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stringclasses
11 values
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stringlengths
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38
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17 values
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stringlengths
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0.07
244
10.1021_jacs.4c05407
O=S(=O)(C(F)(F)F)O.NC1CCCCCC1
29
29
[0.10245527 0.1578125 0.20794829 0.21777346]
[0.22313707 0.14941407 0.90359469 0.2201172 ]
13C NMR
100 MHz
CD3CN
54.3, 32.7, 27.8, 23.8
null
[(54.3, None, None), (32.7, None, None), (27.8, None, None), (23.8, None, None)]
8
5
4
10.1021_jacs.4c05407
O=S(=O)(C(F)(F)F)O.NC1CCCCCC1
29
29
[0.10245527 0.1578125 0.20794829 0.21777346]
[0.22313707 0.14941407 0.90359469 0.2201172 ]
19F NMR
376 MHz
CD3CN
-79.41
null
[(-79.41, None, None)]
3
1
1
10.1021_jacs.4c05407
O=C(c1ccccc1)NC(CC)(C)CC
31
31
[0.11571093 0.47109376 0.20794829 0.51328127]
[0.09113272 0.46328126 0.90414703 0.86875006]
1H NMR
400 MHz
CDCl3
7.77-7.65 (m, 2H), 7.52-7.37 (m, 3H), 5.71 (s, 1H), 2.02-1.87 (m, 2H), 1.79-1.72 (m, 2H), 1.34 (s, 3H), 0.89 (t, J = 7.5 Hz, 6H)
null
[('m', [], '2H', 7.77, 7.65), ('m', [], '3H', 7.52, 7.37), ('s', [], '1H', 5.71, 5.71), ('m', [], '2H', 2.02, 1.87), ('m', [], '2H', 1.79, 1.72), ('s', [], '3H', 1.34, 1.34), ('t', ['7.5Hz'], '6H', 0.89, 0.89)]
19
7
19
10.1021_jacs.4c05407
O=C(c1ccccc1)NC(CC)(C)CC
31
31
[0.11571093 0.47109376 0.20794829 0.51328127]
[0.09113272 0.46328126 0.90414703 0.86875006]
13C NMR
100 MHz
CDCl3
166.9, 136.1, 131.1, 128.5, 126.7, 57.2, 30.5, 23.5, 8.1
null
[(166.9, None, None), (136.1, None, None), (131.1, None, None), (128.5, None, None), (126.7, None, None), (57.2, None, None), (30.5, None, None), (23.5, None, None), (8.1, None, None)]
13
9
9
10.1021_jacs.4c05407
CC1NC(=O)c2ccccc21
44
43
[0.10273143 0.24921876 0.19800654 0.31289064]
[0.09168504 0.77890631 0.90469937 0.90546879]
1H NMR
400 MHz
CDCl3
8.02 (brs, 1H), 7.83 (d, J = 7.5 Hz, 1H), 7.61-7.50 (m, 1H), 7.50-7.36 (m, 2H), 4.70 (q, J = 6.7 Hz, 1H), 1.50 (d, J = 6.7 Hz, 3H)
null
[('brs', [], '1H', 8.02, 8.02), ('d', ['7.5Hz'], '1H', 7.83, 7.83), ('m', [], '1H', 7.61, 7.5), ('m', [], '2H', 7.5, 7.36), ('q', ['6.7Hz'], '1H', 4.7, 4.7), ('d', ['6.7Hz'], '3H', 1.5, 1.5)]
9
7
9
10.1021_jacs.4c05407
CC1NC(=O)c2ccccc21
44
43
[0.10273143 0.24921876 0.19800654 0.31289064]
[0.09168504 0.77890631 0.90469937 0.90546879]
13C NMR
100 MHz
CDCl3
171.2, 149.0, 131.9, 131.7, 128.0, 123.7, 122.2, 52.7, 20.3
null
[(171.2, None, None), (149.0, None, None), (131.9, None, None), (131.7, None, None), (128.0, None, None), (123.7, None, None), (122.2, None, None), (52.7, None, None), (20.3, None, None)]
9
9
9
10.1021_jacs.4c05407
C([C@@](C)(N)c1ccccc1)(OC)=O
51
51
[0.59760972 0.57890628 0.72243394 0.62890625]
[0.09113272 0.64921878 0.90469937 0.83125004]
1H NMR
400 MHz
CDCl3
7.57-7.42 (m, 2H), 7.39-7.28 (m, 3H), 5.42 (s, 2H), 3.74 (s, 3H), 1.77 (s, 3H)
null
[('m', [], '2H', 7.57, 7.42), ('m', [], '3H', 7.39, 7.28), ('s', [], '2H', 5.42, 5.42), ('s', [], '3H', 3.74, 3.74), ('s', [], '3H', 1.77, 1.77)]
13
6
13
10.1039_d4qo00622d
C=C=C(Cc1cccc(OC)c1)C(=O)O
5
5
[0.59760972 0.28046876 0.7610963 0.35234378]
[0.14691699 0.39453129 0.84946742 0.89140628]
1H NMR
300 MHz
CDCl3
11.63 (bs, 1 H, COOH), 7.18 (t, J = 7.8 Hz, 1 H, ArH), 6.92-6.68 (m, 3 H, ArH), 5.17 (t, J = 2.1 Hz, 2 H, =CH2), 3.77 (s, 3 H, OCH3), 3.51 (s, 2 H, CH2)
null
[('brs', [], '1H', 11.63, 11.63), ('t', ['7.8Hz'], '1H', 7.18, 7.18), ('m', [], '3H', 6.92, 6.68), ('t', ['2.1Hz'], '2H', 5.17, 5.17), ('s', [], '3H', 3.77, 3.77), ('s', [], '2H', 3.51, 3.51)]
12
8
12
10.1039_d4qo00622d
C=C=C(Cc1cccc(OC)c1)C(=O)O
5
5
[0.59760972 0.28046876 0.7610963 0.35234378]
[0.14691699 0.39453129 0.84946742 0.89140628]
13C NMR
75 MHz
CDCl3
215.5, 172.7, 159.4, 140.2, 129.2, 121.1, 114.5, 111.7, 99.6, 79.5, 55.0, 34.3
null
[(215.5, None, None), (172.7, None, None), (159.4, None, None), (140.2, None, None), (129.2, None, None), (121.1, None, None), (114.5, None, None), (111.7, None, None), (99.6, None, None), (79.5, None, None), (55.0, None, None), (34.3, None, None)]
12
12
12
10.1039_d4qo00622d
C=C=C(Cc1ccc(C(F)(F)F)cc1)C(=O)O
6
6
[0.6064468 0.2808594 0.7876076 0.33320313]
[0.1474693 0.37656252 0.84946742 0.90859376]
1H NMR
300 MHz
CDCl3
9.42 (bs, 1 H, COOH), 7.53 (d, J = 8.1 Hz, 2 H, ArH), 7.34 (d, J = 7.8 Hz, 2 H, ArH), 5.22 (t, J = 2.4 Hz, 2 H, =CH2), 3.59 (s, 2 H, CH2)
null
[('brs', [], '1H', 9.42, 9.42), ('d', ['8.1Hz'], '2H', 7.53, 7.53), ('d', ['7.8Hz'], '2H', 7.34, 7.34), ('t', ['2.4Hz'], '2H', 5.22, 5.22), ('s', [], '2H', 3.59, 3.59)]
9
5
9
10.1039_d4qo00622d
C=C=C(Cc1ccc(C(F)(F)F)cc1)C(=O)O
6
6
[0.6064468 0.2808594 0.7876076 0.33320313]
[0.1474693 0.37656252 0.84946742 0.90859376]
13C NMR
75 MHz
CDCl3
215.4, 172.2, 142.8, 129.1, 128.9 (q, J = 32.2 Hz), 125.3 (q, J = 3.7 Hz), 124.2 (q, J = 270.2 Hz), 99.1, 80.0, 34.3
null
[(215.4, None, None), (172.2, None, None), (142.8, None, None), (129.1, None, None), (128.9, 'q', 32.2), (125.3, 'q', 3.7), (124.2, 'q', 270.2), (99.1, None, None), (80.0, None, None), (34.3, None, None)]
12
10
10
10.1039_d4qo00622d
C=C=C(Cc1ccc(C(F)(F)F)cc1)C(=O)O
6
6
[0.6064468 0.2808594 0.7876076 0.33320313]
[0.1474693 0.37656252 0.84946742 0.90859376]
19F NMR
282 MHz
CDCl3
62.9
null
[(62.9, None, None)]
3
1
1
10.1039_d4qo00622d
O=C1OCC(C#CC2CC2)=C1CCC
11
11
[0.67162051 0.45781253 0.83621172 0.52500002]
[0.1474693 0.56093751 0.84891508 0.90937504]
13C NMR
75 MHz
CDCl3
174.4, 140.6, 134.2, 110.9, 71.1, 66.7, 26.7, 20.7, 13.7, 9.4, 0.5
null
[(174.4, None, None), (140.6, None, None), (134.2, None, None), (110.9, None, None), (71.1, None, None), (66.7, None, None), (26.7, None, None), (20.7, None, None), (13.7, None, None), (9.4, None, None), (0.5, None, None)]
12
11
11
10.1039_d4qo00622d
C1(CCC)=C(C#CCCCCl)COC1=O
12
12
[0.64179528 0.20820313 0.84504885 0.25976564]
[0.14691699 0.30195315 0.84836274 0.68632815]
1H NMR
300 MHz
CDCl3
4.68 (s, 2 H, OCH2), 3.67 (t, J = 6.2 Hz, 2 H, CH2), 2.70 (t, J = 6.9 Hz, 2 H, CH2), 2.36 (t, J = 7.5 Hz, 2 H, CH2), 2.16-1.93 (m, 2 H, CH2), 1.75-1.53 (m, 2 H, CH2), 0.95 (t, J = 7.4 Hz, 3 H, CH3)
null
[('s', [], '2H', 4.68, 4.68), ('t', ['6.2Hz'], '2H', 3.67, 3.67), ('t', ['6.9Hz'], '2H', 2.7, 2.7), ('t', ['7.5Hz'], '2H', 2.36, 2.36), ('m', [], '2H', 2.16, 1.93), ('m', [], '2H', 1.75, 1.53), ('t', ['7.4Hz'], '3H', 0.95, 0.95)]
15
7
15
10.1039_d4qo00622d
C1(CCC)=C(C#CCCCCl)COC1=O
12
12
[0.64179528 0.20820313 0.84504885 0.25976564]
[0.14691699 0.30195315 0.84836274 0.68632815]
13C NMR
75 MHz
CDCl3
174.2, 140.0, 135.4, 105.0, 72.3, 71.1, 43.2, 30.7, 26.8, 20.8, 17.3, 13.8
null
[(174.2, None, None), (140.0, None, None), (135.4, None, None), (105.0, None, None), (72.3, None, None), (71.1, None, None), (43.2, None, None), (30.7, None, None), (26.8, None, None), (20.8, None, None), (17.3, None, None), (13.8, None, None)]
12
12
12
10.1039_d4qo00622d
C1(CCC)=C(C#CCCBr)COC1=O
12
12
[0.65946949 0.78281256 0.84504885 0.83750006]
[0.18889328 0.87578128 0.84725811 0.89140628]
1H NMR
300 MHz
CDCl3
4.70 (s, 2 H, OCH2), 3.51 (t, J = 6.9 Hz, 2 H, CH2Br), 3.06 (t, J = 6.8 Hz, 2 H, CH2), 2.38 (t, J = 7.5 Hz, 2 H, CH2), 1.73-1.49 (m, 2 H, CH2), 0.95 (t, J = 7.4 Hz, 3 H, CH3)
null
[('s', [], '2H', 4.7, 4.7), ('t', ['6.9Hz'], '2H', 3.51, 3.51), ('t', ['6.8Hz'], '2H', 3.06, 3.06), ('t', ['7.5Hz'], '2H', 2.38, 2.38), ('m', [], '2H', 1.73, 1.49), ('t', ['7.4Hz'], '3H', 0.95, 0.95)]
13
6
13
10.1039_d4qo00622d
C1(CCC)=C(C#CCCBr)COC1=O
12
12
[0.65946949 0.78281256 0.84504885 0.83750006]
[0.18889328 0.87578128 0.84725811 0.89140628]
13C NMR
75 MHz
CDCl3
174.0, 139.5, 136.1, 103.1, 73.2, 71.0, 28.5, 26.8, 24.1, 20.8, 13.8
null
[(174.0, None, None), (139.5, None, None), (136.1, None, None), (103.1, None, None), (73.2, None, None), (71.0, None, None), (28.5, None, None), (26.8, None, None), (24.1, None, None), (20.8, None, None), (13.8, None, None)]
11
11
11
10.1039_d4qo00622d
O=C1OCC(C#CCCO)=C1CCC
13
13
[0.6771437 0.60898443 0.84504885 0.6980469 ]
[0.14691699 0.72890626 0.84836274 0.89140628]
1H NMR
300 MHz
CDCl3
4.69 (s, 2 H, OCH2), 3.83 (q, J = 6.1 Hz, 2 H, OCH2), 2.76 (t, J = 6.5 Hz, 2 H, CH2), 2.63 (t, J = 5.4 Hz, 1 H, OH), 2.36 (t, J = 7.5 Hz, 2 H, CH2), 1.69-1.50 (m, 2 H, CH2), 0.94 (t, J = 7.4 Hz, 3 H, CH3)
null
[('s', [], '2H', 4.69, 4.69), ('q', ['6.1Hz'], '2H', 3.83, 3.83), ('t', ['6.5Hz'], '2H', 2.76, 2.76), ('t', ['5.4Hz'], '1H', 2.63, 2.63), ('t', ['7.5Hz'], '2H', 2.36, 2.36), ('m', [], '2H', 1.69, 1.5), ('t', ['7.4Hz'], '3H', 0.94, 0.94)]
14
7
14
10.1039_d4qo00622d
O=C1OCC(C#CCCO)=C1CCC
13
13
[0.6771437 0.60898443 0.84504885 0.6980469 ]
[0.14691699 0.72890626 0.84836274 0.89140628]
13C NMR
75 MHz
CDCl3
174.5, 140.4, 135.0, 104.2, 72.5, 71.2, 60.4, 26.7, 24.0, 20.7, 13.7
null
[(174.5, None, None), (140.4, None, None), (135.0, None, None), (104.2, None, None), (72.5, None, None), (71.2, None, None), (60.4, None, None), (26.7, None, None), (24.0, None, None), (20.7, None, None), (13.7, None, None)]
11
11
11
10.1039_d4qo00622d
O=C1OCC(C#CCCCCO)=C1CCC
14
14
[0.63737671 0.39179688 0.85388599 0.44257813]
[0.14802163 0.48750004 0.84836274 0.87265631]
13C NMR
75 MHz
CDCl3
174.4, 140.6, 134.8, 107.1, 71.8, 71.2, 62.0, 31.6, 26.8, 24.5, 20.8, 19.7, 13.8
null
[(174.4, None, None), (140.6, None, None), (134.8, None, None), (107.1, None, None), (71.8, None, None), (71.2, None, None), (62.0, None, None), (31.6, None, None), (26.8, None, None), (24.5, None, None), (20.8, None, None), (19.7, None, None), (13.8, None, None)]
13
13
13
10.1039_d4qo00622d
O(CCC#CC1=C(CCC)C(=O)OC1)C1CCCCO1
15
15
[0.63737671 0.17187502 0.84504885 0.22695314]
[0.14802163 0.26621096 0.84836274 0.68515631]
13C NMR
75 MHz
CDCl3
174.2, 140.2, 135.0, 104.3, 98.7, 72.1, 71.1, 64.9, 62.1, 30.4, 26.7, 25.2, 21.3, 20.7, 19.2, 13.7
null
[(174.2, None, None), (140.2, None, None), (135.0, None, None), (104.3, None, None), (98.7, None, None), (72.1, None, None), (71.1, None, None), (64.9, None, None), (62.1, None, None), (30.4, None, None), (26.7, None, None), (25.2, None, None), (21.3, None, None), (20.7, None, None), (19.2, None, None), (13.7, None, No...
16
16
16
10.1039_d4qo00622d
COc1ccc(C#CC2=C(CCC)C(=O)OC2)cc1
19
19
[0.63406277 0.46484379 0.84173492 0.54140626]
[0.1474693 0.58046876 0.84781045 0.89140628]
1H NMR
300 MHz
CDCl3
7.46 (d, J = 8.4 Hz, 2 H, ArH), 6.91 (d, J = 8.7 Hz, 2 H, ArH), 4.79 (s, 2 H, OCH2), 3.85 (s, 3 H, OCH3), 2.45 (t, J = 7.5 Hz, 2 H, CH2), 1.76-1.59 (m, 2 H, CH2), 0.99 (t, J = 7.4 Hz, 3 H, CH3)
null
[('d', ['8.4Hz'], '2H', 7.46, 7.46), ('d', ['8.7Hz'], '2H', 6.91, 6.91), ('s', [], '2H', 4.79, 4.79), ('s', [], '3H', 3.85, 3.85), ('t', ['7.5Hz'], '2H', 2.45, 2.45), ('m', [], '2H', 1.76, 1.59), ('t', ['7.4Hz'], '3H', 0.99, 0.99)]
16
7
16
10.1039_d4qo00622d
COc1ccc(C#CC2=C(CCC)C(=O)OC2)cc1
19
19
[0.63406277 0.46484379 0.84173492 0.54140626]
[0.1474693 0.58046876 0.84781045 0.89140628]
13C NMR
75 MHz
CDCl3
174.0, 160.8, 139.9, 134.4, 133.4, 114.2, 113.2, 105.3, 78.6, 70.9, 55.2, 26.9, 20.8, 13.8
null
[(174.0, None, None), (160.8, None, None), (139.9, None, None), (134.4, None, None), (133.4, None, None), (114.2, None, None), (113.2, None, None), (105.3, None, None), (78.6, None, None), (70.9, None, None), (55.2, None, None), (26.9, None, None), (20.8, None, None), (13.8, None, None)]
16
14
14
10.1039_d4qo00622d
C1(CC#CCCCCCC)=C(C#CCCC(=O)OC(C)(C)C)COC1=O
28
28
[0.59208652 0.38671879 0.86161839 0.54843752]
[0.14802163 0.58046876 0.84836274 0.78046879]
13C NMR
75 MHz
CDCl3
172.9, 170.4, 140.9, 130.6, 107.3, 81.8, 81.1, 73.5, 71.2, 33.8, 31.2, 28.7, 28.4, 28.0, 22.4, 18.7, 15.9, 14.9, 13.9
null
[(172.9, None, None), (170.4, None, None), (140.9, None, None), (130.6, None, None), (107.3, None, None), (81.8, None, None), (81.1, None, None), (73.5, None, None), (71.2, None, None), (33.8, None, None), (31.2, None, None), (28.7, None, None), (28.4, None, None), (28.0, None, None), (22.4, None, None), (18.7, None, N...
22
20
19
10.1039_d4qo00622d
C(=O)(CCC#CC1=C(Cc2ccc(F)cc2)C(=O)OC1)OC(C)(C)C
30
30
[0.61196999 0.16621094 0.85719987 0.23320314]
[0.1474693 0.26640626 0.84891508 0.72343753]
13C NMR
75 MHz
CDCl3
173.6, 170.5, 161.7 (J = 243.4 Hz), 140.6, 134.0, 133.0 (J = 3.5 Hz), 130.4 (J = 7.6 Hz), 115.3 (J = 20.6 Hz), 106.5, 81.2, 71.6, 71.2, 33.8, 30.0, 28.0, 15.8
null
[(173.6, None, None), (170.5, None, None), (161.7, None, 243.4), (140.6, None, None), (134.0, None, None), (133.0, None, 3.5), (130.4, None, 7.6), (115.3, None, 20.6), (106.5, None, None), (81.2, None, None), (71.6, None, None), (71.2, None, None), (33.8, None, None), (30.0, None, None), (28.0, None, None), (15.8, None...
20
16
16
10.1039_d4qo00622d
C(=O)(CCC#CC1=C(Cc2ccc(F)cc2)C(=O)OC1)OC(C)(C)C
30
30
[0.61196999 0.16621094 0.85719987 0.23320314]
[0.1474693 0.26640626 0.84891508 0.72343753]
19F NMR
282 MHz
CDCl3
-116.7
null
[(-116.7, None, None)]
1
1
1
10.1039_d4qo00622d
C(=O)(CCC#CC1=C(Cc2ccc(Br)cc2)C(=O)OC1)OC(C)(C)C
31
31
[0.59981898 0.79687507 0.84504885 0.86250004]
[0.22534636 0.89453132 0.7533638 0.91015632]
13C NMR
75 MHz
CDCl3
173.4, 170.3, 140.8, 136.2, 133.4, 131.4, 130.6, 120.5, 106.7, 81.1, 71.5, 71.2, 33.7, 30.2, 27.9, 15.8
null
[(173.4, None, None), (170.3, None, None), (140.8, None, None), (136.2, None, None), (133.4, None, None), (131.4, None, None), (130.6, None, None), (120.5, None, None), (106.7, None, None), (81.1, None, None), (71.5, None, None), (71.2, None, None), (33.7, None, None), (30.2, None, None), (27.9, None, None), (15.8, Non...
20
16
16
10.1039_d4qo00622d
C(=O)(CCC#CC1=C(Cc2ccc(C(F)(F)F)cc2)C(=O)OC1)OC(C)(C)C
33
33
[0.59871435 0.61093756 0.84615348 0.67343756]
[0.1474693 0.70898445 0.84891508 0.90937504]
13C NMR
75 MHz
CDCl3
173.5, 170.4, 141.3, 133.1, 129.2, 129.0 (q, J = 32.2 Hz), 125.4 (q, J = 3.7 Hz), 124.1 (q, J = 270.3 Hz), 107.0, 81.2, 71.5, 71.3, 33.8, 30.6, 27.9, 15.8
null
[(173.5, None, None), (170.4, None, None), (141.3, None, None), (133.1, None, None), (129.2, None, None), (129.0, 'q', 32.2), (125.4, 'q', 3.7), (124.1, 'q', 270.3), (107.0, None, None), (81.2, None, None), (71.5, None, None), (71.3, None, None), (33.8, None, None), (30.6, None, None), (27.9, None, None), (15.8, None, ...
21
17
16
10.1039_d4qo00622d
C(=O)(CCC#CC1=C(Cc2ccc(C(F)(F)F)cc2)C(=O)OC1)OC(C)(C)C
33
33
[0.59871435 0.61093756 0.84615348 0.67343756]
[0.1474693 0.70898445 0.84891508 0.90937504]
19F NMR
282 MHz
CDCl3
-63.0
null
[(-63.0, None, None)]
3
1
1
10.1039_d4qo00622d
C1(CCC)=C(C#CCCO)C(C)OC1=O
34
34
[0.65946949 0.64687501 0.84394423 0.70781253]
[0.1474693 0.83984382 0.84836274 0.89140628]
1H NMR
300 MHz
CDCl3
4.87 (q, J = 6.7 Hz, 1 H, OCH), 3.84 (t, J = 6.5 Hz, 2 H, OCH2), 2.77 (t, J = 6.5 Hz, 2 H, CH2), 2.34 (t, J = 7.7 Hz, 2 H, CH2), 1.97 (s, 1 H, OH), 1.71-1.52 (m, 2 H, CH2), 1.47 (d, J = 6.9 Hz, 3 H, CH3), 0.94 (t, J = 7.4 Hz, 3 H, CH3)
null
[('q', ['6.7Hz'], '1H', 4.87, 4.87), ('t', ['6.5Hz'], '2H', 3.84, 3.84), ('t', ['6.5Hz'], '2H', 2.77, 2.77), ('t', ['7.7Hz'], '2H', 2.34, 2.34), ('s', [], '1H', 1.97, 1.97), ('m', [], '2H', 1.71, 1.52), ('d', ['6.9Hz'], '3H', 1.47, 1.47), ('t', ['7.4Hz'], '3H', 0.94, 0.94)]
16
8
16
10.1039_d4qo00622d
C1(CCC)=C(C#CCCO)C(C)OC1=O
34
34
[0.65946949 0.64687501 0.84394423 0.70781253]
[0.1474693 0.83984382 0.84836274 0.89140628]
13C NMR
75 MHz
CDCl3
173.6, 145.2, 135.0, 104.6, 78.7, 73.0, 60.6, 26.8, 24.1, 20.8, 18.9, 13.8
null
[(173.6, None, None), (145.2, None, None), (135.0, None, None), (104.6, None, None), (78.7, None, None), (73.0, None, None), (60.6, None, None), (26.8, None, None), (24.1, None, None), (20.8, None, None), (18.9, None, None), (13.8, None, None)]
12
12
12
10.1039_d4qo00622d
O=C1OCC(C#CCCCCO)=C1CCC
39
39
[0.63074889 0.13408204 0.84946742 0.18720704]
[0.1474693 0.22851564 0.84891508 0.68710943]
13C NMR
75 MHz
CDCl3
174.5, 140.7, 134.5, 107.3, 71.6, 71.2, 61.8, 31.5, 26.6, 24.4, 20.7, 19.6, 13.7
null
[(174.5, None, None), (140.7, None, None), (134.5, None, None), (107.3, None, None), (71.6, None, None), (71.2, None, None), (61.8, None, None), (31.5, None, None), (26.6, None, None), (24.4, None, None), (20.7, None, None), (19.6, None, None), (13.7, None, None)]
13
13
13
10.1039_c8qo00919h
CCOC(=O)C=COC(=O)c1cccc(C(=O)OCC)c1
2
2
[0.15078323 0.08798828 0.32227844 0.15751954]
[0.14802163 0.16962891 0.84946742 0.33906251]
1H NMR
400 MHz
CDCl3
8.76 (s, 1H), 8.55 (d, J = 12.5 Hz, 1H), 8.31 (t, J = 7.9 Hz, 2H), 7.61 (t, J = 7.8 Hz, 1H), 5.96 (d, J = 12.5 Hz, 1H), 4.44 (m, 2H), 4.26 (m, 2H), 1.44 (t, J = 7.1 Hz, 3H), 1.33 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.76, 8.76), ('d', ['12.5Hz'], '1H', 8.55, 8.55), ('t', ['7.9Hz'], '2H', 8.31, 8.31), ('t', ['7.8Hz'], '1H', 7.61, 7.61), ('d', ['12.5Hz'], '1H', 5.96, 5.96), ('m', [], '2H', 4.44, 4.44), ('m', [], '2H', 4.26, 4.26), ('t', ['7.1Hz'], '3H', 1.44, 1.44), ('t', ['7.1Hz'], '3H', 1.33, 1.33)]
16
10
16
10.1039_c8qo00919h
CCOC(=O)C=COC(=O)c1cc(C)cc(C(=O)OCC)c1
2
2
[0.1502309 0.35664063 0.32807778 0.42304688]
[0.14802163 0.43593751 0.84836274 0.60468754]
1H NMR
400 MHz
CDCl3
8.53 (d, J = 12.4 Hz, 2H), 8.11 (d, J = 9.6 Hz, 2H), 5.96 (d, J = 12.5 Hz, 1H), 4.42 (m, 2H), 4.26 (m, 2H), 2.49 (s, 3H), 1.43 (t, J = 7.1 Hz, 3H), 1.33 (t, J = 7.1 Hz, 3H)
null
[('d', ['12.4Hz'], '2H', 8.53, 8.53), ('d', ['9.6Hz'], '2H', 8.11, 8.11), ('d', ['12.5Hz'], '1H', 5.96, 5.96), ('m', [], '2H', 4.42, 4.42), ('m', [], '2H', 4.26, 4.26), ('s', [], '3H', 2.49, 2.49), ('t', ['7.1Hz'], '3H', 1.43, 1.43), ('t', ['7.1Hz'], '3H', 1.33, 1.33)]
18
10
18
10.1039_c8qo00919h
CCOC(=O)/C=C/OC(=O)c1cc(Br)cc(C(=O)OCC)c1
2
2
[0.15050707 0.62187503 0.33995265 0.68906256]
[0.1474693 0.70234379 0.84836274 0.87187503]
1H NMR
400 MHz
CDCl3
8.57 (s, 1H), 8.41 (d, J = 12.5 Hz, 1H), 8.32 (d, J = 5.9 Hz, 2H), 5.89 (d, J = 12.5 Hz, 1H), 4.35 (m, 2H), 4.18 (m, 2H), 1.35 (t, J = 7.1 Hz, 3H), 1.25 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.57, 8.57), ('d', ['12.5Hz'], '1H', 8.41, 8.41), ('d', ['5.9Hz'], '2H', 8.32, 8.32), ('d', ['12.5Hz'], '1H', 5.89, 5.89), ('m', [], '2H', 4.35, 4.35), ('m', [], '2H', 4.18, 4.18), ('t', ['7.1Hz'], '3H', 1.35, 1.35), ('t', ['7.1Hz'], '3H', 1.25, 1.25)]
15
9
15
10.1039_c8qo00919h
CCOC(=O)C=COC(=O)c1cc(N)cc(C(=O)OCC)c1
3
3
[0.15050707 0.08867188 0.32559235 0.1576172 ]
[0.14857395 0.16992189 0.84891508 0.3152344 ]
1H NMR
400 MHz
CDCl3
8.52 (d, J = 12.5 Hz, 1H), 8.11 (s, 1H), 7.58 (d, J = 16.0 Hz, 2H), 5.93 (d, J = 12.5 Hz, 1H), 4.40 (m, 2H), 4.25 (m, 2H), 4.04 (s, 2H), 1.41 (t, J = 7.1 Hz, 3H), 1.32 (m, 3H)
null
[('d', ['12.5Hz'], '1H', 8.52, 8.52), ('s', [], '1H', 8.11, 8.11), ('d', ['16.0Hz'], '2H', 7.58, 7.58), ('d', ['12.5Hz'], '1H', 5.93, 5.93), ('m', [], '2H', 4.4, 4.4), ('m', [], '2H', 4.25, 4.25), ('s', [], '2H', 4.04, 4.04), ('t', ['7.1Hz'], '3H', 1.41, 1.41), ('m', [], '3H', 1.32, 1.32)]
17
10
17
10.1039_c8qo00919h
CCOC(=O)C=COC(=O)c1ccc(C(=O)OCC)cc1
3
3
[0.14912627 0.33320313 0.34630433 0.39257816]
[0.14691699 0.40976565 0.84946742 0.55507814]
1H NMR
400 MHz
CDCl3
8.53 (d, J = 12.5 Hz, 1H), 8.26-8.10 (m, 4H), 5.95 (d, J = 12.5 Hz, 1H), 4.43 (m, 2H), 4.26 (m, 2H), 1.43 (t, J = 7.1 Hz, 3H), 1.33 (t, J = 7.1 Hz, 3H)
null
[('d', ['12.5Hz'], '1H', 8.53, 8.53), ('m', [], '4H', 8.26, 8.1), ('d', ['12.5Hz'], '1H', 5.95, 5.95), ('m', [], '2H', 4.43, 4.43), ('m', [], '2H', 4.26, 4.26), ('t', ['7.1Hz'], '3H', 1.43, 1.43), ('t', ['7.1Hz'], '3H', 1.33, 1.33)]
16
8
16
10.1039_c8qo00919h
CCOC(=O)C=COC(=O)c1ccc(C(=O)OCC)cc1
3
3
[0.14912627 0.33320313 0.34630433 0.39257816]
[0.14691699 0.40976565 0.84946742 0.55507814]
13C NMR
100 MHz
CDCl3
165.9, 165.4, 161.8, 149.4, 135.5, 131.3, 130.2, 129.7, 107.0, 77.3, 77.0, 76.7, 61.6, 60.6, 14.2
null
[(165.9, None, None), (165.4, None, None), (161.8, None, None), (149.4, None, None), (135.5, None, None), (131.3, None, None), (130.2, None, None), (129.7, None, None), (107.0, None, None), (77.3, None, None), (77.0, None, None), (76.7, None, None), (61.6, None, None), (60.6, None, None), (14.2, None, None)]
15
13
15
10.1039_c8qo00919h
CCOC(=O)/C=C/OC(=O)c1cc(Br)c(C(=O)OCC)cc1Br
3
3
[0.1502309 0.57500003 0.34575201 0.65078126]
[0.1474693 0.66875003 0.84836274 0.83906254]
1H NMR
400 MHz
CDCl3
8.38 (d, J = 12.5 Hz, 1H), 8.09 (s, 1H), 7.99 (s, 1H), 5.88 (d, J = 12.5 Hz, 1H), 4.36 (m, 2H), 4.18 (m, 2H), 1.35 (t, J = 7.1 Hz, 3H), 1.25 (t, J = 7.1 Hz, 3H)
null
[('d', ['12.5Hz'], '1H', 8.38, 8.38), ('s', [], '1H', 8.09, 8.09), ('s', [], '1H', 7.99, 7.99), ('d', ['12.5Hz'], '1H', 5.88, 5.88), ('m', [], '2H', 4.36, 4.36), ('m', [], '2H', 4.18, 4.18), ('t', ['7.1Hz'], '3H', 1.35, 1.35), ('t', ['7.1Hz'], '3H', 1.25, 1.25)]
14
8
14
10.1039_c8qo00919h
CCOC(=O)/C=C/OC(=O)c1ccc(C(=O)OCC)c2ccccc12
4
4
[0.14967859 0.09628907 0.32365924 0.16816407]
[0.14802163 0.18828126 0.84836274 0.3855469 ]
1H NMR
400 MHz
CDCl3
8.91 (d, J = 9.5 Hz, 1H), 8.79 (d, J = 9.5 Hz, 1H), 8.63 (d, J = 12.5 Hz, 1H), 8.24 (d, J = 7.7 Hz, 1H), 8.05 (d, J = 7.7 Hz, 1H), 7.74-7.60 (m, 2H), 5.95 (d, J = 12.5 Hz, 1H), 4.50 (m, 2H), 4.27 (m, 2H), 1.47 (t, J = 7.1 Hz, 3H), 1.34 (t, J = 7.1 Hz, 3H)
null
[('d', ['9.5Hz'], '1H', 8.91, 8.91), ('d', ['9.5Hz'], '1H', 8.79, 8.79), ('d', ['12.5Hz'], '1H', 8.63, 8.63), ('d', ['7.7Hz'], '1H', 8.24, 8.24), ('d', ['7.7Hz'], '1H', 8.05, 8.05), ('m', [], '2H', 7.74, 7.6), ('d', ['12.5Hz'], '1H', 5.95, 5.95), ('m', [], '2H', 4.5, 4.5), ('m', [], '2H', 4.27, 4.27), ('t', ['7.1Hz'], ...
18
12
18
10.1039_c8qo00919h
CCOC(=O)/C=C/OC(=O)c1ccc2cc(C(=O)OCC)ccc2c1
4
4
[0.14981667 0.39882814 0.35956 0.46914064]
[0.1474693 0.48046879 0.84891508 0.65234375]
1H NMR
400 MHz
CDCl3
8.67 (m, 2H), 8.59 (d, J = 12.5 Hz, 1H), 8.22-8.09 (m, 2H), 8.10-7.93 (m, 2H), 5.98 (d, J = 12.5 Hz, 1H), 4.47 (m, 2H), 4.27 (m, 2H), 1.46 (t, J = 7.1 Hz, 3H), 1.34 (t, J = 7.1 Hz, 3H)
null
[('m', [], '2H', 8.67, 8.67), ('d', ['12.5Hz'], '1H', 8.59, 8.59), ('m', [], '2H', 8.22, 8.09), ('m', [], '2H', 8.1, 7.93), ('d', ['12.5Hz'], '1H', 5.98, 5.98), ('m', [], '2H', 4.47, 4.47), ('m', [], '2H', 4.27, 4.27), ('t', ['7.1Hz'], '3H', 1.46, 1.46), ('t', ['7.1Hz'], '3H', 1.34, 1.34)]
18
12
18
10.1039_c8qo00919h
CCOC(=O)/C=C/OC(=O)c1ccc(-c2ccc(C(=O)OCC)cc2)cc1
4
4
[0.15050707 0.66601562 0.3609408 0.71601567]
[0.14802163 0.72812506 0.84725811 0.90000006]
1H NMR
400 MHz
CDCl3
8.56 (d, J = 12.5 Hz, 1H), 8.17 (m, 4H), 7.71 (m, 4H), 5.92 (d, J = 12.5 Hz, 1H), 4.41 (m, 2H), 4.25 (m, 2H), 1.42 (t, J = 7.1 Hz, 3H), 1.32 (t, J = 7.1 Hz, 3H)
null
[('d', ['12.5Hz'], '1H', 8.56, 8.56), ('m', [], '4H', 8.17, 8.17), ('m', [], '4H', 7.71, 7.71), ('d', ['12.5Hz'], '1H', 5.92, 5.92), ('m', [], '2H', 4.41, 4.41), ('m', [], '2H', 4.25, 4.25), ('t', ['7.1Hz'], '3H', 1.42, 1.42), ('t', ['7.1Hz'], '3H', 1.32, 1.32)]
20
10
20
10.1039_c8qo00919h
CCOC(=O)/C=C/OC(=O)c1ccc(-c2ccc(C(=O)OCC)cc2)cc1
4
4
[0.15050707 0.66601562 0.3609408 0.71601567]
[0.14802163 0.72812506 0.84725811 0.90000006]
13C NMR
100 MHz
CDCl3
166.1, 162.2, 149.7, 145.8, 143.7, 130.9, 130.4, 130.2, 127.5, 127.2, 106.5, 77.3, 77.0, 76.7, 61.1, 60.5, 14.2
null
[(166.1, None, None), (162.2, None, None), (149.7, None, None), (145.8, None, None), (143.7, None, None), (130.9, None, None), (130.4, None, None), (130.2, None, None), (127.5, None, None), (127.2, None, None), (106.5, None, None), (77.3, None, None), (77.0, None, None), (76.7, None, None), (61.1, None, None), (60.5, N...
21
17
17
10.1039_c8qo00919h
CCOC(=O)/C=C/OC(=O)c1ccc(C(=O)OCC)s1
5
5
[0.1488501 0.09282227 0.3438189 0.15097658]
[0.14691699 0.17431642 0.84946742 0.34531252]
1H NMR
400 MHz
CDCl3
8.44 (d, J = 12.5 Hz, 1H), 7.89 (d, J = 3.9 Hz, 1H), 7.78 (d, J = 3.8 Hz, 1H), 5.90 (d, J = 12.5 Hz, 1H), 4.47-4.33 (m, 2H), 4.25 (m, 2H), 1.41 (t, J = 7.1 Hz, 3H), 1.32 (t, J = 7.1 Hz, 3H)
null
[('d', ['12.5Hz'], '1H', 8.44, 8.44), ('d', ['3.9Hz'], '1H', 7.89, 7.89), ('d', ['3.8Hz'], '1H', 7.78, 7.78), ('d', ['12.5Hz'], '1H', 5.9, 5.9), ('m', [], '2H', 4.47, 4.33), ('m', [], '2H', 4.25, 4.25), ('t', ['7.1Hz'], '3H', 1.41, 1.41), ('t', ['7.1Hz'], '3H', 1.32, 1.32)]
14
8
14
10.1039_c8qo00919h
CCCOC(=O)c1cccc(C(=O)OC=CC(=O)OCC)c1
5
5
[0.1502309 0.36250001 0.30488037 0.42500001]
[0.14691699 0.44609378 0.84836274 0.61640629]
1H NMR
400 MHz
CDCl3
8.82 (s, 1H), 8.54 (d, J = 12.5 Hz, 1H), 8.37 (m, 2H), 7.61 (t, J = 7.8 Hz, 1H), 5.96 (d, J = 12.5 Hz, 1H), 4.34 (t, J = 6.7 Hz, 2H), 4.26 (m, 2H), 1.83 (m, 2H), 1.34 (m, 3H), 1.05 (t, J = 7.4 Hz, 3H)
null
[('s', [], '1H', 8.82, 8.82), ('d', ['12.5Hz'], '1H', 8.54, 8.54), ('m', [], '2H', 8.37, 8.37), ('t', ['7.8Hz'], '1H', 7.61, 7.61), ('d', ['12.5Hz'], '1H', 5.96, 5.96), ('t', ['6.7Hz'], '2H', 4.34, 4.34), ('m', [], '2H', 4.26, 4.26), ('m', [], '2H', 1.83, 1.83), ('m', [], '3H', 1.34, 1.34), ('t', ['7.4Hz'], '3H', 1.05,...
18
11
18
10.1039_c8qo00919h
CCCCOC(=O)c1cccc(C(=O)OC=CC(=O)OCC)c1
5
5
[0.15050707 0.63359378 0.30626117 0.69609378]
[0.1474693 0.71210942 0.84946742 0.90625007]
1H NMR
400 MHz
CDCl3
8.82 (s, 1H), 8.54 (d, J = 12.5 Hz, 1H), 8.48-8.21 (m, 2H), 7.61 (t, J = 7.8 Hz, 1H), 5.96 (d, J = 12.5 Hz, 1H), 4.38 (t, J = 6.7 Hz, 2H), 4.33-4.18 (m, 2H), 1.86-1.71 (m, 2H), 1.58-1.43 (m, 2H), 1.35 (m, 3H), 1.00 (t, J = 7.4 Hz, 3H)
null
[('s', [], '1H', 8.82, 8.82), ('d', ['12.5Hz'], '1H', 8.54, 8.54), ('m', [], '2H', 8.48, 8.21), ('t', ['7.8Hz'], '1H', 7.61, 7.61), ('d', ['12.5Hz'], '1H', 5.96, 5.96), ('t', ['6.7Hz'], '2H', 4.38, 4.38), ('m', [], '2H', 4.33, 4.18), ('m', [], '2H', 1.86, 1.71), ('m', [], '2H', 1.58, 1.43), ('m', [], '3H', 1.35, 1.35),...
20
12
20
10.1039_c8qo00919h
CCCCCOC(=O)c1cccc(C(=O)OC=CC(=O)OCC)c1
6
6
[0.15078323 0.08798828 0.32365924 0.15751954]
[0.14691699 0.16953125 0.84836274 0.34140627]
1H NMR
400 MHz
CDCl3
8.82 (s, 1H), 8.55 (d, J = 12.5 Hz, 1H), 8.49-8.16 (m, 2H), 7.61 (t, J = 7.8 Hz, 1H), 5.96 (d, J = 12.5 Hz, 1H), 4.37 (t, J = 6.8 Hz, 2H), 4.33-4.19 (m, 2H), 1.80 (m, 2H), 1.51-1.26 (m, 7H), 1.01-0.89 (m, 3H)
null
[('s', [], '1H', 8.82, 8.82), ('d', ['12.5Hz'], '1H', 8.55, 8.55), ('m', [], '2H', 8.49, 8.16), ('t', ['7.8Hz'], '1H', 7.61, 7.61), ('d', ['12.5Hz'], '1H', 5.96, 5.96), ('t', ['6.8Hz'], '2H', 4.37, 4.37), ('m', [], '2H', 4.33, 4.19), ('m', [], '2H', 1.8, 1.8), ('m', [], '7H', 1.51, 1.26), ('m', [], '3H', 1.01, 0.89)]
22
13
22
10.1039_c8qo00919h
CCCCCCOC(=O)c1cccc(C(=O)OC=CC(=O)OCC)c1
6
6
[0.15133554 0.3621094 0.33249634 0.43515627]
[0.1474693 0.45664065 0.84781045 0.63867188]
1H NMR
400 MHz
CDCl3
8.81 (s, 1H), 8.55 (d, J = 12.5 Hz, 1H), 8.48-8.19 (m, 2H), 7.61 (t, J = 7.8 Hz, 1H), 5.96 (d, J = 12.5 Hz, 1H), 4.37 (t, J = 6.8 Hz, 2H), 4.26 (m, 2H), 1.88-1.72 (m, 2H), 1.56-1.40 (m, 2H), 1.41-1.27 (m, 7H), 0.91 (t, J = 5.8 Hz, 3H)
null
[('s', [], '1H', 8.81, 8.81), ('d', ['12.5Hz'], '1H', 8.55, 8.55), ('m', [], '2H', 8.48, 8.19), ('t', ['7.8Hz'], '1H', 7.61, 7.61), ('d', ['12.5Hz'], '1H', 5.96, 5.96), ('t', ['6.8Hz'], '2H', 4.37, 4.37), ('m', [], '2H', 4.26, 4.26), ('m', [], '2H', 1.88, 1.72), ('m', [], '2H', 1.56, 1.4), ('m', [], '7H', 1.41, 1.27), ...
24
14
24
10.1039_c8qo00919h
CCCCCCCCOC(=O)c1cccc(C(=O)OC=CC(=O)OCC)c1
6
6
[0.15050707 0.66328129 0.33056323 0.73671876]
[0.14691699 0.75585945 0.84946742 0.90000006]
1H NMR
400 MHz
CDCl3
8.81 (s, 1H), 8.54 (d, J = 12.5 Hz, 1H), 8.47-8.09 (m, 2H), 7.61 (t, J = 7.8 Hz, 1H), 5.95 (d, J = 12.5 Hz, 1H), 4.37 (t, J = 6.8 Hz, 2H), 4.31-4.19 (m, 2H), 1.90-1.74 (m, 2H), 1.51-1.41 (m, 2H), 1.35-1.24 (m, 11H), 0.89 (t, J = 6.6 Hz, 3H)
null
[('s', [], '1H', 8.81, 8.81), ('d', ['12.5Hz'], '1H', 8.54, 8.54), ('m', [], '2H', 8.47, 8.09), ('t', ['7.8Hz'], '1H', 7.61, 7.61), ('d', ['12.5Hz'], '1H', 5.95, 5.95), ('t', ['6.8Hz'], '2H', 4.37, 4.37), ('m', [], '2H', 4.31, 4.19), ('m', [], '2H', 1.9, 1.74), ('m', [], '2H', 1.51, 1.41), ('m', [], '11H', 1.35, 1.24),...
28
16
28
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)NCCc2ccccc2)c1
7
7
[0.1502309 0.49140629 0.26345641 0.56328128]
[0.14802163 0.57421879 0.84836274 0.74609382]
1H NMR
400 MHz
CDCl3
8.30 (s, 1H), 8.15 (d, J = 8.9 Hz, 1H), 7.96 (d, J = 9.0 Hz, 1H), 7.50 (t, J = 7.8 Hz, 1H), 7.34 (m, 2H), 7.25 (t, J = 5.9 Hz, 3H), 6.32 (s, 1H), 4.39 (m, 2H), 3.73 (m, 2H), 2.95 (t, J = 7.0 Hz, 2H), 1.40 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.3, 8.3), ('d', ['8.9Hz'], '1H', 8.15, 8.15), ('d', ['9.0Hz'], '1H', 7.96, 7.96), ('t', ['7.8Hz'], '1H', 7.5, 7.5), ('m', [], '2H', 7.34, 7.34), ('t', ['5.9Hz'], '3H', 7.25, 7.25), ('s', [], '1H', 6.32, 6.32), ('m', [], '2H', 4.39, 4.39), ('m', [], '2H', 3.73, 3.73), ('t', ['7.0Hz'], '2H', 2.95, 2.95)...
19
12
19
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)NCCc2ccccc2)c1
7
7
[0.1502309 0.49140629 0.26345641 0.56328128]
[0.14802163 0.57421879 0.84836274 0.74609382]
13C NMR
100 MHz
CDCl3
166.5, 165.8, 138.7, 134.9, 132.3, 131.5, 130.8, 128.7, 127.4, 126.6, 77.3, 77.0, 76.7, 61.3, 41.3, 35.7, 14.3
null
[(166.5, None, None), (165.8, None, None), (138.7, None, None), (134.9, None, None), (132.3, None, None), (131.5, None, None), (130.8, None, None), (128.7, None, None), (127.4, None, None), (126.6, None, None), (77.3, None, None), (77.0, None, None), (76.7, None, None), (61.3, None, None), (41.3, None, None), (35.7, No...
18
16
17
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)NCc2ccccc2)c1
7
7
[0.15050707 0.76367195 0.24881994 0.84218751]
[0.14802163 0.85937507 0.84946742 0.90000006]
1H NMR
400 MHz
CDCl3
8.39 (s, 1H), 8.16 (d, J = 7.8 Hz, 1H), 8.05 (d, J = 7.8 Hz, 1H), 7.51 (t, J = 7.8 Hz, 1H), 7.44-7.26 (m, 5H), 6.64 (s, 1H), 4.65 (d, J = 5.7 Hz, 2H), 4.38 (m, 2H), 1.45-1.33 (m, 3H)
null
[('s', [], '1H', 8.39, 8.39), ('d', ['7.8Hz'], '1H', 8.16, 8.16), ('d', ['7.8Hz'], '1H', 8.05, 8.05), ('t', ['7.8Hz'], '1H', 7.51, 7.51), ('m', [], '5H', 7.44, 7.26), ('s', [], '1H', 6.64, 6.64), ('d', ['5.7Hz'], '2H', 4.65, 4.65), ('m', [], '2H', 4.38, 4.38), ('m', [], '3H', 1.45, 1.33)]
17
11
17
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)NCc2ccccc2)c1
7
7
[0.15050707 0.76367195 0.24881994 0.84218751]
[0.14802163 0.85937507 0.84946742 0.90000006]
13C NMR
100 MHz
CDCl3
166.3, 165.8, 137.9, 134.7, 132.4, 131.7, 130.9, 128.8, 127.9, 127.6, 77.3, 77.0, 76.7, 61.3, 44.2, 14.2
null
[(166.3, None, None), (165.8, None, None), (137.9, None, None), (134.7, None, None), (132.4, None, None), (131.7, None, None), (130.9, None, None), (128.8, None, None), (127.9, None, None), (127.6, None, None), (77.3, None, None), (77.0, None, None), (76.7, None, None), (61.3, None, None), (44.2, None, None), (14.2, No...
17
15
16
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)NCC2CC2)c1
8
8
[0.15050707 0.20820313 0.2546193 0.28320314]
[0.14636467 0.30234377 0.84891508 0.47304689]
1H NMR
400 MHz
CDCl3
8.40 (s, 1H), 8.16 (d, J = 7.7 Hz, 1H), 8.04 (d, J = 9.1 Hz, 1H), 7.52 (t, J = 7.8 Hz, 1H), 6.45 (s, 1H), 4.41 (m, 2H), 3.46-3.11 (m, 2H), 1.41 (t, J = 7.1 Hz, 3H), 1.13-1.00 (m, 1H), 0.64-0.49 (m, 2H), 0.29 (m, 2H)
null
[('s', [], '1H', 8.4, 8.4), ('d', ['7.7Hz'], '1H', 8.16, 8.16), ('d', ['9.1Hz'], '1H', 8.04, 8.04), ('t', ['7.8Hz'], '1H', 7.52, 7.52), ('s', [], '1H', 6.45, 6.45), ('m', [], '2H', 4.41, 4.41), ('m', [], '2H', 3.46, 3.11), ('t', ['7.1Hz'], '3H', 1.41, 1.41), ('m', [], '1H', 1.13, 1.0), ('m', [], '2H', 0.64, 0.49), ('m'...
17
10
17
10.1039_c8qo00919h
CCCCNC(=O)c1cccc(C(=O)OCC)c1
8
8
[0.15050707 0.49296878 0.25765704 0.56953129]
[0.1474693 0.58593754 0.84781045 0.73125003]
1H NMR
400 MHz
CDCl3
8.39 (s, 1H), 8.13 (d, J = 7.8 Hz, 1H), 8.02 (d, J = 7.8 Hz, 1H), 7.48 (t, J = 7.8 Hz, 1H), 6.67 (s, 1H), 4.38 (m, 2H), 3.45 (m, 2H), 1.69-1.53 (m, 2H), 1.40 (m, 5H), 0.94 (t, J = 7.3 Hz, 3H)
null
[('s', [], '1H', 8.39, 8.39), ('d', ['7.8Hz'], '1H', 8.13, 8.13), ('d', ['7.8Hz'], '1H', 8.02, 8.02), ('t', ['7.8Hz'], '1H', 7.48, 7.48), ('s', [], '1H', 6.67, 6.67), ('m', [], '2H', 4.38, 4.38), ('m', [], '2H', 3.45, 3.45), ('m', [], '2H', 1.69, 1.53), ('m', [], '5H', 1.4, 1.4), ('t', ['7.3Hz'], '3H', 0.94, 0.94)]
19
11
19
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)N2CCOCC2)c1
8
8
[0.15078323 0.75156256 0.26842729 0.84531256]
[0.14691699 0.86406253 0.84891508 0.90468751]
1H NMR
400 MHz
CDCl3
8.17-7.95 (m, 2H), 7.61 (d, J = 7.6 Hz, 1H), 7.51 (t, J = 7.7 Hz, 1H), 4.40 (m, 2H), 3.79 (s, 4H), 3.65 (s, 2H), 3.45 (s, 2H), 1.40 (t, J = 7.1 Hz, 3H)
null
[('m', [], '2H', 8.17, 7.95), ('d', ['7.6Hz'], '1H', 7.61, 7.61), ('t', ['7.7Hz'], '1H', 7.51, 7.51), ('m', [], '2H', 4.4, 4.4), ('s', [], '4H', 3.79, 3.79), ('s', [], '2H', 3.65, 3.65), ('s', [], '2H', 3.45, 3.45), ('t', ['7.1Hz'], '3H', 1.4, 1.4)]
17
8
17
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)N2CCOCC2)c1
8
8
[0.15078323 0.75156256 0.26842729 0.84531256]
[0.14691699 0.86406253 0.84891508 0.90468751]
13C NMR
100 MHz
CDCl3
169.4, 165.7, 135.6, 131.3, 130.9, 128.7, 128.1, 77.3, 77.2, 76.5, 66.8, 61.3, 14.2
null
[(169.4, None, None), (165.7, None, None), (135.6, None, None), (131.3, None, None), (130.9, None, None), (128.7, None, None), (128.1, None, None), (77.3, None, None), (77.2, None, None), (76.5, None, None), (66.8, None, None), (61.3, None, None), (14.2, None, None)]
14
12
13
10.1039_c8qo00919h
CCOC(=O)c1ccc(C(=O)NCc2ccccc2)cc1
9
9
[0.15050707 0.16835939 0.33387714 0.2339844 ]
[0.14691699 0.24785157 0.84836274 0.39316408]
1H NMR
400 MHz
CDCl3
8.06 (d, J = 8.5 Hz, 2H), 7.84 (d, J = 8.5 Hz, 2H), 7.34 (d, J = 4.1 Hz, 5H), 6.74 (s, 1H), 4.63 (d, J = 5.7 Hz, 2H), 4.38 (m, 2H), 1.40 (t, J = 7.1 Hz, 3H)
null
[('d', ['8.5Hz'], '2H', 8.06, 8.06), ('d', ['8.5Hz'], '2H', 7.84, 7.84), ('d', ['4.1Hz'], '5H', 7.34, 7.34), ('s', [], '1H', 6.74, 6.74), ('d', ['5.7Hz'], '2H', 4.63, 4.63), ('m', [], '2H', 4.38, 4.38), ('t', ['7.1Hz'], '3H', 1.4, 1.4)]
17
9
17
10.1039_c8qo00919h
CCOC(=O)c1ccc(C(=O)NCc2ccccc2)cc1
9
9
[0.15050707 0.16835939 0.33387714 0.2339844 ]
[0.14691699 0.24785157 0.84836274 0.39316408]
13C NMR
100 MHz
CDCl3
166.6, 165.8, 138.2, 137.9, 133.0, 129.7, 128.7, 127.9, 127.6, 127.0, 77.3, 76.7, 61.3, 44.2, 14.2
null
[(166.6, None, None), (165.8, None, None), (138.2, None, None), (137.9, None, None), (133.0, None, None), (129.7, None, None), (128.7, None, None), (127.9, None, None), (127.6, None, None), (127.0, None, None), (77.3, None, None), (76.7, None, None), (61.3, None, None), (44.2, None, None), (14.2, None, None)]
17
13
15
10.1039_c8qo00919h
CCOC(=O)c1ccc2cc(C(=O)NCc3ccccc3)ccc2c1
9
9
[0.15050707 0.41015629 0.3581792 0.47265629]
[0.1474693 0.48789065 0.84781045 0.65976568]
1H NMR
400 MHz
CDCl3
8.57 (s, 1H), 8.30 (s, 1H), 8.07 (d, J = 8.6 Hz, 1H), 7.95 (d, J = 8.6 Hz, 1H), 7.92-7.79 (m, 2H), 7.46-7.26 (m, 5H), 6.84 (s, 1H), 4.68 (d, J = 5.7 Hz, 2H), 4.43 (m, 2H), 1.44 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.57, 8.57), ('s', [], '1H', 8.3, 8.3), ('d', ['8.6Hz'], '1H', 8.07, 8.07), ('d', ['8.6Hz'], '1H', 7.95, 7.95), ('m', [], '2H', 7.92, 7.79), ('m', [], '5H', 7.46, 7.26), ('s', [], '1H', 6.84, 6.84), ('d', ['5.7Hz'], '2H', 4.68, 4.68), ('m', [], '2H', 4.43, 4.43), ('t', ['7.1Hz'], '3H', 1.44, 1.44)]
19
13
19
10.1039_c8qo00919h
CCOC(=O)c1ccc(C(=O)NCc2ccccc2)c2ccccc12
9
9
[0.14912627 0.67890629 0.26511338 0.77265629]
[0.14636467 0.79062506 0.84725811 0.91093753]
1H NMR
400 MHz
CDCl3
8.78 (d, J = 8.5 Hz, 1H), 8.17 (d, J = 8.4 Hz, 1H), 7.92 (d, J = 7.4 Hz, 1H), 7.55 (t, J = 7.7 Hz, 1H), 7.53-7.45 (m, 1H), 7.43 (d, J = 7.4 Hz, 1H), 7.37-7.22 (m, 5H), 6.75 (s, 1H), 4.61 (d, J = 5.8 Hz, 2H), 4.41 (m, 2H), 1.43 (t, J = 7.1 Hz, 3H)
null
[('d', ['8.5Hz'], '1H', 8.78, 8.78), ('d', ['8.4Hz'], '1H', 8.17, 8.17), ('d', ['7.4Hz'], '1H', 7.92, 7.92), ('t', ['7.7Hz'], '1H', 7.55, 7.55), ('m', [], '1H', 7.53, 7.45), ('d', ['7.4Hz'], '1H', 7.43, 7.43), ('m', [], '5H', 7.37, 7.22), ('s', [], '1H', 6.75, 6.75), ('d', ['5.8Hz'], '2H', 4.61, 4.61), ('m', [], '2H', ...
19
13
19
10.1039_c8qo00919h
CCOC(=O)c1ccc(C(=O)NCc2ccccc2)c2ccccc12
9
9
[0.14912627 0.67890629 0.26511338 0.77265629]
[0.14636467 0.79062506 0.84725811 0.91093753]
13C NMR
100 MHz
CDCl3
166.1, 165.6, 162.1, 149.6, 147.0, 132.2, 129.0, 121.1, 119.8, 106.7, 77.3, 77.0, 76.7, 61.4, 60.5, 14.2
null
[(166.1, None, None), (165.6, None, None), (162.1, None, None), (149.6, None, None), (147.0, None, None), (132.2, None, None), (129.0, None, None), (121.1, None, None), (119.8, None, None), (106.7, None, None), (77.3, None, None), (77.0, None, None), (76.7, None, None), (61.4, None, None), (60.5, None, None), (14.2, No...
21
19
16
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)OCc2ccccc2)c1
10
10
[0.15050707 0.14960938 0.25931401 0.23789065]
[0.1474693 0.2496094 0.84781045 0.39414065]
1H NMR
400 MHz
CDCl3
8.72 (s, 1H), 8.23 (m, 2H), 7.50 (d, J = 7.8 Hz, 1H), 7.48-7.41 (m, 2H), 7.36 (m, 3H), 5.38 (d, J = 4.3 Hz, 2H), 4.39 (m, 2H), 1.39 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.72, 8.72), ('m', [], '2H', 8.23, 8.23), ('d', ['7.8Hz'], '1H', 7.5, 7.5), ('m', [], '2H', 7.48, 7.41), ('m', [], '3H', 7.36, 7.36), ('d', ['4.3Hz'], '2H', 5.38, 5.38), ('m', [], '2H', 4.39, 4.39), ('t', ['7.1Hz'], '3H', 1.39, 1.39)]
16
10
16
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)OCc2ccccc2)c1
10
10
[0.15050707 0.14960938 0.25931401 0.23789065]
[0.1474693 0.2496094 0.84781045 0.39414065]
13C NMR
100 MHz
CDCl3
165.5, 135.8, 133.8, 131.1, 130.5, 128.6, 128.4, 128.1, 77.4, 77.1, 76.8, 67.0, 61.3, 14.3
null
[(165.5, None, None), (135.8, None, None), (133.8, None, None), (131.1, None, None), (130.5, None, None), (128.6, None, None), (128.4, None, None), (128.1, None, None), (77.4, None, None), (77.1, None, None), (76.8, None, None), (67.0, None, None), (61.3, None, None), (14.3, None, None)]
17
15
14
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)OCc2cccc(OC)c2)c1
10
10
[0.1502309 0.4089844 0.25682858 0.51367191]
[0.14802163 0.52734379 0.84836274 0.69765626]
1H NMR
400 MHz
CDCl3
8.73 (s, 1H), 8.25 (t, J = 4.7 Hz, 2H), 7.52 (t, J = 7.8 Hz, 1H), 7.31 (t, J = 7.9 Hz, 1H), 7.07-6.97 (m, 2H), 6.89 (d, J = 8.2 Hz, 1H), 5.37 (s, 2H), 4.40 (m, 2H), 3.82 (s, 3H), 1.41 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.73, 8.73), ('t', ['4.7Hz'], '2H', 8.25, 8.25), ('t', ['7.8Hz'], '1H', 7.52, 7.52), ('t', ['7.9Hz'], '1H', 7.31, 7.31), ('m', [], '2H', 7.07, 6.97), ('d', ['8.2Hz'], '1H', 6.89, 6.89), ('s', [], '2H', 5.37, 5.37), ('m', [], '2H', 4.4, 4.4), ('s', [], '3H', 3.82, 3.82), ('t', ['7.1Hz'], '3H', 1.41, 1.4...
18
12
18
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)OCc2cccc(Br)c2)c1
10
10
[0.1502309 0.71796879 0.24881994 0.81328128]
[0.14802163 0.82968756 0.84836274 0.89843757]
1H NMR
400 MHz
CDCl3
8.72 (s, 1H), 8.24 (d, J = 7.7 Hz, 2H), 7.61 (s, 1H), 7.54 (t, J = 7.8 Hz, 1H), 7.48 (d, J = 8.0 Hz, 1H), 7.38 (d, J = 7.7 Hz, 1H), 7.26 (t, J = 7.8 Hz, 1H), 5.35 (s, 2H), 4.41 (m, 2H), 1.41 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.72, 8.72), ('d', ['7.7Hz'], '2H', 8.24, 8.24), ('s', [], '1H', 7.61, 7.61), ('t', ['7.8Hz'], '1H', 7.54, 7.54), ('d', ['8.0Hz'], '1H', 7.48, 7.48), ('d', ['7.7Hz'], '1H', 7.38, 7.38), ('t', ['7.8Hz'], '1H', 7.26, 7.26), ('s', [], '2H', 5.35, 5.35), ('m', [], '2H', 4.41, 4.41), ('t', ['7.1Hz'], '3H', ...
15
11
15
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)OCc2cccc(Br)c2)c1
10
10
[0.1502309 0.71796879 0.24881994 0.81328128]
[0.14802163 0.82968756 0.84836274 0.89843757]
13C NMR
100 MHz
CDCl3
166.5, 165.8, 138.2, 137.9, 133.1, 129.7, 128.8, 127.9, 127.7, 127.0, 77.3, 77.0, 76.7, 61.3, 44.2, 14.2
null
[(166.5, None, None), (165.8, None, None), (138.2, None, None), (137.9, None, None), (133.1, None, None), (129.7, None, None), (128.8, None, None), (127.9, None, None), (127.7, None, None), (127.0, None, None), (77.3, None, None), (77.0, None, None), (76.7, None, None), (61.3, None, None), (44.2, None, None), (14.2, No...
17
17
16
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)OCc2cc3ccccc3[nH]2)c1
11
11
[0.15050707 0.20390626 0.26815112 0.28750001]
[0.14802163 0.30664062 0.84946742 0.5027344 ]
1H NMR
400 MHz
CDCl3
8.82 (s, 1H), 8.68 (s, 1H), 8.20 (t, J = 6.7 Hz, 2H), 7.60 (d, J = 7.9 Hz, 1H), 7.48 (t, J = 7.8 Hz, 1H), 7.35 (d, J = 8.2 Hz, 1H), 7.19 (t, J = 7.6 Hz, 1H), 7.10 (t, J = 7.5 Hz, 1H), 6.62 (s, 1H), 5.48 (s, 2H), 4.39 (m, 2H), 1.39 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.82, 8.82), ('s', [], '1H', 8.68, 8.68), ('t', ['6.7Hz'], '2H', 8.2, 8.2), ('d', ['7.9Hz'], '1H', 7.6, 7.6), ('t', ['7.8Hz'], '1H', 7.48, 7.48), ('d', ['8.2Hz'], '1H', 7.35, 7.35), ('t', ['7.6Hz'], '1H', 7.19, 7.19), ('t', ['7.5Hz'], '1H', 7.1, 7.1), ('s', [], '1H', 6.62, 6.62), ('s', [], '2H', 5.48, ...
17
13
17
10.1039_c8qo00919h
C#CCOC(=O)c1cccc(C(=O)OCC)c1
11
11
[0.15078323 0.52265629 0.26179944 0.59921877]
[0.14691699 0.6171875 0.84836274 0.73671876]
1H NMR
400 MHz
CDCl3
8.71 (s, 1H), 8.37-8.09 (m, 2H), 7.55 (t, J = 7.8 Hz, 1H), 4.96 (s, 2H), 4.42 (m, 2H), 2.58 (s, 1H), 1.42 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.71, 8.71), ('m', [], '2H', 8.37, 8.09), ('t', ['7.8Hz'], '1H', 7.55, 7.55), ('s', [], '2H', 4.96, 4.96), ('m', [], '2H', 4.42, 4.42), ('s', [], '1H', 2.58, 2.58), ('t', ['7.1Hz'], '3H', 1.42, 1.42)]
12
8
12
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)OC(C(F)(F)F)C(F)(F)F)c1
11
11
[0.15050707 0.75625001 0.266218 0.83281253]
[0.1474693 0.85000001 0.84781045 0.89062507]
1H NMR
400 MHz
CDCl3
8.76 (s, 1H), 8.35 (d, J = 7.8 Hz, 1H), 8.30 (d, J = 7.8 Hz, 1H), 7.62 (t, J = 7.8 Hz, 1H), 6.05 (quint, J = 6 Hz, 1H), 4.44 (m, 2H), 1.43 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.76, 8.76), ('d', ['7.8Hz'], '1H', 8.35, 8.35), ('d', ['7.8Hz'], '1H', 8.3, 8.3), ('t', ['7.8Hz'], '1H', 7.62, 7.62), ('p', ['6Hz'], '1H', 6.05, 6.05), ('m', [], '2H', 4.44, 4.44), ('t', ['7.1Hz'], '3H', 1.43, 1.43)]
10
7
10
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)OC(C(F)(F)F)C(F)(F)F)c1
11
11
[0.15050707 0.75625001 0.266218 0.83281253]
[0.1474693 0.85000001 0.84781045 0.89062507]
19F NMR
376 MHz
CDCl3
-73.1
null
[(-73.1, None, None)]
6
1
1
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)ON2C(=O)CCC2=O)c1
12
12
[0.15050707 0.22773438 0.25959018 0.31757813]
[0.14802163 0.328125 0.84836274 0.44531254]
1H NMR
400 MHz
CDCl3
8.79 (s, 1H), 8.33 (m, 2H), 7.63 (t, J = 7.8 Hz, 1H), 4.42 (m, 2H), 2.93 (s, 4H), 1.42 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.79, 8.79), ('m', [], '2H', 8.33, 8.33), ('t', ['7.8Hz'], '1H', 7.63, 7.63), ('m', [], '2H', 4.42, 4.42), ('s', [], '4H', 2.93, 2.93), ('t', ['7.1Hz'], '3H', 1.42, 1.42)]
13
7
13
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)ON2C(=O)CCC2=O)c1
12
12
[0.15050707 0.22773438 0.25959018 0.31757813]
[0.14802163 0.328125 0.84836274 0.44531254]
13C NMR
100 MHz
CDCl3
169.2, 165.0, 161.2, 135.6, 134.4, 131.4, 129.1, 125.5, 77.4, 77.1, 76.8, 61.6, 25.6, 14.2
null
[(169.2, None, None), (165.0, None, None), (161.2, None, None), (135.6, None, None), (134.4, None, None), (131.4, None, None), (129.1, None, None), (125.5, None, None), (77.4, None, None), (77.1, None, None), (76.8, None, None), (61.6, None, None), (25.6, None, None), (14.2, None, None)]
14
12
14
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)OC2(c3cc4ccccc4o3)CCC2)c1
12
12
[0.15078323 0.46796879 0.28113062 0.56015627]
[0.14691699 0.57968752 0.84836274 0.75078128]
1H NMR
400 MHz
CDCl3
8.70 (s, 1H), 8.36-8.03 (m, 2H), 7.65-7.48 (m, 2H), 7.44 (d, J = 8.3 Hz, 1H), 7.34-7.12 (m, 2H), 6.88 (s, 1H), 4.40 (m, 2H), 3.00-2.87 (m, 2H), 2.88-2.71 (m, 2H), 2.00 (m, 2H), 1.41 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.7, 8.7), ('m', [], '2H', 8.36, 8.03), ('m', [], '2H', 7.65, 7.48), ('d', ['8.3Hz'], '1H', 7.44, 7.44), ('m', [], '2H', 7.34, 7.12), ('s', [], '1H', 6.88, 6.88), ('m', [], '2H', 4.4, 4.4), ('m', [], '2H', 3.0, 2.87), ('m', [], '2H', 2.88, 2.71), ('m', [], '2H', 2.0, 2.0), ('t', ['7.1Hz'], '3H', 1.41, ...
20
13
20
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)OC2(c3cc4ccccc4o3)CCC2)c1
12
12
[0.15078323 0.46796879 0.28113062 0.56015627]
[0.14691699 0.57968752 0.84836274 0.75078128]
13C NMR
100 MHz
CDCl3
165.8, 164.2, 156.7, 154.9, 133.8, 130.8, 128.5, 128.0, 124.3, 122.8, 121.2, 111.3, 104.2, 77.8, 77.3, 77.0, 76.7, 61.3, 34.1, 14.5, 14.3
null
[(165.8, None, None), (164.2, None, None), (156.7, None, None), (154.9, None, None), (133.8, None, None), (130.8, None, None), (128.5, None, None), (128.0, None, None), (124.3, None, None), (122.8, None, None), (121.2, None, None), (111.3, None, None), (104.2, None, None), (77.8, None, None), (77.3, None, None), (77.0,...
22
21
21
10.1039_c8qo00919h
CCCOC(=O)c1cccc(C(=O)OCc2ccccc2)c1
13
13
[0.1502309 0.39003908 0.26345641 0.46953128]
[0.14691699 0.48515628 0.84836274 0.63046881]
1H NMR
400 MHz
CDCl3
8.73 (s, 1H), 8.24 (t, J = 7.2 Hz, 2H), 7.52 (t, J = 7.8 Hz, 1H), 7.46 (d, J = 6.9 Hz, 2H), 7.39 (t, J = 9.7 Hz, 3H), 5.39 (s, 2H), 4.30 (t, J = 6.7 Hz, 2H), 1.80 (m, 2H), 1.03 (t, J = 7.4 Hz, 3H)
null
[('s', [], '1H', 8.73, 8.73), ('t', ['7.2Hz'], '2H', 8.24, 8.24), ('t', ['7.8Hz'], '1H', 7.52, 7.52), ('d', ['6.9Hz'], '2H', 7.46, 7.46), ('t', ['9.7Hz'], '3H', 7.39, 7.39), ('s', [], '2H', 5.39, 5.39), ('t', ['6.7Hz'], '2H', 4.3, 4.3), ('m', [], '2H', 1.8, 1.8), ('t', ['7.4Hz'], '3H', 1.03, 1.03)]
18
11
18
10.1039_c8qo00919h
CCCCCOC(=O)c1cccc(C(=O)OCc2ccccc2)c1
13
13
[0.14995474 0.64687501 0.29687175 0.72656257]
[0.14691699 0.74296878 0.84836274 0.88828131]
1H NMR
400 MHz
CDCl3
8.72 (s, 1H), 8.24 (t, J = 8.2 Hz, 2H), 7.53 (t, J = 7.8 Hz, 1H), 7.46 (d, J = 7.2 Hz, 2H), 7.43-7.29 (m, 3H), 5.40 (s, 2H), 4.34 (t, J = 6.7 Hz, 2H), 1.84-1.71 (m, 2H), 1.40 (m, 4H), 0.93 (t, J = 6.9 Hz, 3H)
null
[('s', [], '1H', 8.72, 8.72), ('t', ['8.2Hz'], '2H', 8.24, 8.24), ('t', ['7.8Hz'], '1H', 7.53, 7.53), ('d', ['7.2Hz'], '2H', 7.46, 7.46), ('m', [], '3H', 7.43, 7.29), ('s', [], '2H', 5.4, 5.4), ('t', ['6.7Hz'], '2H', 4.34, 4.34), ('m', [], '2H', 1.84, 1.71), ('m', [], '4H', 1.4, 1.4), ('t', ['6.9Hz'], '3H', 0.93, 0.93)...
22
13
22
10.1039_c8qo00919h
CCCCCOC(=O)c1cccc(C(=O)OCc2ccccc2)c1
13
13
[0.14995474 0.64687501 0.29687175 0.72656257]
[0.14691699 0.74296878 0.84836274 0.88828131]
13C NMR
100 MHz
CDCl3
165.7, 135.8, 133.8, 131.0, 130.7, 128.6, 128.3, 77.3, 77.0, 76.7, 67.0, 65.5, 28.3, 28.1, 22.3, 13.9
null
[(165.7, None, None), (135.8, None, None), (133.8, None, None), (131.0, None, None), (130.7, None, None), (128.6, None, None), (128.3, None, None), (77.3, None, None), (77.0, None, None), (76.7, None, None), (67.0, None, None), (65.5, None, None), (28.3, None, None), (28.1, None, None), (22.3, None, None), (13.9, None,...
20
18
16
10.1039_c8qo00919h
CCCCCCOC(=O)c1cccc(C(=O)OCc2ccccc2)c1
14
14
[0.14940243 0.09511719 0.299081 0.16894533]
[0.14691699 0.18769532 0.84836274 0.35800783]
1H NMR
400 MHz
CDCl3
8.72 (s, 1H), 8.24 (t, J = 9.5 Hz, 2H), 7.52 (t, J = 7.8 Hz, 1H), 7.46 (d, J = 6.7 Hz, 2H), 7.42-7.31 (m, 3H), 5.39 (s, 2H), 4.34 (t, J = 6.7 Hz, 2H), 1.76 (m, 2H), 1.49-1.39 (m, 2H), 1.34 (m, 4H), 0.90 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.72, 8.72), ('t', ['9.5Hz'], '2H', 8.24, 8.24), ('t', ['7.8Hz'], '1H', 7.52, 7.52), ('d', ['6.7Hz'], '2H', 7.46, 7.46), ('m', [], '3H', 7.42, 7.31), ('s', [], '2H', 5.39, 5.39), ('t', ['6.7Hz'], '2H', 4.34, 4.34), ('m', [], '2H', 1.76, 1.76), ('m', [], '2H', 1.49, 1.39), ('m', [], '4H', 1.34, 1.34), (...
24
14
24
10.1039_c8qo00919h
CCCCCCOC(=O)c1cccc(C(=O)OCc2ccccc2)c1
14
14
[0.14940243 0.09511719 0.299081 0.16894533]
[0.14691699 0.18769532 0.84836274 0.35800783]
13C NMR
100MHz
CDCl3
165.7, 135.8, 133.8, 131.0, 130.8, 130.6, 128.6, 128.3, 77.4, 77.0, 76.7, 67.0, 65.5, 31.4, 28.6, 25.6, 22.5, 14.0
null
[(165.7, None, None), (135.8, None, None), (133.8, None, None), (131.0, None, None), (130.8, None, None), (130.6, None, None), (128.6, None, None), (128.3, None, None), (77.4, None, None), (77.0, None, None), (76.7, None, None), (67.0, None, None), (65.5, None, None), (31.4, None, None), (28.6, None, None), (25.6, None...
21
19
18
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)Sc2ccccc2Cl)c1
14
14
[0.15050707 0.3763672 0.25379082 0.45625001]
[0.14691699 0.47265629 0.84946742 0.61796878]
1H NMR
400 MHz
CDCl3
8.71 (s, 1H), 8.30 (d, J = 9.2 Hz, 1H), 8.21 (d, J = 9.6 Hz, 1H), 7.68-7.51 (m, 3H), 7.39 (m, 2H), 4.44 (m, 2H), 1.43 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.71, 8.71), ('d', ['9.2Hz'], '1H', 8.3, 8.3), ('d', ['9.6Hz'], '1H', 8.21, 8.21), ('m', [], '3H', 7.68, 7.51), ('m', [], '2H', 7.39, 7.39), ('m', [], '2H', 4.44, 4.44), ('t', ['7.1Hz'], '3H', 1.43, 1.43)]
13
10
13
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)SCc2ccccc2)c1
14
14
[0.1502309 0.63671875 0.24605834 0.71328126]
[0.14857395 0.73203131 0.84891508 0.90078126]
1H NMR
400 MHz
CDCl3
8.61 (s, 1H), 8.23 (d, J = 1.8 Hz, 1H), 8.13 (d, J = 7.9 Hz, 1H), 7.52 (t, J = 7.8 Hz, 1H), 7.38 (d, J = 7.1 Hz, 2H), 7.32 (d, J = 6.2 Hz, 2H), 7.25 (m, 1H), 4.44-4.37 (m, 2H), 4.34 (s, 2H), 1.44-1.38 (m, 3H)
null
[('s', [], '1H', 8.61, 8.61), ('d', ['1.8Hz'], '1H', 8.23, 8.23), ('d', ['7.9Hz'], '1H', 8.13, 8.13), ('t', ['7.8Hz'], '1H', 7.52, 7.52), ('d', ['7.1Hz'], '2H', 7.38, 7.38), ('d', ['6.2Hz'], '2H', 7.32, 7.32), ('m', [], '1H', 7.25, 7.25), ('m', [], '2H', 4.44, 4.37), ('s', [], '2H', 4.34, 4.34), ('m', [], '3H', 1.44, 1...
16
10
16
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)SCc2ccccc2)c1
14
14
[0.1502309 0.63671875 0.24605834 0.71328126]
[0.14857395 0.73203131 0.84891508 0.90078126]
13C NMR
100 MHz
CDCl3
190.5, 165.5, 137.0, 134.1, 133.6, 131.2, 129.0, 128.7, 128.3, 127.4, 77.4, 77.0, 76.7, 61.4, 33.5, 14.3
null
[(190.5, None, None), (165.5, None, None), (137.0, None, None), (134.1, None, None), (133.6, None, None), (131.2, None, None), (129.0, None, None), (128.7, None, None), (128.3, None, None), (127.4, None, None), (77.4, None, None), (77.0, None, None), (76.7, None, None), (61.4, None, None), (33.5, None, None), (14.3, No...
17
15
16
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)SCCc2ccccc2)c1
15
15
[0.15078323 0.08813477 0.27229351 0.1576172 ]
[0.14691699 0.17441407 0.84836274 0.31972658]
1H NMR
400 MHz
CDCl3
8.61 (s, 1H), 8.24 (d, J = 7.8 Hz, 1H), 8.13 (d, J = 3.8 Hz, 1H), 7.54 (t, J = 7.8 Hz, 1H), 7.36-7.21 (m, 5H), 4.42 (m, 2H), 3.43-3.23 (m, 2H), 3.08-2.91 (m, 2H), 1.42 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.61, 8.61), ('d', ['7.8Hz'], '1H', 8.24, 8.24), ('d', ['3.8Hz'], '1H', 8.13, 8.13), ('t', ['7.8Hz'], '1H', 7.54, 7.54), ('m', [], '5H', 7.36, 7.21), ('m', [], '2H', 4.42, 4.42), ('m', [], '2H', 3.43, 3.23), ('m', [], '2H', 3.08, 2.91), ('t', ['7.1Hz'], '3H', 1.42, 1.42)]
18
11
18
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)SCCc2ccccc2)c1
15
15
[0.15078323 0.08813477 0.27229351 0.1576172 ]
[0.14691699 0.17441407 0.84836274 0.31972658]
13C NMR
100 MHz
CDCl3
191.1, 165.6, 139.9, 137.4, 134.0, 131.1, 128.6, 128.2, 126.6, 77.3, 77.0, 76.7, 61.4, 35.8, 30.6, 14.3
null
[(191.1, None, None), (165.6, None, None), (139.9, None, None), (137.4, None, None), (134.0, None, None), (131.1, None, None), (128.6, None, None), (128.2, None, None), (126.6, None, None), (77.3, None, None), (77.0, None, None), (76.7, None, None), (61.4, None, None), (35.8, None, None), (30.6, None, None), (14.3, Non...
18
16
16
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)SC2CCCCC2)c1
15
15
[0.15105939 0.34062503 0.26345641 0.41328126]
[0.1474693 0.43281251 0.84836274 0.6039063 ]
1H NMR
400 MHz
CDCl3
8.60 (s, 1H), 8.21 (s, 1H), 8.12 (d, J = 7.8 Hz, 1H), 7.52 (t, J = 7.8 Hz, 1H), 4.41 (m, 2H), 3.76 (m, 1H), 2.03 (m, 2H), 1.82-1.69 (m, 2H), 1.65 (m, 2H), 1.52 (m, 4H), 1.42 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.6, 8.6), ('s', [], '1H', 8.21, 8.21), ('d', ['7.8Hz'], '1H', 8.12, 8.12), ('t', ['7.8Hz'], '1H', 7.52, 7.52), ('m', [], '2H', 4.41, 4.41), ('m', [], '1H', 3.76, 3.76), ('m', [], '2H', 2.03, 2.03), ('m', [], '2H', 1.82, 1.69), ('m', [], '2H', 1.65, 1.65), ('m', [], '4H', 1.52, 1.52), ('t', ['7.1Hz'], ...
20
10
20
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)SCC)c1
15
15
[0.15105939 0.62265631 0.27091271 0.70078131]
[0.1474693 0.71718751 0.84891508 0.83671878]
1H NMR
400 MHz
CDCl3
8.61 (s, 1H), 8.24 (d, J = 7.8 Hz, 1H), 8.13 (d, J = 8.0 Hz, 1H), 7.54 (t, J = 7.8 Hz, 1H), 4.42 (m, 2H), 3.11 (m, 2H), 1.42 (t, J = 7.1 Hz, 3H), 1.37 (t, J = 7.4 Hz, 3H)
null
[('s', [], '1H', 8.61, 8.61), ('d', ['7.8Hz'], '1H', 8.24, 8.24), ('d', ['8.0Hz'], '1H', 8.13, 8.13), ('t', ['7.8Hz'], '1H', 7.54, 7.54), ('m', [], '2H', 4.42, 4.42), ('m', [], '2H', 3.11, 3.11), ('t', ['7.1Hz'], '3H', 1.42, 1.42), ('t', ['7.4Hz'], '3H', 1.37, 1.37)]
14
8
14
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)O)c1
16
16
[0.14995474 0.45781253 0.24605834 0.52109377]
[0.14802163 0.53593753 0.85167668 0.62968753]
1H NMR
400 MHz
CDCl3
8.78 (s, 1H), 8.31 (d, J = 7.8 Hz, 2H), 7.58 (t, J = 7.8 Hz, 1H), 4.43 (m, 2H), 1.43 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.78, 8.78), ('d', ['7.8Hz'], '2H', 8.31, 8.31), ('t', ['7.8Hz'], '1H', 7.58, 7.58), ('m', [], '2H', 4.43, 4.43), ('t', ['7.1Hz'], '3H', 1.43, 1.43)]
10
7
9
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)O)c1
16
16
[0.14995474 0.45781253 0.24605834 0.52109377]
[0.14802163 0.53593753 0.85167668 0.62968753]
13C NMR
100 MHz
CDCl3
165.6, 134.6, 134.2, 131.2, 128.7, 77.3, 77.0, 76.7, 61.4, 14.3
null
[(165.6, None, None), (134.6, None, None), (134.2, None, None), (131.2, None, None), (128.7, None, None), (77.3, None, None), (77.0, None, None), (76.7, None, None), (61.4, None, None), (14.3, None, None)]
10
10
10
10.1039_c8qo00919h
CCOC(=O)c1ccc(C(=O)O)cc1
16
16
[0.15050707 0.64687501 0.28223527 0.70625004]
[0.1474693 0.72421881 0.84891508 0.81640632]
1H NMR
400 MHz
CDCl3
8.17 (m, 4H), 4.42 (m, 2H), 1.43 (t, J = 7.1 Hz, 3H)
null
[('m', [], '4H', 8.17, 8.17), ('m', [], '2H', 4.42, 4.42), ('t', ['7.1Hz'], '3H', 1.43, 1.43)]
10
5
9
10.1039_c8qo00919h
CCOC(=O)c1ccccc1-c1ccccc1C(=O)O
17
17
[0.15050707 0.46406251 0.29466246 0.53125004]
[0.1474693 0.54492191 0.84836274 0.66367193]
1H NMR
400 MHz
CDCl3
8.00 (m, 2H), 7.52 (m, 2H), 7.43 (t, J = 7.6 Hz, 2H), 7.18 (t, J = 7.4 Hz, 2H), 4.05 (m, 2H), 0.99 (t, J = 7.1 Hz, 3H)
null
[('m', [], '2H', 8.0, 8.0), ('m', [], '2H', 7.52, 7.52), ('t', ['7.6Hz'], '2H', 7.43, 7.43), ('t', ['7.4Hz'], '2H', 7.18, 7.18), ('m', [], '2H', 4.05, 4.05), ('t', ['7.1Hz'], '3H', 0.99, 0.99)]
14
11
13
10.1039_c8qo00919h
CCOC(=O)c1ccccc1-c1ccccc1C(=O)O
17
17
[0.15050707 0.46406251 0.29466246 0.53125004]
[0.1474693 0.54492191 0.84836274 0.66367193]
13C NMR
100 MHz
CDCl3
170.8, 167.5, 143.6, 142.6, 131.8, 131.3, 130.2, 129.8, 128.8, 127.2, 77.3, 77.0, 76.7, 60.8, 13.6
null
[(170.8, None, None), (167.5, None, None), (143.6, None, None), (142.6, None, None), (131.8, None, None), (131.3, None, None), (130.2, None, None), (129.8, None, None), (128.8, None, None), (127.2, None, None), (77.3, None, None), (77.0, None, None), (76.7, None, None), (60.8, None, None), (13.6, None, None)]
16
16
15
10.1039_c8qo00919h
N(C)(Cc1ccccc1)C(C#CCOC(=O)c1cccc(C(=O)OCC)c1)CCC
18
18
[0.1502309 0.25312501 0.30294725 0.35351566]
[0.14857395 0.3681641 0.84891508 0.56640629]
1H NMR
400 MHz
CDCl3
8.75 (s, 1H), 8.26 (t, J = 7.5 Hz, 2H), 7.54 (t, J = 7.8 Hz, 1H), 7.40-7.09 (m, 5H), 5.04 (s, 2H), 4.41 (m, 2H), 3.67 (d, J = 13.2 Hz, 1H), 3.45 (m, 2H), 2.21 (s, 3H), 1.66 (m, 2H), 1.47 (m, 2H), 1.41 (t, J = 7.1 Hz, 3H), 0.90 (t, J = 7.4 Hz, 3H)
null
[('s', [], '1H', 8.75, 8.75), ('t', ['7.5Hz'], '2H', 8.26, 8.26), ('t', ['7.8Hz'], '1H', 7.54, 7.54), ('m', [], '5H', 7.4, 7.09), ('s', [], '2H', 5.04, 5.04), ('m', [], '2H', 4.41, 4.41), ('d', ['13.2Hz'], '1H', 3.67, 3.67), ('m', [], '2H', 3.45, 3.45), ('s', [], '3H', 2.21, 2.21), ('m', [], '2H', 1.66, 1.66), ('m', []...
29
16
29
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)Nc2ccccc2)c1
19
19
[0.15078323 0.09296876 0.26069481 0.17187502]
[0.14691699 0.18789064 0.84836274 0.33320313]
1H NMR
400 MHz
CDCl3
8.48 (s, 1H), 8.19 (d, J = 10.4 Hz, 1H), 8.10 (d, J = 9.2 Hz, 2H), 7.66 (d, J = 7.7 Hz, 2H), 7.55 (t, J = 7.8 Hz, 1H), 7.37 (t, J = 7.9 Hz, 2H), 7.16 (t, J = 7.4 Hz, 1H), 4.40 (m, 2H), 1.41 (t, J = 7.1 Hz, 3H)
null
[('s', [], '1H', 8.48, 8.48), ('d', ['10.4Hz'], '1H', 8.19, 8.19), ('d', ['9.2Hz'], '2H', 8.1, 8.1), ('d', ['7.7Hz'], '2H', 7.66, 7.66), ('t', ['7.8Hz'], '1H', 7.55, 7.55), ('t', ['7.9Hz'], '2H', 7.37, 7.37), ('t', ['7.4Hz'], '1H', 7.16, 7.16), ('m', [], '2H', 4.4, 4.4), ('t', ['7.1Hz'], '3H', 1.41, 1.41)]
15
10
15
10.1039_c8qo00919h
CCOC(=O)c1cccc(C(=O)Nc2ccccc2)c1
19
19
[0.15078323 0.09296876 0.26069481 0.17187502]
[0.14691699 0.18789064 0.84836274 0.33320313]
13C NMR
100 MHz
CDCl3
165.8, 164.8, 137.7, 135.2, 132.6, 131.9, 130.9, 129.0, 127.5, 124.8, 120.4, 77.3, 77.0, 76.7, 61.5, 14.3
null
[(165.8, None, None), (164.8, None, None), (137.7, None, None), (135.2, None, None), (132.6, None, None), (131.9, None, None), (130.9, None, None), (129.0, None, None), (127.5, None, None), (124.8, None, None), (120.4, None, None), (77.3, None, None), (77.0, None, None), (76.7, None, None), (61.5, None, None), (14.3, N...
16
14
16
10.1021_acscatal.8b04073
CC(C)OC(=O)CBr
1
1
[0.48807446 0.33359377 0.60560668 0.37343752]
[0.11424633 0.40546876 0.8826287 0.70937502]
1H NMR
500 MHz
CDCl3
5.00 (m, 1H), 3.72 (s, 2H), 1.20 (d, J = 6.3 Hz, 6H)
none
[('m', [], '1H', 5.0, 5.0), ('s', [], '2H', 3.72, 3.72), ('d', ['6.3Hz'], '6H', 1.2, 1.2)]
9
3
9
10.1021_acscatal.8b04073
CC(C)OC(=O)CBr
1
1
[0.48807446 0.33359377 0.60560668 0.37343752]
[0.11424633 0.40546876 0.8826287 0.70937502]
13C NMR
125 MHz
CDCl3
166.7, 70.0, 26.4, 23.0, 21.5
none
[(166.7, None, None), (70.0, None, None), (26.4, None, None), (23.0, None, None), (21.5, None, None)]
5
4
5
10.1021_acscatal.8b04073
CC(C)OC(=O)C=N
1
2
[0.63998164 0.78359377 0.72693021 0.84453128]
[0.11424633 0.09306641 0.8826287 0.42343752]
1H NMR
500 MHz
CDCl3
5.07 (m, 1H), 4.65 (bs, 1H), 1.21 (d, J = 6.5 Hz, 6H)
none
[('m', [], '1H', 5.07, 5.07), ('brs', [], '1H', 4.65, 4.65), ('d', ['6.5Hz'], '6H', 1.21, 1.21)]
9
4
8
10.1021_acscatal.8b04073
CC(C)OC(=O)C=N
1
2
[0.63998164 0.78359377 0.72693021 0.84453128]
[0.11424633 0.09306641 0.8826287 0.42343752]
13C NMR
125 MHz
CDCl3
165.5, 68.4, 46.3, 22.0
none
[(165.5, None, None), (68.4, None, None), (46.3, None, None), (22.0, None, None)]
5
4
4
10.1021_acscatal.8b04073
C(Cl)(Cl)(Cl)COC(CNC(OC(C)(C)C)=O)=O
2
2
[0.56769302 0.54687504 0.76383274 0.63125005]
[0.11475184 0.66171881 0.88313423 0.88671883]
1H NMR
500 MHz
CDCl3
5.04 (bs, 1H), 4.75 (s, 1H), 4.03 (d, J = 6.0 Hz, 2H), 1.41 (s, 9H)
none
[('brs', [], '1H', 5.04, 5.04), ('s', [], '1H', 4.75, 4.75), ('d', ['6.0Hz'], '2H', 4.03, 4.03), ('s', [], '9H', 1.41, 1.41)]
14
4
13