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} | ['gnd:4223132-2', 'gnd:4155626-4', 'gnd:4327218-6'] | ['Fulvene', 'Titankomplexe', 'Stickstoffbrücke'] | ['che'] | ['gnd:1126046434'] | [['(ppn)642180857', '(firstid)GBV:642180857']] | [''] | [['(classificationName=ddc-dbn)540', '(classificationName=bk, id=106419269)35.60 - Metallorganische Verbindungen', '(classificationName=ddc)547.05512', '(classificationName=linseach:mapping)che', '(classificationName=bk, id=106408704)35.45 - Übergangselemente und ihre Verbindungen', '(classificationName=bk, id=106419234)35.43 - Koordinationsverbindungen, Komplexchemie']] | ['Darstellung und Verwendung von Titan-Pentafulven-Distickstoff-Komplexen'] | [['Sodium amalgam reduction of substituted cyclopentadienyl titanium trichlorides CpTiCl3 (Cp: C5H5, C5H4(t-Bu), C5Me4H, C5Me4(SiMe3) in the presence of pentafulvenes (C5H4=CR2, R: p-Tol, CR2: adamantyl) under nitrogen leads to dinuclear titanium complexes [{eta5-Cp)(eta6-C5H4=CR2)Ti}2(my2-eta1:eta1-N2)] with a moderately activated, bridging end-on coordinated dinitrogen ligand. The reactions of these N2 complexes with electrophilic substrates were investigated. The reaction with phenylsilane leads to a Si–H/C–H dehydrogenative coupling reaction of the pentafulvene ligand and the formation of a new N2 complex (R: p-Tol). Treatment with phenylacetylene results in an alkyne oligomerization (R: p-Tol), the lewis acid trimethylgallium gives a titanium trimethylgallium adduct with bridging CH3 groups (R: adamantyl). A possible functionalization of the N2 ligand is observed with trimethylsilylazide. <engl.>', 'Durch Reduktion von substituierten Cyclopentadienyltitantrichloriden CpTiCl3 (Cp: C5H5, C5H4(t-Bu), C5Me4H, C5Me4(SiMe3) mit Natriumamalgam in Gegenwart von Pentafulvenen (C5H4=CR2, R: p-Tol, CR2: Adamantyl) unter N2-Atmosphäre können end-on-distickstoffverbrückte Titankomplexe der allgemeinen Formel [{eta5-Cp)(eta6-C5H4=CR2)Ti}2(my2-eta1:eta1-N2)] mit moderat aktiviertem N2-Liganden in hoher Ausbeute synthetisiert werden. Die Reaktionen der Titan-Pentafulven-Distickstoff-Komplexe mit elektrophilen Reagenzien wurden untersucht. Die Umsetzung mit Phenylsilan führt zur Bildung eines N2-Komplexes mit einer Si–H/C–H-Dehydrokopplungsreaktion des Pentafulvenliganden (R: p-Tol). Bei Einsatz von Phenylacetylen kann eine Alkin-Oligomerisierung beobachtet werden (R: p-Tol). Mit Trimethylgallium bildet sich ein Addukt mit verbrückenden CH3-Gruppen (CR2 = Adamantyl). Mit Trimethylsilylazid kann eine mögliche Funktionalisierung des N2-Liganden beobachtet werden. <dt.>']] | ['2010'] | ['http://id.loc.gov/vocabulary/iso639-1/de'] | ['commercial licence'] | [[{'@id': 'gnd:4223132-2'}, {'@id': 'gnd:4155626-4'}, {'@id': 'gnd:4327218-6'}]] | ['gnd:1126046434', 'gnd:143288903', 'gnd:4155626-4', 'gnd:4223132-2', 'gnd:4327218-6', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A642180857'] | ['Beckhaus, Rüdiger', 'Oslage, Annika Margarete', 'Fulvene', 'Titankomplexe', 'Stickstoffbrücke'] | 5 |
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} | [] | [] | ['elt'] | [['gnd:172335477', 'gnd:122165527']] | [['(firstid)GBV:642698511', '(ppn)642698511']] | ['Techn. Univ. Hamburg-Harburg, Univ.-Bibl.'] | [['zellulares Netz', '(classificationName=linseach:mapping)elt', '(classificationName=bk, id=106417665)53.74 - Hochfrequenztechnik, Funktechnik', '(classificationName=ddc-dbn)620', 'radio communication', 'Funkübertragung', 'cellular network']] | ['Self-organized radio resource management in OFDM based cellular systems'] | [['Future mobile communication systems require higher data rates and more flexibility. The OFDM transmission technique, as a special form of multi-carrier transmission, achieves high efficiency by subdividing the bandwidth into narrow and orthogonal subcarriers with specific spectra. The consequent long symbol duration also facilitates a simple receiver structure in a multi-path propagation environment. Moreover, each subcarrier can use independently individual transmission parameters. In this thesis, a scheme for a self-organized radio resource management (SO-RRM) is proposed for an OFDM based cellular system. All base stations in a cellular network operate on the same central carrier frequency, but with different radio resources. A resource can be defined as a timeslot, a subcarrier, or any frequency-time block. All resources are accessible at any cell in the cellular network. Neither central controllers nor direct communication between base stations is needed. Each base station allocates radio resources and selects transmission parameters independently in accordance with the requirement and the measured real-time network condition. The powers of signal and interference are measured at both base stations and mobile terminals. To have an interference free measurement of the signal power, a dedicated signal measurement timeslot is designed in the uplink. A resource quality function is defined to predict the transmission result in a time variant channel, applying both adaptive modulation and coding, and link adaptation. Those resources with highest possible data rates are allocated. In this way, an adaptive and up-to-date resource reuse can be realized. To reduce the amount of dropped connections due to unpredictable new interference after allocation, a security margin is introduced, which reserves a priori a space for new interference. A suitable margin brings a 13% capacity increase. More efficiently, a reallocation procedure can be triggered when service degradation is observed for certain duration. This method can even bring about two times more capacity. The SO-RRM shows its high flexibility in a cellular network with a non-uniform or fast changing user distribution. Hotspot cells can claim more resources, while the cells with few users use only few resources. Furthermore, the multi-user diversity enables adaptive resource rearrangement in the downlink. Resources used inside a cell are exchanged based on instantaneous channel conditions. Three different algorithms are compared. They can bring a higher spectral efficiency of up to 80%.', 'Die OFDM-Übertragungstechnik erreicht eine hohe Effizienz in zukünftigen breitbandigen Mobilfunksystemen. Mit selbstorganisierender Verwaltung der zur Verfügung stehenden Funkressourcen kann ein OFDM-basiertes zellulares Gleichwellennetz die volle Flexibilität erreichen, insbesondere in einem Netzwerk mit ungleichmäßiger Nutzerverteilung (Hotspots). Jede Basisstation vergibt die Ressourcen bei Bedarf und basierend auf Echtzeit-Messungen des Nutzsignals sowie der Interferenzen. Weder eine zentrale Kontrollinstanz noch eine direkte Kommunikation zwischen den Basisstationen wird damit benötigt. In der Arbeit werden verschiedene Verfahren einer solchen selbstorganisierenden Ressourcenvergabe entwickelt und quantitativ verglichen. Dabei wird gezeigt, dass sich im Vergleich zu herkömmlicher Frequenzplanung eine Steigerung der spektralen Effizienz von bis zu 80% erreichen lässt.']] | ['2010'] | ['http://id.loc.gov/vocabulary/iso639-1/en'] | ['open access'] | [''] | ['gnd:10167110-6', 'gnd:122165527', 'gnd:143269097', 'gnd:172335477', 'gnd:4511937-5', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A642698511'] | ['Technische Universität Hamburg-Harburg, Institut für Nachrichtentechnik', 'Turau, Volker', 'Chen, Ting', 'Rohling, Hermann', 'Online-Ressource'] | 6 |
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} | ['gnd:4154684-2', 'gnd:7679140-3'] | ['Flügelfruchtgewächse', 'DNA Barcoding'] | ['bio'] | ['Technische Informationsbibliothek (TIB)'] | [['(firstid)GBV:645202290', '(ppn)645202290']] | ['Niedersächsische Staats- und Universitätsbibliothek'] | [['(classificationName=rvk)ZC 74300', '(classificationName=linseach:mapping)bio', '(classificationName=bk, id=106421654)48.46 - Holz', '(classificationName=ddc-dbn)500', '(classificationName=ddc)500', '(classificationName=linseach:mapping)hor', '(classificationName=bk, id=106410458)42.13 - Molekularbiologie']] | ['Isolation of DNA from unprocessed and processed wood of Dipterocarpaceae'] | ['Forest destruction and degradation (deforestation) remain major threats to the global biodiversity and cause enormous environmental damage in particular in tropical regions, where the highest density of species is accommodated. One third of global deforestation was caused by logging, in which more than 50% was illegally done (Brack, 2003). Dipterocarpaceae (dipterocarpsʺ) is a species-rich tree family distributed over the tropical belt of three continents of South America, Africa and Asia. Dipterocarps predominate the international tropical timber market (trade names: meranti, balau for Shorea spp., keruing for Dipterocarpus spp., kapur for Dryobalanops, etc.), and therefore play an important role in the economy of many Southeast Asian countries. However, in many regions dipterocarps are critically endangered due to forest destruction and non-sustainable forest management. Many activities have been initiated by government or non-government organizations to fight illegal logging. Several associations of wood-product manufacturers have released policy statements, in which member companies are committed to sourcing their wood or timber from legal and well-managed forests. Therefore, the development of tools to test the origin of wood particularly to check the plausibility of statements concerning the origin of wood from a certain forest enterprise is required. Molecular genetic methods can be useful to infer species identity and are promising tools to control the geographic origin of logged timber ...'] | ['2010'] | ['http://id.loc.gov/vocabulary/iso639-1/en'] | ['open access'] | [[{'@id': 'gnd:4154684-2'}, {'@id': 'gnd:7679140-3'}]] | ['gnd:4154684-2', 'gnd:7679140-3', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A645202290'] | ['Flügelfruchtgewächse', 'DNA Barcoding'] | 3 |
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