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471
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float64
0
489
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int64
0
489
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stringlengths
37
45
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stringlengths
37
61
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stringclasses
11 values
NMR_frequency
stringlengths
3
38
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stringclasses
17 values
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stringlengths
1
1.36k
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stringlengths
2
352
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stringlengths
17
2.43k
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int64
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244
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int64
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float64
0.07
244
10.1039_d4qo00735b
O=S(=O)(/C=c1\o/c(=C\c2ccccc2)c2ccccc12)c1ccccc1
15
15
[0.15105939 0.44609378 0.32117378 0.55859379]
[0.14802163 0.57500003 0.84946742 0.75468753]
13C NMR
100 MHz
DMSO-d6
159.3, 149.6, 143.1, 134.6, 133.4, 133.2, 132.9, 130.1, 129.7, 129.4, 129.3, 128.7, 127.9, 126.1, 122.7, 120.5, 104.6, 99.0
null
[(159.3, None, None), (149.6, None, None), (143.1, None, None), (134.6, None, None), (133.4, None, None), (133.2, None, None), (132.9, None, None), (130.1, None, None), (129.7, None, None), (129.4, None, None), (129.3, None, None), (128.7, None, None), (127.9, None, None), (126.1, None, None), (122.7, None, None), (120...
22
18
18
10.1039_d4qo00735b
C(\c1ccccc1)=c1\o/c(=C\S(=O)(=O)c2ccc(F)cc2)c2ccccc12
16
16
[0.15133554 0.09448243 0.34906593 0.20703127]
[0.14802163 0.22265627 0.84946742 0.43164066]
1H NMR
400 MHz
DMSO-d6
8.12-8.08 (m, 2H), 8.06 (d, J = 8.0 Hz, 1H), 8.01 (d, J = 8.0 Hz, 1H), 7.92 (d, J = 7.6 Hz, 2H), 7.74-7.70 (m, 1H), 7.61-7.57 (m, 1H), 7.49 (t, J = 7.8 Hz, 2H), 7.46-7.41 (m, 2H), 7.38-7.34 (m, 1H), 7.03 (s, 1H), 6.83 (s, 1H)
null
[('m', [], '2H', 8.12, 8.08), ('d', ['8.0Hz'], '1H', 8.06, 8.06), ('d', ['8.0Hz'], '1H', 8.01, 8.01), ('d', ['7.6Hz'], '2H', 7.92, 7.92), ('m', [], '1H', 7.74, 7.7), ('m', [], '1H', 7.61, 7.57), ('t', ['7.8Hz'], '2H', 7.49, 7.49), ('m', [], '2H', 7.46, 7.41), ('m', [], '1H', 7.38, 7.34), ('s', [], '1H', 7.03, 7.03), ('...
15
11
15
10.1039_d4qo00735b
C(\c1ccccc1)=c1\o/c(=C\S(=O)(=O)c2ccc(F)cc2)c2ccccc12
16
16
[0.15133554 0.09448243 0.34906593 0.20703127]
[0.14802163 0.22265627 0.84946742 0.43164066]
13C NMR
100 MHz
DMSO-d6
164.6 (d, J = 251.8 Hz), 159.4, 149.6, 139.5 (d, J = 3.0 Hz), 134.6, 133.4, 132.9, 130.1, 129.7, 129.4, 129.2 (d, J = 9.8 Hz), 128.8, 128.0, 122.7, 120.5, 116.6 (d, J = 22.8 Hz), 104.7, 98.8
null
[(164.6, 'd', 251.8), (159.4, None, None), (149.6, None, None), (139.5, 'd', 3.0), (134.6, None, None), (133.4, None, None), (132.9, None, None), (130.1, None, None), (129.7, None, None), (129.4, None, None), (129.2, 'd', 9.8), (128.8, None, None), (128.0, None, None), (122.7, None, None), (120.5, None, None), (116.6, ...
22
18
18
10.1039_d4qo00735b
O=S(=O)(/C=c1\o/c(=C\c2ccccc2)c2ccccc12)c1ccc(Cl)cc1
16
16
[0.15133554 0.50078128 0.35348449 0.61484381]
[0.1474693 0.63125001 0.84836274 0.78359376]
1H NMR
400 MHz
DMSO-d6
8.08-7.99 (m, 4H), 7.90 (d, J = 7.6 Hz, 2H), 7.74-7.65 (m, 3H), 7.59 (t, J = 7.6 Hz, 1H), 7.49 (t, J = 7.8 Hz, 2H), 7.36 (t, J = 7.4 Hz, 1H), 7.04 (s, 1H), 6.83 (s, 1H)
null
[('m', [], '4H', 8.08, 7.99), ('d', ['7.6Hz'], '2H', 7.9, 7.9), ('m', [], '3H', 7.74, 7.65), ('t', ['7.6Hz'], '1H', 7.59, 7.59), ('t', ['7.8Hz'], '2H', 7.49, 7.49), ('t', ['7.4Hz'], '1H', 7.36, 7.36), ('s', [], '1H', 7.04, 7.04), ('s', [], '1H', 6.83, 6.83)]
15
11
15
10.1039_d4qo00735b
O=S(=O)(/C=c1\o/c(=C\c2ccccc2)c2ccccc12)c1ccc(Cl)cc1
16
16
[0.15133554 0.50078128 0.35348449 0.61484381]
[0.1474693 0.63125001 0.84836274 0.78359376]
13C NMR
100 MHz
DMSO-d6
159.7, 149.6, 141.9, 138.1, 134.7, 133.3, 133.0, 130.1, 129.7, 129.5, 129.4, 128.8, 128.1, 128.0, 122.7, 120.5, 104.8, 98.4
null
[(159.7, None, None), (149.6, None, None), (141.9, None, None), (138.1, None, None), (134.7, None, None), (133.3, None, None), (133.0, None, None), (130.1, None, None), (129.7, None, None), (129.5, None, None), (129.4, None, None), (128.8, None, None), (128.1, None, None), (128.0, None, None), (122.7, None, None), (120...
22
18
18
10.1039_d4qo00735b
C(\c1ccccc1)=c1\o/c(=C\S(=O)(=O)c2ccc(Br)cc2)c2ccccc12
17
17
[0.15133554 0.09458008 0.3567984 0.20625001]
[0.1474693 0.22265627 0.84946742 0.40390627]
1H NMR
400 MHz
DMSO-d6
8.06 (d, J = 8.0 Hz, 1H), 8.01 (d, J = 7.6 Hz, 1H), 7.98-7.93 (m, 2H), 7.92-7.88 (m, 2H), 7.83-7.79 (m, 2H), 7.72 (t, J = 7.6 Hz, 1H), 7.59 (t, J = 7.4 Hz, 1H), 7.49 (t, J = 7.6 Hz, 2H), 7.38-7.34 (m, 1H), 7.04 (s, 1H), 6.83 (s, 1H)
null
[('d', ['8.0Hz'], '1H', 8.06, 8.06), ('d', ['7.6Hz'], '1H', 8.01, 8.01), ('m', [], '2H', 7.98, 7.93), ('m', [], '2H', 7.92, 7.88), ('m', [], '2H', 7.83, 7.79), ('t', ['7.6Hz'], '1H', 7.72, 7.72), ('t', ['7.4Hz'], '1H', 7.59, 7.59), ('t', ['7.6Hz'], '2H', 7.49, 7.49), ('m', [], '1H', 7.38, 7.34), ('s', [], '1H', 7.04, 7...
15
11
15
10.1039_d4qo00735b
C(\c1ccccc1)=c1\o/c(=C\S(=O)(=O)c2ccc(Br)cc2)c2ccccc12
17
17
[0.15133554 0.09458008 0.3567984 0.20625001]
[0.1474693 0.22265627 0.84946742 0.40390627]
13C NMR
100 MHz
DMSO-d6
159.7, 149.6, 142.3, 134.7, 133.3, 133.0, 132.4, 130.1, 129.7, 129.4, 128.8, 128.1, 128.0, 127.2, 122.7, 120.5, 104.8, 98.3
null
[(159.7, None, None), (149.6, None, None), (142.3, None, None), (134.7, None, None), (133.3, None, None), (133.0, None, None), (132.4, None, None), (130.1, None, None), (129.7, None, None), (129.4, None, None), (128.8, None, None), (128.1, None, None), (128.0, None, None), (127.2, None, None), (122.7, None, None), (120...
22
18
18
10.1039_d4qo00735b
Cc1ccc(S(=O)(=O)/C=c2\o/c(=C\c3ccc(Cl)cc3)c3ccccc23)cc1
17
17
[0.15133554 0.44609378 0.35956 0.55859379]
[0.1474693 0.57500003 0.84836274 0.75625001]
1H NMR
400 MHz
DMSO-d6
8.06 (d, J = 8.0 Hz, 1H), 7.98 (d, J = 8.0 Hz, 1H), 7.93 (t, J = 8.8 Hz, 4H), 7.71 (t, J = 7.4 Hz, 1H), 7.60 (d, J = 7.2 Hz, 1H), 7.55 (d, J = 8.8 Hz, 2H), 7.41 (d, J = 8.0 Hz, 2H), 7.04 (s, 1H), 6.82 (s, 1H), 2.34 (s, 3H)
null
[('d', ['8.0Hz'], '1H', 8.06, 8.06), ('d', ['8.0Hz'], '1H', 7.98, 7.98), ('t', ['8.8Hz'], '4H', 7.93, 7.93), ('t', ['7.4Hz'], '1H', 7.71, 7.71), ('d', ['7.2Hz'], '1H', 7.6, 7.6), ('d', ['8.8Hz'], '2H', 7.55, 7.55), ('d', ['8.0Hz'], '2H', 7.41, 7.41), ('s', [], '1H', 7.04, 7.04), ('s', [], '1H', 6.82, 6.82), ('s', [], '...
17
11
17
10.1039_d4qo00735b
Cc1ccc(S(=O)(=O)/C=c2\o/c(=C\c3ccc(Cl)cc3)c3ccccc23)cc1
17
17
[0.15133554 0.44609378 0.35956 0.55859379]
[0.1474693 0.57500003 0.84836274 0.75625001]
13C NMR
100 MHz
DMSO-d6
158.8, 150.1, 143.8, 140.2, 134.4, 132.9, 132.4, 132.3, 130.9, 130.3, 129.9, 129.8, 128.8, 126.2, 122.7, 120.6, 103.1, 99.8, 21.0
null
[(158.8, None, None), (150.1, None, None), (143.8, None, None), (140.2, None, None), (134.4, None, None), (132.9, None, None), (132.4, None, None), (132.3, None, None), (130.9, None, None), (130.3, None, None), (129.9, None, None), (129.8, None, None), (128.8, None, None), (126.2, None, None), (122.7, None, None), (120...
23
19
19
10.1039_d4qo00735b
C(\c1ccc(Cl)cc1)=c1\o/c(=C\S(=O)(=O)c2ccccc2)c2ccccc12
18
18
[0.15133554 0.09492188 0.32863012 0.20664063]
[0.14802163 0.22265627 0.84836274 0.40429691]
1H NMR
400 MHz
DMSO-d6
8.07 (d, J = 8.0 Hz, 1H), 8.04 (d, J = 7.6 Hz, 2H), 7.98 (d, J = 8.0 Hz, 1H), 7.92 (d, J = 8.8 Hz, 2H), 7.71 (t, J = 7.6 Hz, 1H), 7.67-7.58 (m, 4H), 7.58-7.53 (m, 2H), 7.07 (s, 1H), 6.83 (s, 1H)
null
[('d', ['8.0Hz'], '1H', 8.07, 8.07), ('d', ['7.6Hz'], '2H', 8.04, 8.04), ('d', ['8.0Hz'], '1H', 7.98, 7.98), ('d', ['8.8Hz'], '2H', 7.92, 7.92), ('t', ['7.6Hz'], '1H', 7.71, 7.71), ('m', [], '4H', 7.67, 7.58), ('m', [], '2H', 7.58, 7.53), ('s', [], '1H', 7.07, 7.07), ('s', [], '1H', 6.83, 6.83)]
15
11
15
10.1039_d4qo00735b
C(\c1ccc(Cl)cc1)=c1\o/c(=C\S(=O)(=O)c2ccccc2)c2ccccc12
18
18
[0.15133554 0.09492188 0.32863012 0.20664063]
[0.14802163 0.22265627 0.84836274 0.40429691]
13C NMR
100 MHz
DMSO-d6
159.1, 150.1, 143.0, 134.4, 133.3, 133.0, 132.4, 132.3, 130.9, 130.3, 129.9, 129.4, 128.8, 126.2, 122.7, 120.6, 103.3, 99.4
null
[(159.1, None, None), (150.1, None, None), (143.0, None, None), (134.4, None, None), (133.3, None, None), (133.0, None, None), (132.4, None, None), (132.3, None, None), (130.9, None, None), (130.3, None, None), (129.9, None, None), (129.4, None, None), (128.8, None, None), (126.2, None, None), (122.7, None, None), (120...
22
18
18
10.1039_d4qo00735b
O=S(=O)(/C=c1\o/c(=C\c2ccc(Cl)cc2)c2ccccc12)c1ccc(Cl)cc1
18
18
[0.15133554 0.47460941 0.35348449 0.58632814]
[0.14691699 0.60312502 0.84836274 0.75625001]
1H NMR
400 MHz
DMSO-d6
8.08-7.98 (m, 4H), 7.90 (d, J = 8.0 Hz, 2H), 7.75-7.69 (m, 3H), 7.63-7.54 (m, 3H), 7.09 (s, 1H), 6.85 (s, 1H)
null
[('m', [], '4H', 8.08, 7.98), ('d', ['8.0Hz'], '2H', 7.9, 7.9), ('m', [], '3H', 7.75, 7.69), ('m', [], '3H', 7.63, 7.54), ('s', [], '1H', 7.09, 7.09), ('s', [], '1H', 6.85, 6.85)]
14
10
14
10.1039_d4qo00735b
O=S(=O)(/C=c1\o/c(=C\c2ccc(Cl)cc2)c2ccccc12)c1ccc(Cl)cc1
18
18
[0.15133554 0.47460941 0.35348449 0.58632814]
[0.14691699 0.60312502 0.84836274 0.75625001]
13C NMR
100 MHz
DMSO-d6
159.6, 150.1, 141.8, 138.3, 134.5, 133.1, 132.4, 132.4, 130.9, 130.4, 129.8, 129.6, 128.9, 128.2, 122.8, 120.7, 103.5, 98.8
null
[(159.6, None, None), (150.1, None, None), (141.8, None, None), (138.3, None, None), (134.5, None, None), (133.1, None, None), (132.4, None, None), (132.4, None, None), (130.9, None, None), (130.4, None, None), (129.8, None, None), (129.6, None, None), (128.9, None, None), (128.2, None, None), (122.8, None, None), (120...
22
18
18
10.1039_d4qo00735b
C(\c1ccc(Cl)cc1)=c1\o/c(=C\S(=O)(=O)c2ccc(Br)cc2)c2ccccc12
19
19
[0.15133554 0.09453125 0.3567984 0.20664063]
[0.14691699 0.22265627 0.84836274 0.40429691]
1H NMR
400 MHz
DMSO-d6
8.06 (d, J = 8.0 Hz, 1H), 7.99 (d, J = 8.0 Hz, 1H), 7.95 (d, J = 8.4 Hz, 2H), 7.90 (d, J = 8.4 Hz, 2H), 7.84 (d, J = 8.4 Hz, 2H), 7.73 (t, J = 7.6 Hz, 1H), 7.61 (t, J = 7.6 Hz, 1H), 7.56 (d, J = 8.8 Hz, 2H), 7.08 (s, 1H), 6.85 (s, 1H)
null
[('d', ['8.0Hz'], '1H', 8.06, 8.06), ('d', ['8.0Hz'], '1H', 7.99, 7.99), ('d', ['8.4Hz'], '2H', 7.95, 7.95), ('d', ['8.4Hz'], '2H', 7.9, 7.9), ('d', ['8.4Hz'], '2H', 7.84, 7.84), ('t', ['7.6Hz'], '1H', 7.73, 7.73), ('t', ['7.6Hz'], '1H', 7.61, 7.61), ('d', ['8.8Hz'], '2H', 7.56, 7.56), ('s', [], '1H', 7.08, 7.08), ('s'...
14
10
14
10.1039_d4qo00735b
C(\c1ccc(Cl)cc1)=c1\o/c(=C\S(=O)(=O)c2ccc(Br)cc2)c2ccccc12
19
19
[0.15133554 0.09453125 0.3567984 0.20664063]
[0.14691699 0.22265627 0.84836274 0.40429691]
13C NMR
100 MHz
DMSO-d6
159.5, 150.1, 142.2, 134.5, 133.1, 132.5, 132.4, 132.3, 130.9, 130.4, 129.8, 128.8, 128.2, 127.2, 122.8, 120.6, 103.5, 98.7
null
[(159.5, None, None), (150.1, None, None), (142.2, None, None), (134.5, None, None), (133.1, None, None), (132.5, None, None), (132.4, None, None), (132.3, None, None), (130.9, None, None), (130.4, None, None), (129.8, None, None), (128.8, None, None), (128.2, None, None), (127.2, None, None), (122.8, None, None), (120...
22
18
18
10.1039_d4qo00735b
Cc1ccc(S(=O)(=O)/C=c2\o/c(=C\c3cccc(Cl)c3)c3ccccc23)cc1
19
19
[0.15119747 0.44453126 0.35900769 0.57890628]
[0.14691699 0.59375004 0.84891508 0.77421878]
1H NMR
400 MHz
DMSO-d6
8.19 (s, 1H), 8.06 (d, J = 7.6 Hz, 1H), 7.98-7.93 (m, 3H), 7.77 (d, J = 8.0 Hz, 1H), 7.71 (t, J = 7.6 Hz, 1H), 7.59 (t, J = 7.6 Hz, 1H), 7.50 (t, J = 7.8 Hz, 1H), 7.43-7.37 (m, 3H), 7.07 (s, 1H), 6.82 (s, 1H), 2.33 (s, 3H)
null
[('s', [], '1H', 8.19, 8.19), ('d', ['7.6Hz'], '1H', 8.06, 8.06), ('m', [], '3H', 7.98, 7.93), ('d', ['8.0Hz'], '1H', 7.77, 7.77), ('t', ['7.6Hz'], '1H', 7.71, 7.71), ('t', ['7.6Hz'], '1H', 7.59, 7.59), ('t', ['7.8Hz'], '1H', 7.5, 7.5), ('m', [], '3H', 7.43, 7.37), ('s', [], '1H', 7.07, 7.07), ('s', [], '1H', 6.82, 6.8...
17
13
17
10.1039_d4qo00735b
Cc1ccc(S(=O)(=O)/C=c2\o/c(=C\c3cccc(Cl)c3)c3ccccc23)cc1
19
19
[0.15119747 0.44453126 0.35900769 0.57890628]
[0.14691699 0.59375004 0.84891508 0.77421878]
13C NMR
100 MHz
DMSO-d6
158.8, 150.6, 143.9, 140.2, 135.6, 134.2, 133.7, 132.9, 130.5, 130.0, 129.8, 128.4, 128.0, 127.6, 126.2, 122.7, 120.7, 102.9, 100.2, 21.0
null
[(158.8, None, None), (150.6, None, None), (143.9, None, None), (140.2, None, None), (135.6, None, None), (134.2, None, None), (133.7, None, None), (132.9, None, None), (130.5, None, None), (130.0, None, None), (129.8, None, None), (128.4, None, None), (128.0, None, None), (127.6, None, None), (126.2, None, None), (122...
23
21
20
10.1039_d4qo00735b
O=S(=O)(/C=c1\o/c(=C\c2cccc(Cl)c2)c2ccccc12)c1ccc(Cl)cc1
20
20
[0.15105939 0.09331055 0.35376064 0.22695314]
[0.14857395 0.24140626 0.84891508 0.42265628]
1H NMR
400 MHz
DMSO-d6
8.15 (s, 1H), 8.09-8.03 (m, 3H), 7.99 (d, J = 7.6 Hz, 1H), 7.75 (dd, J = 15.0, 7.8 Hz, 2H), 7.68 (d, J = 8.4 Hz, 2H), 7.62 (t, J = 7.6 Hz, 1H), 7.52 (t, J = 7.8 Hz, 1H), 7.42 (d, J = 8.0 Hz, 1H), 7.12 (s, 1H), 6.87 (s, 1H)
null
[('s', [], '1H', 8.15, 8.15), ('m', [], '3H', 8.09, 8.03), ('d', ['7.6Hz'], '1H', 7.99, 7.99), ('dd', ['15.0Hz', '7.8Hz'], '2H', 7.75, 7.75), ('d', ['8.4Hz'], '2H', 7.68, 7.68), ('t', ['7.6Hz'], '1H', 7.62, 7.62), ('t', ['7.8Hz'], '1H', 7.52, 7.52), ('d', ['8.0Hz'], '1H', 7.42, 7.42), ('s', [], '1H', 7.12, 7.12), ('s',...
14
12
14
10.1039_d4qo00735b
O=S(=O)(/C=c1\o/c(=C\c2cccc(Cl)c2)c2ccccc12)c1ccc(Cl)cc1
20
20
[0.15105939 0.09331055 0.35376064 0.22695314]
[0.14857395 0.24140626 0.84891508 0.42265628]
13C NMR
100 MHz
DMSO-d6
160.0, 151.0, 142.3, 138.8, 136.0, 134.8, 134.2, 133.6, 131.0, 130.4, 130.0, 129.0, 128.5, 128.4, 128.2, 123.3, 121.20 103.7, 99.5
null
[(160.0, None, None), (121.2, None, None), (151.0, None, None), (142.3, None, None), (138.8, None, None), (136.0, None, None), (134.8, None, None), (134.2, None, None), (133.6, None, None), (131.0, None, None), (130.4, None, None), (130.0, None, None), (129.0, None, None), (128.5, None, None), (128.4, None, None), (128...
22
20
19
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1ccccc1B1OB(c2ccccc2[Si](C)(C)c2ccccc2)OB(c2ccccc2[Si](C)(C)c2ccccc2)O1
3
3
[0.14786963 0.24765627 0.37727484 0.36757814]
[0.14151261 0.38222658 0.86013137 0.56640629]
1H NMR
400 MHz
CDCl3
7.62 (3H, dd, J = 7.2 Hz, 0.8 Hz), 7.53 (3H, dd, J = 7.2 Hz, 0.8 Hz), 7.44 (3H, ddd, J = 7.4 Hz, 7.4 Hz, 1.2 Hz), 7.36 (3H, ddd, J = 7.4 Hz, 7.4 Hz, 1.2 Hz), 7.30-7.25 (6H, m), 7.21-7.12 (9H, m), 0.43 (18H, s)
null
[('dd', ['7.2Hz', '0.8Hz'], '3H', 7.62, 7.62), ('dd', ['7.2Hz', '0.8Hz'], '3H', 7.53, 7.53), ('ddd', ['7.4Hz', '7.4Hz', '1.2Hz'], '3H', 7.44, 7.44), ('ddd', ['7.4Hz', '7.4Hz', '1.2Hz'], '3H', 7.36, 7.36), ('m', [], '6H', 7.3, 7.25), ('m', [], '9H', 7.21, 7.12), ('s', [], '18H', 0.43, 0.43)]
45
8
45
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1ccccc1B1OB(c2ccccc2[Si](C)(C)c2ccccc2)OB(c2ccccc2[Si](C)(C)c2ccccc2)O1
3
3
[0.14786963 0.24765627 0.37727484 0.36757814]
[0.14151261 0.38222658 0.86013137 0.56640629]
13C NMR
126 MHz
CDCl3
143.9, 139.5, 135.6, 135.4, 134.5, 129.8, 129.0, 128.1, 127.8,-0.35
null
[(143.9, None, None), (139.5, None, None), (135.6, None, None), (135.4, None, None), (134.5, None, None), (129.8, None, None), (129.0, None, None), (128.1, None, None), (127.8, None, None), (-0.35, None, None)]
42
11
10
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1ccccc1B1OB(c2ccccc2[Si](C)(C)c2ccccc2)OB(c2ccccc2[Si](C)(C)c2ccccc2)O1
3
3
[0.14786963 0.24765627 0.37727484 0.36757814]
[0.14151261 0.38222658 0.86013137 0.56640629]
11B NMR
128 MHz
CDCl3
30.0
null
[(30.0, None, None)]
3
1
1
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1ccccc1B1NC(=O)c2ccccc2N1
4
4
[0.1453821 0.21562501 0.29214616 0.32890628]
[0.14261818 0.33710938 0.85681465 0.49257814]
1H NMR
400 MHz
CDCl3
8.17 (1H, dd, J = 8.0 Hz, 1.6 Hz), 7.84-7.79 (1H, m), 7.56-7.34 (9H, m), 7.20 (1H, ddd, J = 8.0 Hz, 7.2 Hz, 1.2 Hz), 7.07 (1H, brs), 6.23 (1H, dd, J = 8.0 Hz, 0.6 Hz), 5.96 (1H, brs), 0.49 (6H, s)
null
[('dd', ['8.0Hz', '1.6Hz'], '1H', 8.17, 8.17), ('m', [], '1H', 7.84, 7.79), ('m', [], '9H', 7.56, 7.34), ('ddd', ['8.0Hz', '7.2Hz', '1.2Hz'], '1H', 7.2, 7.2), ('brs', [], '1H', 7.07, 7.07), ('dd', ['8.0Hz', '0.6Hz'], '1H', 6.23, 6.23), ('brs', [], '1H', 5.96, 5.96), ('s', [], '6H', 0.49, 0.49)]
21
14
21
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1ccccc1B1NC(=O)c2ccccc2N1
4
4
[0.1453821 0.21562501 0.29214616 0.32890628]
[0.14261818 0.33710938 0.85681465 0.49257814]
13C NMR
126 MHz
CDCl3
166.2, 143.4, 141.4, 140.0, 135.3, 134.0, 133.6, 132.8, 129.4, 128.9, 128.8, 128.4, 121.7, 118.7, 117.6,-1.4
null
[(166.2, None, None), (143.4, None, None), (141.4, None, None), (140.0, None, None), (135.3, None, None), (134.0, None, None), (133.6, None, None), (132.8, None, None), (129.4, None, None), (128.9, None, None), (128.8, None, None), (128.4, None, None), (121.7, None, None), (118.7, None, None), (117.6, None, None), (-1....
21
18
16
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1ccccc1B1NC(=O)c2ccccc2N1
4
4
[0.1453821 0.21562501 0.29214616 0.32890628]
[0.14261818 0.33710938 0.85681465 0.49257814]
11B NMR
128 MHz
CDCl3
31.5
null
[(31.5, None, None)]
1
1
1
10.1021_ol200764g
[Si](CC)(CC)(CC)c1ccccc1B1NC(=O)c2ccccc2N1
4
4
[0.14455292 0.54218754 0.2634014 0.65468751]
[0.14206539 0.66796882 0.85736746 0.80312501]
1H NMR
400 MHz
CDCl3
8.28 (1H, d, J = 8.0 Hz), 7.62-7.59 (1H, m), 7.58-7.54 (1H, m), 7.49-7.45 (1H, m), 7.44-7.37 (1H, m), 7.22-7.18 (1H, m), 7.15 (1H, brs), 7.02 (1H, d, J = 8.0 Hz), 6.48 (1H, brs), 0.93-0.89 (6H, m), 0.78-0.72 (9H, m)
null
[('d', ['8.0Hz'], '1H', 8.28, 8.28), ('m', [], '1H', 7.62, 7.59), ('m', [], '1H', 7.58, 7.54), ('m', [], '1H', 7.49, 7.45), ('m', [], '1H', 7.44, 7.37), ('m', [], '1H', 7.22, 7.18), ('brs', [], '1H', 7.15, 7.15), ('d', ['8.0Hz'], '1H', 7.02, 7.02), ('brs', [], '1H', 6.48, 6.48), ('m', [], '6H', 0.93, 0.89), ('m', [], '...
25
12
24
10.1021_ol200764g
[Si](CC)(CC)(CC)c1ccccc1B1NC(=O)c2ccccc2N1
4
4
[0.14455292 0.54218754 0.2634014 0.65468751]
[0.14206539 0.66796882 0.85736746 0.80312501]
13C NMR
126 MHz
CDCl3
166.1, 143.9, 140.1, 135.4, 133.9, 132.2, 129.3, 128.3, 128.0, 122.0, 118.9, 1117.5, 7.5, 4.3
null
[(166.1, None, None), (143.9, None, None), (140.1, None, None), (135.4, None, None), (133.9, None, None), (132.2, None, None), (129.3, None, None), (128.3, None, None), (128.0, None, None), (122.0, None, None), (118.9, None, None), (1117.5, None, None), (7.5, None, None), (4.3, None, None)]
19
15
14
10.1021_ol200764g
[Si](CC)(CC)(CC)c1ccccc1B1NC(=O)c2ccccc2N1
4
4
[0.14455292 0.54218754 0.2634014 0.65468751]
[0.14206539 0.66796882 0.85736746 0.80312501]
11B NMR
128 MHz
CDCl3
32.3
null
[(32.3, None, None)]
1
1
1
10.1021_ol200764g
O=C1NB(c2ccc(Cl)cc2)Nc2ccccc21
5
5
[0.14510571 0.4246094 0.23907894 0.55976567]
[0.14151261 0.57343754 0.85681465 0.70546876]
1H NMR
400 MHz
DMSO-d6
9.77 (1H, s), 9.38 (1H, m), 8.09-8.05 (2H, m), 8.01 (1H, dd, J = 8.0 Hz, 1.6 Hz), 7.61-7.55 (1H, m), 7.55-7.51 (2H, m), 7.44-7.39 (1H, m), 7.15-7.09 (1H, m)
null
[('s', [], '1H', 9.77, 9.77), ('m', [], '1H', 9.38, 9.38), ('m', [], '2H', 8.09, 8.05), ('dd', ['8.0Hz', '1.6Hz'], '1H', 8.01, 8.01), ('m', [], '1H', 7.61, 7.55), ('m', [], '2H', 7.55, 7.51), ('m', [], '1H', 7.44, 7.39), ('m', [], '1H', 7.15, 7.09)]
10
8
10
10.1021_ol200764g
O=C1NB(c2ccc(Cl)cc2)Nc2ccccc21
5
5
[0.14510571 0.4246094 0.23907894 0.55976567]
[0.14151261 0.57343754 0.85681465 0.70546876]
13C NMR
126 MHz
DMSO-d6
167.2, 146.3, 136.6, 136.2, 134.4, 128.9, 122.0, 119.7, 119.1
null
[(167.2, None, None), (146.3, None, None), (136.6, None, None), (136.2, None, None), (134.4, None, None), (128.9, None, None), (122.0, None, None), (119.7, None, None), (119.1, None, None)]
13
11
9
10.1021_ol200764g
O=C1NB(c2ccc(Cl)cc2)Nc2ccccc21
5
5
[0.14510571 0.4246094 0.23907894 0.55976567]
[0.14151261 0.57343754 0.85681465 0.70546876]
11B NMR
128 MHz
DMSO-d6
34.4
null
[(34.4, None, None)]
1
1
1
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(Cl)ccc1B1NC(=O)c2ccccc2N1
6
6
[0.14565849 0.12187501 0.29242254 0.25664064]
[0.14151261 0.26562502 0.85792021 0.39882814]
1H NMR
400 MHz
CDCl3
8.18-8.14 (1H, m), 7.76-7.73 (1H, m), 7.46-7.36 (8H, m), 7.12 (1H, ddd, J = 8.0 Hz, 7.2 Hz, 1.2 Hz), 7.00 (1H, brs), 6.24-6.19 (1H, m), 5.88 (1H, brs), 0.49 (6H, s)
null
[('m', [], '1H', 8.18, 8.14), ('m', [], '1H', 7.76, 7.73), ('m', [], '8H', 7.46, 7.36), ('ddd', ['8.0Hz', '7.2Hz', '1.2Hz'], '1H', 7.12, 7.12), ('brs', [], '1H', 7.0, 7.0), ('m', [], '1H', 6.24, 6.19), ('brs', [], '1H', 5.88, 5.88), ('s', [], '6H', 0.49, 0.49)]
20
13
20
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(Cl)ccc1B1NC(=O)c2ccccc2N1
6
6
[0.14565849 0.12187501 0.29242254 0.25664064]
[0.14151261 0.26562502 0.85792021 0.39882814]
13C NMR
126 MHz
CDCl3
166.1, 144.4, 143.3, 139.2, 135.7, 135.0, 134.3, 133.9, 133.7, 129.7, 129.0, 128.9, 128.5, 121.9, 118.7, 117.6,-1.6
null
[(166.1, None, None), (144.4, None, None), (143.3, None, None), (139.2, None, None), (135.7, None, None), (135.0, None, None), (134.3, None, None), (133.9, None, None), (133.7, None, None), (129.7, None, None), (129.0, None, None), (128.9, None, None), (128.5, None, None), (121.9, None, None), (118.7, None, None), (117...
21
18
17
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(Cl)ccc1B1NC(=O)c2ccccc2N1
6
6
[0.14565849 0.12187501 0.29242254 0.25664064]
[0.14151261 0.26562502 0.85792021 0.39882814]
11B NMR
128 MHz
CDCl3
32.1
null
[(32.1, None, None)]
1
1
1
10.1021_ol200764g
O=C1NB(c2ccc(C(F)(F)F)cc2)Nc2ccccc21
6
6
[0.14482931 0.46914064 0.23935531 0.60664067]
[0.14095983 0.62265631 0.85736746 0.77890631]
1H NMR
400 MHz
DMSO-d6
9.88 (1H, s), 9.51 (1H, s), 8.27-8.22 (2H, m), 8.03 (1H, dd, J = 8.0 Hz, 1.2 Hz), 7.80 (2H, d, J = 8.0 Hz), 7.59 (1H, ddd, J = 8.0 Hz, 7.2 Hz, 1.6 Hz), 7.43 (1H, dd, J = 7.6 Hz, 0.8 Hz), 7.13 (1H, ddd, J = 7.6 Hz, 7.2 Hz, 1.2 Hz)
null
[('s', [], '1H', 9.88, 9.88), ('s', [], '1H', 9.51, 9.51), ('m', [], '2H', 8.27, 8.22), ('dd', ['8.0Hz', '1.2Hz'], '1H', 8.03, 8.03), ('d', ['8.0Hz'], '2H', 7.8, 7.8), ('ddd', ['8.0Hz', '7.2Hz', '1.6Hz'], '1H', 7.59, 7.59), ('dd', ['7.6Hz', '0.8Hz'], '1H', 7.43, 7.43), ('ddd', ['7.6Hz', '7.2Hz', '1.2Hz'], '1H', 7.13, 7...
10
8
10
10.1021_ol200764g
O=C1NB(c2ccc(C(F)(F)F)cc2)Nc2ccccc21
6
6
[0.14482931 0.46914064 0.23935531 0.60664067]
[0.14095983 0.62265631 0.85736746 0.77890631]
13C NMR
126 MHz
DMSO-d6
167.2, 146.2, 138.2, 135.0, 134.4, 131.4 (q, J = 31.2 Hz), 128.9, 125.2, 125.2 (q, J = 277.2 Hz), 122.1, 119.9, 119.2
null
[(167.2, None, None), (146.2, None, None), (138.2, None, None), (135.0, None, None), (134.4, None, None), (131.4, 'q', 31.2), (128.9, None, None), (125.2, None, None), (125.2, 'q', 277.2), (122.1, None, None), (119.9, None, None), (119.2, None, None)]
14
12
12
10.1021_ol200764g
O=C1NB(c2ccc(C(F)(F)F)cc2)Nc2ccccc21
6
6
[0.14482931 0.46914064 0.23935531 0.60664067]
[0.14095983 0.62265631 0.85736746 0.77890631]
11B NMR
128 MHz
DMSO-d6
37.2
null
[(37.2, None, None)]
1
1
1
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(C(F)(F)F)ccc1B1NC(=O)c2ccccc2N1
7
7
[0.14565849 0.11992189 0.29214616 0.25683596]
[0.14261818 0.26601564 0.85792021 0.42304688]
1H NMR
400 MHz
CDCl3
8.20-8.15 (1H, m), 8.03-8.00 (1H, m), 7.74-7.69 (1H, m), 7.63 (1H, d, J = 7.6 Hz), 7.45-7.33 (6H, m), 7.14 (1H, ddd, J = 8.0 Hz, 7.2 Hz, 1.2 Hz), 7.00 (1H, brs), 6.27-6.23 (1H, m), 5.89 (1H, brs), 0.53 (6H, s)
null
[('m', [], '1H', 8.2, 8.15), ('m', [], '1H', 8.03, 8.0), ('m', [], '1H', 7.74, 7.69), ('d', ['7.6Hz'], '1H', 7.63, 7.63), ('m', [], '6H', 7.45, 7.33), ('ddd', ['8.0Hz', '7.2Hz', '1.2Hz'], '1H', 7.14, 7.14), ('brs', [], '1H', 7.0, 7.0), ('m', [], '1H', 6.27, 6.23), ('brs', [], '1H', 5.89, 5.89), ('s', [], '6H', 0.53, 0....
20
13
20
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(C(F)(F)F)ccc1B1NC(=O)c2ccccc2N1
7
7
[0.14565849 0.11992189 0.29214616 0.25683596]
[0.14261818 0.26601564 0.85792021 0.42304688]
13C NMR
126 MHz
CDCl3
166.2, 143.4, 143.3, 139.0, 134.1, 133.9, 133.2, 131.2, 130.8 (q, J = 37.8 Hz), 129.9, 129.1, 128.6, 125.5, 124.4 (q, J = 340.2 Hz), 122.2, 118.9, 117.8,-1.4
null
[(166.2, None, None), (143.4, None, None), (143.3, None, None), (139.0, None, None), (134.1, None, None), (133.9, None, None), (133.2, None, None), (131.2, None, None), (130.8, 'q', 37.8), (129.9, None, None), (129.1, None, None), (128.6, None, None), (125.5, None, None), (124.4, 'q', 340.2), (122.2, None, None), (118....
22
19
18
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(C(F)(F)F)ccc1B1NC(=O)c2ccccc2N1
7
7
[0.14565849 0.11992189 0.29214616 0.25683596]
[0.14261818 0.26601564 0.85792021 0.42304688]
11B NMR
128 MHz
CDCl3
31.8
null
[(31.8, None, None)]
1
1
1
10.1021_ol200764g
Cc1ccc(B2NC(=O)c3ccccc3N2)cc1
7
7
[0.1452439 0.47187504 0.23894074 0.60625003]
[0.14040704 0.62265631 0.85736746 0.75546881]
1H NMR
400 MHz
CDCl3
8.27-8.22 (1H, m), 7.60 (2H, d, J = 7.6 Hz), 7.55 (1H, ddd, J = 8.0 Hz, 7.2 Hz, 1.6 Hz), 7.49 (1H, brs), 7.33-7.28 (2H, m), 7.20-7.13 (1H, m), 7.12-7.07 (1H, m), 6.75 (1H, brs), 2.42 (3H, s)
null
[('m', [], '1H', 8.27, 8.22), ('d', ['7.6Hz'], '2H', 7.6, 7.6), ('ddd', ['8.0Hz', '7.2Hz', '1.6Hz'], '1H', 7.55, 7.55), ('brs', [], '1H', 7.49, 7.49), ('m', [], '2H', 7.33, 7.28), ('m', [], '1H', 7.2, 7.13), ('m', [], '1H', 7.12, 7.07), ('brs', [], '1H', 6.75, 6.75), ('s', [], '3H', 2.42, 2.42)]
13
9
13
10.1021_ol200764g
Cc1ccc(B2NC(=O)c3ccccc3N2)cc1
7
7
[0.1452439 0.47187504 0.23894074 0.60625003]
[0.14040704 0.62265631 0.85736746 0.75546881]
13C NMR
126 MHz
DMSO-d6
167.3, 146.5, 141.1, 134.3, 134.3, 129.4, 128.9, 121.6, 119.6, 119.0, 22.1
null
[(167.3, None, None), (146.5, None, None), (141.1, None, None), (134.3, None, None), (134.3, None, None), (129.4, None, None), (128.9, None, None), (121.6, None, None), (119.6, None, None), (119.0, None, None), (22.1, None, None)]
14
12
11
10.1021_ol200764g
Cc1ccc(B2NC(=O)c3ccccc3N2)cc1
7
7
[0.1452439 0.47187504 0.23894074 0.60625003]
[0.14040704 0.62265631 0.85736746 0.75546881]
11B NMR
128 MHz
DMSO-d6
33.1
null
[(33.1, None, None)]
1
1
1
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(C)ccc1B1NC(=O)c2ccccc2N1
8
8
[0.14565849 0.11523438 0.29214616 0.25117188]
[0.14261818 0.2654297 0.85792021 0.39902346]
1H NMR
400 MHz
CDCl3
8.18-8.13 (1H, m), 7.64-7.61 (1H, m), 7.48-7.34 (7H, m), 7.32-7.28 (1H, m), 7.09 (1H, ddd, J = 8.0 Hz, 7.2 Hz, 0.8 Hz), 7.04 (1H, brs), 6.19-6.15 (1H, m), 5.91 (1H, brs), 2.46 (3H, s), 0.48 (6H, s)
null
[('m', [], '1H', 8.18, 8.13), ('m', [], '1H', 7.64, 7.61), ('m', [], '7H', 7.48, 7.34), ('m', [], '1H', 7.32, 7.28), ('ddd', ['8.0Hz', '7.2Hz', '0.8Hz'], '1H', 7.09, 7.09), ('brs', [], '1H', 7.04, 7.04), ('m', [], '1H', 6.19, 6.15), ('brs', [], '1H', 5.91, 5.91), ('s', [], '3H', 2.46, 2.46), ('s', [], '6H', 0.48, 0.48)...
23
14
23
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(C)ccc1B1NC(=O)c2ccccc2N1
8
8
[0.14565849 0.11523438 0.29214616 0.25117188]
[0.14261818 0.2654297 0.85792021 0.39902346]
13C NMR
126 MHz
CDCl3
166.3, 143.5, 141.3, 140.2, 138.4, 136.2, 134.0, 133.5, 133.0, 129.6, 129.4, 128.9, 128.4, 121.6, 118.6, 117.5, 21.6,-1.4
null
[(166.3, None, None), (143.5, None, None), (141.3, None, None), (140.2, None, None), (138.4, None, None), (136.2, None, None), (134.0, None, None), (133.5, None, None), (133.0, None, None), (129.6, None, None), (129.4, None, None), (128.9, None, None), (128.4, None, None), (121.6, None, None), (118.6, None, None), (117...
22
19
18
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(C)ccc1B1NC(=O)c2ccccc2N1
8
8
[0.14565849 0.11523438 0.29214616 0.25117188]
[0.14261818 0.2654297 0.85792021 0.39902346]
11B NMR
128 MHz
CDCl3
31.8
null
[(31.8, None, None)]
1
1
1
10.1021_ol200764g
COc1ccc(B2NC(=O)c3ccccc3N2)cc1
8
8
[0.14482931 0.44843751 0.23907894 0.58281253]
[0.14151261 0.59687504 0.85792021 0.73203131]
1H NMR
400 MHz
CDCl3
8.26-8.22 (1H, m), 7.66-7.62 (2H, m), 7.57-7.51 (1H, m), 7.44 (1H, brs), 7.16 (1H, ddd, J = 8.0 Hz, 7.2 Hz, 0.8 Hz), 7.11-7.07 (1H, m), 7.04-6.99 (2H, m), 6.69 (1H, brs), 3.87 (3H, s)
null
[('m', [], '1H', 8.26, 8.22), ('m', [], '2H', 7.66, 7.62), ('m', [], '1H', 7.57, 7.51), ('brs', [], '1H', 7.44, 7.44), ('ddd', ['8.0Hz', '7.2Hz', '0.8Hz'], '1H', 7.16, 7.16), ('m', [], '1H', 7.11, 7.07), ('m', [], '2H', 7.04, 6.99), ('brs', [], '1H', 6.69, 6.69), ('s', [], '3H', 3.87, 3.87)]
13
9
13
10.1021_ol200764g
COc1ccc(B2NC(=O)c3ccccc3N2)cc1
8
8
[0.14482931 0.44843751 0.23907894 0.58281253]
[0.14151261 0.59687504 0.85792021 0.73203131]
13C NMR
126 MHz
DMSO-d6
166.4, 161.3, 145.6, 135.1, 133.3, 127.9, 120.6, 118.6, 118.0, 113.5, 55.0
null
[(166.4, None, None), (161.3, None, None), (145.6, None, None), (135.1, None, None), (133.3, None, None), (127.9, None, None), (120.6, None, None), (118.6, None, None), (118.0, None, None), (113.5, None, None), (55.0, None, None)]
14
12
11
10.1021_ol200764g
COc1ccc(B2NC(=O)c3ccccc3N2)cc1
8
8
[0.14482931 0.44843751 0.23907894 0.58281253]
[0.14151261 0.59687504 0.85792021 0.73203131]
11B NMR
128 MHz
DMSO-d6
30.7
null
[(30.7, None, None)]
1
1
1
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(OC)ccc1B1NC(=O)c2ccccc2N1
9
9
[0.14565849 0.11523438 0.29214616 0.25097658]
[0.14151261 0.26562502 0.85902577 0.39921878]
1H NMR
400 MHz
CDCl3
8.18-8.12 (1H, m), 7.50 (1H, d, J = 8.0 Hz), 7.48-7.35 (7H, m), 7.11-7.07 (1H, m), 7.05 (1H, brs), 7.01 (1H, dd, J = 8.0 Hz, 2.8 Hz), 6.14 (1H, d, J = 8.4 Hz), 5.91 (1H, brs), 3.90 (3H, s), 0.48 (6H, s)
null
[('m', [], '1H', 8.18, 8.12), ('d', ['8.0Hz'], '1H', 7.5, 7.5), ('m', [], '7H', 7.48, 7.35), ('m', [], '1H', 7.11, 7.07), ('brs', [], '1H', 7.05, 7.05), ('dd', ['8.0Hz', '2.8Hz'], '1H', 7.01, 7.01), ('d', ['8.4Hz'], '1H', 6.14, 6.14), ('brs', [], '1H', 5.91, 5.91), ('s', [], '3H', 3.9, 3.9), ('s', [], '6H', 0.48, 0.48)...
23
14
23
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(OC)ccc1B1NC(=O)c2ccccc2N1
9
9
[0.14565849 0.11523438 0.29214616 0.25097658]
[0.14151261 0.26562502 0.85902577 0.39921878]
13C NMR
126 MHz
CDCl3
166.3, 159.8, 143.5, 143.4, 139.8, 134.7, 133.9, 133.5, 129.5, 128.8, 128.4, 122.4, 121.5, 118.6, 117.5, 113.0, 55.0,-1.4
null
[(166.3, None, None), (159.8, None, None), (143.5, None, None), (143.4, None, None), (139.8, None, None), (134.7, None, None), (133.9, None, None), (133.5, None, None), (129.5, None, None), (128.8, None, None), (128.4, None, None), (122.4, None, None), (121.5, None, None), (118.6, None, None), (117.5, None, None), (113...
22
19
18
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(OC)ccc1B1NC(=O)c2ccccc2N1
9
9
[0.14565849 0.11523438 0.29214616 0.25097658]
[0.14151261 0.26562502 0.85902577 0.39921878]
11B NMR
128 MHz
CDCl3
31.6
null
[(31.6, None, None)]
1
1
1
10.1021_ol200764g
Cc1cccc(B2NC(=O)c3ccccc3N2)c1
9
9
[0.1453821 0.45625001 0.256768 0.57421879]
[0.14261818 0.59765629 0.85681465 0.70781253]
1H NMR
400 MHz
CDCl3
8.28-8.24 (1H, m), 7.59-7.47 (4H, m), 7.41-7.31 (2H, m), 7.17 (1H, ddd, J = 8.0 Hz, 7.2 Hz, 0.8 Hz), 7.13-7.09 (1H, m), 6.78 (1H, brs), 2.43 (3H, s)
null
[('m', [], '1H', 8.28, 8.24), ('m', [], '4H', 7.59, 7.47), ('m', [], '2H', 7.41, 7.31), ('ddd', ['8.0Hz', '7.2Hz', '0.8Hz'], '1H', 7.17, 7.17), ('m', [], '1H', 7.13, 7.09), ('brs', [], '1H', 6.78, 6.78), ('s', [], '3H', 2.43, 2.43)]
13
11
13
10.1021_ol200764g
Cc1cccc(B2NC(=O)c3ccccc3N2)c1
9
9
[0.1453821 0.45625001 0.256768 0.57421879]
[0.14261818 0.59765629 0.85681465 0.70781253]
13C NMR
126 MHz
DMSO-d6
166.4, 145.6, 136.7, 134.0, 133.4, 131.1, 130.4, 128.0, 127.7, 120.8, 118.8, 118.2, 21.1
null
[(166.4, None, None), (145.6, None, None), (136.7, None, None), (134.0, None, None), (133.4, None, None), (131.1, None, None), (130.4, None, None), (128.0, None, None), (127.7, None, None), (120.8, None, None), (118.8, None, None), (118.2, None, None), (21.1, None, None)]
14
14
13
10.1021_ol200764g
Cc1cccc(B2NC(=O)c3ccccc3N2)c1
9
9
[0.1453821 0.45625001 0.256768 0.57421879]
[0.14261818 0.59765629 0.85681465 0.70781253]
11B NMR
128 MHz
DMSO-d6
33.1
null
[(33.1, None, None)]
1
1
1
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1ccc(C)cc1B1NC(=O)c2ccccc2N1
10
10
[0.14648767 0.1248047 0.30817689 0.2417969 ]
[0.14151261 0.26484376 0.85902577 0.39882814]
1H NMR
400 MHz
CDCl3
8.19-8.14 (1H, m), 7.71 (1H, d, J = 7.6 Hz), 7.47-7.32 (8H, m), 7.12-7.07 (1H, m), 7.05 (1H, brs), 6.20-6.16 (1H, m), 5.92 (1H, brs), 2.40 (3H, s), 0.46 (6H, s)
null
[('m', [], '1H', 8.19, 8.14), ('d', ['7.6Hz'], '1H', 7.71, 7.71), ('m', [], '8H', 7.47, 7.32), ('m', [], '1H', 7.12, 7.07), ('brs', [], '1H', 7.05, 7.05), ('m', [], '1H', 6.2, 6.16), ('brs', [], '1H', 5.92, 5.92), ('s', [], '3H', 2.4, 2.4), ('s', [], '6H', 0.46, 0.46)]
23
14
23
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1ccc(C)cc1B1NC(=O)c2ccccc2N1
10
10
[0.14648767 0.1248047 0.30817689 0.2417969 ]
[0.14151261 0.26484376 0.85902577 0.39882814]
13C NMR
126 MHz
CDCl3
166.3, 143.5, 140.3, 138.7, 137.7, 135.5, 133.9, 133.9, 133.5 129.5, 129.4, 128.9, 128.4, 121.7, 118.7, 117.6, 21.4,-1.38
null
[(166.3, None, None), (133.5, None, None), (143.5, None, None), (140.3, None, None), (138.7, None, None), (137.7, None, None), (135.5, None, None), (133.9, None, None), (133.9, None, None), (129.5, None, None), (129.4, None, None), (128.9, None, None), (128.4, None, None), (121.7, None, None), (118.7, None, None), (117...
22
19
18
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1ccc(C)cc1B1NC(=O)c2ccccc2N1
10
10
[0.14648767 0.1248047 0.30817689 0.2417969 ]
[0.14151261 0.26484376 0.85902577 0.39882814]
11B NMR
128 MHz
CDCl3
32.0
null
[(32.0, None, None)]
1
1
1
10.1021_ol200764g
Cc1ccccc1B1NC(=O)c2ccccc2N1
10
10
[0.1453821 0.44765626 0.25538604 0.56015627]
[0.14151261 0.57343754 0.85792021 0.70781253]
1H NMR
400 MHz
CDCl3
8.25-8.29 (1H, m), 7.56 (1H, ddd, J = 8.0 Hz, 7.2 Hz, 1.6 Hz), 7.48-7.45 (1H, m), 7.39-7.34 (1H, m), 7.28-7.23 (3H, m), 7.19 (1H, ddd, J = 8.0 Hz, 7.2 Hz, 0.8 Hz), 7.08-7.04 (1H, m), 6.60 (1H, brs), 2.49 (3H, s)
null
[('m', [], '1H', 8.29, 8.25), ('ddd', ['8.0Hz', '7.2Hz', '1.6Hz'], '1H', 7.56, 7.56), ('m', [], '1H', 7.48, 7.45), ('m', [], '1H', 7.39, 7.34), ('m', [], '3H', 7.28, 7.23), ('ddd', ['8.0Hz', '7.2Hz', '0.8Hz'], '1H', 7.19, 7.19), ('m', [], '1H', 7.08, 7.04), ('brs', [], '1H', 6.6, 6.6), ('s', [], '3H', 2.49, 2.49)]
13
11
13
10.1021_ol200764g
Cc1ccccc1B1NC(=O)c2ccccc2N1
10
10
[0.1453821 0.44765626 0.25538604 0.56015627]
[0.14151261 0.57343754 0.85792021 0.70781253]
13C NMR
126 MHz
DMSO-d6
166.9, 146.4, 141.5, 134.2, 134.0, 130.1, 130.0, 128.9, 125.7, 121.8, 119.7, 119.0, 23.1
null
[(166.9, None, None), (146.4, None, None), (141.5, None, None), (134.2, None, None), (134.0, None, None), (130.1, None, None), (130.0, None, None), (128.9, None, None), (125.7, None, None), (121.8, None, None), (119.7, None, None), (119.0, None, None), (23.1, None, None)]
14
14
13
10.1021_ol200764g
Cc1ccccc1B1NC(=O)c2ccccc2N1
10
10
[0.1453821 0.44765626 0.25538604 0.56015627]
[0.14151261 0.57343754 0.85792021 0.70781253]
11B NMR
128 MHz
DMSO-d6
38.7
null
[(38.7, None, None)]
1
1
1
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cccc(C)c1B1NC(=O)c2ccccc2N1
11
11
[0.14593488 0.11347657 0.30817689 0.22714844]
[0.14151261 0.24101564 0.85792021 0.39726565]
1H NMR
400 MHz
CDCl3
7.59 (1H, d, J = 7.2 Hz), 7.46-7.41 (1H, m), 7.38 (1H, dd, J = 7.6 Hz, 7.6 Hz), 7.32-7.20 (7H, m), 7.14 (1H, ddd, J = 8.0 Hz, 7.6 Hz, 1.2 Hz), 6.88 (1H, brs), 6.44-6.40 (1H, m), 5.84 (1H, brs), 2.30 (3H, s), 0.45 (6H, s)
null
[('d', ['7.2Hz'], '1H', 7.59, 7.59), ('m', [], '1H', 7.46, 7.41), ('dd', ['7.6Hz', '7.6Hz'], '1H', 7.38, 7.38), ('m', [], '7H', 7.32, 7.2), ('ddd', ['8.0Hz', '7.6Hz', '1.2Hz'], '1H', 7.14, 7.14), ('brs', [], '1H', 6.88, 6.88), ('m', [], '1H', 6.44, 6.4), ('brs', [], '1H', 5.84, 5.84), ('s', [], '3H', 2.3, 2.3), ('s', [...
23
14
23
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cccc(C)c1B1NC(=O)c2ccccc2N1
11
11
[0.14593488 0.11347657 0.30817689 0.22714844]
[0.14151261 0.24101564 0.85792021 0.39726565]
13C NMR
126 MHz
CDCl3
166.0, 143.7, 141.8, 140.3, 139.8, 134.0, 133.7, 132.4, 130.6, 129.1, 128.6, 128.1, 122.0, 118.9, 117.8, 22.7,-1.7
null
[(166.0, None, None), (143.7, None, None), (141.8, None, None), (140.3, None, None), (139.8, None, None), (134.0, None, None), (133.7, None, None), (132.4, None, None), (130.6, None, None), (129.1, None, None), (128.6, None, None), (128.1, None, None), (122.0, None, None), (118.9, None, None), (117.8, None, None), (22....
22
19
17
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cccc(C)c1B1NC(=O)c2ccccc2N1
11
11
[0.14593488 0.11347657 0.30817689 0.22714844]
[0.14151261 0.24101564 0.85792021 0.39726565]
11B NMR
128 MHz
CDCl3
30.3
null
[(30.3, None, None)]
1
1
1
10.1021_ol200764g
O=C1NB(c2ccc3ccccc3c2)Nc2ccccc21
11
11
[0.14482931 0.44609378 0.23880254 0.58515629]
[0.14040704 0.59843753 0.85681465 0.73125003]
1H NMR
400 MHz
CDCl3
8.30-8.27 (1H, m), 8.23 (1H, s), 7.97-7.87 (3H, m), 7.76-7.72 (1H, m), 7.69 (1H, brs), 7.61-7.53 (3H, m), 7.23-7.18 (1H, m), 7.15-7.14 (1H, m), 6.92 (1H, brs)
null
[('m', [], '1H', 8.3, 8.27), ('s', [], '1H', 8.23, 8.23), ('m', [], '3H', 7.97, 7.87), ('m', [], '1H', 7.76, 7.72), ('brs', [], '1H', 7.69, 7.69), ('m', [], '3H', 7.61, 7.53), ('m', [], '1H', 7.23, 7.18), ('m', [], '1H', 7.15, 7.14), ('brs', [], '1H', 6.92, 6.92)]
13
13
13
10.1021_ol200764g
O=C1NB(c2ccc3ccccc3c2)Nc2ccccc21
11
11
[0.14482931 0.44609378 0.23880254 0.58515629]
[0.14040704 0.59843753 0.85681465 0.73125003]
13C NMR
126 MHz
DMSO-d6
166.4, 145.6, 134.4, 134.1, 133.4, 132.5, 129.9, 129.6, 128.4, 128.0, 127.6, 127.0, 126.9, 126.1, 120.9, 118.9, 118.2
null
[(166.4, None, None), (145.6, None, None), (134.4, None, None), (134.1, None, None), (133.4, None, None), (132.5, None, None), (129.9, None, None), (129.6, None, None), (128.4, None, None), (128.0, None, None), (127.6, None, None), (127.0, None, None), (126.9, None, None), (126.1, None, None), (120.9, None, None), (118...
17
17
17
10.1021_ol200764g
O=C1NB(c2ccc3ccccc3c2)Nc2ccccc21
11
11
[0.14482931 0.44609378 0.23880254 0.58515629]
[0.14040704 0.59843753 0.85681465 0.73125003]
11B NMR
128 MHz
DMSO-d6
28.9
null
[(28.9, None, None)]
1
1
1
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc2ccccc2cc1B1NC(=O)c2ccccc2N1
12
12
[0.1453821 0.11210938 0.29242254 0.25234376]
[0.14095983 0.26484376 0.85792021 0.42304688]
1H NMR
400 MHz
CDCl3
8.29 (1H, s), 8.21-8.17 (1H, m), 8.04 (1H, s), 7.96-7.91 (1H, m), 7.88-7.84 (1H, m), 7.62-7.55 (2H, m), 7.50-7.35 (6H, m), 7.17 (1H, brs), 7.11 (1H, ddd, J = 8.0 Hz, 7.2 Hz, 0.8 Hz), 6.18-6.14 (1H, m), 5.96 (1H, brs), 0.57 (6H, s)
null
[('s', [], '1H', 8.29, 8.29), ('m', [], '1H', 8.21, 8.17), ('s', [], '1H', 8.04, 8.04), ('m', [], '1H', 7.96, 7.91), ('m', [], '1H', 7.88, 7.84), ('m', [], '2H', 7.62, 7.55), ('m', [], '6H', 7.5, 7.35), ('brs', [], '1H', 7.17, 7.17), ('ddd', ['8.0Hz', '7.2Hz', '0.8Hz'], '1H', 7.11, 7.11), ('m', [], '1H', 6.18, 6.14), (...
23
16
23
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc2ccccc2cc1B1NC(=O)c2ccccc2N1
12
12
[0.1453821 0.11210938 0.29242254 0.25234376]
[0.14095983 0.26484376 0.85792021 0.42304688]
13C NMR
126 MHz
CDCl3
166.5, 143.6, 140.2, 137.5, 136.4, 134.2, 133.7, 133.6, 133.1, 133.0, 129.7, 129.1, 128.7, 128.2, 128.0, 127.4, 127.3, 121.9, 118.9, 117.8,-1.2
null
[(166.5, None, None), (143.6, None, None), (140.2, None, None), (137.5, None, None), (136.4, None, None), (134.2, None, None), (133.7, None, None), (133.6, None, None), (133.1, None, None), (133.0, None, None), (129.7, None, None), (129.1, None, None), (128.7, None, None), (128.2, None, None), (128.0, None, None), (127...
25
22
21
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc2ccccc2cc1B1NC(=O)c2ccccc2N1
12
12
[0.1453821 0.11210938 0.29242254 0.25234376]
[0.14095983 0.26484376 0.85792021 0.42304688]
11B NMR
128 MHz
CDCl3
30.1
null
[(30.1, None, None)]
1
1
1
10.1021_ol200764g
O=C1NB(c2cccc3ccccc23)Nc2ccccc21
12
12
[0.14565849 0.47031252 0.25842636 0.58359377]
[0.14151261 0.59687504 0.85847301 0.73203131]
1H NMR
400 MHz
DMSO-d6
9.66 (1H, s), 9.43 (1H, s), 8.07 (1H, dd, J = 8.0 Hz, 1.2 Hz), 8.04-7.94 (3H, m), 7.74-7.69 (1H, m), 7.61-7.51 (4H, m), 7.35 (1H, d, J = 8.0 Hz), 7.18-7.12 (1H, m)
null
[('s', [], '1H', 9.66, 9.66), ('s', [], '1H', 9.43, 9.43), ('dd', ['8.0Hz', '1.2Hz'], '1H', 8.07, 8.07), ('m', [], '3H', 8.04, 7.94), ('m', [], '1H', 7.74, 7.69), ('m', [], '4H', 7.61, 7.51), ('d', ['8.0Hz'], '1H', 7.35, 7.35), ('m', [], '1H', 7.18, 7.12)]
13
13
13
10.1021_ol200764g
O=C1NB(c2cccc3ccccc23)Nc2ccccc21
12
12
[0.14565849 0.47031252 0.25842636 0.58359377]
[0.14151261 0.59687504 0.85847301 0.73203131]
13C NMR
126 MHz
DMSO-d6
167.0, 146.4, 136.0, 135.3, 134.3, 133.7, 132.6, 130.0, 129.3, 128.9, 127.0, 126.6, 126.2, 121.9, 119.9, 119.1
null
[(167.0, None, None), (146.4, None, None), (136.0, None, None), (135.3, None, None), (134.3, None, None), (133.7, None, None), (132.6, None, None), (130.0, None, None), (129.3, None, None), (128.9, None, None), (127.0, None, None), (126.6, None, None), (126.2, None, None), (121.9, None, None), (119.9, None, None), (119...
17
17
16
10.1021_ol200764g
O=C1NB(c2cccc3ccccc23)Nc2ccccc21
12
12
[0.14565849 0.47031252 0.25842636 0.58359377]
[0.14151261 0.59687504 0.85847301 0.73203131]
11B NMR
128 MHz
DMSO-d6
33.3
null
[(33.3, None, None)]
1
1
1
10.1021_ol200764g
O=C1NB(c2ccsc2)Nc2ccccc21
13
13
[0.1453821 0.49687503 0.23907894 0.60625003]
[0.14095983 0.62265631 0.85681465 0.77890631]
1H NMR
400 MHz
CDCl3
8.27-8.22 (1H, m), 7.84 (1H, dd, J = 2.8 Hz, 1.2 Hz), 7.61 (1H, brs), 7.55 (1H, ddd, J = 8.4 Hz, 7.2 Hz, 1.6 Hz), 7.50 (1H, dd, J = 4.8 Hz, 2.4 Hz), 7.41 (1H, dd, J = 4.8 Hz, 1.2 Hz), 7.17 (1H, ddd, J = 8.0 Hz, 7.6 Hz, 1.2 Hz), 7.10 (1H, ddd, J = 8.0 Hz, 0.8 Hz, 0.4 Hz), 6.72 (1H, brs)
null
[('m', [], '1H', 8.27, 8.22), ('dd', ['2.8Hz', '1.2Hz'], '1H', 7.84, 7.84), ('brs', [], '1H', 7.61, 7.61), ('ddd', ['8.4Hz', '7.2Hz', '1.6Hz'], '1H', 7.55, 7.55), ('dd', ['4.8Hz', '2.4Hz'], '1H', 7.5, 7.5), ('dd', ['4.8Hz', '1.2Hz'], '1H', 7.41, 7.41), ('ddd', ['8.0Hz', '7.6Hz', '1.2Hz'], '1H', 7.17, 7.17), ('ddd', ['8...
9
9
9
10.1021_ol200764g
O=C1NB(c2ccsc2)Nc2ccccc21
13
13
[0.1453821 0.49687503 0.23907894 0.60625003]
[0.14095983 0.62265631 0.85681465 0.77890631]
13C NMR
126 MHz
DMSO-d6
166.3, 145.5, 134.9, 133.4, 131.7, 128.0, 126.1, 120.7, 118.8, 118.0
null
[(166.3, None, None), (145.5, None, None), (134.9, None, None), (133.4, None, None), (131.7, None, None), (128.0, None, None), (126.1, None, None), (120.7, None, None), (118.8, None, None), (118.0, None, None)]
11
11
10
10.1021_ol200764g
O=C1NB(c2ccsc2)Nc2ccccc21
13
13
[0.1453821 0.49687503 0.23907894 0.60625003]
[0.14095983 0.62265631 0.85681465 0.77890631]
11B NMR
128 MHz
DMSO-d6
27.2
null
[(27.2, None, None)]
1
1
1
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1sccc1B1NC(=O)c2ccccc2N1
14
14
[0.14621127 0.11679688 0.30264905 0.22617188]
[0.14151261 0.24101564 0.85902577 0.39882814]
13C NMR
126 MHz
CDCl3
166.6, 144.8, 143.9, 138.9, 134.2, 134.1, 133.7, 131.2, 130.2, 129.0, 128.8, 121.8, 118.8, 117.5,-0.81
null
[(166.6, None, None), (144.8, None, None), (143.9, None, None), (138.9, None, None), (134.2, None, None), (134.1, None, None), (133.7, None, None), (131.2, None, None), (130.2, None, None), (129.0, None, None), (128.8, None, None), (121.8, None, None), (118.8, None, None), (117.5, None, None), (-0.81, None, None)]
19
16
15
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1sccc1B1NC(=O)c2ccccc2N1
14
14
[0.14621127 0.11679688 0.30264905 0.22617188]
[0.14151261 0.24101564 0.85902577 0.39882814]
11B NMR
128 MHz
CDCl3
28.3
null
[(28.3, None, None)]
1
1
1
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1csc([Si](C)(C)c2ccccc2)c1B1NC(=O)c2ccccc2N1
14
14
[0.14593488 0.47265629 0.35433432 0.58203129]
[0.14151261 0.59687504 0.85736746 0.73125003]
1H NMR
400 MHz
CDCl3
8.10 (1H, d, J = 8.0 Hz), 7.95 (1H, s), 7.49-7.23 (11H, m), 7.09 (1H, dd, J = 7.6 Hz, 7.6 Hz), 6.18 (1H, d, J = 8.0 Hz), 5.62 (1H, brs), 0.54 (6H, s), 0.47 (6H, s)
null
[('d', ['8.0Hz'], '1H', 8.1, 8.1), ('s', [], '1H', 7.95, 7.95), ('m', [], '11H', 7.49, 7.23), ('dd', ['7.6Hz', '7.6Hz'], '1H', 7.09, 7.09), ('d', ['8.0Hz'], '1H', 6.18, 6.18), ('brs', [], '1H', 5.62, 5.62), ('s', [], '6H', 0.54, 0.54), ('s', [], '6H', 0.47, 0.47)]
29
15
28
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1csc([Si](C)(C)c2ccccc2)c1B1NC(=O)c2ccccc2N1
14
14
[0.14593488 0.47265629 0.35433432 0.58203129]
[0.14151261 0.59687504 0.85736746 0.73125003]
13C NMR
126 MHz
CDCl3
165.5, 145.8, 145.5, 143.5, 139.6, 138.9, 138.4, 134.0, 133.9, 133.5, 129.7, 129.5, 129.0, 128.2, 128.2, 121.8, 118.7, 117.6,-0.65,-1.38
null
[(165.5, None, None), (145.8, None, None), (145.5, None, None), (143.5, None, None), (139.6, None, None), (138.9, None, None), (138.4, None, None), (134.0, None, None), (133.9, None, None), (133.5, None, None), (129.7, None, None), (129.5, None, None), (129.0, None, None), (128.2, None, None), (128.2, None, None), (121...
27
21
20
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1csc([Si](C)(C)c2ccccc2)c1B1NC(=O)c2ccccc2N1
14
14
[0.14593488 0.47265629 0.35433432 0.58203129]
[0.14151261 0.59687504 0.85736746 0.73125003]
11B NMR
128 MHz
CDCl3
30.0
null
[(30.0, None, None)]
1
1
1
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1csc([Si](C)(C)c2ccccc2)c1
14
14
[0.14648767 0.76562507 0.35212318 0.81250007]
[0.14206539 0.83437501 0.8557091 0.89687501]
13C NMR
126 MHz
CDCl3
140.4, 140.3, 139.1, 138.6, 138.6, 138.2, 134.1, 134.0, 129.4, 129.2, 128.0, 127.9, 0.94,-1.45
null
[(140.4, None, None), (140.3, None, None), (139.1, None, None), (138.6, None, None), (138.6, None, None), (138.2, None, None), (134.1, None, None), (134.0, None, None), (129.4, None, None), (129.2, None, None), (128.0, None, None), (127.9, None, None), (0.94, None, None), (-1.45, None, None)]
20
14
14
10.1021_ol200764g
O=C1NB(c2ccc(Br)cc2)Nc2ccccc21
15
15
[0.1452439 0.18740236 0.23921711 0.32109378]
[0.14151261 0.33574222 0.85902577 0.46875004]
1H NMR
400 MHz
DMSO-d6
9.77 (1H, s), 9.38 (1H, s), 8.03-7.97 (3H, m), 7.68-7.64 (2H, m), 7.57 (1H, ddd, J = 8.4 Hz, 7.2 Hz, 1.6 Hz), 7.43-7.39 (1H, m), 7.11 (1H, ddd, J = 8.0 Hz, 7.2 Hz, 1.2 Hz)
null
[('s', [], '1H', 9.77, 9.77), ('s', [], '1H', 9.38, 9.38), ('m', [], '3H', 8.03, 7.97), ('m', [], '2H', 7.68, 7.64), ('ddd', ['8.4Hz', '7.2Hz', '1.6Hz'], '1H', 7.57, 7.57), ('m', [], '1H', 7.43, 7.39), ('ddd', ['8.0Hz', '7.2Hz', '1.2Hz'], '1H', 7.11, 7.11)]
10
8
10
10.1021_ol200764g
O=C1NB(c2ccc(Br)cc2)Nc2ccccc21
15
15
[0.1452439 0.18740236 0.23921711 0.32109378]
[0.14151261 0.33574222 0.85902577 0.46875004]
13C NMR
126 MHz
DMSO-d6
166.2, 145.3, 135.4, 133.4, 130.8, 127.9, 124.7, 121.0, 118.8, 118.2
null
[(166.2, None, None), (145.3, None, None), (135.4, None, None), (133.4, None, None), (130.8, None, None), (127.9, None, None), (124.7, None, None), (121.0, None, None), (118.8, None, None), (118.2, None, None)]
13
11
10
10.1021_ol200764g
O=C1NB(c2ccc(Br)cc2)Nc2ccccc21
15
15
[0.1452439 0.18740236 0.23921711 0.32109378]
[0.14151261 0.33574222 0.85902577 0.46875004]
11B NMR
128 MHz
DMSO-d6
31.4
null
[(31.4, None, None)]
1
1
1
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(-c2ccc(C)cc2)ccc1B1NC(=O)c2ccccc2N1
15
15
[0.14510571 0.54375003 0.29297534 0.72500001]
[0.14151261 0.73906253 0.85902577 0.89843757]
1H NMR
400 MHz
CDCl3
8.20-8.16 (1H, m), 8.01 (1H, dd, J = 1.6 Hz, 0.8 Hz), 7.69 (1H, dd, J = 7.6 Hz, 2.0 Hz), 7.60 (1H, dd, J = 7.6 Hz, 0.4 Hz), 7.59-7.55 (2H, m), 7.50-7.46 (2H, m), 7.44-7.35 (4H, m), 7.34-7.29 (2H, m), 7.14-7.07 (2H, m), 6.20 (1H, dd, J = 8.0 Hz, 0.8 Hz), 5.96 (1H, brs), 2.43 (3H, s), 0.53 (6H, s)
null
[('m', [], '1H', 8.2, 8.16), ('dd', ['1.6Hz', '0.8Hz'], '1H', 8.01, 8.01), ('dd', ['7.6Hz', '2.0Hz'], '1H', 7.69, 7.69), ('dd', ['7.6Hz', '0.4Hz'], '1H', 7.6, 7.6), ('m', [], '2H', 7.59, 7.55), ('m', [], '2H', 7.5, 7.46), ('m', [], '4H', 7.44, 7.35), ('m', [], '2H', 7.34, 7.29), ('m', [], '2H', 7.14, 7.07), ('dd', ['8....
27
16
27
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(-c2ccc(C)cc2)ccc1B1NC(=O)c2ccccc2N1
15
15
[0.14510571 0.54375003 0.29297534 0.72500001]
[0.14151261 0.73906253 0.85902577 0.89843757]
13C NMR
126 MHz
CDCl3
166.5, 143.6, 142.2, 141.4, 140.1, 138.1, 137.7, 134.1, 134.0, 133.7, 133.6, 129.8, 129.6, 129.1, 128.6, 127.5, 127.2, 121.9, 118.8, 117.7, 21.3,-1.2
null
[(166.5, None, None), (143.6, None, None), (142.2, None, None), (141.4, None, None), (140.1, None, None), (138.1, None, None), (137.7, None, None), (134.1, None, None), (134.0, None, None), (133.7, None, None), (133.6, None, None), (129.8, None, None), (129.6, None, None), (129.1, None, None), (128.6, None, None), (127...
28
23
22
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1cc(-c2ccc(C)cc2)ccc1B1NC(=O)c2ccccc2N1
15
15
[0.14510571 0.54375003 0.29297534 0.72500001]
[0.14151261 0.73906253 0.85902577 0.89843757]
11B NMR
128 MHz
CDCl3
30.3
null
[(30.3, None, None)]
1
1
1
10.1021_ol200764g
O=C1NB(c2cccc(Br)c2)Nc2ccccc21
16
16
[0.14621127 0.20156251 0.25262213 0.31953126]
[0.14151261 0.33593754 0.85792021 0.46953128]
1H NMR
400 MHz
CDCl3
8.26 (1H, d, J = 7.6 Hz), 7.83 (1H, s), 7.68-7.49 (4H, m), 7.37 (1H, dd, J = 7.6 Hz, 7.6 Hz), 7.20 (1H, dd, J = 7.6 Hz, 7.6 Hz), 7.12 (1H, d, J = 7.6 Hz), 6.77 (1H, brs)
null
[('d', ['7.6Hz'], '1H', 8.26, 8.26), ('s', [], '1H', 7.83, 7.83), ('m', [], '4H', 7.68, 7.49), ('dd', ['7.6Hz', '7.6Hz'], '1H', 7.37, 7.37), ('dd', ['7.6Hz', '7.6Hz'], '1H', 7.2, 7.2), ('d', ['7.6Hz'], '1H', 7.12, 7.12), ('brs', [], '1H', 6.77, 6.77)]
10
10
10
10.1021_ol200764g
O=C1NB(c2cccc(Br)c2)Nc2ccccc21
16
16
[0.14621127 0.20156251 0.25262213 0.31953126]
[0.14151261 0.33593754 0.85792021 0.46953128]
13C NMR
126 MHz
DMSO-d6
166.3, 145.3, 135.8, 135.4, 133.4, 133.2, 132.2, 130.1, 128.0, 122.2, 121.0, 118.9, 118.2
null
[(166.3, None, None), (145.3, None, None), (135.8, None, None), (135.4, None, None), (133.4, None, None), (133.2, None, None), (132.2, None, None), (130.1, None, None), (128.0, None, None), (122.2, None, None), (121.0, None, None), (118.9, None, None), (118.2, None, None)]
13
13
13
10.1021_ol200764g
O=C1NB(c2cccc(Br)c2)Nc2ccccc21
16
16
[0.14621127 0.20156251 0.25262213 0.31953126]
[0.14151261 0.33593754 0.85792021 0.46953128]
11B NMR
128 MHz
DMSO-d6
28.5
null
[(28.5, None, None)]
1
1
1
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1ccc(-c2ccc(C)cc2)cc1B1NC(=O)c2ccccc2N1
17
17
[0.14621127 0.13759766 0.3551635 0.27656251]
[0.14151261 0.28984376 0.85792021 0.47031252]
1H NMR
400 MHz
CDCl3
7.87 (1H, dd, J = 7.6 Hz, 0.4 Hz), 7.76 (1H, d, J = 1.6 Hz), 7.72 (1H, dd, J = 7.6 Hz, 2.0 Hz), 7.56-7.52 (2H, m), 7.51-7.46 (2H, m), 7.46-7.35 (5H, m), 7.28 (2H, d, J = 8.0 Hz), 7.19 (1H, brs), 7.11 (1H, ddd, J = 8.0 Hz, 7.2 Hz, 0.8 Hz), 6.23 (1H, dd, J = 8.0 Hz, 0.8 Hz), 6.01 (1H, brs), 2.41 (3H, s), 0.52 (6H, s)
null
[('dd', ['7.6Hz', '0.4Hz'], '1H', 7.87, 7.87), ('d', ['1.6Hz'], '1H', 7.76, 7.76), ('dd', ['7.6Hz', '2.0Hz'], '1H', 7.72, 7.72), ('m', [], '2H', 7.56, 7.52), ('m', [], '2H', 7.51, 7.46), ('m', [], '5H', 7.46, 7.35), ('d', ['8.0Hz'], '2H', 7.28, 7.28), ('brs', [], '1H', 7.19, 7.19), ('ddd', ['8.0Hz', '7.2Hz', '0.8Hz'], ...
27
16
27
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1ccc(-c2ccc(C)cc2)cc1B1NC(=O)c2ccccc2N1
17
17
[0.14621127 0.13759766 0.3551635 0.27656251]
[0.14151261 0.28984376 0.85792021 0.47031252]
13C NMR
126 MHz
CDCl3
166.5, 143.6, 141.5, 140.2, 139.8, 137.7, 137.7, 136.1, 134.2, 133.7, 131.6, 129.8, 129.6, 129.1, 128.6, 127.2, 127.1, 121.9, 118.9, 117.7, 21.3,-1.2
null
[(166.5, None, None), (143.6, None, None), (141.5, None, None), (140.2, None, None), (139.8, None, None), (137.7, None, None), (137.7, None, None), (136.1, None, None), (134.2, None, None), (133.7, None, None), (131.6, None, None), (129.8, None, None), (129.6, None, None), (129.1, None, None), (128.6, None, None), (127...
28
23
22
10.1021_ol200764g
[Si](C)(C)(c1ccccc1)c1ccc(-c2ccc(C)cc2)cc1B1NC(=O)c2ccccc2N1
17
17
[0.14621127 0.13759766 0.3551635 0.27656251]
[0.14151261 0.28984376 0.85792021 0.47031252]
11B NMR
128 MHz
CDCl3
29.8
null
[(29.8, None, None)]
1
1
1
10.1021_ol200764g
CN1B(c2ccccc2)NC(=O)c2ccccc21
17
17
[0.14482931 0.52421878 0.23935531 0.63828131]
[0.13985426 0.64687501 0.85792021 0.77968751]
1H NMR
400 MHz
CDCl3
8.36 (1H, ddd, J = 7.6 Hz, 1.6 Hz, 0.4 Hz), 7.69 (1H, ddd, J = 8.4 Hz, 7.2 Hz, 1.6 Hz), 7.61-7.56 (2H, m), 7.50-7.44 (3H, m), 7.32 (1H, d, J = 8.0 Hz), 7.28-7.21 (2H, m), 3.40 (3H, s)
null
[('ddd', ['7.6Hz', '1.6Hz', '0.4Hz'], '1H', 8.36, 8.36), ('ddd', ['8.4Hz', '7.2Hz', '1.6Hz'], '1H', 7.69, 7.69), ('m', [], '2H', 7.61, 7.56), ('m', [], '3H', 7.5, 7.44), ('d', ['8.0Hz'], '1H', 7.32, 7.32), ('m', [], '2H', 7.28, 7.21), ('s', [], '3H', 3.4, 3.4)]
13
9
13
10.1021_ol200764g
CN1B(c2ccccc2)NC(=O)c2ccccc21
17
17
[0.14482931 0.52421878 0.23935531 0.63828131]
[0.13985426 0.64687501 0.85792021 0.77968751]
13C NMR
126 MHz
DMSO-d6
165.2, 146.4, 133.7, 133.1, 129.0, 128.4, 127.7, 121.2, 120.0, 115.2, 34.3
null
[(165.2, None, None), (146.4, None, None), (133.7, None, None), (133.1, None, None), (129.0, None, None), (128.4, None, None), (127.7, None, None), (121.2, None, None), (120.0, None, None), (115.2, None, None), (34.3, None, None)]
14
12
11
10.1021_ol200764g
CN1B(c2ccccc2)NC(=O)c2ccccc21
17
17
[0.14482931 0.52421878 0.23935531 0.63828131]
[0.13985426 0.64687501 0.85792021 0.77968751]
11B NMR
128 MHz
DMSO-d6
31.5
null
[(31.5, None, None)]
1
1
1
10.1021_ol200764g
CN1B(c2ccccc2)Nc2ccccc2C1=O
18
18
[0.14565849 0.12031251 0.23907894 0.2341797 ]
[0.14151261 0.24121096 0.85736746 0.37324219]
1H NMR
400 MHz
CDCl3
8.33-8.28 (1H, m), 7.63-7.56 (2H, m), 7.54-7.48 (1H, m), 7.48-7.42 (3H, m), 7.20-7.14 (1H, m), 7.02 (1H, d, J = 8.0 Hz), 6.61 (1H, brs), 3.29 (3H, s)
null
[('m', [], '1H', 8.33, 8.28), ('m', [], '2H', 7.63, 7.56), ('m', [], '1H', 7.54, 7.48), ('m', [], '3H', 7.48, 7.42), ('m', [], '1H', 7.2, 7.14), ('d', ['8.0Hz'], '1H', 7.02, 7.02), ('brs', [], '1H', 6.61, 6.61), ('s', [], '3H', 3.29, 3.29)]
13
9
13
10.1021_ol200764g
CN1B(c2ccccc2)Nc2ccccc2C1=O
18
18
[0.14565849 0.12031251 0.23907894 0.2341797 ]
[0.14151261 0.24121096 0.85736746 0.37324219]
13C NMR
126 MHz
DMSO-d6
166.2, 144.3, 135.3, 133.0, 132.8, 129.1, 128.0, 127.7, 121.0, 118.2, 117.8, 31.5
null
[(166.2, None, None), (144.3, None, None), (135.3, None, None), (133.0, None, None), (132.8, None, None), (129.1, None, None), (128.0, None, None), (127.7, None, None), (121.0, None, None), (118.2, None, None), (117.8, None, None), (31.5, None, None)]
14
12
12
10.1021_ol200764g
CN1B(c2ccccc2)Nc2ccccc2C1=O
18
18
[0.14565849 0.12031251 0.23907894 0.2341797 ]
[0.14151261 0.24121096 0.85736746 0.37324219]
11B NMR
128 MHz
DMSO-d6
31.5
null
[(31.5, None, None)]
1
1
1