4 (d, J = 5.0 Hz, 1C), 127.7, 127.4, 126.8, 126.0, 125.7 (d, J = 2.0 Hz, 1C), 125.7, 122.7 (d, J = 19...
null
[(144.1, 'd', 20.0), (136.7, 'd', 15.0), (133.4, 'd', 10.0), (131.9, 'd', 5.0), (131.5, None, None), (131.4, None, None), (131.2, None, None), (130.1, 'd', 3.0), (129.6, 'd', 18.0), (129.0, 'd', 17.0), (128.4, 'd', 5.0), (127.7, None, None), (127.4, None, None), (126.8, None, None), (126.0, None, None), (125.7, 'd', 2....
27
19
19
10.1039_d4cc03507k
Cc1c(P(c2ccccc2)c2ccccc2)c2ccccc2c2ccccc12
18
18
[0.15078323 0.58515629 0.24550602 0.64375004]
[0.14802163 0.68671879 0.84946742 0.89453132]
31P NMR
162 MHz
CDCl3
-17.58
null
[(-17.58, None, None)]
1
1
1
10.1039_d4cc03507k
CCOC(=O)CC(c1c(C)c2ccccc2c2ccccc12)P(c1ccccc1)(c1ccccc1)=O
19
19
[0.15078323 0.43007814 0.26400872 0.50195316]
[0.1474693 0.54843752 0.84891508 0.86718757]
1H NMR
400 MHz
CDCl3
8.60-8.52 (m, 3H), 8.07 (d, J = 12.0 Hz, 1H), 7.82 (dd, J1 = 12.0 Hz, J2 = 8.0 Hz, 2H), 7.65 (t, J = 8.0 Hz, 1H), 7.56 (t, J = 8.0 Hz, 1H), 7.52-7.39 (m, 5H), 7.09 (d, J = 4.0 Hz, 2H), 6.82 (d, J = 8.0 Hz, 3H), 4.78-4.72 (m, 1H), 4.07-3.99 (m, 2H), 3.56-3.50 (m, 1H), 3.49-3.35 (m, 1H), 2.91 (s, 3H), 1.09 (t, J = 8.0 Hz...
null
[('m', [], '3H', 8.6, 8.52), ('d', ['12.0Hz'], '1H', 8.07, 8.07), ('dd', "['12.0Hz', '8.0Hz']", '2H', 7.82, 7.82), ('t', ['8.0Hz'], '1H', 7.65, 7.65), ('t', ['8.0Hz'], '1H', 7.56, 7.56), ('m', [], '5H', 7.52, 7.39), ('d', ['4.0Hz'], '2H', 7.09, 7.09), ('d', ['8.0Hz'], '3H', 6.82, 6.82), ('m', [], '1H', 4.78, 4.72), ('m...
29
16
29
10.1039_d4cc03507k
CCOC(=O)CC(c1c(C)c2ccccc2c2ccccc12)P(c1ccccc1)(c1ccccc1)=O
19
19
[0.15078323 0.43007814 0.26400872 0.50195316]
[0.1474693 0.54843752 0.84891508 0.86718757]
13C NMR
100 MHz
CDCl3
171.8 (d, J = 16.0 Hz, 1C), 144.1 (d, J = 9.0 Hz, 1C), 137.1, 136.0 (d, J = 5.0 Hz, 1C), 131.6, 131.4-131.3 (m, 1C), 130.3 (d, J = 9.0 Hz, 1C), 129.2 (d, J = 9.0 Hz, 1C), 128.9 (d, J = 11.0 Hz, 1C), 128.7 (d, J = 6.0 Hz, 1C), 128.3, 127.6 (d, J = 2.0 Hz, 1C), 127.1 (d, J = 5.0 Hz, 1C), 126.9 (d, J = 2.0 Hz, 1C), 126.8,...
null
[(171.8, 'd', 16.0), (144.1, 'd', 9.0), (137.1, None, None), (136.0, 'd', 5.0), (131.6, None, None), ([131.4, 131.3], 'm', None), (130.3, 'd', 9.0), (129.2, 'd', 9.0), (128.9, 'd', 11.0), (128.7, 'd', 6.0), (128.3, None, None), (127.6, 'd', 2.0), (127.1, 'd', 5.0), (126.9, 'd', 2.0), (126.8, None, None), (125.8, 'd', 1...
32
24
24
10.1039_d4cc03507k
CCOC(=O)CC(c1c(C)c2ccccc2c2ccccc12)P(c1ccccc1)(c1ccccc1)=O
19
19
[0.15078323 0.43007814 0.26400872 0.50195316]
[0.1474693 0.54843752 0.84891508 0.86718757]
31P NMR
162 MHz
CDCl3
40.91
null
[(40.91, None, None)]
1
1
1
10.1039_d4cc02865a
CS(=O)(=O)C=C(c1ccccc1)N(Cc1ccccc1)C(C)=O
2
2
[0.15078323 0.12343751 0.26842729 0.19648438]
[0.1474693 0.21445313 0.85001971 0.3933594 ]
1H NMR
400 MHz
CDCl3
7.57-7.43 (m, 5H), 7.36-7.23 (m, 3H), 7.20-7.12 (m, 2H), 6.21 (s, 1H), 4.62 (s, 2H), 2.67 (s, 3H), 2.20 (s, 3H)
null
[('m', [], '5H', 7.57, 7.43), ('m', [], '3H', 7.36, 7.23), ('m', [], '2H', 7.2, 7.12), ('s', [], '1H', 6.21, 6.21), ('s', [], '2H', 4.62, 4.62), ('s', [], '3H', 2.67, 2.67), ('s', [], '3H', 2.2, 2.2)]
19
10
19
10.1039_d4cc02865a
CS(=O)(=O)C=C(c1ccccc1)N(Cc1ccccc1)C(C)=O
2
2
[0.15078323 0.12343751 0.26842729 0.19648438]
[0.1474693 0.21445313 0.85001971 0.3933594 ]
13C NMR
100 MHz
CDCl3
170.2, 151.9, 136.2, 132.1, 131.7, 129.8, 128.74, 128.70, 128.4, 127.9, 127.5, 50.5, 43.2, 23.2
null
[(170.2, None, None), (151.9, None, None), (136.2, None, None), (132.1, None, None), (131.7, None, None), (129.8, None, None), (128.74, None, None), (128.7, None, None), (128.4, None, None), (127.9, None, None), (127.5, None, None), (50.5, None, None), (43.2, None, None), (23.2, None, None)]
18
14
14
10.1039_d4cc02865a
S(/C=C(\c1ccccc1C)N(Cc1ccccc1)C(C)=O)(C)(=O)=O
2
2
[0.15409714 0.43867188 0.26566569 0.51132815]
[0.14691699 0.52890627 0.84836274 0.71015629]
1H NMR
400 MHz
CDCl3
7.39 (td, J = 7.5, 1.6 Hz, 1H), 7.35-7.17 (m, 6H), 7.09-7.02 (m, 2H), 6.49 (s, 1H), 4.55 (s, 2H), 2.70 (s, 3H), 2.34 (s, 3H), 2.25 (s, 3H)
null
[('td', ['7.5Hz', '1.6Hz'], '1H', 7.39, 7.39), ('m', [], '6H', 7.35, 7.17), ('m', [], '2H', 7.09, 7.02), ('s', [], '1H', 6.49, 6.49), ('s', [], '2H', 4.55, 4.55), ('s', [], '3H', 2.7, 2.7), ('s', [], '3H', 2.34, 2.34), ('s', [], '3H', 2.25, 2.25)]
21
12
21
10.1039_d4cc02865a
S(/C=C(\c1ccccc1C)N(Cc1ccccc1)C(C)=O)(C)(=O)=O
2
2
[0.15409714 0.43867188 0.26566569 0.51132815]
[0.14691699 0.52890627 0.84836274 0.71015629]
13C NMR
100 MHz
CDCl3
170.8, 152.2, 137.0, 136.4, 131.3, 131.2, 130.9, 130.8, 128.7, 127.6, 127.0, 125.7, 125.3, 50.1, 43.8, 23.7, 19.7
null
[(170.8, None, None), (152.2, None, None), (137.0, None, None), (136.4, None, None), (131.3, None, None), (131.2, None, None), (130.9, None, None), (130.8, None, None), (128.7, None, None), (127.6, None, None), (127.0, None, None), (125.7, None, None), (125.3, None, None), (50.1, None, None), (43.8, None, None), (23.7,...
19
17
17
10.1039_d4cc02865a
CS(=O)(=O)C=C(c1ccc(-c2ccccc2)cc1)N(Cc1ccccc1)C(C)=O
2
2
[0.15133554 0.74687503 0.28113062 0.81406256]
[0.14802163 0.82578131 0.84836274 0.89609381]
1H NMR
400 MHz
CDCl3
7.69 (d, J = 8.3 Hz, 2H), 7.65-7.60 (m, 2H), 7.57 (d, J = 8.2 Hz, 2H), 7.47 (t, J = 7.4 Hz, 2H), 7.43-7.37 (m, 1H), 7.36-7.24 (m, 3H), 7.23-7.16 (m, 2H), 6.21 (s, 1H), 4.67 (s, 2H), 2.72 (s, 3H), 2.22 (s, 3H)
null
[('d', ['8.3Hz'], '2H', 7.69, 7.69), ('m', [], '2H', 7.65, 7.6), ('d', ['8.2Hz'], '2H', 7.57, 7.57), ('t', ['7.4Hz'], '2H', 7.47, 7.47), ('m', [], '1H', 7.43, 7.37), ('m', [], '3H', 7.36, 7.24), ('m', [], '2H', 7.23, 7.16), ('s', [], '1H', 6.21, 6.21), ('s', [], '2H', 4.67, 4.67), ('s', [], '3H', 2.72, 2.72), ('s', [],...
23
12
23
10.1039_d4cc02865a
CS(=O)(=O)C=C(c1ccc(-c2ccccc2)cc1)N(Cc1ccccc1)C(C)=O
2
2
[0.15133554 0.74687503 0.28113062 0.81406256]
[0.14802163 0.82578131 0.84836274 0.89609381]
13C NMR
100 MHz
CDCl3
170.3, 151.7, 144.5, 139.5, 136.4, 130.9, 130.5, 129.0, 128.8, 128.6, 128.3, 128.0, 127.5, 127.4, 127.2, 50.7, 43.4, 23.3
null
[(170.3, None, None), (151.7, None, None), (144.5, None, None), (139.5, None, None), (136.4, None, None), (130.9, None, None), (130.5, None, None), (129.0, None, None), (128.8, None, None), (128.6, None, None), (128.3, None, None), (128.0, None, None), (127.5, None, None), (127.4, None, None), (127.2, None, None), (50....
24
18
18
10.1039_d4cc02865a
CS(=O)(=O)C=C(c1ccc(C(F)(F)F)cc1)N(Cc1ccccc1)C(C)=O
4
4
[0.15078323 0.31093751 0.2874823 0.37968753]
[0.14857395 0.39218752 0.84946742 0.59921877]
1H NMR
400 MHz
CDCl3
7.70 (d, J = 8.1 Hz, 2H), 7.57 (d, J = 8.0 Hz, 2H), 7.37-7.27 (m, 3H), 7.18-7.11 (m, 2H), 6.31 (s, 1H), 4.61 (s, 2H), 2.77 (s, 3H), 2.24 (s, 3H)
null
[('d', ['8.1Hz'], '2H', 7.7, 7.7), ('d', ['8.0Hz'], '2H', 7.57, 7.57), ('m', [], '3H', 7.37, 7.27), ('m', [], '2H', 7.18, 7.11), ('s', [], '1H', 6.31, 6.31), ('s', [], '2H', 4.61, 4.61), ('s', [], '3H', 2.77, 2.77), ('s', [], '3H', 2.24, 2.24)]
18
9
18
10.1039_d4cc02865a
CS(=O)(=O)C=C(c1ccc(C(F)(F)F)cc1)N(Cc1ccccc1)C(C)=O
4
4
[0.15078323 0.31093751 0.2874823 0.37968753]
[0.14857395 0.39218752 0.84946742 0.59921877]
13C NMR
100 MHz
CDCl3
170.1, 150.5, 135.9, 135.7, 133.1 (q, J = 33.0 Hz), 130.2, 128.9, 128.22, 128.18, 128.1, 125.5 (q, J = 3.7 Hz), 123.43 (q, J = 271.3 Hz), 50.7, 43.6, 23.2
null
[(170.1, None, None), (150.5, None, None), (135.9, None, None), (135.7, None, None), (133.1, 'q', 33.0), (130.2, None, None), (128.9, None, None), (128.22, None, None), (128.18, None, None), (128.1, None, None), (125.5, 'q', 3.7), (123.43, 'q', 271.3), (50.7, None, None), (43.6, None, None), (23.2, None, None)]
19
15
15