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2020-08-01
Critical cooling rates for amorphous-to-ordered complexion transitions in Cu-rich nanocrystalline alloys
Amorphous complexions in nanocrystalline metals have the potential to improve mechanical properties and radiation tolerance, as well as resistance to grain growth. In this study, the stability of amorphous complexions in binary and ternary Cu-based alloys is investigated by observing the effect of cooling rate from high temperature on the occurrence of amorphous-to-ordered complexion transitions. Bulk Cu-Zr and Cu-Zr-Hf alloy samples were annealed to induce boundary premelting and then quenched through a procedure that induces a gradient of local cooling rate through the sample height. Amorphous complexion thickness distributions were found to be invariant to local cooling rate in the Cu-Zr-Hf alloy, demonstrating enhanced stability of the amorphous complexion structure compared to the Cu-Zr alloy, which had thinner amorphous complexions in the regions that were slowly cooled. The experimental results are used to construct time-temperature-transformation diagrams of the amorphous-to-ordered complexion transition for both the binary and ternary alloys, enabling a deeper understanding of the influence of cooling rate and grain boundary chemistry on complexion transitions. The critical cooling rate necessary to avoid complexion transitions in the ternary alloy is found to be at least three orders of magnitude slower than that for the binary alloy.
2008.00292v2
2019-05-30
Ab initio theory of the spin-dependent conductivity tensor and the spin Hall effect in random alloys
We present an extension of the relativistic electron transport theory for the standard (charge) conductivity tensor of random alloys within the tight-binding linear muffin-tin orbital method to the so-called spin-dependent conductivity tensor, which describes the Kubo linear response of spin currents to external electric fields. The approach is based on effective charge- and spin-current operators, that correspond to intersite electron transport and that are nonrandom, which simplifies the configuration averaging by means of the coherent potential approximation. Special attention is paid to the Fermi sea term of the spin-dependent conductivity tensor, which contains a nonzero incoherent part, in contrast to the standard conductivity tensor. The developed formalism is applied to the spin Hall effect in binary random nonmagnetic alloys, both on a model level and for Pt-based alloys with an fcc structure. We show that the spin Hall conductivity consists of three contributions (one intrinsic and two extrinsic) which exhibit different concentration dependences in the dilute limit of an alloy. Results for selected Pt alloys (Pt-Re, Pt-Ta) lead to the spin Hall angles around 0.2; these sizable values are obtained for compositions that belong to thermodynamically equilibrium phases. These alloys can thus be considered as an alternative to other systems for efficient charge to spin conversion, which are often metastable crystalline or amorphous alloys.
1905.12855v2
2019-08-01
Valley Phenomena in the Candidate Phase Change Material WSe$_{2(1-x)}$Te$_{2x}$
Alloyed transition metal dichalcogenides provide an opportunity for coupling band engineering with valleytronic phenomena in an atomically-thin platform. However, valley properties in alloys remain largely unexplored. We investigate the valley degree of freedom in monolayer alloys of the phase change candidate material WSe$_{2(1-x)}$Te$_{2x}$. Low temperature Raman measurements track the alloy-induced transition from the semiconducting 1H phase of WSe$_2$ to the semimetallic 1T$_d$ phase of WTe$_2$. We correlate these observations with density functional theory calculations and identify new Raman modes from W-Te vibrations in the 1H alloy phase. Photoluminescence measurements show ultra-low energy emission features that highlight alloy disorder arising from the large W-Te bond lengths. Interestingly, valley polarization and coherence in alloys survive at high Te compositions and are more robust against temperature than in WSe$_2$. These findings illustrate the persistence of valley properties in alloys with highly dissimilar parent compounds and suggest band engineering can be utilized for valleytronic devices.
1908.00506v2
2020-05-30
Tribocorrosion under galvanic interaction of Ti6Al4V and NiCr implant alloys
Micromovements that occur in the joint between dental prostheses and implants can lead to wear-induced degradation. This process can be enhanced by corrosion in the oral environment influenced by the presence of solutions containing fluoride. Moreover, the eventual galvanic interactions between NiCr and Ti alloys can accelerate the wear-corrosion process. In this work, the tribocorrosion process of Ti6Al4V and NiCr alloys used in dental implant rehabilitations immersed in fluoride solutions at different pH values was investigated. The galvanic interaction effect between the alloys was also assessed. Tribocorrosion tests in corrosive media were performed with isolated Ti6Al4V and NiCr alloys, followed by testing with both alloys in contact. The media selected were based on fluoride concentrations and pH values that are possible to be found in oral environments. Analysis of the surfaces after the tribocorrosion tests was carried out using confocal laser microscopy. The wear profile and volume losses were determined by confocal measurements. It was concluded that the galvanic interaction between the alloys increased the tribocorrosion resistance of Ti6Al4V, compared with that of the isolated Ti6Al4V alloy. Ti6Al4V coupled with NiCr reduced the electrochemical potential decay during sliding. The increased resistance was explained by the electrochemical shift of the Ti6Al4V potential from active dissolution to the passive domain.
2006.00270v1
2021-06-01
The effect of local chemical ordering on dislocation activity in multi-principle element alloys: a three-dimensional discrete dislocation dynamics study
The exceptional combination of strength and ductility in multi-component alloys is often attributed to the interaction of dislocations with the various solute atoms in the alloy. To study these effects on the mechanical properties of such alloys there is a need to develop a modeling framework capable of quantifying the effect of these solutes on the evolution of dislocation networks. Large scale three-dimensional (3D) Discrete dislocation dynamics (DDD) simulations can provide access to such studies but to date no relevant approaches are available that aim for a complete representation of real alloys with arbitrary chemical compositions. Here, we introduce a formulation of dislocation interaction with substitutional solute atoms in fcc alloys in 3D DDD simulations that accounts for solute strengthening induced by atomic misfit as well as fluctuations in the cross-slip activation energy. Using this model, we show that local fluctuations in the chemical composition of various CrFeCoNi-based multi-principal element alloys (MPEA) lead to sluggish dislocation motion, frequent cross-slip and alignment of dislocations with solute aggregation features, explaining experimental observations related to mechanical behavior and dislocation activity. It is also demonstrated, that this behavior observed for certain MPEAs cannot be reproduced by assuming a perfect solid solution. The developed method also provides a basis for further investigations of dislocation plasticity in any real arbitrary fcc alloy with substitutional solutes.
2106.00823v2
2021-11-11
Controlling transition metal atomic ordering in two-dimensional Mo$_{1-x}$W$_{x}$S$_{2}$ alloys
The unique optical and electronic properties of two-dimensional transition metal dichalcogenides (2D TMDs) make them promising materials for applications in (opto-)electronics, catalysis and more. Specifically, alloys of 2D TMDs have broad potential applications owing to their composition-controlled properties. Several important challenges remain regarding controllable and scalable fabrication of these alloys, such as achieving control over their atomic ordering (i.e. clustering or random mixing of the transition metal atoms within the 2D layers). In this work, atomic layer deposition (ALD) is used to synthesize the TMD alloy Mo$_{1-x}$W$_{x}$S$_{2}$ with excellent composition control along the complete composition range 0 $\leq$ x $\leq$ 1. Importantly, this composition control allows us to control the atomic ordering of the alloy from well-mixed to clustered while keeping the alloy composition fixed, as is confirmed directly through atomic-resolution HAADF-STEM imaging. The control over atomic ordering leads to tuning of the bandgap, as is demonstrated using optical transmission spectroscopy. The relation between this tuning of the electronic structure and the atomic ordering of the alloy was further confirmed through ab-initio calculations. Furthermore, as the atomic ordering modulates from clustered to well-mixed, the typical MoS$_{2}$ and WS$_{2}$ A$_{1g}$ vibrational modes converge. Our results demonstrate that atomic ordering is an important parameter that can be tuned experimentally to finely tune the fundamental properties of 2D TMD alloys for specific applications.
2111.06289v1
2022-10-21
Effective Mg Incorporation in CdMgO Alloy on Quartz Substrate Grown by Plasma-assisted MBE
The development of CdMgO ternary alloy with a single cubic phase is challenging but meaningful work for technological advancement. In this work, we have grown a series of Cd1-xMgxO ternary random alloys with various Mg concentrations (x = 0, 30, 32, 45, and 55%) on quartz substrate by plasma-assisted molecular beam epitaxy (PA-MBE) technique. The structural investigations of alloys were performed using the X-ray diffraction (XRD) technique. The decreases in average crystallite size and lattice parameters were observed with an increase in Mg content in the alloys. XRD analysis confirms a single cubic phase is obtained for alloy compositions. The elemental and morphological studies were carried out using energy dispersive x-ray (EDX) spectroscopy and atomic force microscope (AFM) technique, respectively. The optical investigation was carried out using UV-Vis spectroscopy. The optical bandgaps were estimated using the Tauc relation and it was varied from 2.34 eV to 3.47 eV by varying the Mg content from zero to 55% in the alloys. The Urbach energy increases from 112 meV to 350 meV which suggests a more disordered localized state with an increase in Mg incorporation in the alloys.
2210.11785v1
2023-01-04
Plasticity in irradiated FeCrAl nanopillars investigated using discrete dislocation dynamics
In this paper, we investigate plasticity in irradiated FeCrAl nanopillars using discrete dislocation dynamics simulations (DDD), with comparisons to transmission electron microscopic (TEM) in situ tensile tests of ion and neutron irradiated commercial FeCrAl alloy C35M. The effects of irradiation-induced defects, such as a/2 111 and a 100 type loops and composition fluctuations representative of phase separation in irradiated FeCrAl alloys, are investigated separately as well as superposed together in simulations. We explore the effects of defects on the stress-strain behavior, specifically yield strength and hardening response, of FeCrAl nanopillars. Our simulations confirm the widely accepted fact that irradiated alloys exhibit a stress-strain response with higher yield strength and hardening as compared to homogeneous alloys. However, our DDD calculations reveal an atypical superposition of the hardening contributions due to composition inhomogeneity and irradiation loops wherein hardening due composition inhomogeneity counteracts hardening due to irradiation loops at small scales. As a result, we observe that the yield strength in irradiated alloys, after taking into consideration the effects of both composition inhomogeneity and irradiation loops, is smaller than the yield strength of the alloys with only irradiation loops and is approximately same for the alloy with composition inhomogeneity alone. We identify this destructive interference in the superposition in our parallel TEM in situ tensile tests on unirradiated, ion irradiated, and neutron irradiated C35M FeCrAl alloy as well. This destructive interference in the hardening contributions contrasts with the widely utilized dispersed barrier hardening (DBH) models by the experimental community to model the hardening contributions due to different irradiation induced defects.
2301.01812v1
2023-05-27
A novel and sustainable method to develop non-equiatomic CoCrFeNiMox high entropy alloys via spark plasma sintering using commercial commodity powders and evaluation of its mechanical behaviour
A novel approach to developing high entropy alloys (HEAs) using spark plasma sintering (SPS) was explored in this work where a mix of commercial commodity powders like Ni625, CoCrF75, and 316L was used instead of pre-alloyed powders avoiding the expensive pre-alloying steps like mechanical alloying or gas atomizing. Three non-equiatomic HEAs, based on Co, Cr, Fe, Ni, and Mo were designed and developed by blending the powders which were sintered via SPS and resulted in a single FCC phase after homogenization. The HEAs were microstructurally and mechanically characterized with tensile and hot compression tests up to a temperature of 750oC showing excellent properties. The maximum room temperature tensile strength and ductility demonstrated was 712 MPa and 62% respectively, by the alloy Co23.28Cr28.57Fe25.03Ni21.01Mo2.1. Moreover, the same alloy exhibited a compression strength greater than 640 MPa with a ductility above 45% at a temperature of 750oC. Also, this study paves the way for a novel fabrication route that offers more flexibility to develop new HEAs cost-effectively and efficiently which is crucial for the discovery of new materials over high-throughput techniques. Using such commodity alloys also opens the possibility of developing ingot casting from recycled scraps avoiding the direct use of critical metals.
2305.17407v1
2023-06-14
Machine learning-based prediction of elastic properties of amorphous metal alloys
The Young's modulus $E$ is the key mechanical property that determines the resistance of solids to tension/compression. In the present work, the correlation of the quantity $E$ with such characteristics as the total molar mass $M$ of alloy components, the number of components $n$ forming an alloy, the yield stress $\sigma_{y}$ and the glass transition temperature $T_{g}$ has been studied in detail based on a large set of empirical data for the Young's modulus of different amorphous metal alloys. It has been established that the values of the Young's modulus of metal alloys under normal conditions correlate with such a mechanical characteristic as the yield stress as well as with the glass transition temperature. As found, the specificity of the ``chemical formula'' of alloy, which is determined by molar mass $M$ and number of components $n$, does not affect on elasticity of the material. The machine learning algorithm identified both the quantities $M$ and $n$ as insignificant factors in determining $E$. A simple non-linear regression model is obtained that relates the Young's modulus with $T_{g}$ and $\sigma_{y}$, and this model correctly reproduces the experimental data for metal alloys of different types. This obtained regression model generalizes the previously presented empirical relation $E\simeq49.8\sigma_{y}$ for amorphous metal alloys.
2306.08387v1
2023-09-07
Enhanced strength-ductility combination by introducing bimodal grains structures in high-density oxide dispersion strengthened FeCrAl alloys fabricated by spark plasma sintering technology
Oxide dispersion strengthened FeCrAl alloys dispersed high-density nano-oxides in the matrix show outstanding corrosion resistance and mechanical properties. However, ODS FeCrAl alloys achieve the high strength generally at the expense of ductility in some way. Here, a method by introducing a bimodal grain structure was designed to overcome the strength-ductility tradeoff. In this work, ODS FeCrAl alloys were successfully fabricated through various mechanical alloying time, combined with spark plasma sintering under the vacuum of less than 4Pa. Microstructural characterization showed that the average grains size and nano-oxides size decrease gradually, and the density of nano-oxides increases, as the milling time increases. Mechanical properties revealed that both the strength and ductility were significantly synergistic enhanced with increasing milling time. The bimodal grain distribution characterized by electron backscatter diffraction (EBSD) (vacuum degree was less than 5E-5pa) was beneficial for the activation of the back stress strengthening and the annihilation of these microcracks, thus achieving the excellent ductility (27.65%). In addition, transmission electron microscope (TEM) characterization under the vacuum degree of less than 10-6pa illustrated that ultra-high-density nano-oxides (9.61E22/m3) was crucial for enhancing the strength of ODS FeCrAl alloys (993MPa). The strengthening mechanism superposition, based on the model of nano-oxides interrelated with the dislocation, illustrated an excellent agreement with experimental results from yield strength strengthening mechanisms. To our best knowledge, H40 (milled for 40h, and sintered at 1100C) alloy presents the outstanding strength with the exceptional ductility among all studied ODS FeCrAl alloys, which makes it the promising cladding materials for the accident tolerant fuel cladding.
2309.03703v1
2024-01-23
Thermal emissivity spectra and structural phase transitions of the eutectic Mg-51%Zn alloy: A candidate for thermal energy storage
The thermal emissivity spectrum in the mid infrared range (3 to 21 $\mu$m) as well as its dependence on temperature between 225 and 320 $^{\circ}$C has been obtained for the Mg-51%Zn (weight %) eutectic alloy, a candidate for thermal storage. The spectral curves show the typical behaviour of metals and alloys, with emissivity values between 0.05 and 0.2. It was also found that the emissivity spectrum shows variations in each heating cycle during the first few cycles. These changes are associated with the presence of metastable phases in the solid solid phase transition, present in the alloy below the melting point. The absence of signs of oxidation in air is very favourable for the use of this alloy in thermal energy storage systems. Moreover, the total normal emissivity curves obtained from dynamic spectral measurements have allowed analysing the behaviour phase transition sequence present in this alloy. These experimental results indicate that accurate emissivity measurements can be sensitive enough to account for the structural phase transitions in metals and alloys.
2401.13102v2
2024-02-16
Electronic structure-property relationship in an Al0.5TiZrPdCuNi high-entropy alloy
The valence band (VB) structure of an Al0.5TiZrPdCuNi high-entropy alloy (HEA) obtained from X-ray photoelectron spectroscopy has been compared to that recently calculated by Odbadrakh et al, 2019. Both experimental and theoretical VBs show split-band structures typical of alloys composed from the early (TE) and late (TL) transition metals. Accordingly, several properties of this alloy (both in the glassy and crystalline state) associated with the electronic structure (ES), are compared with those of similar TE-TL alloys. The comparison shows in addition to the usual dependence on the total TL content strong effect of alloying with Al on the density of states at the Fermi level, N(EF) and on the magnetic susceptibility of Al0.5TiZrPdCuNi HEA, which is like that of conventional glassy alloys, such as Zr-Cu-Al ones. Despite some similarity between the shapes of theoretical and corresponding experimental VBs there are significant quantitative differences between them which should be taken into account in any future studies of ES in HEAs and other compositionally complex alloys (CCA).
2402.10490v1
2024-03-25
Facile synthesis of CoSi alloy with rich vacancy for base- and solvent-free aerobic oxidation of aromatic alcohols
Rational design and green synthesis of low-cost and robust catalysts efficient for the selective oxidation of various alcohols are full of challenges. Herein, we report a fast and solvent-free arc-melting (AM) method to controllably synthesize semimetal CoSi alloy (abbreviated as AM-CoSi) that is efficient for the base- and solvent-free oxidation of six types of aromatic alcohols. X-ray absorption fine structure (XAFS), electron paramagnetic resonance (EPR), and aberration corrected high angle annular dark field scanning transmission electron microscope (AC HAADF-STEM) confirmed the successful synthesis of AM-CoSi with rich Si vacancy (Siv). The as-prepared CoSi alloy catalysts exhibit an order of magnitude activity enhancement in the oxidation of model reactant benzyl alcohol (BAL) to benzyl benzoate (BBE) compared with its mono counterparts, whereas 70 % yield of BBE which is the highest yield to date. Experimental results and DFT calculations well verify that the CoSi alloy structure improves the BAL conversion and Si vacancy mainly contributes to the generation of BBE. After that, CoSi alloy maintains high stability and a potential pathway is rationally proposed. Besides, CoSi alloy also efficiently works for the selective oxidation of various alcohols with different groups. This work demonstrates for the first time that semimetal CoSi alloy is robust for the green oxidation of various alcohols and provides a vast opportunity for reasonable design and application of other semimetal alloy catalysts.
2403.16708v1
2024-03-28
AlloyBERT: Alloy Property Prediction with Large Language Models
The pursuit of novel alloys tailored to specific requirements poses significant challenges for researchers in the field. This underscores the importance of developing predictive techniques for essential physical properties of alloys based on their chemical composition and processing parameters. This study introduces AlloyBERT, a transformer encoder-based model designed to predict properties such as elastic modulus and yield strength of alloys using textual inputs. Leveraging the pre-trained RoBERTa encoder model as its foundation, AlloyBERT employs self-attention mechanisms to establish meaningful relationships between words, enabling it to interpret human-readable input and predict target alloy properties. By combining a tokenizer trained on our textual data and a RoBERTa encoder pre-trained and fine-tuned for this specific task, we achieved a mean squared error (MSE) of 0.00015 on the Multi Principal Elemental Alloys (MPEA) data set and 0.00611 on the Refractory Alloy Yield Strength (RAYS) dataset. This surpasses the performance of shallow models, which achieved a best-case MSE of 0.00025 and 0.0076 on the MPEA and RAYS datasets respectively. Our results highlight the potential of language models in material science and establish a foundational framework for text-based prediction of alloy properties that does not rely on complex underlying representations, calculations, or simulations.
2403.19783v1
2011-05-02
Design scheme of new multifunctional Heusler compounds for spin-transfer torque applications
This paper has been withdrawn.
1105.0337v2
2018-01-10
Prediction of a magnetic Weyl semimetal without spin-orbit coupling and strong anomalous Hall effect in the Heusler compensated ferrimagnet Ti2MnAl
We predict a magnetic Weyl semimetal in the inverse Heusler Ti2MnAl, a compensated ferrimagnet with a vanishing net magnetic moment and a Curie temperature of over 650 K. Despite the vanishing net magnetic moment, we calculate a large intrinsic anomalous Hall effect (AHE) of about 300 S/cm. It derives from the Berry curvature distribution of the Weyl points, which are only 14 meV away from the Fermi level and isolated from trivial bands. Different from antiferromagnets Mn3X (X= Ge, Sn, Ga, Ir, Rh, and Pt), where the AHE originates from the non-collinear magnetic structure, the AHE in Ti2MnAl stems directly from the Weyl points and is topologically protected. The large anomalous Hall conductivity (AHC) together with a low charge carrier concentration should give rise to a large anomalous Hall angle. In contrast to the Co-based ferromagnetic Heusler compounds, the Weyl nodes in Ti2MnAl do not derive from nodal lines due to the lack of mirror symmetries in the inverse Heusler structure. Since the magnetic structure breaks spin-rotation symmetry, the Weyl nodes are stable without SOC. Moreover, because of the large separation between Weyl points of opposite topological charge, the Fermi arcs extent up to 75% of the reciprocal lattice vectors in length. This makes Ti2MnAl an excellent candidate for the comprehensive study of magnetic Weyl semimetals. It is the first example of a material with Weyl points, large anomalous Hall effect and angle despite a vanishing net magnetic moment.
1801.03273v3
2022-02-14
$Ab$ $Initio$ Study of Magnetic Tunnel Junctions Based on Half-Metallic and Spin-Gapless Semiconducting Heusler Compounds: Reconfigurable Diode and Inverse Tunnel-Magnetoresistance Effect
Magnetic tunnel junctions (MTJs) have attracted strong research interest within the last decades due to their potential use as nonvolatile memory such as MRAM as well as for magnetic logic applications. Half-metallic magnets (HMMs) have been suggested as ideal electrode materials for MTJs to achieve an extremely large tunnel-magnetoresistance (TMR) effect. Despite their high TMR ratios, MTJs based on HMMs do not exhibit current rectification, i.e., a diode effect, which was achieved in a magnetic tunnel junction concept based on HMMs and type-II spin-gapless semiconductors (SGSs). The proposed concept has recently been experimentally demonstrated using Heusler compounds. In the present work, we investigate from first-principles MTJs based on type-II SGS and HMM quaternary Heusler compounds FeVTaAl, FeVTiSi, MnVTiAl, and CoVTiSb. Our $ab$ $initio$ quantum transport calculations based on a nonequilibrium Green's function method have demonstrated that the MTJs under consideration exhibit current rectification with relatively high on:off ratios. We show that, in contrast to conventional semiconductor diodes, the rectification bias voltage window (or breakdown voltage) of the MTJs is limited by the spin gap of the HMM and SGS Heusler compounds. A unique feature of the present MTJs is that the diode effect can be configured dynamically, i.e., depending on the relative orientation of the magnetization of the electrodes, the MTJ allows the electrical current to pass either in one or the other direction, which leads to an inverse TMR effect. The combination of nonvolatility, reconfigurable diode functionality, tunable rectification voltage window, and high Curie temperature of the electrode materials makes the proposed MTJs very promising for room-temperature spintronic applications and opens ways to magnetic memory and logic concepts as well as logic-in-memory computing.
2202.06752v2
2024-02-08
Inflation and Isotropization in Quintom Cosmology
This paper studies inflation and isotropization in the quintom model in the Bianchi I, Bianchi III, and Kantowski-Sachs backgrounds. First, we investigate inherent properties and generalize Heusler's proposition. Then by the use of the dynamical system approach, we consider the system in multiplicative and collective modes of potentials. The conclusions of Collins and Hawking and also Burd and Barrow are discussed.
2402.05454v1
2001-03-02
Non-linear macroscopic polarization in III-V nitride alloys
We study the dependence of macroscopic polarization on composition and strain in wurtzite III-V nitride ternary alloys using ab initio density-functional techniques. The spontaneous polarization is characterized by a large bowing, strongly dependent on the alloy microscopic structure. The bowing is due to the different response of the bulk binaries to hydrostatic pressure, and to internal strain effects (bond alternation). Disorder effects are instead minor. Deviations from parabolicity (simple bowing) are of order 10 % in the most extreme case of AlInN alloy, much less at all other compositions. Piezoelectric polarization is also strongly non-linear. At variance with the spontaneous component, this behavior is independent of microscopic alloy structure or disorder effects, and due entirely to the non-linear strain dependence of the bulk piezoelectric response. It is thus possible to predict the piezoelectric polarization for any alloy composition using the piezoelectricity of the parent binaries.
0103050v1
2001-08-27
Kinetics of formation of twinned structures under L1_0 type orderings in alloys
The earlier-developed master equation approach and kinetic cluster methods are applied to study kinetics of L1_0 type orderings in alloys, including the formation of twinned structures characteristic of cubic-tetragonal-type phase transitions. A microscopical model of interatomic deformational interactions is suggested which generalizes a similar model of Khachaturyan for dilute alloys to the physically interesting case of concentrated alloys. The model is used to simulate A1->L1_0 transformations after a quench of an alloy from the disordered A1 phase to the single-phase L1_0 state for a number of alloy models with different chemical interactions, temperatures, concentrations, and tetragonal distortions. We find a number of peculiar features in both transient microstructures and transformation kinetics, many of them agreeng well with experimental data. The simulations also demonstrate a phenomenon of an interaction-dependent alignment of antiphase boundaries in nearly-equilibrium twinned bands which seems to be observed in some experiments.
0108422v1
2002-02-21
Screened Coulomb interactions in metallic alloys: I. Universal screening in the atomic sphere approximation
We have used the locally self-consistent Green's function (LSGF) method in supercell calculations to establish the distribution of the net charges assigned to the atomic spheres of the alloy components in metallic alloys with different compositions and degrees of order. This allows us to determine the Madelung potential energy of a random alloy in the single-site mean field approximation which makes the conventional single-site density-functional- theory coherent potential approximation (SS-DFT-CPA) method practically identical to the supercell LSGF method with a single-site local interaction zone that yields an exact solution of the DFT problem. We demonstrate that the basic mechanism which governs the charge distribution is the screening of the net charges of the alloy components that makes the direct Coulomb interactions short-ranged. In the atomic sphere approximation, this screening appears to be almost independent of the alloy composition, lattice spacing, and crystal structure. A formalism which allows a consistent treatment of the screened Coulomb interactions within the single-site mean-filed approximation is outlined. We also derive the contribution of the screened Coulomb interactions to the S2 formalism and the generalized perturbation method.
0202370v1
2003-04-29
EXAFS, XRD and RMC studies of an Amorphous Ga$_{50}$Se$_{50}$ Alloy Produced by Mechanical Alloying
The local atomic order of an amorphous Ga$_{50}$Se$_{50}$ alloy produced by Mechanical Alloying (MA) was studied by the Extended X-ray Absorption Fine Structure (EXAFS) and X-ray Diffraction (XRD) techniques and by Reverse Monte Carlo (RMC) simulations of its total x-ray structure factor. The coordination numbers and interatomic distances for the first neighbors were determined by means of EXAFS analysis and RMC simulations. The RMC simulations also furnished the partial pair distribution functions $G^{\text{RMC}}_{\text{Ga-Ga}}(r)$, $G^{\text{RMC}}_{\text{Ga-Se}}(r)$ and $G^{\text{RMC}}_{\text{Se-Se}}(r)$. The results obtained indicated that there are important differences among the local structure of the amorphous Ga$_{50}$Se$_{50}$ alloy produced by MA and those of the corresponding crystals, since there are Se-Se pairs in the first coordination shell of the amorphous alloy that are forbidden in the Ga$_{50}$Se$_{50}$ crystals.
0304666v1
2004-01-31
Reverse Monte Carlo Simulations and Raman Scattering of an Amorphous GeSe$_4$ Alloy Produced by Mechanical Alloying
The short and intermediate range order of an amorphous GeSe$_4$ alloy produced by Mechanical Alloying were studied by Reverse Monte Carlo simulations of its x-ray total structure factor and Raman scattering. The simulations were used to compute the $G^{\text{RMC}}_{\text{Ge-Ge}}(r)$, $G^{\text{RMC}}_{\text{Ge-Se}}(r)$ and $G^{\text{RMC}}_{\text{Se-Se}}(r)$ partial distribution functions and the ${\cal S}^{\text{RMC}}_{\text{Ge-Ge}}(K)$, ${\cal S}^{\text{RMC}}_{\text{Ge-Se}}(K)$ and ${\cal S}^{\text{RMC}}_{\text{Se-Se}}(K)$ partial structure factors. We calculated the coordination numbers and interatomic distances for the first and second neighbors and the bond-angle distribution functions $\Theta_{ijl}(\cos\theta)$. The data obtained indicate that the structure of the alloy has important differences when compared to alloys prepared by other techniques. There are a high number of Se-Se pairs in the first shell, and some of the tetrahedral units formed seemed to be connected by Se-Se bridges.
0402015v1
2006-04-04
Comparative study of the Portevin-Le Chatelier effect in interstitial and substitutional alloy
Tensile tests were carried out by deforming polycrystalline samples of an interstitial alloy, low carbon steel at room temperature in a wide range of strain rates where the Portevin-Le Chatelier (PLC) effect was observed. The observed stress time series data were analyzed using the nonlinear dynamical methods. From the analyses, we could establish the presence of marginal deterministic chaos in the PLC effect of the low carbon steel. Moreover, we made a comparative study of the PLC effect of this interstitial alloy with the substitutional Al-Mg alloy which shows that the dynamics of the PLC effect in the interstitial alloy is more complex compared to that of the substitutional alloy.
0604080v2
2006-05-30
Complex Precipitation Pathways in Multi-Component Alloys
One usual way to strengthen a metal is to add alloying elements and to control the size and the density of the precipitates obtained. However, precipitation in multicomponent alloys can take complex pathways depending on the relative diffusivity of solute atoms and on the relative driving forces involved. In Al-Zr-Sc alloys, atomic simulations based on first-principle calculations combined with various complementary experimental approaches working at different scales reveal a strongly inhomogeneous structure of the precipitates: owing to the much faster diffusivity of Sc compared with Zr in the solid solution, and to the absence of Zr and Sc diffusion inside the precipitates, the precipitate core is mostly Sc-rich, whereas the external shell is Zr-rich. This explains previous observations of an enhanced nucleation rate in Al-Zr-Sc alloys compared with binary Al-Sc alloys, along with much higher resistance to Ostwald ripening, two features of the utmost importance in the field of light high-strength materials.
0605738v1
2008-11-22
A simple theory of the Invar effect in iron-nickel alloys
Certain alloys of iron and nickel (so-called 'Invar' alloys) exhibit almost no thermal expansion over a wide range of temperature. It is clear that this is the result of an anomalous contraction upon heating which counteracts the normal thermal expansion arising from the anharmonicity of lattice vibrations. This anomalous contraction seems to be related to the alloys' magnetic properties, since the effect vanishes at a temperature close to the Curie temperature. However, despite many years of intensive research, a widely accepted microscopic theory of the Invar effect in face-centered-cubic Fe-Ni alloys is still lacking. Here we present a simple theory of the Invar effect in these alloys based on Ising magnetism, ab initio total energy calculations, and the Debye-Gruneisen model. We show that this theory accurately reproduces several well known properties of these materials, including Guillaume's famous plot1 of the thermal expansion coefficient as a function of the concentration of nickel. Within the same framework, we are able to account in a straightforward way for experimentally observed deviations from Vegard's law. Our approach supports the idea that the lattice constant is governed by a few parameters, including the fraction of iron-iron nearest-neighbour pairs.
0811.3673v1
2010-11-08
Tuning the spin texture in binary and ternary surface alloys on Ag(111)
Recently, a giant spin splitting has been observed in surface alloys on noble metal (111) surfaces as a result of a strong structural modification at the surface as well as the large atomic spin-orbit interaction (SOI) of the alloy atoms. These surface alloys are an ideal playground to manipulate both the size of the spin splitting as well as the position of the Fermi level as it is possible to change the atomic SOI as well as the relaxation by varying alloy atoms and substrates. Using spin- and angle-resolved photoemission spectroscopy in combination with quantitative low energy electron diffraction we have studied the mixed binary Bi(x)Sb(1-x)/Ag(111) and the mixed ternary Bi(x)Pb(y)Sb(1-x-y)/Ag(111) surface alloys where we observed a continuous evolution of the band structure with x and y.
1011.1829v1
2011-09-14
The Effect of dopants on magnetic properties of the ordered Fe_{65-x}Al_{35-y}M_{x,y} (M=Ga,B,V; x,y=5,10) alloys
The results of X-ray diffraction, complex in-field (up to 9 T) and temperature (5-300 K) Moessbauer and magnetometric studies of the ordered Fe_{65}Al_{35-x}M_x (M=Ga, B; x=0,5,10) and Fe_{65-x}V_xAl_{35} (x=5,10) alloys are presented. Analysis of the magnetometry studies shows that the systems Fe_{65}Al_{35} and Fe_{65}Al_{35-x}Ga_x (x=5, 10) are characterized by two different magnetic states with essentially distinguishing hysteresis loops and AC susceptibility values. The temperature and external magnetic field values inducing the transition from one magnetic state to another are higher in the Ga-doped alloys than in the reference Fe_{65}Al_{35} alloy. The boron addition transforms the magnetic state of the initial alloy Fe_{65}Al_{35} into a ferromagnetic one exhibiting high magnetic characteristics. Substitution of V for Fe in the ternary alloys Fe_{65-x}V_xAl_{35} results in reduction of magnetic characteristics and collapsing of 57Fe hyperfine magnetic filed.
1109.3064v1
2011-11-21
Ab initio theory of galvanomagnetic phenomena in ferromagnetic metals and disordered alloys
We present an ab initio theory of transport quantities of metallic ferromagnets developed in the framework of the fully relativistic tight-binding linear muffin-tin orbital method. The approach is based on the Kubo-Streda formula for the conductivity tensor, on the coherent potential approximation for random alloys, and on the concept of interatomic electron transport. The developed formalism is applied to pure 3d transition metals (Fe, Co, Ni) and to random Ni-based ferromagnetic alloys (Ni-Fe, Ni-Co, Ni-Mn). High values of the anisotropic magnetoresistance (AMR), found for Ni-rich alloys, are explained by a negligible disorder in the majority spin channel while a change of the sign of the anomalous Hall effect (AHE) on alloying is interpreted as a band-filling effect without a direct relation to the high AMR. The influence of disorder on the AHE in concentrated alloys is investigated as well.
1111.4793v2
2012-04-20
First-principles based modeling of hydrogen permeation through Pd-Cu alloys
The solubility and diffusivity of hydrogen in disordered Pd1-xCux alloys are investigated using a combination of first-principles calculations, a composition-dependent local cluster expansion (CDLCE) technique, and kinetic Monte Carlo simulations. We demonstrate that a linear CDCLE model can already accurately describe interstitial H in Pd1-xCux alloys over the entire composition range (0\leqx\leq1) with accuracy comparable to that of direct first-principles calculations. Our predicted H solubility and permeability results are in reasonable agreement with experimental measurements. The proposed model is quite general and can be employed to rapidly and accurately screen a large number of alloy compositions for potential membrane applications. Extension to ternary or higher-order alloy systems should be straightforward. Our study also highlights the significant effect of local lattice relaxations on H energetics in size-mismatched disordered alloys, which has been largely overlooked in the literature.
1204.4512v1
2012-10-03
Magnetic anisotropy energy of disordered tetragonal Fe-Co systems from ab initio alloy theory
We present results of systematic fully relativistic first-principles calculations of the uniaxial magnetic anisotropy energy (MAE) of a disordered and partially ordered tetragonal Fe-Co alloy using the coherent potential approximation (CPA). This alloy has recently become a promising system for thin ferromagnetic films with a perpendicular magnetic anisotropy. We find that existing theoretical approaches to homogeneous random bulk Fe-Co alloys, based on a simple virtual crystal approximation (VCA), overestimate the maximum MAE values obtained in the CPA by a factor of four. This pronounced difference is ascribed to the strong disorder in the minority spin channel of real alloys, which is neglected in the VCA and which leads to a broadening of the d-like eigenstates at the Fermi energy and to the reduction of the MAE. The ordered Fe-Co alloys with a maximum L1_0-like atomic long-range order can exhibit high values of the MAE, which, however, get dramatically reduced by small perturbations of the perfect order.
1210.1028v2
2013-01-10
First-principles calculation of the Gilbert damping parameter via the linear response formalism with application to magnetic transition-metals and alloys
A method for the calculations of the Gilbert damping parameter $\alpha$ is presented, which based on the linear response formalism, has been implemented within the fully relativistic Korringa-Kohn-Rostoker band structure method in combination with the coherent potential approximation alloy theory. To account for thermal displacements of atoms as a scattering mechanism, an alloy-analogy model is introduced. This allows the determination of $\alpha$ for various types of materials, such as elemental magnetic systems and ordered magnetic compounds at finite temperature, as well as for disordered magnetic alloys at $T = 0$ K and above. The effects of spin-orbit coupling, chemical and temperature induced structural disorder are analyzed. Calculations have been performed for the 3$d$ transition-metals bcc Fe, hcp Co, and fcc Ni, their binary alloys bcc Fe$_{1-x}$Co$_{x}$, fcc Ni$_{1-x}$Fe$_x$, fcc Ni$_{1-x}$Co$_x$ and bcc Fe$_{1-x}$V$_{x}$, and for 5d impurities in transition-metal alloys. All results are in satisfying agreement with experiment.
1301.2114v1
2013-11-15
Effects of Irradiation Temperature and Dose Rate on the Mechanical Properties of Self-Ion Implanted Fe and Fe-Cr Alloys
Pure Fe and model Fe-Cr alloys containing 5, 10 and 14%Cr were irradiated with Fe+ ions at a maximum energy of 2MeV to the same dose of 0.6dpa at temperatures of 300 C, 400 C and 500 C, and at dose rates corresponding to 6 x 10-4 dpa/s and 3 x 10-5 dpa/s. All materials exhibited an increase in hardness after irradiation at 300 C. After irradiation at 400 C, hardening was observed only in Fe-Cr alloys, and not in the pure Fe. After irradiation at 500 C, no hardening was observed in any of the materials tested. For irradiations at both 300 C and 400 C, greater hardening was found in the Fe-Cr alloys irradiated at the lower dose rate. Transmission electron microscopy and atom probe tomography of Fe 5%Cr identified larger dislocation loop densities and sizes in the alloy irradiated with the high dose rate and Cr precipitation in the alloy irradiated with the low dose rate.
1311.3786v1
2014-05-09
Thermodynamics, kinetics and fragility of bulk metallic glass forming liquids
This review deals with the kinetic and thermodynamic fragility of bulk metallic glass forming liquids. The experimental methods to determine the kinetic fragility, relaxation behavior and thermodynamic functions of undercooled metallic liquids are introduced. Existing data are assessed and discussed using the Vogel-Fulcher-Tammann equation and in the frameworks of the Adam-Gibbs as well as the Cohen-Turnbull free volume approach. In contrast to pure metals and most non glass forming alloys, bulk glass formers are moderately strong liquids. In general the fragility parameter $D^{*} $ increases with the complexity of the alloy with differences between the alloy families, e.g. noble-metal based alloys being more fragile than Zr-based alloys. At least some bulk metallic glass forming liquids, such as Vitreloy 1, undergo transitions from a fragile state at high temperatures to a strong state at low temperatures with indications that in Zr-based alloys this behavior is a common phenomenon.
1405.2251v1
2014-11-01
Ferromagnetic interactions and martensitic transformation in Fe doped Ni-Mn-In shape memory alloys
The structure, magnetic and martensitic properties of Fe doped Ni-Mn-In magnetic shape memory alloys have been studied by differential scanning calorimetry, magnetization, resistivity, X-ray diffraction (XRD) and EXAFS. While Ni$_{2}$MnIn$_{1-x}$Fe$_{x}$ ($0 \le x \le 0.6$) alloys are ferromagnetic and non martensitic, the martensitic transformation temperature in Ni$_{2}$Mn$_{1.5} $In$_{1-y}$Fe$_{y}$ and Ni$_{2}$Mn$ _{1.6} $In$_{1-y}$Fe$_{y}$ increases for lower Fe concentrations ($y \le 0.05$) before decreasing sharply for higher Fe concentrations. XRD analysis reveals presence of cubic and tetragonal structural phases in Ni$_{2}$MnIn$_{1-x}$Fe$_{x}$ at room temperature with tetragonal phase content increasing with Fe doping. Even though the local structure around Mn and Ni in these Fe doped alloys is similar to martensitic Mn rich Ni-Mn-In alloys, presence of ferromagnetic interactions and structural disorder induced by Fe affect Mn-Ni-Mn antiferromagnetic interactions resulting in suppression of martensitic transformation in these Fe doped alloys.
1411.0058v1
2015-05-04
Analyzing Alloy Formulas using an SMT Solver: A Case Study
This paper describes how Yices, a modern SAT Modulo theories solver, can be used to analyze the address-book problem expressed in Alloy, a first-order relational logic with transitive closure. Current analysis of Alloy models - as performed by the Alloy Analyzer - is based on SAT solving and thus, is done only with respect to finitized types. Our analysis generalizes this approach by taking advantage of the background theories available in Yices, and avoiding type finitization when possible. Consequently, it is potentially capable of proving that an assertion is a tautology - a capability completely missing from the Alloy Analyzer. This paper also reports on our experimental results that compare the performance of our analysis to that of the Alloy Analyzer for various versions of the address book problem.
1505.00672v1
2015-06-12
Ab initio study of structural, electronic, and thermal properties of Ir$_{1-x}$Rh$_{x}$ alloys
The structural, electronic, mechanical and thermal properties of Ir$_{1-x}$Rh$_{x}$ alloys were studied systematically using ab initio density functional theory at different concentrations (x = 0.00, 0.25, 0.50, 0.75, 1.00). A Special Quasirandom Structure method was used to make alloys having FCC structure with four atoms per unit cell. The ground state properties such as lattice constant and bulk modulus were calculated to find the equilibrium atomic position for stable alloys. The calculated ground state properties are in good agreement with the experimental and previously presented other theoretical data. The electronic band structure and density of states were calculated to study the electronic properties for these alloys at different concentrations. The electronic properties substantiate the metallic behavior of alloys. The first principle density functional perturbation theory as implemented in quasiharmonic approximation was used for the calculation of thermal properties. We have calculated the thermal properties such as Debye temperatures, vibration energy, entropy, constant-volume specific heat and internal energy. The ab initio linear-response method was used to calculate phonon densities of states.
1506.03966v1
2015-07-23
Deformation behavior of Mg-8.5wt.%Al alloy under reverse loading investigated by in-situ neutron diffraction and elastic viscoplastic self-consistent modeling
The cyclic deformation behavior of extruded Mg-8.5wt.%Al alloy with a conventional extrusion texture and a modified texture is systematically investigated by in-situ neutron diffraction and elastic viscoplastic self-consistent (EVPSC) modeling incorporating a twinning/de-twinning (TDT) scheme. The role of twinning and de-twinning on the deformation behavior of Mg-8.5wt.% Al alloy is investigated in terms of the macroscopic stress-strain response, the evolution of the activities of various deformation mechanisms, the texture evolution, the evolution of the internal elastic strains, and the evolution of the diffraction peak intensities. The alloy with the conventional extrusion texture undergoes twinning during initial compression and de-twinning during reverse tension. The same alloy does not favor twinning during initial tension, but rather during reverse compression. The alloy with a modified texture undergoes twinning during initial tension followed by detwinning during reverse compression. The results provide insights into the effect of initial texture, loading path, slip, twinning, de-twinning on the cyclic behavior of magnesium.
1507.06384v1
2016-01-11
Water-Induced Bimetallic Alloy Surface Segregation: A First Principle Study
Bimetallic alloys have drawn extensive attentions in materials science due to their widespread applications in electronics, engineering and catalysis. A very fundamental question of alloy is its surface segregation phenomenon. Many recent observations have shown that reactive gases or supports may have strong effects on alloy segregation. However, segregation in water, the most common solvent and environment, has not received enough attention. In this paper we give the quantitative descriptions on the surface segregation energies of 23 transition-metal impurities in Cu hosts under the conditions of water adsorption by performing density functional theory (DFT) calculations. The general trends in the changes of segregation energies caused by water adsorption are established. Our results show water adsorption could induce strong surface segregation tendencies for early and middle transition metals in Cu alloys. This finding not only prompts us to re-examine the potential effects of water on bimetallic alloy surfaces, but would be also very helpful as a guide for the further theoretical and experimental studies in this field.
1601.02346v1
2016-01-27
On the origin of bulk glass forming ability in Cu-Hf, Zr alloys
Understanding the formation of bulk metallic glasses (BMG) in metallic systems and finding a reliable criterion for selection of BMG compositions are among the most important issues in condensed matter physics and material science. Using the results of magnetic susceptibility measurements performed on both amorphous and crystallized Cu-Hf alloys (30-70 at% Cu) we find a correlation between the difference in magnetic susceptibilities of corresponding glassy and crystalline alloys and the variation in the glass forming ability (GFA) in these alloys. Since the same correlation can be inferred from data for the properties associated with the electronic structure of Cu-Zr alloys, it seems quite general and may apply to other glassy alloys based on early and late transition metals. This correlation is plausible from the free energy considerations and provides a simple way to select the compositions with high GFA.
1601.07397v2
2016-10-12
Effect of Electron Count and Chemical Complexity in the Ta-Nb-Hf-Zr-Ti High-Entropy Alloy Superconductor
High-entropy alloys are made from random mixtures of principal elements on simple lattices, stabilized by a high mixing entropy. The recently discovered BCC Ta-Nb-Hf-Zr-Ti high entropy alloy superconductor appears to display properties of both simple crystalline intermetallics and amorphous materials, e.g. it has a well defined superconducting transition along with an exceptional robustness against disorder. Here we show that the valence-electron count dependence of the superconducting transition temperature in the high entropy alloy falls between those of analogous simple solid solutions and amorphous materials, and test the effect of alloy complexity on the superconductivity. We propose high-entropy alloys as excellent intermediate systems for studying superconductivity as it evolves between crystalline and amorphous materials.
1610.03746v1
2016-11-03
High pressure synthesis of a hexagonal close-packed phase of the high-entropy alloy CrMnFeCoNi
High-entropy alloys, near-equiatomic solid solutions of five or more elements, represent a new strategy for the design of materials with properties superior to those of conventional alloys. However, their phase space remains constrained, with transition metal high-entropy alloys exhibiting only face- or body-centered cubic structures. Here, we report the high-pressure synthesis of a hexagonal close-packed phase of the prototypical high-entropy alloy CrMnFeCoNi. This martensitic transformation begins at 14 GPa and is attributed to suppression of the local magnetic moments, destabilizing the initial fcc structure. Similar to fcc-to-hcp transformations in Al and the noble gases, the transformation is sluggish, occurring over a range of >40 GPa. However, the behaviour of CrMnFeCoNi is unique in that the hcp phase is retained following decompression to ambient pressure, yielding metastable fcc-hcp mixtures. This demonstrates a means of tuning the structures and properties of high-entropy alloys in a manner not achievable by conventional processing techniques.
1611.00876v2
2017-01-09
Magnetic properties of ultra-thin 3d transition-metal binary alloys I: spin and orbital moments, anisotropy, and confirmation of Slater-Pauling behavior
The structure and static magnetic properties - saturation magnetization, perpendicular anisotropy, spectroscopic g-factor, and orbital magnetization - of thin-film 3d transition metal alloys are determined over the full range of alloy compositions via X-ray diffraction, magnetometry, and ferromagnetic resonance measurements. We determine the interfacial perpendicular magnetic anisotropy by use of samples sets with varying thickness for specific alloy concentrations. The results agree with prior published data and theoretical predictions. They provide a comprehensive compilation of the magnetic properties of thin-film Ni-Co, Ni-Fe and Co-Fe alloys that goes well beyond the often-cited Slater-Pauling dependence of magnetic moment on alloy concentration.
1701.02177v1
2017-07-29
Experimental study of extrinsic spin Hall effect in CuPt alloy
We have experimentally studied the effects on the spin Hall angle due to systematic addition of Pt into the light metal Cu. We perform spin torque ferromagnetic resonance measurements on Py/CuPt bilayer and find that as the Pt concentration increases, the spin Hall angle of CuPt alloy increases. Moreover, only 28% Pt in CuPt alloy can give rise to a spin Hall angle close to that of Pt. We further extract the spin Hall resistivity of CuPt alloy for different Pt concentrations and find that the contribution of skew scattering is larger for lower Pt concentrations, while the side-jump contribution is larger for higher Pt concentrations. From technological perspective, since the CuPt alloy can sustain high processing temperatures and Cu is the most common metallization element in the Si platform, it would be easier to integrate the CuPt alloy based spintronic devices into existing Si fabrication technology.
1707.09525v1
2018-03-27
Evidence of multiband superconductivity in the $β$-phase Mo$_{1-x}$Re$_x$ alloys
We present a detailed study of the superconducting properties in the beta-phase Mo$_{1-x}$Re$_x$ (x = 0.25 and 0.4) solid solution alloys pursued through magnetization and heat capacity measurements. The temperature dependence of the upper critical field H$_{C2}$(T) in these binary alloys shows a deviation from the prediction of the Werthamer-Helfand-Hohenberg (WHH) theory. The temperature dependence of superfluid density estimated from the variation of lower critical field H$_{C1}$ with temperature, cannot be explained within the framework of a single superconducting energy gap. The heat capacity also shows an anomalous feature in its temperature dependence. All these results can be reasonably explained by considering the existence of two superconducting energy gaps in these Mo$_{1-x}$Re$_x$ alloys. Initial results of electronic structure calculations and resonant photoelectron spectroscopy measurements support this possibility and suggest that the Re-5d like states at the Fermi level may not intermix with the Mo-5p and 5s like states in the beta-phase Mo$_{1-x}$Re$_x$ alloys and contribute quite distinctly to the superconductivity of these alloys.
1803.10315v1
2018-11-03
Modern Data Analytics Approach to Predict Creep of High-Temperature Alloys
A breakthrough in alloy design often requires comprehensive understanding in complex multi-component/multi-phase systems to generate novel material hypotheses. We introduce a modern data analytics workflow that leverages high-quality experimental data augmented with advanced features obtained from high-fidelity models. Herein, we use an example of a consistently-measured creep dataset of developmental high-temperature alloy combined with scientific alloy features populated from a high-throughput computational thermodynamic approach. Extensive correlation analyses provide ranking insights for most impactful alloy features for creep resistance, evaluated from a large set of candidate features suggested by domain experts. We also show that we can accurately train machine learning models by integrating high-ranking features obtained from correlation analyses. The demonstrated approach can be extended beyond incorporating thermodynamic features, with input from domain experts used to compile lists of features from other alloy physics, such as diffusion kinetics and microstructure evolution.
1811.01239v1
2020-01-19
Linking electronic structure calculations to generalized stacking fault energies in multicomponent alloys
The generalized stacking fault energy is a key ingredient to mesoscale models of dislocations. Here we develop an approach to quantify the dependence of generalized stacking fault energies on the degree of chemical disorder in multicomponent alloys. We introduce the notion of a "configurationally-resolved planar fault" (CRPF) energy and extend the cluster expansion method from alloy theory to express the CRPF as a function of chemical occupation variables of sites surrounding the fault. We apply the approach to explore the composition and temperature dependence of the unstable stacking fault energy (USF) in binary Mo-Nb alloys. First-principles calculations are used to parameterize a formation energy and CRPF cluster expansion. Monte Carlo simulations show that the distribution of USF energies is significantly affected by chemical composition and temperature. The formalism can be applied to any multicomponent alloy and will enable the development of rigorous models for deformation mechanisms in high-entropy alloys.
2001.06912v1
2019-04-23
Large-area synthesis of continuous two-dimensional MoTexSe2-x alloy films by chemical vapor deposition
Great achievements have been made in alloying of two-dimensional (2D) semiconducting transition metal dichalcogenides (TMDs), which can allow tunable band gaps for practical applications in optoelectronic devices. However, telluride-based TMDs alloys were less studied due to the difficulties of sample synthesis. Here, in this work we report the large-area synthesis of 2D MoTexSe2-x alloy films with controllable Te composition by a modified alkali metal halides assisted chemical vapor deposition method. The as-prepared films have millimeter-scale transverse size. Raman spectra experiments combining calculated Raman spectra and vibrational images obtained by density functional theory (DFT) confirmed the 2H-phase of the MoTexSe2-x alloys. The A1g mode of MoSe2 shows a significant downshift accompanied by asymmetric broadening to lower wavenumber with increasing value of x, while E12g mode seems unchanged, which were well explained by a phonon confinement model. Our work provides a simple method to synthesize large-scale 2H phase Te-based 2D TMDs alloys for their further applications.
1904.10218v1
2019-10-28
The spin Hall effect of Bi-Sb alloys driven by thermally excited Dirac-like electrons
We have studied the charge to spin conversion in Bi$_{1-x}$Sb$_x$/CoFeB heterostructures. The spin Hall conductivity (SHC) of the sputter deposited heterostructures exhibits a high plateau at Bi-rich compositions, corresponding to the topological insulator phase, followed by a decrease of SHC for Sb-richer alloys, in agreement with the calculated intrinsic spin Hall effect of Bi$_{1-x}$Sb$_x$ alloy. The SHC increases with increasing thickness of the Bi$_{1-x}$Sb$_x$ alloy before it saturates, indicating that it is the bulk of the alloy that predominantly contributes to the generation of spin current; the topological surface states, if present in the films, play little role. Surprisingly, the SHC is found to increase with increasing temperature, following the trend of carrier density. These results suggest that the large SHC at room temperature, with a spin Hall efficiency exceeding 1 and an extremely large spin current mobility, is due to increased number of Dirac-like, thermally-excited electrons in the $L$ valley of the narrow gap Bi$_{1-x}$Sb$_x$ alloy.
1910.12433v1
2019-10-29
Improvement on corrosion resistance and biocompability of ZK60 magnesium alloy by carboxyl ion implantation
Magnesium alloys have been considered to be potential biocompatible metallic materials. Further improvement on the anti-corrosion is expected to make this type of materials more suitable for biomedical applications in the fields of orthopedics, cardiovascular surgery and others. In this paper, we introduce a method of carboxyl ion (COOH+) implantation to reduce the degradation of ZK60 Mg alloy and improve its functionality in physiological environment. X-ray photoelectron spectroscopy (XPS) and atomic force microscopy (AFM) experiments show the formation of a smooth layer containing carbaxylic group, carbonate, metal oxides and hydroxides on the ion implanted alloy surface. Corrosion experiments and in vitro cytotoxicity tests demonstrate that the ion implantation treatment can both reduce the corrosion rate and improve the biocompatibility of the alloy. The promising results indicate that organic functional group ion implantation may be a practical method of improving the biological and corrosion properties of magnesium alloys.
1910.13219v1
2019-06-23
Effect of elastic anisotropy on phase separation in ternary alloys: A phase-field study
The precipitate shape, size and distribution are crucial factors which determine the properties of several technologically important alloys. Elastic interactions between the inclusions modify their morphology and align them along elastically favourable crystallographic directions. Among the several factors contributing to the elastic interaction energy between precipitating phases, anisotropy in elastic moduli is decisive in the emergence of modulated structures during phase separation in elastically coherent alloy systems. We employ a phase-field model incorporating elastic interaction energy between the misfitting phases to study microstructural evolution in ternary three-phase alloy systems when the elastic moduli are anisotropic. The spatiotemporal evolution of the composition field variables is governed by solving a set of coupled Cahn-Hilliard equations numerically using a semi-implicit Fourier spectral technique. We methodically vary the misfit strains, alloy chemistry and elastic anisotropy to investigate their influence on domain morphology during phase separation. The coherency strains between the phases and alloy composition alter the coherent phase equilibria and decomposition pathways. The degree of anisotropy in elastic moduli modifies the elastic interaction energy between the precipitates depending on the sign and magnitude of relative misfits, and thus determines the shape and alignment of the inclusions in the microstructure.
1906.09637v1
2020-05-20
Can experiment determine the stacking fault energy of metastable alloys?
Stacking fault energy (SFE) plays an important role in deformation mechanisms and mechanical properties of face-centered cubic (fcc) metals and alloys. In metastable fcc alloys, the SFEs determined from density functional theory (DFT) calculations and experimental methods often have opposite signs. Here, we show that the negative SFE by DFT reflects the thermodynamic instability of the fcc phase relative to the hexagonal close-packed one; while the experimentally determined SFEs are restricted to be positive by the models behind the indirect measurements. We argue that the common models underlying the experimental measurements of SFE fail in metastable alloys. In various concentrated solid solutions, we demonstrate that the SFEs obtained by DFT calculations correlate well with the primary deformation mechanisms observed experimentally, showing a better resolution than the experimentally measured SFEs. Furthermore, we believe that the negative SFE is important for understanding the abnormal behaviors of partial dislocations in metastable alloys under deformation. The present work advances the fundamental understanding of SFE and its relation to plastic deformations, and sheds light on future alloy design by physical metallurgy.
2005.09983v1
2020-08-26
Edge Dislocations Can Control Yield Strength in Refractory Body-Centered-Cubic High Entropy Alloys
Energy efficiency is motivating the search for new high-temperature metals. Some new body-centered-cubic random multicomponent "high entropy alloys (HEAs)" based on refractory elements (Cr-Mo-Nb-Ta-V-W-Hf-Ti-Zr) possess exceptional strengths at high temperatures but the physical origins of this outstanding behavior are not known. Here we show, using integrated neutron-diffraction (ND), high-resolution transmission electron microscopy (HRTEM), and theory, that the high strength and strength retention of a NbTaVTi alloy and a new high-strength/low-density CrMoNbV alloy are attributable to edge dislocations. This is surprising because plastic-flow in BCC elemental metals and dilute alloys is universally accepted to be controlled by screw dislocations. We use the insight and theory to perform a computationally-guided search over $10^7$ BCC HEAs and identify over $10^6$ possible ultra-strong high-temperature alloy compositions for future exploration.
2008.11671v1
2018-04-25
A multidisciplinary approach to study precipitation kinetics and hardening in an Al-4Cu (wt. %) alloy
A multidisciplinary approach is presented to analyse the precipitation process in a model Al-Cu alloy. Although this topic has been extensively studied in the past, most of the investigations are focussed either on transmission electron microscopy or on thermal analysis of the processes. The information obtained from these techniques cannot, however, provide a coherent picture of all the complex transformations that take place during decomposition of supersaturated solid solution. Thermal analysis, high resolution dilatometry, (high resolution) transmission electron microscopy and density functional calculations are combined to study precipitation kinetics, interfacial energies, and the effect of second phase precipitates on the mechanical strength of the alloy. Data on both the coherent and semi-coherent orientations of the {\theta}"/Al interface are reported for the first time. The combination of the different characterization and modelling techniques provides a detailed picture of the precipitation phenomena that take place during aging and of the different contributions to the strength of the alloy. This strategy can be used to analyse and design more complex alloys.
1804.09634v1
2019-03-03
Near-Unity Spin Hall Ratio in Ni$_x$Cu$_{1-x}$ Alloys
We report a large spin Hall effect in the 3$d$ transition metal alloy Ni$_x$Cu$_{1-x}$ for $x\in\left\{ 0.3,0.75\right\} $, detected via the ferromagnetic resonance of a Permalloy (Py = Ni$_{80}$Fe$_{20}$) film deposited in a bilayer with the alloy. A thickness series at $x$ = 0.6, for which the alloy is paramagnetic at room temperature, allows us to determine the spin Hall ratio $\theta_{\rm{SH}}\approx1$, spin diffusion length $\lambda_{\rm{s}}$, spin mixing conductance $G_{\uparrow\downarrow}$, and damping $\alpha_{\rm{SML}}$ due to spin memory loss . We compare our results with similar experiments on Py/Pt bilayers measured using the same method. Ab initio band structure calculations with disorder and spin-orbit coupling suggest an intrinsic spin Hall effect in Ni$_x$Cu$_{1-x}$ alloys, although the experiments here cannot distinguish between extrinsic and intrinsic mechanisms.
1903.00910v2
2019-03-19
Anomalous Ground State in Fe$_{1-x}$Ni$_{x}$ Invar alloys
This paper reports high resolution X-ray photoelectron spectroscopy (XPS) studies on Fe$_{1-x}$Ni$_x$ (x=0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.9) alloys down to 10 K temperature. Core levels and Auger transitions of the alloys except the invar alloy (x=0.4) exhibit no observable temperature induced changes. The invar alloy exhibits changes in the core levels below 20 K temperature that strongly depend on the core level. Such core level dependent changes with temperature were attributed to the precipitation of spin glass like phase below 20 K only in the invar alloy. Ni L$_3$M$_{45}$M$_{45}$ Auger transition also supported such precipitation below 20 K.
1903.08221v3
2019-08-10
Multielemental single-atom-thick A layers in nanolaminated V2(Sn, A)C (A=Fe, Co, Ni, Mn) for tailoring magnetic properties
Tailoring of individual single-atom-thick layers in nanolaminated materials offers atomic-level control over material properties. Nonetheless, multielement alloying in individual atomic layers in nanolaminates is largely unexplored. Here, we report a series of inherently nanolaminated V2(A'xSn1-x)C (A'=Fe, Co, Ni and Mn, and combinations thereof, with x=1/3) synthesized by an alloy-guided reaction. The simultaneous occupancy of the four magnetic elements and Sn, the individual single-atom-thick A layers in the compound constitute high-entropy-alloy analogues, two-dimensional in the sense that the alloying exclusively occurs in the A layers. V2(A'xSn1-x)C exhibit distinct ferromagnetic behavior that can be compositionally tailored from the multielement A-layer alloying. This two-dimensional alloying provides a structural-design route with expanded chemical space for discovering materials and exploit properties.
1908.03709v1
2019-12-10
Grain refinement and enhancement of critical current density in the V_0.60Ti_0.40 alloy superconductors with Gd addition
The V-Ti alloys are promising materials as alternate to the commercial Nb-based superconductors for high current-high magnetic field applications. However, the critical current density (J_c) of these alloys are somewhat low due to their low grain-boundary density. We show here that grain refinement of the V-Ti alloys and enhancement of the J_c can be achieved by the addition of Gd into the system, which precipitates as clusters along the grain boundaries. Both the J_c and the pinning force density (F_P) increase with the increasing Gd content up to 1 at. % Gd, where they are more than 20 times higher than those of the parent V_0.60Ti_0.40 alloy. Introduction of Gd into the system also leads to ferromagnetic (FM) correlations, and the alloys containing more than 0.5 at. % Gd exhibit spontaneous magnetization. In spite of the FM correlations, the superconducting transition temperature increases slightly with Gd-addition.
1912.04507v2
2020-03-20
Experimental and theoretical study of tracer diffusion in a series of (CoCrFeMn)$_{100-x}$Ni$_x$ alloys
Tracer diffusion of all constituting elements is studied at various temperatures in a series of (CoCrFeMn)$_{100-x}$Ni$_x$ alloys with compositions ranging from pure Ni to the equiatomic CoCrFeMnNi high-entropy alloy. At a given homologous temperature, the measured tracer diffusion coefficients change non-monotonically along the transition from pure Ni to the concentrated alloys and finally to the equiatomic CoCrFeMnNi alloy. This is explained by atomistic Monte-Carlo simulations based on a modified embedded-atom potentials, which reveal that local heterogeneities of the atomic configurations around a vacancy cause correlation effects and induce significant deviations from predictions of the random alloy model.
2003.09474v1
2020-06-13
Structural properties of Fe-Ni/Cu/Fe-Ni trilayers on Si (100)
We investigate the structural properties of Fe$_{1-x}$Ni$_x$/Cu/Fe$_{1-x}$Ni$_x$ ( $x=0.5$, non Invar and $x=0.36$, Invar) trilayers deposited on Si~(100)~at room temperature using dc magnetron sputtering technique in ultra high vacuum conditions taking high purity Fe, Ni and Cu metals with Cu layer thickness 4, 6 and 8 nm for each alloy composition. The structure of the alloy films of the trilayers was investigated using x-ray diffraction and the thickness \& roughness of the layers were obtained by x-ray reflectivity measurement. Both the as prepared and annealed trilayers exhibit layered structure. The as deposited Fe-Ni alloy in non Invar trilayer exhibits only fcc structure whereas in Invar alloy it exhibits a mixed fcc and bcc phases. Interestingly after annealing at 425$^0$C in ultra high vacuum, the Invar alloy completely transformed to fcc structure for all Cu thicknesses. In both Invar and non Invar trilayers, the Bragg reflections corresponding to Fe-Ni alloy layers become sharp after annealing. The induced structural transformation in Invar trilayer is explained using enhanced diffusion of Fe and Ni atoms at high temperatures.
2006.07662v1
2020-07-02
Free-standing 2D metals from binary metal alloys
Recent experiment demonstrated the formation of free-standing Au monolayers by exposing Au-Ag alloy to electron beam irradiation. Inspired by this discovery, we used semi-empirical effective medium theory simulations to investigate monolayer formation in 30 different binary metal alloys composed of late d-series metals Ni, Cu, Pd, Ag, Pt, and Au. In qualitative agreement with the experiment, we find that the beam energy required to dealloy Ag atoms from Au-Ag alloy is smaller than the energy required to break the dealloyed Au monolayer. Our simulations suggest that similar method could also be used to form Au monolayers from Au-Cu alloy and Pt monolayers from Pt-Cu, Pt-Ni, and Pt-Pd alloys.
2007.01291v1
2020-07-22
The origin of jerky dislocation motion in high-entropy alloys
Dislocations in single-phase concentrated random alloys, including high- entropy alloys (HEAs), repeatedly encounter pinning during glide, resulting in jerky dislocation motion. While solute-dislocation interaction is well understood in conventional alloys, the origin of individual pinning points in concentrated random alloys is a matter of debate. In this work, we investigate the origin of dislocation pinning in the CoCrFeMnNi HEA. In- situ transmission electron microscopy studies reveal wavy dislocation lines and a jagged glide motion under external loading, even though no segregation or clustering is found around Shockley partial dislocations. Atomistic simulations reproduce the jerky dislocation motion and link the repeated pinning to local fluctuations in the Peierls friction. We demonstrate that the density of high local Peierls friction is proportional to the critical stress required for dislocation glide and the dislocation mobility.
2007.11489v3
2020-07-22
An atomistic description of alloys and core shells nanoparticles
Using the extended discrete interaction model we investigate the tuneabilty of surface plasmon resonance in alloys and core-shell nanoparticles made from silver and gold. We show that the surface plasmon resonance of these alloys and core-shell particles to a large extent follow Vegard's law irrespective of the geometry of the nanoparticle. We show the evolution of the polarizability with size and demonstrate the highly non-linear behaviour of the polarizability with the ratio of the constituents and geometry in alloys and core-shell nanoparticles, with the exception for nanorod alloys. A thorough statistical investigation reveals that there is only a small dependence of the surface plasmon resonance on atomic arrangement and exact distribution in a nanoparticle and that the standard deviation decrease rapidly with the size of the nanoparticles. The physical reasoning for the random distribution algorithm for alloys in discrete interaction models is explained in details and verified by the statistical analysis.
2007.11688v1
2020-09-15
Alloy Engineering of Polar (Si,Ge)2N2O System for Controllable Second Harmonic Performance
Although silicon oxynitrides are important semiconductors for many practical applications, their potential second-order nonlinear optical (NLO) applications, regardless of balanced or controllable performance, have never been systemically explored. Using the first-principles calculations, in this article, we discover that the sinoite (i.e., typical silicon oxynitride Si2N2O) can simultaneously exhibit wide optical bandgap, strong second-harmonic generation (SHG) effect, and large birefringence, which are further confirmed by our preliminary experimental data. Importantly, we propose that alloying engineering can be further applied to control the balanced NLO properties in the Si2N2O system. Combining first-principles calculations and cluster expansion theory, we demonstrate that alloying Ge into Si2N2O can easily form low formation energy Si2(1-x)Ge2xN2O alloys, which can in turn achieve controllable phase-matching harmonic output with high SHG efficiency at different energy ranges. Therefore, alloy engineering could provide a unique approach to effectively control the balanced NLO performance of Si2(1-x)Ge2xN2O, making this polar alloy system holding potential applications in tunable laser frequency conversion and controllable all-optical devices.
2009.06932v2
2020-10-29
Plasma frequency in doped highly mismatched alloys
Highly mismatched alloys (HMAs) have band structures strongly modified due to the introduction of the alloying element. We consider HMAs where the isolated state of the alloying element is near the host conduction band, which causes the conduction band to split into two bands. We determine the bulk plasma frequency when the lower-energy band is partially occupied, as by doping, using a semi-analytical method based on a disorder-averaged Green's function. We include the nontrivial effects of interband transitions to the higher-energy band, which limit the plasma frequency to be less than an effective band gap. We show that the distribution of states in the split bands causes plasmons in HMAs to behave differently than plasmons in standard metals and semiconductors. The effective mass of the lower split band $m^*$ changes with alloy fraction, and we find that the plasmon frequency with small carrier concentration $n$ scales with $\sqrt{n}/m^*$ rather than the $\sqrt{n/m^*}$ that is expected in standard materials. We suggest experiments to observe these phenomena. Considering the typical range of material parameters in this group of alloys and taking a realistic example, we suggest that HMAs can serve as highly tunable low-frequency plasmonic materials.
2010.15953v1
2020-12-01
The Benefits of Trace Cu in Wrought Al-Mg Alloys
The softening and strengthening contributions in pre-deformed and aged Al-Mg-Cu alloys containing 3wt.%Mg and 0.5wt.%Cu are evaluated by a combination of microscopy, mechanical testing and modelling. A refined phenomenological model for the work hardening response, accounting for the separate effects of recovery and precipitation, is shown to be suitable for an unambiguous determination of the precipitation hardening contribution in these alloys. Significantly, it is found that the mechanical response of these alloys is not strongly impacted by Cu content (in the low Cu content regime), pre-deformation level or aging temperature meaning that the alloys are robust with respect to variations in composition. This is interesting from the perspective of alloy design concepts based on `recycling friendly' compositions in applications that include paint-baking.
2012.00277v1
2021-01-14
Neural-networks model for force prediction in multi-principal-element alloys
Atomistic simulations can provide useful insights into the physical properties of multi-principal-element alloys. However, classical potentials mostly fail to capture key quantum (electronic-structure) effects. We present a deep 3D convolutional neural network (3D CNN) based framework combined with a voxelization technique to design interatomic potentials for chemically complex alloys. We highlight the performance of the 3D CNN model and its efficacy in computing potentials using the medium-entropy alloy TaNbMo. In order to provide insights into the effect of voxel resolution, we implemented two approaches based on the inner and outer bounding boxes. An efficient 3D CNN model, which is as accurate as the density-functional theory (DFT) approach, for calculating potentials will provide a promising schema for accurate atomistic simulations of structure and dynamics of general multi-principle element alloys.
2101.05867v2
2021-01-29
Surface lattice Green's functions for high-entropy alloys
We study the surface elastic response of pure Ni, the random alloy FeNiCr and an average FeNiCr alloy in terms of the surface lattice Green's function. We propose a scheme for computing per-site Green's function and study their per-site variations. The average FeNiCr alloy accurately reproduces the mean Green's function of the full random alloy. Variation around this mean is largest near the edge of the surface Brillouin-zone and decays as $q^{-2}$ with wavevector $q$ towards the $\Gamma$-point. We also present expressions for the continuum surface Green's function of anisotropic solids of finite and infinite thickness and show that the atomistic Green's function approaches continuum near the $\Gamma$-point. Our results are a first step towards efficient contact calculations and Peierls-Nabarro type models for dislocations in high-entropy alloys.
2101.12519v1
2021-02-26
Data Analytics Approach to Predict High-Temperature Cyclic Oxidation Kinetics of NiCr-based Alloys
Although of practical importance, there is no established modeling framework to accurately predict high-temperature cyclic oxidation kinetics of multi-component alloys due to the inherent complexity. We present a data analytics approach to predict the oxidation rate constant of NiCr-based alloys as a function of composition and temperature with a highly consistent and well-curated experimental dataset. Two characteristic oxidation models, i.e., a simple parabolic law and a statistical cyclic-oxidation model, have been chosen to numerically represent the high-temperature oxidation kinetics of commercial and model NiCr-based alloys. We have successfully trained machine learning (ML) models using highly ranked key input features identified by correlation analysis to accurately predict experimental parabolic rate constants (kp). This study demonstrates the potential of ML approaches to predict oxidation kinetics of alloys over a wide composition and temperature ranges. This approach can also serve as a basis for introducing more physically meaningful ML input features to predict the comprehensive cyclic oxidation behavior of multi-component high-temperature alloys with proper constraints based on the known underlying mechanisms.
2102.13261v1
2021-04-12
CALPHAD-informed phase-field modeling of grain boundary microchemistry and precipitation in Al-Zn-Mg-Cu alloys
The grain boundary (GB) microchemistry and precipitation behaviour in high-strength Al-Zn-Mg-Cu alloys has an important influence on their mechanical and electrochemical properties. Simulation of the GB segregation, precipitation, and solute distribution in these alloys requires an accurate description of the thermodynamics and kinetics of this multi-component system. CALPHAD databases have been successfully developed for equilibrium thermodynamic calculations in complex multi-component systems, and in recent years have been combined with diffusion simulations. In this work, we have directly incorporated a CALPHAD database into a phase-field framework, to simulate, with high fidelity, the complex kinetics of the non-equilibrium GB microstructures that develop in these important commercial alloys during heat treatment. In particular, the influence of GB solute segregation, GB diffusion, precipitate number density, and far-field matrix composition, on the growth of a population of GB precipitates, was systematically investigated in a model Al-Zn-Mg-Cu alloy of near AA7050 composition. The simulation results were compared with scanning transmission electron microscopy and atom probe tomography characterisation of alloys of the similar composition, with good agreement.
2104.05791v1
2021-04-15
Optimization of High Entropy Alloy Catalyst for Ammonia Decomposition and Ammonia Synthesis
The successful synthesis of high entropy alloy (HEA) nanoparticles, a long-sought goal in materials science, opens a new frontier in materials science with applications across catalysis, electronics, structural alloys, and energetic materials. Recently, a Co25Mo45Fe10Ni10Cu10 HEA made of earth-abundant elements was shown to have a high catalytic activity for ammonia decomposition, which rivals that of state-of-the-art, but prohibitively expensive, ruthenium catalyst. Using a computational approach based on first-principles calculations in conjunction with data analytics and machine learning, we build a model to rapidly compute the adsorption energy of H, N, and NHx (x=1,3) species on CoMoFeNiCu alloy surfaces with varied alloy compositions and atomic arrangement. We show that the 25/45 Co/Mo ratio identified experimentally as the most active composition for ammonia decomposition increases the likelihood that the surface adsorbs nitrogen equivalently to that of ruthenium while at the same time interacting moderately strongly with intermediates. Our study underscores the importance of computational modeling and machine learning to identify and optimize HEA alloys across their near-infinite materials design space.
2104.07827v2
2021-05-06
Low temperature annealing method for fabricating alloy nanostructures and metasurfaces: Unlocking a novel degree of freedom
The material and exact shape of a nanostructure determine its optical response, which is especially strong for plasmonic metals. Unfortunately, only a very few plasmonic metals are available, which limits the spectral range where these strong optical effects can be utilized. Alloying different plasmonic metals can overcome this limitation, at the expense of using a high temperature alloying process, which adversely destroys the nanostructure shape. Here, we develop a low temperature alloying process at only 300{\deg}C and fabricate Au-Ag nanostructures with a broad diversity of shapes, aspect ratios and stoichiometries. EDX and XPS analyses confirm the homogeneous alloying through the entire sample. Varying the alloy stoichiometry tunes the optical response of the nanostructure and controls spectral features such as Fano resonances. Binary metasurfaces that combine nanostructures with different stoichiometries are fabricated using multiple-step electron beam lithography, and their optical function as hologram or Fresnel zone plate is demonstrated at the visible wavelength of 532 nm. This low temperature annealing technique provides a versatile and cost-effective way of fabricating complex Au-Ag nanostructures with arbitrary stoichiometry.
2105.02461v1
2021-05-11
Exploring the Correlation between Solvent Diffusion and Creep Resistance of Mg-Ga HCP Alloys from High Throughput Liquid-Solid Diffusion Couple
The liquid-solid diffusion couple technique, supported by phenomenological analysis and nano-indentation tests, is proposed on account of the relatively low melting points of Mg to explore the diffusion mobility and creep deformation. The potential of this strategy is demonstrated in Mg-Ga hcp alloys where Ga solute (i.e. impurity) and Mg solvent diffusions in hcp Mg-Ga alloys were both unveiled. It was followed by mapping the compressive creep behavior via nanoindentation along the composition arrays within the same Mg-Ga couple sample. The compressive creep resistance of Mg-Ga hcp alloys increased with the Ga content, and this enhancement was similar to the one found in Mg-Zn alloys and superior to the one reported in Mg-Al alloys though Al is a slower impurity diffuser in hcp-Mg than Zn and Ga. Thereby, the solvent diffusion and its variation with the composition, rather than the solute diffusion, was suggested to govern the creep properties at high temperatures and low stresses.
2105.05096v1
2021-05-31
Aluminium Alloy Design and Discovery using Machine Learning
The traditional design and development of metallic alloys has taken a hill-climbing approach to date, with incremental advances. Throughout the last century, aluminium (Al) alloy design has been essentially empirical and iterative, based on lessons learned from in service use and human experience. Incremental alloy development is costly, slow, and doesn't fully harness the data that exists in the field of Al-alloy metallurgy. In the present work, an attempt has been made to utilise a data science approach to develop a machine learning (ML) model for Al-alloy design. An objective-optimisation process has also been developed, to exploit the ML model, for user experience and practical application. A successful model was developed and presented herein, along with the open-access software.
2105.14806v2
2021-06-23
First-principles study of the robust superconducting state of NbTi alloys under ultrahigh pressures
A recent experiment reported that robust superconductivity appears in NbTi alloys under ultrahigh pressures with an almost constant superconducting $T_c$ of ~19 K from 120 to 261.7 GPa [J. Guo et al., Adv. Mater. 31, 1807240 (2019)], which is very rare among the known superconductors. We investigate the origin of this novel superconducting behavior in NbTi alloys based on density functional theory and density functional perturbation theory calculations. Our results indicate that the pressure tends to transform NbTi alloys from a random phase to a uniformly ordered crystal phase, and the exotic robust superconductivity of NbTi alloys can still be understood in the framework of BCS theory. The Nb element in NbTi alloys plays a dominant role in the superconductivity at low pressure, while the NbTi crystal with an alternative and uniform Nb and Ti atomic arrangement may be responsible for the stable superconductivity under high pressures. The robust superconducting transition temperature of NbTi under ultrahigh pressure can be explained by a synergistic effect of the enhanced phonon frequency, the modestly reduced total electron-phonon coupling, and the pressure-dependent screened Coulomb repulsion.
2106.12371v1
2021-11-05
Towards Stacking Fault Energy Engineering in FCC High Entropy Alloys
Stacking Fault Energy (SFE) is an intrinsic alloy property that governs much of the plastic deformation mechanisms observed in fcc alloys. While SFE has been recognized for many years as a key intrinsic mechanical property, its inference via experimental observations or prediction using, for example, computationally intensive first-principles methods is challenging. This difficulty precludes the explicit use of SFE as an alloy design parameter. In this work, we combine DFT calculations (with necessary configurational averaging), machine-learning (ML) and physics-based models to predict the SFE in the fcc CoCrFeMnNiV-Al high-entropy alloy space. The best-performing ML model is capable of accurately predicting the SFE of arbitrary compositions within this 7-element system. This efficient model along with a recently developed model to estimate intrinsic strength of fcc HEAs is used to explore the strength-SFE Pareto front, predicting new-candidate alloys with particularly interesting mechanical behavior.
2111.03591v1
2022-01-20
Coexistence of two types of short-range order in SiGeSn medium-entropy alloys
Short-range chemical order (SRO) has been recently demonstrated to play a decisive role in modulating a wide range of physical properties in medium-entropy alloy (MEA) and high-entropy alloy (HEA). The enormous configurational space of these alloys implies multiple forms of SRO are likely to develop concurrently but such structural diversity has not been reported. Here we show, through extensive {\em ab initio}-based sampling study, that SiGeSn medium-entropy alloys spontaneously develop two distinct forms of SRO. Remarkably, the two types of SROs, which carry different energies, distinct degrees of local ordering, and dissimilar electronic structures, are found to co-exist in a wide range of compositions of SiGeSn alloys. The co-existence of two SROs is rationalized through their virtual degeneracy of thermodynamic stability, due to the subtle balance in the change of enthalpy and configurational entropy upon the transformation between the two SROs. Such co-existence of SROs thus suggests an inherent structural heterogeneity, a diffuse electronic structure, and a new route for band engineering in SiGeSn MEA. More generally, our finding indicates the possible ubiquity of the co-existence of multiple forms of SRO in a broad range of MEAs and HEAs, which has profound implications on their diverse physical properties.
2201.08256v1
2022-08-24
Low-temperature ordering in a substitutional alloy with injecting nonequilibrium vacancies: The FePt case
Achieving the compositionally ordered state in a substitutional alloy of two or more species can often be even critical for improving its functional properties. To produce a highly ordered alloy, a longtime high-temperature (up to T=1000 K) treatment of the alloy is typically necessary because of insufficient vacancy concentration (c_v) and their mobility. However, such processing affects the morphology and complicates the technology of functional alloys. We show theoretically that the ordering in the practically important FePt system (Fe_xPt_1-x with x being close to 0.5) is already achievable at T=450 K for reasonable times t<10^3 s due to frozen nonequilibrium vacancies. Our simulation is based on the Dienes equation for relaxation of the long-range order parameter (S), with taking additionally into account that the ordering kinetics in the alloy is mediated by vacancies. Importantly, the results of such simulation are in good agreement with previous experimental data on the ordering kinetics. We also find that nanosecond laser pulses can be employed to achieve a sufficient level of c_v=10^-5 for effective low-temperature ordering.
2208.11720v3
2022-10-07
Radiation-resistant aluminium alloy for space missions in the extreme environment of the solar system
Future human-based exploration of our solar system requires the invention of materials that can resist harsh environments. Age-hardenable aluminium alloys would be attractive candidates for structural components in long-distance spacecrafts, but their radiation resistance to solar energetic particles is insufficient. Common hardening phases dissolve and displacement damage occurs in the alloy matrix, which strongly degrades properties. Here we present an alloy where hardening is achieved by T-phase, featuring a giant unit cell and highly-negative enthalpy of formation. The phase shows record radiation survivability and can stabilize an ultrafine-grained structure upon temperature and radiation in the alloy, therby successfully preventing displacement damage to occur. Such concept can be considered ideal for the next-generation space materials and the design of radiation resistant alloy.
2210.03397v3
2022-12-31
Investigating representation schemes for surrogate modeling of High Entropy Alloys
The design of new High Entropy Alloys that can achieve exceptional mechanical properties is presently of great interest to the materials science community. However, due to the difficulty of designing these alloys using traditional methods, machine learning has recently emerged as an essential tool. Particularly, the screening of candidate alloy compositions using surrogate models has become a mainstay of materials design in recent years. Many of these models use the atomic fractions of the alloying elements as inputs. However, there are many possible representation schemes for encoding alloy compositions, including both unstructured and structured variants. As the input features play a critical role in determining surrogate model performance, we have systematically compared these representation schemes on the basis of their performance in single-task deep learning models and in transfer learning scenarios. The results from these tests indicate that compared to the unstructured and randomly ordered schemes, chemically meaningful arrangements of elements within spatial representation schemes generally lead to better models. However, we also observed that tree-based models using only the atomic fractions as input were able to outperform these models in transfer learning.
2301.00179v1
2023-03-08
Atomic Representations of Local and Global Chemistry in Complex Alloys
The exceptional properties observed in complex concentrated alloys (CCAs) arise from the interplay between crystalline order and chemical disorder at the atomic scale, complicating a unique determination of properties. In contrast to conventional alloys, CCA properties emerge as distributions due to varying local chemical environments and the specific scale of measurement. Currently there are few ways to quantitatively define, track, and compare local alloy compositions (versus a global label, i.e. equiatomic) contained in a CCA. Molecular dynamics is used here to build descriptive metrics that connect a global alloy composition to the diverse local alloy compositions that define it. A machine-learned interatomic potential for MoNbTaTi is developed and we use these metrics to investigate how property distributions change with excursions in global-local composition space. Short-range order is examined through the lens of local chemistry for the equiatomic composition, demonstrating stark changes in vacancy formation energy with local chemistry evolution.
2303.04311v3
2023-05-20
A Computational Approach for Mapping Electrochemical Activity of Multi-Principal Element Alloys
Multi principal element alloys (MPEAs) comprise a unique class of metal alloys. MPEAs have been demonstrated to possess several exceptional properties, including, as most relevant to the present study, a high corrosion resistance. In the context of MPEA design, the vast number of potential alloying elements and the staggering number of elemental combinations favours a computational alloy design approach. In order to computationally assess the prospective corrosion performance of MPEA, an approach was developed in this study. A density functional theory (DFT) based Monte Carlo method was used for the development of MPEA structure, with the AlCrTiV alloy used as a model. High-throughput DFT calculations were performed to create training datasets for surface activity towards different adsorbate species: O2-, Cl- and H+. Machine learning (ML) with combined representation was then utilised to predict the adsorption and vacancy energies as descriptors for surface activity. The capability of the combined computational methods of MC, DFT and ML, as a virtual electrochemical performance simulator for MPEAs was established and may be useful in exploring other MPEAs.
2305.12059v1
2023-06-29
Structure-Dynamics Relationship in Al-Mg-Si Liquid Alloys
Enhancing properties and performances of aluminium alloys by a control of their solidification is pivotal in automotive and aerospace industries. The fundamental role of the structure-diffusion relationship is investigated for Al-Mg-Si liquid alloys taken as a prototype of Al-6xxx. For this purpose, first principles-based molecular dynamics simulations were performed for various Si and Mg content for Al-rich compositions, including the binary alloy counterparts. Results indicate that Mg and/or Si in alloys create a more compact ordering around Al than in pure Al, lowering diffusion. Mg promotes icosahedral short-range order, while Si displays a preference towards cubic local ordering, impacting diffusion based on their respective content. It suggests a mechanism whereby an increase in Mg content generally lowers the diffusion of each species, whereas an increase in Si content enhances their diffusion, providing insights for future alloy design.
2306.17264v1
2023-12-07
Integrated Design of Aluminum-Containing High-entropy Refractory B2 Alloys with Synergy of High Strength and Ductility
Refractory high-entropy alloys, RHEAs, are promising high-temperature structural materials. Their large compositional space poses great design challenges for phase control and high strength-ductility synergy. The present research pioneers using integrated high-throughput machine learning with Monte Carlo simulations to effectively navigate phase-selection and mechanical-properties predictions, developing aluminum-containing RHEAs in single-phase ordered B2 alloys demonstrating both high strength and ductility. These aluminum-containing RHEAs achieve remarkable mechanical properties, including compressive yield strengths up to 1.6 GPa, fracture strains exceeding 50 percent, and significant high-temperature strength retention. They also demonstrate a tensile yield strength of 1.1 GPa with a tension ductility of 6.3 percent. Besides, we identify a valence-electron-count domain for alloy brittleness with the explanation from density-functional theory and provide crucial insights into elements' influence on atomic ordering and mechanical performance. The work sets forth a strategic blueprint for high-throughput alloy design and reveals fundamental principles that govern the mechanical properties of advanced structural alloys.
2312.04708v1
2024-01-30
Empirical tight-binding method for large-supercell simulations of disordered semiconductor alloys
We analyze and present applications of a recently proposed empirical tight-binding scheme for investigating the effects of alloy disorder on various electronic and optical properties of semiconductor alloys, such as the band gap variation, the localization of charge carriers, and the optical transitions. The results for a typical antimony-containing III-V alloy, GaAsSb, show that the new scheme greatly improves the accuracy in reproducing the experimental alloy band gaps compared to other widely used schemes. The atomistic nature of the empirical tight-binding approach paired with a reliable parameterization enables more detailed physical insights into the effects of disorder in alloyed materials.
2401.16951v1
2024-01-31
Investigation of Microstructure and Corrosion Resistance of Ti-Al-V Titanium Alloys Obtained by Spark Plasma Sintering
The research results of the microstructure and corrosion resistance of Ti and Ti-Al-V Russian industrial titanium alloys obtained by spark plasma sintering (SPS) are described. Investigations of the microstructure, phase composition, hardness, tensile strength, electrochemical corrosion resistance and hot salt corrosion of Ti-Al-V titanium alloy specimens were carried out. It was shown that the alloy specimens have a uniform highly dense microstructure and high hardness values. The studied alloys also have high resistance to electrochemical corrosion during tests in acidic aqueous solution causing the intergranular corrosion as well as high resistance to the hot salt corrosion. The assumption that the high hardness of the alloys as well as the differences in the corrosion resistance of the central and lateral parts of the specimens are due to the diffusion of carbon from the graphite mold into the specimen surface was suggested.
2401.17941v1
2024-02-09
Right or Wrong -- Understanding How Novice Users Write Software Models
Writing declarative models has numerous benefits, ranging from automated reasoning and correction of design-level properties before systems are built, to automated testing and debugging of their implementations after they are built. Alloy is a declarative modeling language that is well-suited for verifying system designs. A key strength of Alloy is its scenario-finding toolset, the Analyzer, which allows users to explore all valid scenarios that adhere to the model's constraints up to a user-provided scope. However, even with visualized scenarios, it is difficult to write correct Alloy models. To address this, a growing body of work explores different techniques for debugging Alloy models. In order to develop and evaluate these techniques in an effective manor, this paper presents an empirical study of over 97,000 models written by novice users trying to learn Alloy. We investigate how users write both correct and incorrect models in order to produce a comprehensive benchmark for future use as well as a series of observations to guide debugging and educational efforts for Alloy model development.
2402.06624v3
2024-02-29
Searching for magnetically hard monoborides (and finding a few): A first-principles investigation
New hard magnetic materials with zero or low rare earth content are in demand due to the high prices of the rare earth metals. Among the candidates for such materials, we consider MnB, FeB and their alloys, because previous experiments suggest that FeB has a relatively high magnetic hardness of about 0.83 at room temperature. Using first-principles calculations, we examine the full range of alloys from CrB, through MnB, FeB, to CoB. Furthrmore, we consider alloys of MnB and FeB with substitutions of 3$d$, 4$d$ and 5$d$ transition metals. For the above ninety compositions, we determine magnetic moment, magnetocrystalline anisotropy energy and magnetic hardness. For (Fe-Co)B alloys, the calculated values of magnetic hardness exceed five, which is an exceptionally high. While these values are inflated by the virtual crystal approximation used, we still expect actual magnetic hardnesses well above unity. Furthermore, we classify considered MnB alloys substituted with transition metals as magnetically soft or semi-hard and FeB alloys with Sc, Ti, V, Zr, Nb, Mo, Hf, Ta or W as magnetically hard (with magnetic hardness exceeding unity).
2403.00138v1
2024-03-25
Enhanced mobility of ternary InGaAs quantum wells through digital alloying
High In content InGaAs quantum wells (In $\geq$ 75%) are potentially useful for topological quantum computing and spintronics applications. In high mobility InGaAs quantum wells, alloy disorder scattering is a limiting factor. In this report, we demonstrate that by growing the InGaAs quantum wells as a digital alloy, or a short period superlattice, we can reduce the alloy disorder scattering within the quantum well and increase the peak 2 K electron mobility to 545,000 cm^2/V s, which is the highest reported mobility for high In content InGaAs quantum wells to the best of the authors' knowledge. Our results demonstrate that the digital alloy approach can be used to increase the mobility of quantum wells in random alloy ternary materials.
2403.17166v2
2024-03-31
First Principles Studies of Stacking Fault Energies in Ternary Magnesium Alloys
Magnesium (Mg) alloys have emerged as promising materials due to their low density and high strength-to-weight ratio, offering a wide range of applications across multiple industries. Nevertheless, the inherent brittleness of Mg alloys poses a significant hurdle, necessitating innovative approaches to enhance their mechanical performance. Among the various strategies, manipulating stacking fault energy (SFE) has been a key focus, although primarily within the realm of binary alloys. This study investigates SFE in Mg alloys, focusing on ternary compositions. Utilizing first-principles DFT calculations, we analyze solute interactions and their influence on SFE, particularly in Mg-Al-X and Mg-Zn-X configurations. Predictive models are developed for estimating SFE effects, revealing solute pairs that mimic rare earth elements and show potential for improved ductility. The findings contribute to fundamental insights into Mg alloy behavior, offering practical directions for designing advanced materials with superior mechanical properties.
2404.00564v1
2012-09-29
The effect of precipitation on strength and ductility in a Mg-Zn-Y alloy
The effect of pre-ageing deformation on the size and distribution of beta-prime precipitates and subsequently on the resulting strength and ductility have been measured in a Mg-3.0at.%Zn-0.5at.%Y alloy. The alloy was extruded and then subjected to a T8 heat treatment comprised of a solution-treatment, cold-work and artificial ageing. Extrusion was used to introduce texture, ensuring that deformation occurred via slip rather than twinning. Samples were subjected to controlled uniaxial deformation and then isothermally aged to peak hardness. Precipitate length, diameter and number density were measured and evaluated in terms of the strength and ductility of the alloy. The nucleation of the beta-prime precipitates in peak-aged condition without pre-ageing deformation (i.e.T6 treatment) was poor, with only 0.5% volume fraction, compared to approximately 3.5% in T6 treated binary Mg-3.0at.%Zn alloy. The microstructure of the Mg-Zn-Y alloy was less refined, with larger diameter precipitates and lower beta-prime number densities compared to a binary Mg-3.0at.%Zn alloy. Deformation to 5% plastic strain increased the volume fraction of beta-prime precipitates to approximately 2.3% and refined the beta-prime precipitate length and diameter. The combination of these effects increased the yield strength after isothermal ageing from 217MPa (0% cold-work) to 287 MPa (5% cold-work). The yield stress increased linearly with reciprocal interparticle spacing on the basal and prismatic planes and the alloy showed similar strengthening against basal slip to Mg-Zn. The elongation increased linearly with particle spacing. The ductility of Mg-Zn-Y alloys was similar to that of Mg-Zn for equivalently spaced particles.
1210.0079v1
2013-04-18
Alloying effect on the ideal tensile strength of ferromagnetic and paramagnetic bcc iron
Using \emph{ab initio} alloy theory formulated within the exact muffin-tin orbitals theory in combination with the coherent potential approximation, we investigate the ideal tensile strength (ITS) in the $[001]$ direction of bcc ferro-/ferrimagnetic (FFM) and paramagnetic (PM) Fe$_{1-x}M_{x}$ ($M=$ Al, V, Cr, Mn, Co, or Ni) random alloys. The ITS of ferromagnetic (FM) Fe is calculated to be $12.6$\,GPa, in agreement with available data, while the PM phase turns out to posses a significantly lower value of $0.7\,$GPa. Alloyed to the FM matrix, we predict that V, Cr, and Co increase the ITS of Fe, while Al and Ni decrease it. Manganese yields a weak non-monotonic alloying behavior. In comparison to FM Fe, the alloying effect of Al and Co to PM Fe is reversed and the relative magnitude of the ITS can be altered more strongly for any of the solutes. All considered binaries are intrinsically brittle and fail by cleavage of the $(001)$ planes under uniaxial tensile loading in both magnetic phases. We show that the previously established ITS model based on structural energy differences proves successful in the PM Fe-alloys but is of limited use in the case of the FFM Fe-based alloys. The different performance is attributed to the specific interplay between magnetism and volume change in response to uniaxial tension. We establish a strong correlation between the compositional effect on the ITS and the one on the shear elastic constant $C'$ for the PM alloys and briefly discuss the relation between hardenability and the ITS.
1304.5129v2
2020-11-12
Alloying behavior of wide band gap alkaline-earth chalcogenides
Alloying is a powerful tool for tuning materials that facilitates the targeted design of desirable properties for a variety of applications. In this work, we provide a comprehensive investigation of the synthetic accessibility and electronic properties of nine alkaline-earth chalcogenide anion alloys (CaS$_{1-x}$O$_x$, CaS$_{1-x}$Se$_x$, CaS$_{1-x}$Te$_x$, SrS$_{1-x}$O$_x$, SrS$_{1-x}$Se$_x$, SrS$_{1-x}$Te$_x$, MgS$_{1- x}$O$_x$, MgS$_{1-x}$Se$_x$, and MgS$_{1-x}$Te$_x$). We show that isostructural alloying within the rock salt structure is favored for all systems except MgS$_{1-x}$Te$_x$, which is predicted to be a heterostructural alloy between the rock salt and wurtzite structures. Alloys of S and Se are shown to be readily accessible for all cations with low miscibility critical temperatures, enabling continuous tuning of electronic properties across this composition space. Alloys of S and Te have higher critical temperatures but may be accessible through non-equilibrium synthesis strategies and are predicted here to have desirable electronic properties for optoelectronics with wide band gaps and lower effective masses than alloys of S and Se. Anion alloying in MgS$_{1-x}$Te$_x$ stabilizes the wurtzite structure across a significant fraction of composition space, which may make it of particular interest as a transparent conducting material due to its lower effective masses and a higher band gap than the rock salt structure. Zero-point corrected random phase approximation (RPA) energies were computed to resolve the small polymorph energy differences of the Mg compounds and are shown to be critical for accurately describing the thermodynamic properties of the corresponding alloys.
2011.06628v1
2023-08-15
Electronic and optical properties of boron containing GaN alloys: The role boron atom clustering
Boron (B) containing III-nitride materials, such as wurtzite (B,Ga)N alloys, have recently attracted significant interest to tailor the electronic and optical properties of optoelectronic devices operating in the visible and ultraviolet spectral range. However, the growth of high quality samples is challenging and B atom clustering is often observed in (B,Ga)N alloys. To date, fundamental understanding of the impact of such clustering on electronic and optical properties of these alloys is sparse. In this work we employ density functional theory (DFT) in the framework of the meta generalized gradient approximation (modified Becke Johnson (mBJ) functional) to provide insight into this question. We use mBJ DFT calculations, benchmarked against state-of-the-art hybrid functional DFT, on (B,Ga)N alloys in the experimentally relevant B content range of up to 7.4%. Our results reveal that B atom clustering can lead to a strong reduction in the bandgap of such an alloy, in contrast to alloy configurations where B atoms are not forming clusters, thus not sharing nitrogen (N) atoms. We find that the reduction in bandgap is linked mainly to carrier localization effects in the valence band, which stem from local strain and polarization field effects. However, our study also reveals that the alloy microstructure of a B atom cluster plays an important role: B atom chains along the wurtzite c-axis impact the electronic structure far less strongly when compared to a chain formed within the c-plane. This effect is again linked to local polarization field effects and the orbital character of the involved valence states in wurtzite BN and GaN. Overall, our calculations show that controlling the alloy microstructure of (B,Ga)N alloys is of central importance when it comes to utilizing these systems in future optoelectronic devices with improved efficiencies.
2308.07759v1
2002-09-11
Exchange bias in [Co2MnGe/Au],[Co2MnGe/Cr] and [Co2MnGe/Cu2MnAl] multilayers
We report structural and magnetic properties of multilayers composed of thin layers of the half metallic ferromagnetic Heusler compound Co2MnGe and layers of Au, Cr and the Heusler compound Cu2MnAl. The hysteresis loops measured at low temperatures reveal the existence of an exchange bias field HEB in all of these multilayers. For the [Co2MnGe/Au] multilayer system HEB is largest reaching up to 1 kOe at a temperature of 2 K. We characterize the exchange bias phenomenon in detail and show that it originates from a spin glass type of magnetic order for a thin interlayer at the interfaces. We discuss the results in the light of different models proposed for the explanation of the exchange bias effect.
0209259v1
2003-04-15
First-principles study of lattice instabilities in the ferromagnetic martensite Ni$_2$MnGa
The phonon dispersion relations and elastic constants for ferromagnetic Ni$_2$MnGa in the cubic and tetragonally distorted Heusler structures are computed using density-functional and density-functional perturbation theory within the spin-polarized generalized-gradient approximation. For $0.9<c/a<1.06$, the TA$_2$ tranverse acoustic branch along $[110]$ and symmetry-related directions displays a dynamical instability at a wavevector that depends on $c/a$. Through examination of the Fermi-surface nesting and electron-phonon coupling, this is identified as a Kohn anomaly. In the parent cubic phase the computed tetragonal shear elastic constant, C$^\prime$=(C$_{11}-$C$_{12}$)/2, is close to zero, indicating a marginal elastic instability towards a uniform tetragonal distortion. We conclude that the cubic Heusler structure is unstable against a family of energy-lowering distortions produced by the coupling between a uniform tetragonal distortion and the corresponding $[110]$ modulation. The computed relation between the $c/a$ ratio and the modulation wavevector is in excellent agreement with structural data on the premartensitic ($c/a$ = 1) and martensitic ($c/a$ = 0.94) phases of Ni$_2$MnGa.
0304349v1
2006-06-21
Magnetic anisotropies and magnetization reversal of the Co$_2$Cr$_{0.6}$Fe$_{0.4}$Al Heusler compound
Magnetic anisotropies and magnetization reversal properties of the epitaxial Heusler compound Co$_2$Cr$_{0.6}$Fe$_{0.4}$Al (CCFA) deposited on Fe and Cr buffer layers are studied. Both samples exhibit a growth-induced fourfold anisotropy, and magnetization reversal occurs through the formation of stripy domains or 90 degree domains. During rotational magnetometric scans the sample deposited on Cr exhibits about 2 degree sharp peaks in the angular dependence of the coercive field, which are oriented along the hard axis directions. These peaks are a consequence of the specific domain structure appearing in this particular measurement geometry. A corresponding feature in the sample deposited on Fe is not observed.
0606542v1
2006-12-01
Epitaxial Co2Cr0.6Fe0.4Al thin films and magnetic tunneling junctions
Epitaxial thin films of the theoretically predicted half metal Co2Cr0.6Fe0.4Al were deposited by dc magnetron sputtering on different substrates and buffer layers. The samples were characterized by x-ray and electron beam diffraction (RHEED) demonstrating the B2 order of the Heusler compound with only a small partition of disorder on the Co sites. Magnetic tunneling junctions with Co2Cr0.6Fe0.4Al electrode, AlOx barrier and Co counter electrode were prepared. From the Julliere model a spin polarisation of Co2Cr0.6Fe0.4Al of 54% at T=4K is deduced. The relation between the annealing temperature of the Heusler electrodes and the magnitude of the tunneling magnetoresistance effect was investigated and the results are discussed in the framework of morphology and surface order based of in situ STM and RHEED investigations.
0612022v1
1994-11-21
A Mass Bound for Spherically Symmetric Black Hole Spacetimes
Requiring that the matter fields are subject to the dominant energy condition, we establish the lower bound $(4\pi)^{-1} \kappa {\cal A}$ for the total mass $M$ of a static, spherically symmetric black hole spacetime. (${\cal A}$ and $\kappa$ denote the area and the surface gravity of the horizon, respectively.) Together with the fact that the Komar integral provides a simple relation between $M - (4\pi)^{-1} \kappa A$ and the strong energy condition, this enables us to prove that the Schwarzschild metric represents the only static, spherically symmetric black hole solution of a selfgravitating matter model satisfying the dominant, but violating the strong energy condition for the timelike Killing field $K$ at every point, that is, $R(K,K) \leq 0$. Applying this result to scalar fields, we recover the fact that the only black hole configuration of the spherically symmetric Einstein-Higgs model with arbitrary non-negative potential is the Schwarzschild spacetime with constant Higgs field. In the presence of electromagnetic fields, we also derive a stronger bound for the total mass, involving the electromagnetic potentials and charges. Again, this estimate provides a simple tool to prove a ``no-hair'' theorem for matter fields violating the strong energy condition.
9411054v1