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2011-12-05
Chemical Composition Tuning of the Anomalous Hall Effect in Isoelectronic L10 FePd1-xPtx Alloy Films
The anomalous Hall effect (AHE) in L10 FePd1-xPtx alloy films is studied both experimentally and theoretically. We find that the intrinsic contribution (?sigma^int_AH) to the AHE can be significantly increased whereas the extrinsic side-jump contribution (sigma^?sj_AH) can be continuously reduced from being slightly larger than sigma^?int_AH in L10 FePd to being much smaller than sigma^?int_AH in L10 FePt, by increasing the Pt composition x. We show that this chemical composition tuning of the intrinsic contribution is afforded by the stronger spin-orbit coupling strength on the Pd/Pt site when the lighter Pd atoms are replaced by the heavier Pt atoms. Our results provide a means of manipulating the competing AHE mechanisms in ferromagnetic alloys for fuller understanding the AHE and also for technological applications of ferromagnetic alloys.
1112.0834v2
2012-01-03
CHUF and `unfreezing' (or de-arrest) of kinetic arrest in magnetic shape memory alloys
CHUF (cooling and heating in unequal field) protocol allows establishing phase coexistence through macroscopic measurements and enables distinguishing the metastable and stable phases (amongst the coexisting phase fractions across a first order magnetic transition) of a glass-like arrested state (GLAS). The observation of kinetic arrest in magnetic shape memory alloys has become a very active area of research. We highlight recent CHUF measurements on these materials that show behaviour similar to that reported earlier in manganites and other intermetallic alloys, emphasizing the generality. The martensitic transition provides an opportunity to study various properties as the CHUF protocol enables tuning of phase fractions, and controlled devitrification, of GLAS.
1201.0575v1
2012-01-13
Towards predictive modelling of near-edge structures in electron energy loss spectra of AlN based ternary alloys
Although electron energy loss near edge structure analysis provides a tool for experimentally probing unoccupied density of states, a detailed comparison with simulations is necessary in order to understand the origin of individual peaks. This paper presents a density functional theory based technique for predicting the N K-edge for ternary (quasi-binary) nitrogen alloys by adopting a core hole approach, a methodology that has been successful for binary nitride compounds. It is demonstrated that using the spectra of binary compounds for optimising the core hole charge ($0.35\,\mathrm{e}$ for cubic Ti$_{1-x}$Al$_x$N and $0.45\,\mathrm{e}$ for wurtzite Al$_x$Ga$_{1-x}$N), the predicted spectra evolutions of the ternary alloys agree well with the experiments. The spectral features are subsequently discussed in terms of the electronic structure and bonding of the alloys.
1201.2842v1
2012-01-20
Magnetic origin of chemical balance in alloyed Fe-Cr stainless steels: first-principles and Ising model study
Iron-chromium forms the basis of most of the stainless steel grades in the markets. Recently new insights into the physical and chemical properties of Fe-Cr based alloys have been obtained. Some of the new results are quite unexpected and call for further investigations. The present study addresses the magnetic contribution in the atomic driving forces behind the chemical composition in Fe-Cr alloyed with Al, Ti, V, Mn, Co, Ni, and Mo. Using the ab initio exact muffin-tin orbitals method and an Ising-type spin model, it is found that the magnetic moment of the solute atom combined with the induced changes in the magnetic moments of the host atoms form the main framework in determining the mixing energy and chemical potentials of low-Cr Fe-Cr based alloys. The results obtained in the present work are related to tuning of the microstructure and corrosion protection of low-Cr steels.
1201.4336v1
2012-01-29
Statistical Derivation of Basic Equations of Diffusional Kinetics in Alloys with Application to the Description of Diffusion of Carbon in Austenite
Basic equations of diffusional kinetics in alloys are statistically derived using the master equation approach. To describe diffusional transformations in substitution alloys, we derive the "quasi-equilibrium" kinetic equation which generalizes its earlier versions by taking into account possible "interaction renormalization" effects. For the interstitial alloys Me-X, we derive the explicit expression for the diffusivity D of an interstitial atom X which notably differs from those used in previous phenomenological treatments. This microscopic expression for D is applied to describe the diffusion of carbon in austenite basing on some simple models of carbon-carbon interaction. The results obtained enable us to make certain conclusions about the real form of these interactions, and about the scale of the "transition state entropy" for diffusion of carbon in austenite.
1201.6056v1
2012-02-29
Magneto-transport in a binary alloy ring
Magneto-transport properties are investigated in a binary alloy ring subjected to an Aharonov-Bohm (AB) flux \phi within a single-band non-interacting tight-binding framework. In the first part, we expose analytically the behavior of persistent current in an isolated ordered binary alloy ring as functions of electron concentration N_e and AB flux \phi. While, in the second part of the article, we discuss electron transport properties through a binary alloy ring attached to two semi-infinite one-dimensional metallic electrodes. The effect of impurities is also analyzed. From our study we propose that under suitable choices of the parameter values the system can act as a p-type or an n-type semiconductor.
1202.6519v3
2012-03-21
Structural and electronic properties of Pb1-xCdxTe and Pb1-xMnxTe ternary alloys
A systematic theoretical study of two PbTe-based ternary alloys, Pb1-xCdxTe and Pb1-xMnxTe, is reported. First, using ab initio methods we study the stability of the crystal structure of CdTe - PbTe solid solutions, to predict the composition for which rock-salt structure of PbTe changes into zinc-blende structure of CdTe. The dependence of the lattice parameter on Cd (Mn) content x in the mixed crystals is studied by the same methods. The obtained decrease of the lattice constant with x agrees with what is observed in both alloys. The band structures of PbTe-based ternary compounds are calculated within a tight-binding approach. To describe correctly the constituent materials new tight-binding parameterizations for PbTe and MnTe bulk crystals as well as a tight-binding description of rock-salt CdTe are proposed. For both studied ternary alloys, the calculated band gap in the L point increases with x, in qualitative agreement with photoluminescence measurements in the infrared. The results show also that in p-type Pb1-xCdxTe and Pb1-xMnxTe mixed crystals an enhancement of thermoelectrical power can be expected.
1203.4763v1
2012-04-17
Orientation relationships between icosahedral clusters in hexagonal MgZn2 and monoclinic Mg4Zn7 phases in Mg-Zn(-Y) alloys
Intermetallic precipitates formed in heat-treated and aged Mg-Zn and Mg-Zn-Y alloys have been investigated via electron microscopy. Coarse spheroidal precipitates formed on deformation twin boundaries contained domains belonging to either the MgZn2 hexagonal Laves phase or the monoclinic Mg4Zn7 phase. Both phases are structurally related to the quasi-crystalline phase formed in Mg-Zn-Y alloys, containing icosahedrally coordinated zinc atoms arranged as a series of broad rhombohedral units. This rhombohedral arrangement was also visible in intragranular precipitates where local regions with the structures of hexagonal MgZn2 and Mg4Zn7 were found. The orientation adopted by the MgZn2 and Mg4Zn7 phases in twin-boundary and intragranular precipitates was such that the icosahedral clusters were aligned similarly. These results highlight the close structural similarities between the precipitates of the Mg-Zn-Y alloy system.
1204.3708v1
2012-08-21
Theory of the electronic structure of dilute bismide and bismide-nitride alloys of GaAs: Tight-binding and k.p models
The addition of dilute concentrations of bismuth (Bi) into GaAs to form GaBiAs alloys results in a large reduction of the band gap energy Eg accompanied by a significant increase of the spin-orbit-splitting energy (delta_SO), leading to an Eg < delta_SO regime for ~10% Bi composition which is technologically relevant for the design of highly efficient photonic devices. The quaternary alloy GaBiNAs offers further flexibility for band gap tuning, because both nitrogen and bismuth can independently induce band gap reduction. This work reports sp3s* tight binding and 14-band k.p models for the study of the electronic structure of GaBiAs and GaBiNAs alloys. Our results are in good agreement with the available experimental data.
1208.4296v1
2012-10-11
Contributions of point defects, chemical disorder, and thermal vibrations to electronic properties of Cd(1-x)Zn(x)Te alloys
We present a first principles study based on density functional theory of thermodynamic and electronic properties of the most important intrinsic defects in the semiconductor alloy Cd(1-x)Zn(x)Te with x<0.13. The alloy is represented by a set of supercells with disorder on the Cd/Zn sublattice. Defect formation energies as well as electronic and optical transition levels are analyzed as a function of composition. We show that defect formation energies increase with Zn content with the exception of the neutral Te vacancy. This behavior is qualitatively similar to but quantitatively rather different from the effect of volumetric strain on defect properties in pure CdTe. Finally, the relative carrier scattering strengths of point defects, alloy disorder, and phonons are obtained. It is demonstrated that for realistic defect concentrations carrier mobilities are limited by phonon scattering for temperature above approximately 150 K.
1210.3305v1
2012-10-31
A Multi-Component Phase Field Crystal Model for Structural Transformations in Metal Alloys
We present a new phase field crystal model for structural transformations in multi-component alloys. The formalism builds upon the two-point correlation kernel developed in Greenwood et al. for describing structural transformations in pure materials [Phys. Rev. Lett. 105, 045702 (2010)]. We introduce an effective twopoint correlation function for multi-component alloys that uses the local species concentrations to interpolate between different crystal structures. A simplified version of the model is derived for the particular case of threecomponent (ternary) alloys, and its equilibrium properties are demonstrated. Dynamical equations of motion for the density and multiple species concentration fields are derived, and the robustness of the model is illustrated with examples of complex microstructure evolution in dendritic solidification and solid-state precipitation.
1211.0003v1
2012-11-21
Grain boundary segregation in UFG alloys processed by severe plastic deformation
Grain boundary segregations were investigated by Atom Probe Tomography in an Al-Mg alloy, a carbon steel and Armco\trademark Fe processed by severe plastic deformation (SPD). In the non-deformed state, the GBs of the aluminium alloy are Mg depleted, but after SPD some local enrichment up to 20 at.% was detected. In the Fe-based alloys, large carbon concentrations were also exhibited along GBs after SPD. These experimental observations are attributed to the specific structure of GBs often described as "non-equilibrum" in ultra fine grained materials processed by SPD. The grain boundary segregation mechanisms are discussed and compared in the case of substitutional (Mg in fcc Al) and interstitial (C in bcc Fe) solute atoms.
1211.5036v1
2012-11-29
Phase diagram, ferromagnetic martensitic transformation and magnetoresponsive properties of Fe-doped MnCoGe alloys
The crystal structure and magnetoresponsive properties of Fe-doped MnCoGe alloys have been investigated using x-ray diffraction (XRD) and magnetic measurements. By alloying the Fe-containing isostructure compounds into MnCoGe, a magnetostructural transition from paramagnetic austenite to ferromagnetic martensite with large magnetization difference can be realized in a temperature window between the Curie temperatures of the austenite and martensite, resulting in magnetic-field-induced martensitic transformations and large magnetic-entropy changes. A structural and magnetic phase diagram of Fe-doped MnCoGe alloys has been proposed.
1211.6815v1
2013-01-08
Deformation mechanisms in a TiNi shape memory alloy during cyclic loading
The deformation mechanisms governing the cyclic stress-strain behaviour of a TiNi shape memory alloy were investigated in this work. To understand the development of these mechanisms during cyclic loading, three low-cycle fatigue tests were performed and stopped at different stages. The first test was stopped after the first cycle; the second one was stopped after 40 cycles, corresponding to the beginning of the stabilisation of the cyclic strain-stress behaviour; and the last one was carried out to failure (3324 cycles). Submitted to fatigue loading, the response of the TiNi shape memory alloy presents a classical pseudoelastic response. Two deformation mechanisms, identified by TEM observations, are highlighted, the first one by twins and the second by dislocation slip and its interaction with precipitates. These two mechanisms evolve without competition during cyclic loading. The nanomechanical properties of the alloy were also examined, and the evolution of the microhardness or indentation modulus was monitored.
1301.1433v1
2013-01-21
Role of critical spin fluctuations in ultrafast demagnetization of transition-metal rare-earth alloys
Ultrafast magnetization dynamics induced by femtosecond laser pulses have been measured in ferrimagnetic Co0.8Gd0.2, Co.74Tb.26 and Co.86Tb.14 alloys. Using element sensitivity of X-ray magnetic circular dichroism at the Co L3, Tb M5 and Gd M5 edges we evidence that the demagnetization dynamics is element dependent. We show that a thermalization time as fast as 280 fs is observed for the rare-earth in the alloy, when the laser excited state temperature is below the compensation temperature. It is limited to 500 fs when the laser excited state temperature is below the Curie temperature (Tc). We propose critical spin fluctuations in the vicinity of TC as the mechanism which reduces the demagnetization rates of the 4f electrons in transition-metal rare-earth alloys whereas at any different temperature the limited demagnetization rates could be avoided.
1301.4885v3
2013-02-07
Tight-binding branch-point energies and band offsets for cubic InN, GaN, AlN and AlGaN alloys
Starting with empirical tight-binding band structures, the branch-point (BP) energies and resulting valence band offsets (VBOs) for the zincblende phase of InN, GaN and AlN are calculated from their k-averaged midgap energy. Furthermore, the directional dependence of the BPs of GaN and AlN is discussed using the Green's function method of Tersoff. We then show how to obtain the BPs for binary semiconductor alloys within a band-diagonal representation of the coherent potential approximation (CPA) and apply this method to cubic AlGaN alloys. The resulting band offsets show good agreement to available experimental and theoretical data from the literature. Our results can be used to determine the band alignment in isovalent heterostructures involving pure cubic III-nitrides or AlGaN alloys for arbitrary concentrations.
1302.1725v1
2013-02-10
Measurement of orbital asymmetry and strain in Co90Fe10/Ni multilayers and alloys: Origins of perpendicular anisotropy
We use broadband ferromagnetic resonance spectroscopy and x-ray diffraction to investigate the fundamental origin of perpendicular anisotropy in Co90Fe10/Ni multilayers. By careful evaluation of the spectroscopic g-factor, we determine the orbital moment along the out-of-plane and in-plane directions. For the multilayers, we find a direct relationship between the orbital moment asymmetry and the perpendicular anisotropy, consistent with the theory of Bruno [P.Bruno, Phys. Rev. B, 39, 865 (1989)]. A systematic x-ray diffraction study revealed the presence of a trigonal strain as high as 0.7 % in some samples. However, we found no direct correlation between the strain and the anisotropy, indicating that the anisotropy is not dominated by magnetoelastic effects. In order to further study the interface structure on the anisotropy, we prepared a set of equivalent alloy samples. The strain in the alloy samples was comparable to that of the multilayer samples; however the orbital moment asymmetry in the alloy samples showed a very different trend allowing us to isolate the effect of the interfaces in the multilayers.
1302.2366v1
2013-02-13
Ideal strength of random alloys from first-principles theory
The all-electron exact muffin-tin orbitals method in combination with the coherent-potential appproximation has been employed to investigate the ideal tensile strengths of elemental V, Mo solids and V- and Mo-based random solid solutions. The present ideal tensile strengths, calculated assuming isotropic Poisson contraction, are 16.1, 26.7 and 37.6 GPa for bcc V in the [001], [111] and [110] directions, respectively, and 26.7 GPa for bcc Mo in the [001] direction, which are all in good agreement with the available theoretical data. When a few percent Tc is introduced in Mo, it is found that the ideal strength decreases in the [001] direction. For the V-based alloys, Cr increases and Ti decreases the ideal tensile strength in all principal directions. Adding the same concentration of Cr and Ti to V leads to ternary alloys with similar ideal strength values as that of pure V. The alloying effects on the ideal strength is explained using the electronic band structure.
1302.3042v2
2013-02-23
Atomistic origin of doping-enhanced rapid crystallization in Ag-doped Ge-Sb-Te alloys: a joint experimental and theoretical study
We have applied extended X-ray absorption fine structure (EXAFS) analyses and ab-initio molecular dynamics (AIMD) simulations to study the atomic structure of Ag-doped (up to 42%) Ge1Sb2Te4 alloys. Analysis of the models that are consistent with the EXAFS experiment reveals that the Ge environment is significantly modified by Ag doping whereas those of Sb and Te are barely affected (except for high Ag concentrations), and suggests that Ag prefers bonding with Te to Ge or Sb. Doping with Ag promotes the conversion of tetrahedral Ge sites to octahedral Ge sites and enhances the speed of crystallization of Ge-Sb-Te (GST) alloys as evidenced directly from the MD simulations. Our study shed light on the atomistic mechanism of rapid crystallization of GST alloys enhanced by Ag doping.
1302.5757v3
2013-03-07
Studies of homogeneous precipitation in very dilute iron-coper alloys using kinetic Monte Carlo simulations and statistical theory of nucleation
Kinetics of homogeneous nucleation and growth of copper precipitates under electron irradiation of Fe_{1-x}Cu_x alloys at concentrations x from 0.06 at.% to 0.4 at.% and temperatures T from 290 to 450C is studied using the kinetic Monte Carlo (KMC) simulations and the statistical theory of nucleation (STN). The conventional assumption about the similarity of mechanisms of precipitation under electron irradiation and during thermal aging is adopted. The earlier-developed ab initio model of interactions in Fe-Cu alloys is used for both the KMC simulations and the STN calculations. Values of the nucleation barrier F_c and the prefactor J_0 in the Zeldovich-Volmer relation for the nucleation rate J are calculated for a number of concentrations and temperatures. For the dilute alloys with x less then 0.2%, the STN and the KMC results for the nucleation barrier F_c do virtually coincide with each other, which seems to confirm a high reliability of the STN for this problem. The STN calculations are also used to estimate the temperature dependencies of concentrations which correspond to the homogeneous or the heterogeneous precipitation limit and both dependencies are found to be rather sharp.
1303.1753v1
2013-03-14
Prediction of (TiO2)x(Cu2O)y Alloys for Photoelectrochemical Water Splitting
The formation of (TiO2)x(Cu2O)y solid-solutions are investigated using a global optimization evolutionary algorithm. First-principles calculations based on density functional theory are then used to gain insight into the electronic properties of these alloys. We find that: (i) Ti and Cu in (TiO2)x(Cu2O)y alloys have similar local environments as in bulk TiO2 and Cu2O except for (TiO2)(Cu2O) which has some trigonal-planar Cu ions. (ii) The predicted optical band gaps are around 2.1 eV (590 nm), thus having much better performance for the absorption of visible light compared with both binary oxides. (iii) (TiO2)2(Cu2O) has the lowest formation energy amongst all studied alloys and the positions of its band edges are found to be suitable for solar-driven water splitting applications.
1303.3355v1
2013-06-13
Investigation of the quaternary Fe2-xCoxMnSi alloys by structural, magnetic, resistivity and spin polarization measurements
Effects of the Co substitution have been observed on the structural, magnetic and magneto-transport properties of Fe2-xCoxMnSi alloy. Curie temperature (TC) and saturation magnetization (MS) of these alloys increased linearly with the Co substitution. Competitive magnetic interaction between ferromagnetic (FM) and anti-ferromagnetic (AFM) phases exists in Fe2-xCoxMnSi for x less than 0.2, AFM phase is completely disappears for x greater than or equal to 0.2. The value of Rhodes-Wohlfarth ratio pc/ps is greater than one for these alloys which is the characteristics of iterant magnetism present in the system. M\"ossbauer spectroscopic measurements have been done to investigate the atomic disorder and local magnetic moment for some x values. Resistivity measurements also confirm the stability of ferromagnetism with the concentration of Co and also show a sign of half metallicity. Resistivity shows semiconducting behaviour for x = 0.4 which is interesting in view of spin gapless semiconductors.
1306.3086v3
2013-08-31
Wegner estimate and localization for alloy-type models with sign-changing exponentially decaying single-site potentials
We study Schr\"odinger operators on $L^2 (\RR^d)$ and $\ell^2(\ZZ^d)$ with a random potential of alloy-type. The single-site potential is assumed to be exponentially decaying but not necessarily of fixed sign. In the continuum setting we require a generalized step-function shape. Wegner estimates are bounds on the average number of eigenvalues in an energy interval of finite box restrictions of these types of operators. In the described situation a Wegner estimate which is polynomial in the volume of the box and linear in the size of the energy interval holds. We apply the established Wegner estimate as an ingredient for a localization proof via multiscale analysis.
1309.0109v2
2014-01-16
Plasticity of Zr-Nb-Ti-Ta-Hf high-entropy alloys
We have investigated the plastic deformation properties of non-equiatomic single phase Zr-Nb-Ti-Ta-Hf high-entropy alloys from room temperature up to 300 {\deg}C. Uniaxial deformation tests at a constant strain rate of 10$^{-4}$ s$^{-1}$ were performed including incremental tests such as stress-relaxations, strain-rate- and temperature changes in order to determine the thermodynamic activation parameters of the deformation process. The microstructure of deformed samples was characterized by transmission electron microscopy. The strength of the investigated Zr-Nb-Ti-Ta-Hf phase is not as high as the values frequently reported for high-entropy alloys in other systems. We find an activation enthalpy of about 1 eV and a stress dependent activation volume between 0.5 and 2 nm$^3$. The measurement of the activation parameters at higher temperatures is affected by structural changes evolving in the material during plastic deformation.
1401.3997v1
2014-03-28
Discrete alloy-type models: Regularity of distributions and recent results
We consider discrete random Schr\"odinger operators on $\ell^2 (\mathbb{Z}^d)$ with a potential of discrete alloy-type structure. That is, the potential at lattice site $x \in \mathbb{Z}^d$ is given by a linear combination of independent identically distributed random variables, possibly with sign-changing coefficients. In a first part we show that the discrete alloy-type model is not uniformly $\tau$-H\"older continuous, a frequently used condition in the literature of Anderson-type models with general random potentials. In a second part we review recent results on regularity properties of spectral data and localization properties for the discrete alloy-type model.
1403.7329v2
2014-05-06
Formal Safety and Security Assessment of an Avionic Architecture with Alloy
We propose an approach based on Alloy to formally model and assess a system architecture with respect to safety and security requirements. We illustrate this approach by considering as a case study an avionic system developed by Thales, which provides guidance to aircraft. We show how to define in Alloy a metamodel of avionic architectures with a focus on failure propagations. We then express the specific architecture of the case study in Alloy. Finally, we express and check properties that refer to the robustness of the architecture to failures and attacks.
1405.1113v1
2014-05-09
Spin Spirals in Surface Alloys on Ru(0001): A First-principles Study
We have used ab initio density functional theory to compute the magnetic ground states of the surface alloy systems FeAu$_2$/Ru(0001) and MnAu$_2$/Ru(0001). For both systems, we find that the lowest energy magnetic configuration corresponds to a left-rotating spin spiral, in which the sense of rotation is determined by the Dzyaloshinskii-Moriya interaction. These spirals are lower in energy than the ferromagnetic configuration by 3-4 meV per nm$^2$. We also find that FeAu$_2$/Ru(0001) has a significantly high magnetic anisotropy energy, of the order 1 meV per Fe atom. By comparing with the corresponding freestanding alloy monolayers, we find that the presence of the Ru substrate plays a significant role in determining the magnetic properties of the surface alloy systems.
1405.2152v1
2014-05-28
Barocaloric and Magnetocaloric Effects in Fe49Rh51
We report on calorimetry under applied hydrostatic pressure and magnetic field at the antiferromagnetic (AFM)-ferromagnetic (FM) transition of Fe$_{49}$Rh$_{51}$. Results demonstrate the existence of a giant barocaloric effect in this alloy, a new functional property that adds to the magnetocaloric and elastocaloric effects previously reported for this alloy. All caloric effects originate from the AFM/FM transition which encompasses changes in volume, magnetization and entropy. The strong sensitivity of the transition temperatures to both hydrostatic pressure and magnetic field confers to this alloy outstanding values for the barocaloric and magnetocaloric strengths ($|\Delta S|$/$\Delta p$ $\sim$ 12 J kg$^{-1}$ K $^{-1}$ kbar$^{-1}$ and $|\Delta S|$/$\mu_0\Delta H$ $\sim$ 12 J kg$^{-1}$ K$^{-1}$ T$^{-1}$). Both barocaloric and magnetocaloric effects have been found to be reproducible upon pressure and magnetic field cycling. Such a good reproducibility and the large caloric strengths make Fe-Rh alloys particularly appealing for solid-state cooling technologies at weak external stimuli.
1405.7156v1
2014-07-07
Efficient determination of alloy ground-state structures
We propose an efficient approach to accurately finding the ground-state structures in alloys based on the cluster expansion method. In this approach, a small number of candidate ground-state structures are obtained without any information of the energy. To generate the candidates, we employ the convex hull constructed from the correlation functions of all possible structures by using an efficient algorithm. This approach is applicable to not only simple lattices but also complex lattices. Firstly, we evaluate the convex hulls for binary alloys with four types of simple lattice. Then we discuss the structures on the vertices. To examine the accuracy of this approach, we perform a set of density functional theory calculations and the cluster expansion for Ag-Au alloy and compare the formation energies of the vertex structures with those of all possible structures. As applications, the ground-state structures of the intermetallic compounds CuAu, CuAg, CuPd, AuAg, AuPd, AgPd, MoTa, MoW and TaW are similarly evaluated. Finally, the energy distribution is obtained for different cation arrangements in MgAl$_2$O$_4$ spinel, for which long-range interactions are essential for the accurate description of its energetics.
1407.1734v1
2014-07-08
Robustness against Disorder of Relativistic Spectral Properties in Chalcogenide Alloys
In order to carefully address the interplay between substitutional disorder and spin-orbit-coupling in IV-VI alloys, we propose a novel theoretical approach that integrates the reliability of plane-wave based density-functional theory beyond the local-density approximation with the Coherent Potential Approximation. By applying the proposed method to ternary chalcogenide alloys, we predict a substantial robustness of spectral features close to the Fermi energy against substitutional disorder. Supplementing our first-principles calculations with the analysis of the $k \cdot p$ model for rock-salt chalcogenides, we show that the disorder self-energy is vanishingly small close to the band gap, thus allowing for bulk Rashba-like spin splitting to be observed in ferroelectric alloys, such as PbS$_x$Te$_{1-x}$, and protecting the band-character inversion related to the topological transition in the recently discovered Topological Crystalline Insulator Pb$_{1-x}$Sn$_x$Te.
1407.2064v1
2014-09-08
CD2Alloy: Class Diagrams Analysis Using Alloy Revisited
We present CD2Alloy, a novel, powerful translation of UML class diagrams (CDs) to Alloy. Unlike existing translations, which are based on a shallow embedding strategy, and are thus limited to checking consistency and generating conforming object models of a single CD, and support a limited set of CD language features, CD2Alloy uses a deeper embedding strategy. Rather than mapping each CD construct to a semantically equivalent Alloy construct, CD2Alloy defines (some) CD constructs as new concepts within Alloy. This enables solving several analysis problems that involve more than one CD and could not be solved by earlier works, and supporting an extended list of CD language features. The ideas are implemented in a prototype Eclipse plug-in. The work advances the state-of-the-art in CD analysis, and can also be viewed as an interesting case study for the different possible translations of one modeling language to another, their strengths and weaknesses.
1409.2314v1
2014-09-22
Three dimensional thermal-solute phase field simulation of binary alloy solidification
We employ adaptive mesh refinement, implicit time stepping, a nonlinear multigrid solver and parallel computation, to solve a multi-scale, time dependent, three dimensional, nonlinear set of coupled partial differential equations for three scalar field variables. The mathematical model represents the non-isothermal solidification of a metal alloy into a melt substantially cooled below its freezing point at the microscale. Underlying physical molecular forces are captured at this scale by a specification of the energy field. The time rate of change of the temperature, alloy concentration and an order parameter to govern the state of the material (liquid or solid) is controlled by the diffusion parameters and variational derivatives of the energy functional. The physical problem is important to material scientists for the development of solid metal alloys and, hitherto, this fully coupled thermal problem has not been simulated in three dimensions, due to its computationally demanding nature. By bringing together state of the art numerical techniques this problem is now shown here to be tractable at appropriate resolution with relatively moderate computational resources.
1409.6213v1
2014-10-01
Coherent phonon study of (GeTe)$_{l}$(Sb$_{2}$Te$_{3}$)$_{m}$ interfacial phase change memory materials
The time-resolved reflectivity measurements were carried out on the interfacial phase change memory (iPCM) materials ([(GeTe)$_{2}$(Sb$_{2}$Te$_{3}$)$_{4}$]$_{8}$ and [(GeTe)$_{2}$(Sb$_{2}$Te$_{3}$)$_{1}$]$_{20}$) as well as conventional Ge$_{2}$Sb$_{2}$Te$_{5}$ alloy at room temperature and above the RESET-SET phase transition temperature. In the high-temperature phase, coherent phonons were clearly observed in the iPCM samples while drastic attenuation of coherent phonons was induced in the alloy. This difference strongly suggests the atomic rearrangement during the phase transition in iPCMs is much smaller than that in the alloy. These results are consistent with the unique phase transition model in which a quasi-one-dimensional displacement of Ge atoms occurs for iPCMs and a conventional amorphous-crystalline phase transition takes place for the alloy.
1410.0097v1
2014-10-27
Ti$_{1-x}$Au$_x$ Alloys: Hard Biocompatible Metals and Their Possible Applications
The search for new hard materials is often challenging from both theoretical and experimental points of view. Furthermore, using materials for biomedical applications calls for alloys with high biocompatibility which are even more sparse. The Ti$_{1-x}$Au$_x$ ($0.22 \leq x \leq 0.8$) exhibit extreme hardness and strength values, elevated melting temperatures (compared to those of constituent elements), reduced density compared to Au, high malleability, bulk metallicity, high biocompatibility, low wear, reduced friction, potentially high radio opacity, as well as osseointegration. All these properties render the Ti$_{1-x}$Au$_x$ alloys particularly useful for orthopedic, dental, and prosthetic applications, where they could be used as both permanent and temporary components. Additionally, the ability of Ti$_{1-x}$Au$_x$ alloys to adhere to ceramic parts could reduce the weight and cost of these components.
1410.7308v1
2014-11-15
Mixed-bond spin-1 Ising model with nonlinear interactions for the Fe-Mn alloys
In this letter, we apply the mixed-bond spin-1 Ising model to the study of the magnetic properties of Fe-Mn alloys in the $\alpha$ phase by employing the effective field theory (EFT). Here, we suggest a new approach to the ferromagnetic coupling between nearest neighbours Fe-Fe that depends on the ratio between the Mn-Mn coupling and Fe-Mn coupling and of second power of the Mn concentration $q$ in contrast with linear dependence proposed in the other papers. Also, we propose a new probability distribution for binary alloys with mixed-bonds based on the distribution for ternary alloys and we obtain a very good agreement for all considered values of $q$ in $T-q$ plane, in particular for $q>0.11$.
1411.4181v1
2014-11-19
Structural ${γ\textrm{-}\varepsilon}$ phase transition in Fe-Mn alloys from CPA+DMFT approach
We present a computational scheme for total energy calculations of disordered alloys with strong electronic correlations. It employs the coherent potential approximation combined with the dynamical mean-field theory and allows one to study the structural transformations. The material-specific Hamiltonians in the Wannier function basis are obtained by density functional theory. The proposed computational scheme is applied to study the ${\gamma\textrm{-}\varepsilon}$ structural transition in paramagnetic Fe-Mn alloys for Mn content from 10 to 20 at. %. The electronic correlations are found to play a crucial role in this transition. The calculated transition temperature decreases with increasing Mn content and is in a good agreement with experiment. We demonstrate that in contrast to the ${\alpha\textrm{-}\gamma}$ transition in pure iron, the ${\gamma\textrm{-}\varepsilon}$ transition in Fe-Mn alloys is driven by a combination of kinetic and Coulomb energies. The latter is found to be responsible for the decrease of the ${\gamma\textrm{-}\varepsilon}$ transition temperature with Mn content.
1411.5356v3
2014-12-02
The glass-forming ability of model metal-metalloid alloys
Bulk metallic glasses (BMGs) are amorphous alloys with desirable mechanical properties and processing capabilities. To date, the design of new BMGs has largely employed empirical rules and trial-and-error experimental approaches. Ab initio computational methods are currently prohibitively slow to be practically used in searching the vast space of possible atomic combinations for bulk glass formers. Here, we perform molecular dynamics simulations of a coarse-grained, anisotropic potential, which mimics interatomic covalent bonding, to measure the critical cooling rates for metal-metalloid alloys as a function of the atomic size ratio $\sigma_S/\sigma_L$ and number fraction $x_S$ of the metalloid species. We show that the regime in the space of $\sigma_S/\sigma_L$ and $x_S$ where well-mixed, optimal glass formers occur for patchy and LJ particle mixtures coincides with that for experimentally observed metal-metalloid glass formers. Our simple computational model provides the capability to perform combinatorial searches to identify novel glass-forming alloys.
1412.0766v1
2015-01-22
Atomistic analysis of the impact of alloy and well-width fluctuations on the electronic and optical properties of InGaN/GaN quantum wells
We present an atomistic description of the electronic and optical properties of $\text{In}_{0.25}\text{Ga}_{0.75}$N/GaN quantum wells. Our analysis accounts for fluctuations of well width, local alloy composition, strain and built-in field fluctuations as well as Coulomb effects. We find a strong hole and much weaker electron wave function localization in InGaN random alloy quantum wells. The presented calculations show that while the electron states are mainly localized by well-width fluctuations, the holes states are already localized by random alloy fluctuations. These localization effects affect significantly the quantum well optical properties,leading to strong inhomogeneous broadening of the lowest interband transition energy. Our results are compared with experimental literature data.
1501.05482v1
2015-04-01
Multiscale modeling of ultrafast element-specific magnetization dynamics of ferromagnetic alloys
A hierarchical multiscale approach to model the magnetization dynamics of ferromagnetic ran- dom alloys is presented. First-principles calculations of the Heisenberg exchange integrals are linked to atomistic spin models based upon the stochastic Landau-Lifshitz-Gilbert (LLG) equation to calculate temperature-dependent parameters (e.g., effective exchange interactions, damping param- eters). These parameters are subsequently used in the Landau-Lifshitz-Bloch (LLB) model for multi-sublattice magnets to calculate numerically and analytically the ultrafast demagnetization times. The developed multiscale method is applied here to FeNi (permalloy) as well as to copper- doped FeNi alloys. We find that after an ultrafast heat pulse the Ni sublattice demagnetizes faster than the Fe sublattice for the here-studied FeNi-based alloys.
1504.00199v1
2015-04-05
Pathway to oxide photovoltaics via band-structure engineering of SnO
The prospects of scaling current photovoltaic technologies to terawatt levels remain uncertain. All-oxide photovoltaics could open rapidly scalable manufacturing routes, if only oxide materials with suitable electronic and optical properties were developed. A potential candidate material is tin monoxide (SnO), which has exceptional doping and transport properties among oxides, but suffers from a low adsorption coefficient due to its strongly indirect band gap. Here, we address this shortcoming of SnO by band-structure engineering through isovalent but heterostructural alloying with divalent cations (Mg, Ca, Sr, Zn). Using first-principles calculations, we show that suitable band gaps and optical properties close to that of direct-gap semiconductors are achievable in such SnO based alloys. Due to the defect tolerant electronic structure of SnO, the dispersive band-structure features and comparatively small effective masses are preserved in the alloys. Initial Sn1-xZnxO thin films deposited by sputtering exhibit crystal structure and optical properties in accord with the theoretical predictions, which confirms the feasibility of the alloying approach. Thus, the implications of this work are important not only for terawatt scale photovoltaics, but also for other large-scale energy technologies where defect-tolerant semiconductors with high quality electronic properties are required.
1504.01168v2
2015-05-21
Compositional bowing of band energies and their deformation potentials in strained InGaAs ternary alloys: a first-principles study
Using first-principles calculations, we show that the conduction and valence band energies and their deformation potentials exhibit a non-negligible compositional bowing in strained ternary semiconductor alloys such as InGaAs. The electronic structure of these compounds has been calculated within the framework of local density approximation and hybrid functional approach for large cubic supercells and special quasi-random structures, which represent two kinds of model structures for random alloys. We find that the predicted bowing effect for the band energy deformation potentials is rather insensitive to the choice of the functional and alloy structural model. The direction of bowing is determined by In cations that give a stronger contribution to the formation of the In$_{x}$Ga$_{1-x}$As valence band states with $x\gtrsim 0.5$, compared to Ga cations.
1505.05659v2
2015-08-10
Electronic structure and spin polarization of Fe$_{1-x}$Mn(Co,Ni)$_x$S$_2$ alloys from first principles
Alloying effects by T=Mn,Co,Ni-substitution on FeS$_2$ have been investigated using density-functional calculations. The ferromagnetic alloys Fe$_{1-x}$T$_x$S$_2$ have been investigated for concentrations $x=\frac{1}{4},\frac{1}{2},\frac{3}{4}$ together with the ground states of the pure compounds. The electronic structure is discussed with the goal to identify candidates for half metals, which are of interest for spintronics applications. We find interesting candidates at high concentration of the Mn-doped FeS$_2$ and at low concentrations for Ni-doped materials. For the Mn alloys we also note the proximity to a low-spin to high spin transition. For Co-doped materials we reproduce the well known finding of half metallicity over the entire concentration range.
1508.02191v2
2015-08-18
Effects of temperature gradient on the interface microstructure and diffusion of diffusion couples: phase-field simulation
The temporal interface microstructure and diffusion in the diffusion couples with the mutual interactions of temperature gradient, concentration difference and initial aging time of the alloys were studied by phase-field simulation, the diffusion couples are produced by the initial aged spinodal alloys with different compositions. Temporal composition evolution and volume fraction of the separated phase indicates the element diffusion direction through the interface under the temperature gradient. The increased temperature gradient induces a wide single-phase region at two sides of the interface. The uphill diffusion proceeds through the interface, no matter the diffusion directions are up or down to the temperature gradient. For an alloy with short initial aging time, phase transformation accompanying the interdiffusion results in the straight interface with the single-phase regions at both sides. Comparing with the temperature gradient, composition difference of diffusion couple and initial aging time of the alloy show greater effect on the diffusion and interface microstructure.
1508.04367v1
2015-09-15
Temperature and composition dependence of the band gaps of Ga$_{1-x}$In$_x$N alloy: a first-principles study based on the virtual crystal approximation
We report on the structural, electronic and vibrational properties of the Ga$_{1-x}$In$_x$N alloy using virtual crystal approximation (VCA) from first-principles. A band gap bowing parameter of 3.85 eV is obtained with the TB09 functional. Phonon density of states shifts to lower frequency as the In content is increased. However, VCA ignores disorder effect and is therefore unable to describe the broadening of the phonon spectra upon alloying. The role of electron-phonon interaction in the temperature dependence of the band gap is also studied for GaN, InN and their alloy Ga$_{1-x}$In$_x$N. The calculated zero-point motion renormalization and the fitted Varshni parameter over the entire composition range are discussed.
1509.04735v1
2015-10-03
Strong Suppression of the Spin Hall Effect in the Spin Glass State
We have measured spin Hall effects in spin glass metals, CuMnBi alloys, with the spin absorption method in the lateral spin valve structure. Far above the spin glass temperature Tg where the magnetic moments of Mn impurities are randomly frozen, the spin Hall angle of CuMnBi ternary alloy is as large as that of CuBi binary alloy. Surprisingly, however, it starts to decrease at about 4Tg and becomes as little as 7 times smaller at 0.5Tg. A similar tendency was also observed in anomalous Hall effects in the ternary alloys. We propose an explanation in terms of a simple model considering the relative dynamics between the localized moment and the conduction electron spin.
1510.00808v2
2015-10-13
Nonlocal torque operators in ab initio theory of the Gilbert damping in random ferromagnetic alloys
We present an ab initio theory of the Gilbert damping in substitutionally disordered ferromagnetic alloys. The theory rests on introduced nonlocal torques which replace traditional local torque operators in the well-known torque-correlation formula and which can be formulated within the atomic-sphere approximation. The formalism is sketched in a simple tight-binding model and worked out in detail in the relativistic tight-binding linear muffin-tin orbital (TB-LMTO) method and the coherent potential approximation (CPA). The resulting nonlocal torques are represented by nonrandom, non-site-diagonal and spin-independent matrices, which simplifies the configuration averaging. The CPA-vertex corrections play a crucial role for the internal consistency of the theory and for its exact equivalence to other first-principles approaches based on the random local torques. This equivalence is also illustrated by the calculated Gilbert damping parameters for binary NiFe and FeCo random alloys, for pure iron with a model atomic-level disorder, and for stoichiometric FePt alloys with a varying degree of L10 atomic long-range order.
1510.03571v2
2015-10-26
Misfit stabilized embedded nanoparticles in metallic alloys
Nanoscale inhomogeneities are typical for numerous metallic alloys and crucially important for their practical applications. At the same time, stabilization mechanisms of such a state are poorly understood. We present a general overview of the problem, together with a more detailed discussion of the prototype example, namely, Guinier-Preston zones in Al-based alloys. It is shown that coherent strain due to a misfit between inclusion and host crystal lattices plays a decisive role in the emergence of the inhomogeneous state. We suggest a model explaining formation of ultrathin plates (with the thickness of a few lattice constants) typical for Al-Cu alloys. Discreteness of the array of misfit dislocations and long-ranged elastic interactions between them are the key ingredients of the model. This opens a way to a general understanding of the nature of (meta)stable embedded nanoparticles in practically important systems.
1510.07443v1
2015-10-28
Scaling of alloy interfacial properties under compositional strain
Complex morphologies and microstructures that emerge during materials growth and solidification are often determined by both equilibrium and kinetic properties of the interface and their crystalline anisotropies. However limited knowledge is available for the alloying and particularly the compositionally generated elastic effects on these interface characteristics. Here we systematically investigate such compositional effects on the interfacial properties of an alloy model system based on the phase-field-crystal analysis, including the solid-liquid interfacial free energy, kinetic coefficient, and lattice pinning strength. Scaling relations for these interfacial quantities over various ranges of material parameters are identified and predicted. Our results indicate the important effects of couplings among mesoscopic and microscopic length scales of alloy structure and concentration, and also the influence of compressive and tensile interface stresses induced by composition variations. The approach developed here provides an efficient way to systematically identify these key material properties beyond the traditional atomistic and continuum methods.
1510.08180v2
2015-12-11
Nanoscale Origins of the Damage Tolerance of the High-Entropy Alloy CrMnFeCoNi
Damage-tolerance can be an elusive characteristic of structural materials requiring both high strength and ductility, properties that are often mutually exclusive. High-entropy alloys are of interest in this regard. Specifically, the single-phase CrMnFeCoNi alloy displays tensile strength levels of ~1 GPa, excellent ductility (~60-70%) and exceptional fracture toughness (KJIc > 200 MPa/m). Here, through the use of in-situ straining in an aberration-corrected transmission electron microscope, we report on the salient atomistic to micro-scale mechanisms underlying the origin of these properties. We identify a synergy of multiple deformation mechanisms, rarely achieved in metallic alloys, which generates high strength, work hardening and ductility, including the easy motion of Shockley partials, their interactions to form stacking-fault parallelepipeds, and arrest at planar-slip bands of undissociated dislocations. We further show that crack propagation is impeded by twinned, nano-scale bridges that form between the near-tip crack faces and delay fracture by shielding the crack tip.
1512.03621v1
2015-12-18
The effect of quenching from different temperatures on Bi 0.88 Sb 0.12 alloy
Structural, thermal, resistive and magnetic properties of melt quenched Bi 0.88 Sb 0.12 alloys are reported. The samples are heated at three different temperatures, followed by rapid quenching in liquid nitrogen. Large temperature difference between liquidus and solidus lines, led to microscopic in-homogeneity in the alloy. The effect of quenching from different temperatures in polycrystalline Bi 0.88 Sb 0.12 alloy has been studied. The parameters such as strain, unit cell volume, and resistivity are found to increase with temperature. Thermal variation of resistivity depicts non monotonic temperature dependence. The total negative susceptibility increases and band gap of semiconducting Bi 0.88 Sb 0.12 samples decreases with increasing temperature.
1512.05883v1
2015-12-23
Preferential site occupancy of alloying elements in TiAl-based phases
First principles calculations are used to study the preferential occupation of ternary alloying additions into the binary Ti-Al phases, namely $\gamma$-TiAl, $\alpha_2$-Ti$_3$Al, $\beta_{\mathrm{o}}$-TiAl, and B19-TiAl. While the early transition metals (TMs, group IVB, VB , and VIB elements) prefer to substitute for Ti atoms in the $\gamma$-, $\alpha_2$-, and B19-phases, they preferentially occupy Al sites in the $\beta_{\mathrm{o}}$-TiAl. Si is in this context an anomaly, as it prefers to sit on the Al sublattice for all four phases. B and C are shown to prefer octahedral Ti-rich interstitial positions instead of substitutional incorporation. The site preference energy is linked with the alloying-induced changes of energy of formation, hence alloying-related (de)stabilisation of the phases. We further show that the phase-stabilisation effect of early TMs on $\beta_{\mathrm{o}}$-phase has a different origin depending on their valency. Finally, an extensive comparison of our predictions with available theoretical and experimental data (which is, however, limited mostly to the $\gamma$-phase) shows a consistent picture.
1512.07601v2
2016-01-21
Multiscale model of global inner-core anisotropy induced by hcp-alloy plasticity
$\bullet$ Multiscale model of inner-core anisotropy produced by hcp alloy deformation$\bullet$ 5 to 20% single-crystal elastic anisotropy and plastic deformation by pyramidal slip $\bullet$ Low-degree inner-core formation model with faster crystallization at the equatorThe Earth's solid inner-core exhibits a global seismic anisotropy of several percents. It results from a coherent alignment of anisotropic Fe-alloy crystals through the inner-core history that can be sampled by present-day seismic observations. By combining self-consistent polycrystal plasticity, inner-core formation models, Monte-Carlo search for elastic moduli, and simulations of seismic measurements, we introduce a multiscale model that can reproduce a global seismic anisotropy of several percents aligned with the Earth's rotation axis. Conditions for a successful model are an hexagonal-close-packed structure for the inner-core Fe-alloy, plastic deformation by pyramidal \textless{}c+a\textgreater{} slip, and large-scale flow induced by a low-degree inner-core formation model. For global anisotropies ranging between 1 and 3%, the elastic anisotropy in the single crystal ranges from 5 to 20% with larger velocities along the c-axis.
1601.05674v1
2016-02-08
A Generalized Ising Model for studying Alloy Evolution under Irradiation and its use in Kinetic Monte Carlo Simulations
We derive an Ising Hamiltonian for kinetic simulations involving interstitial and vacancy defects in binary alloys. Our model, which we term `ABVI', incorporates solute transport by both interstitial defects and vacancies into a mathematically-consistent framework , and thus represents a generalization to the widely-used ABV model for alloy evolution simulations. The Hamiltonian captures the three possible interstitial configurations in a binary alloy: A-A, A-B, and B-B, which makes it particularly useful for irradiation damage simulations. All the constants of the Hamiltonian are expressed in terms of bond energies that can be computed using first-principles calculations. We implement our ABVI model in kinetic Monte Carlo simulations and perform a verification exercise by comparing our results to published irradiation damage simulations in simple binary systems with Frenkel pair defect production and several microstructural scenarios, with matching agreement found.
1602.02470v1
2016-04-29
Hydrostatic pressure tuned magneto-structural transition and occurrence of pressure induced exchange bias effect in Mn$_{0.85}$Fe$_{0.15}$NiGe alloy
Magnetic and magneto-functional behavior of a Fe-doped MnNiGe alloy with nominal composition Mn$_{0.85}$Fe$_{0.15}$NiGe have been investigated in ambient as well as in high pressure condition. The alloy undergoes first order martensitic phase transition (MPT) around 200 K and also shows large conventional magnetocaloric effect (MCE) ($\Delta S$ $\sim$ -21 J/kg-K for magnetic field ($H$) changing from 0-50 kOe) around the transition in ambient condition. Application of external hydrostatic pressure ($P$) results a shift in MPT towards the lower temperature and a clear decrease in the saturation moment of the alloy at 5 K. The peak value of MCE is also found to decrease with increasing external $P$ ($\sim$ 18 J/kg-K decrease in $\Delta S$ has been observed for $P$ = 12.5 kbar). The most interesting observation is the occurance of exchange bias effect (EBE) on application of external $P$. The competing ferromagnetic and antiferromagnetic interaction in presence of external $P$ plays the pivotal role towards the observation of $P$ induced EBE.
1604.08761v1
2016-04-30
Effects of aluminum on hydrogen solubility and diffusion in deformed Fe-Mn alloys
We discuss hydrogen diffusion and solubility in aluminum alloyed Fe-Mn alloys. The systems of interest are subjected to tetragonal and isotropic deformations. Based on ab initio modelling, we calculate solution energies, then employ Oriani's theory which reflects the influence of Al alloying via trap site diffusion. This local equilibrium model is complemented by qualitative considerations of Einstein diffusion. Therefore, we apply the climbing image nudged elastic band method to compute the minimum energy paths and energy barriers for hydrogen diffusion. Both for diffusivity and solubility of hydrogen, we find that the influence of the substitutional Al atom has both local chemical and nonlocal volumetric contributions.
1605.00084v2
2016-05-18
Shear Melting and High Temperature Embrittlement: Theory and Application to Machining Titanium
We show that alloying with rare earth metals (REMs) can dramatically improve the machineability of a range of titanium alloys, even though the REM is not incorporated in the alloy matrix. The mechanism for this is that under cutting, shear bands are formed within which the nano-precipitates of REM are shear mixed. This lowers the melting point such that the mechanism of deformation changes from dislocation mechanism to localised amorphisation and shear softening. The material then fractures along the thin, amorphous shear-band. Outside the shear band, the REM remains as precipitates. The new alloys have similar mechanical properties and biocompatibility to conventional materials.
1605.05514v1
2016-06-29
Improved model for the thermal conductivity of binary metallic systems
We extended and corrected Mott's two-band model for the composition-dependence of thermal and electrical conductivity in binary metal alloys based on high-throughput time-domain thermoreflectance (TDTR) measurements on diffusion multiples and scatterer-density calculations from first principles. Examining PdAg, PtRh, AuAg, AuCu, PdCu, PdPt, and NiRh binary alloys, we found that the nature of the two dominant scatterer-bands considered in the Mott model changes with the alloys, and should be interpreted as a combination of the dominant element-specific s- and/or d-orbitals. Using calculated orbital and element-resolved density-of-states values calculated with density functional theory as input, we determined the correct orbital mix that dominates electron scattering for all examined alloys and find excellent agreement between fitted models and experiments. The proposed description of the composition dependence of the resistivity can be readily implemented into the CALPHAD framework.
1606.09287v2
2017-01-11
Morphology and mechanical properties of nanocrystalline Cu/Ag alloy
Hybrid Monte Carlo (MC)/molecular dynamics (MD) simulations are conducted to study the microstructures of nanocrystalline (nc) Cu/Ag alloys with various Ag concentrations. When the Ag concentration is below 50 Ag atoms/nm!, an increase in Ag concentration leads to a gradual growth of monolayer grain boundary (GB) complexions into nanolayer complexions. Above the concentration of 50 Ag atoms/nm!, wetting layers with a bulk crystalline phase are observed. The effects of Ag on mechanical properties and deformation mechanisms of nc Cu/Ag alloys are investigated in MD simulations of uniaxial tension. GB sliding resistance is found to first increase and then decrease with an increase in Ag concentration. Surprisingly, we also find that the dislocation density decreases monotonically with an increase in Ag concentration, which suggests that the grain interiors are softened by the introduction of Ag dopants at GBs. In addition, there is a critical Ag concentration that maximizes flow stress of nc Cu/Ag alloys. The flow stress, GB sliding resistance, and the intragranular dislocation densities become less sensitive to Ag dopants when the grain diameter increases from 5nm to 40nm.
1701.03013v1
2017-07-04
Short-Range-Order for fcc-based binary alloys Revisited from Microscopic Geometry
Short-range order (SRO) in disordered alloys is typically interpreted as competition between chemical effect of negative (or positive) energy gain by mixing constituent elements and geometric effects comes from difference in effective atomic radius. Although we have a number of theoretical approaches to quantitatively estimate SRO at given temperatures, it is still unclear to systematically understand trends in SRO for binary alloys in terms of geometric character, e.g., effective atomic radius for constituents. Since chemical effect plays significant role on SRO, it has been believed that purely geometric character cannot quantitatively explain the SRO trends. Despite these considerations, based on the density functional theory (DFT) calculations on fcc-based 28 equiatomic binary alloys, we find that while convensional Goldschmidt or DFT-based atomic radius for constituents have no significant correlation with SRO, atomic radius for specially selected structure, constructed purely from information about underlying lattice, can successfully capture the magnitude of SRO. These facts strongly indicate that purely geometric information of the system plays central role to determine characteristic disordered structure.
1707.00901v1
2018-01-09
Micro(point)contact spectroscopy of dilute magnetic (Kondo) alloys CuMn and CuFe
The method of microcontact spectroscopy is used to study alloys with magnetic impurities CuMn and CuFe in the range of concentrations 0.01-1 at.%. Minima or maxima (so-called zero-bias anomalies) were observed in the microcontact spectra of these alloys at voltages ~ 1 mV. The Lande g-factor for the Mn impurity in a Cu matrix was determined from the splitting of the minimum of the zero-bias anomaly in a magnetic field. The quantitative calculations carried out agree well with theory and permit determining both the important geometric contact parameter <K> i.e., the averaged geometric form factor, and the characteristics of the alloy itself, for example, J/E_F, i.e., the ratio of the magnitude of the exchange interaction energy between an electron and the magnetic impurity to the Fermi energy, from the microcontact spectra.
1801.02972v1
2018-01-16
Vortex-glass transformation within the surface superconducting state of $β$-phase Mo$_{1-x}$Re$_x$ alloys
We have performed an experimental study on the temperature dependence of electrical resistivity $\rho$($T$) and heat capacity $C$($T$) of the Mo$_{1-x}$Re$_x$ $(x = 0.20, 0.25)$ alloy superconductors in different magnetic fields. In the presence of applied magnetic field, the electrical resistivity of these alloys go to zero at a temperature well above the bulk superconducting transition temperature obtained with the help of heat capacity measurements in the same magnetic field. Our study indicates the presence of surface superconducting state in these alloys, where the flux lines are pinned in the surface sheath of the superconductor. The configuration of the flux-lines (2d pancake-like) in the surface sheath is understood in the realm of the flux-spot model. Experimental evidence in support of the surface mixed-state state or "Kulik vortex-state" and the occurrence of a vortex-liquid to vortex-glass transition is presented.
1801.05080v1
2018-01-25
Sensitivity of ferromagnetic resonance in PdCo alloyed films to hydrogen gas
In this work we studied the ferromagnetic resonance response of Co(x)Pd(1-x) alloy samples with different cobalt contents (x = 0.65, 0.39, 0.24 & 0.14). We found significant differences in the response of the samples to the presence of hydrogen gas in the samples' environment. Two particular films (with x=0.39 and 0.24) demonstrated behaviour which is promising for application in hydrogen gas sensing. Using the Co(39)Pd(61) alloy thin film, we were able to measure hydrogen gas concentration in a very broad range (from <0.1% to 100%) at a fixed value of the external magnetic field. Finally, we demonstrate that the Co(24)Pd(76) alloy thin film is sensitive to ultra-low hydrogen gas concentrations - from 10 to 10000 ppm.
1801.08324v1
2018-03-10
Alloy engineering of topological semimetal phase transition in MgTa$_{2-x}$Nb$_x$N$_3$
Dirac, triple-point and Weyl fermions represent three topological semimetal phases, characterized with a descending degree of band degeneracy, which have been realized separately in specific crystalline materials with different lattice symmetries. Here we demonstrate an alloy engineering approach to realize all three types of fermions in one single material system of MgTa$_{2-x}$Nb$_x$N$_3$. Based on symmetry analysis and first-principles calculations, we map out a phase diagram of topological order in the parameter space of alloy concentration and crystalline symmetry, where the intrinsic MgTa$_2$N$_3$ with the highest symmetry hosts the Dirac semimetal phase which transforms into the triple-point and then the Weyl semimetal phase with the increasing Nb concentration that lowers the crystalline symmetries. Therefore, alloy engineering affords a unique approach for experimental investigation of topological transitions of semimetallic phases manifesting different fermionic behaviors.
1803.03773v1
2018-03-28
High field paramagnetic Meissner effect in Mo$_{100-x}$Re$_x$ alloy superconductors
We have performed an experimental study on the temperature and field dependence of magnetization of a series of superconducting Mo$_{100-x}$Re$_x$ alloys. Our studies reveal the presence of high field paramagnetic effect (HFPME) in these low temperature superconductors. The results of our studies indicate that the HFPME in the Mo$_{100-x}$Re$_x$ alloys is related to the inhomogeneous distribution of strong and weak flux-line pinning centers, and the flux compression resulting due to the same while cooling down the samples in the presence of high magnetic fields. The results are complemented by the studies on the temperature dependence of the electrical resistivity and heat capacity of these alloys in different constant magnetic fields. We compare our findings with the studies reported in literature on both low $T_C$ and high $T_C$ superconductors.
1803.10845v1
2018-09-06
Atomistic modeling of interfacial segregation and structural transitions in ternary alloys
Grain boundary engineering via dopant segregation can dramatically change the properties of a material. For metallic systems, most current studies concerning interfacial segregation and subsequent transitions of grain boundary structure are limited to binary alloys, yet many important alloy systems contain more than one type of dopant. In this work, hybrid Monte Carlo/molecular dynamics simulations are performed to investigate the behavior of dopants at interfaces in two model ternary alloy systems: Cu-Zr-Ag and Al-Zr-Cu. Trends in boundary segregation are studied, as well as the propensity for the grain boundary structure to become disordered at high temperature and doping concentration. For Al-Zr-Cu, we find that the two solutes prefer to occupy different sites at the grain boundary, leading to a synergistic doping effect. Alternatively, for Cu-Zr-Ag, there is site competition because the preferred segregation sites are the same. Finally, we find that thicker amorphous intergranular films can be formed in ternary systems by controlling the concentration ratio of different solute elements.
1809.02218v2
2018-11-27
Atomistic Insights Into Cluster Strengthening in Aluminum Alloys
In certain naturally aged aluminum alloys, significant strengthening can be obtained due to the decomposition of a super-saturated solid solution into clusters. The origins of such strengthening remain unclear due to the challenge of differentiating solute cluster strengthening from solid solution or precipitate strengthening. To shed light on the origin of cluster strengthening in aluminum alloys, the interaction between the smallest possible type of clusters (i.e. dimers) and moving dislocations in a model Al-Mg alloy is studied using atomistic simulations. Additionally, theoretical models for both the parelastic and dielastic interactions between clusters and dislocations is used to identify which factor among order strengthening, elastic interaction, and change of stacking fault energy controls cluster strengthening. The comparison of the results from these models to that of the atomistic simulations show that in the case of Mg dimers, the strength of the strongest ones are dominated by the dielastic contribution through the change of stacking fault energy.
1811.10774v1
2018-11-27
Improving the Visualization of Alloy Instances
Alloy is a lightweight formal specification language, supported by an IDE, which has proven well-suited for reasoning about software design in early development stages. The IDE provides a visualizer that produces graphical representations of analysis results, which is essential for the proper validation of the model. Alloy is a rich language but inherently static, so behavior needs to be explicitly encoded and reasoned about. Even though this is a common scenario, the visualizer presents limitations when dealing with such models. The main contribution of this paper is a principled approach to generate instance visualizations, which improves the current Alloy Visualizer, focusing on the representation of behavior.
1811.10817v1
2019-11-27
Study of RF Sputtered Antimony Alloyed Bismuth Vanadium Oxide (Sb:BiVO4) Thin Films for Enhanced Photoelectrochemical (PEC) performance from Bandgap Modulation to Thickness Optimization
Monoclinic scheelite bismuth vanadate (BiVO4) is a promising photoanode for water splitting yet the PEC performance is limited due to its relatively higher (2.4 eV) band gap. Here, we successfully decreased its the band gap to 1.72 eV by controlled antimony alloying. Low bandgap antimony alloyed bismuth vanadium oxide (Sb:BiVO4) thin film was prepared by RF sputtering of high purity homemade target, fabricated by solid-state reaction using a mixture of Sb2O3, Bi2O3, and V2O5 powders with desired stoichiometric ratios. Several growth parameters, powder crystallography, post-deposition effects, and surface treatments, thickness dependence, effect of electrolytes on photocorrosion were studied along with its optical and electrochemical characterization. We discovered that Sb:BiVO4 is a direct band gap material in the visible light range (1.72 eV) and a valence band position suitable for driving water oxidation reaction under illumination. Furthermore, hole diffusion length is increased with antimony alloying and achieved optimum thickness of 400 nm for higher photocurrent. The controllably prepared Sb:BiVO4 particles are having the sizes of 10-15 nm in room temperature deposition and can be grown up to 0.5 microns under air annealing.
1911.12191v1
2021-07-07
Ultra strong and ductile eutectic high entropy alloy fabricated by selective laser melting
With important application prospects, eutectic high entropy alloys have received extensive attention for their excellent strength and ductility in a large temperature range. The excellent casting characteristics of eutectic high entropy alloys make it possible to achieve well manufacturability of selective laser melting. For the first time, we have achieved crack-free eutectic high entropy alloy fabricated by selective laser melting, which has excellent mechanical properties in a wide temperature range of -196 degrees Celsius~760 degrees Celsius due to ultra-fine eutectic lamellar spacing of 150 ~ 200nm and lamellar colony of 2 ~ 6 {\mu}m. Specifically, the room temperature tensile strength exceeds 1400MPa and the elongation is more than 20%, significantly improved compared with those manufactured by other techniques with lower cooling rate.
2107.03202v1
2021-07-12
Laser Ablation of Al-Ni Alloys and Al-Ni Layer Systems simulated with Molecular Dynamics and the Two-Temperature Model
Laser ablation of Al-Ni alloys and Al films on Ni substrates has been studied by molecular dynamics simulations (MD). The MD method was combined with a two-temperature model to describe the interaction between the laser beam, the electrons and the atoms. The challenge for alloys and mixtures is to find the electronic parameters: electron heat conductivity, electron heat capacity and electron-phonon coupling parameter. The challenge for layered systems is to run simulations of an inhomogeneous system which requires modification of the simulation code. Ablation and laser-induced melting was studied for several Al-Ni compounds. At low fluences above the threshold ordinary ablation behavior occurred while at high fluences the ablation mechanism changed in Al$_3$Ni and AlNi$_3$ from phase explosion to vaporization. Al films of various thicknesses on a Ni substrate have also been simulated. Above threshold, 8 nm Al films are ablated as a whole while 24 nm Al films are only partially removed. Below threshold, alloying with a mixture gradient has been observed in the thin layer system.
2107.05415v1
2017-04-11
CoFeAlB alloy with low damping and low magnetization for spin transfer torque switching
We investigate the effect of Al doping on the magnetic properties of the alloy CoFeB. Comparative measurements of the saturation magnetization, the Gilbert damping parameter $\alpha$ and the exchange constant as a function of the annealing temperature for CoFeB and CoFeAlB thin films are presented. Our results reveal a strong reduction of the magnetization for CoFeAlB in comparison to CoFeB. If the prepared CoFeAlB films are amorphous, the damping parameter $\alpha$ is unaffected by the Al doping in comparison to the CoFeB alloy. In contrast, in the case of a crystalline CoFeAlB film, $\alpha$ is found to be reduced. Furthermore, the x-ray characterization and the evolution of the exchange constant with the annealing temperature indicate a similar crystallization process in both alloys. The data proves the suitability of CoFeAlB for spin torque switching properties where a reduction of the switching current in comparison with CoFeB is expected.
1704.03326v1
2017-05-04
Short-range order in high entropy alloys:Theoretical formulation and application to Mo-Nb-Ta-V-W system
In high-entropy alloys (HEAs), the local chemical fluctuations from disordered solute solution state into segregation, precipitation and ordering configurations are complex due to the large number of elements. In this work, the cluster expansion (CE) Hamiltonian for multi-component alloy systems is developed in order to investigate the dependence of chemical ordering of HEAs as a function of temperature dependence due to derivation of configuration entropy from the ideal solute solution. Analytic expressions for Warren-Cowley short-range order (SRO) parameters are derived for a five component alloy system. The theoretical formulation is used to investigate the evolution of the ten different SRO parameters in the MoNbTaVW and the sub-quaternary systems obtained by MonteCarlo simulations within the combined CE and first-principles formalism.
1705.01844v1
2017-05-15
The bi-layered precipitate phase zeta in the Al-Ag alloy system
The Al-Ag system is thought to be a well-understood model system used to study diffusional phase transformations in alloys. Here we report the existence of a new precipitate phase, zeta, in this classical system using scanning transmission electron microscopy (STEM). The zeta phase has a modulated structure composed of alternating bilayers enriched in Al or Ag. Our in situ annealing experiments reveal that the zeta phase is an intermediate precipitate phase between GP zones epsilon and gamma prime. First-principles calculations show that z is a local energy minimum state formed during Ag clustering in Al. The layered structure of zeta is analogous to the well-known Ag segregation at the precipitate-matrix interfaces when Ag is micro- alloyed in various aluminium alloys.
1705.05175v1
2018-07-23
Fault Localization for Declarative Models in Alloy
Fault localization is a popular research topic and many techniques have been proposed to locate faults in imperative code, e.g. C and Java. In this paper, we focus on the problem of fault localization for declarative models in Alloy -- a first order relational logic with transitive closure. We introduce AlloyFL, the first set of fault localization techniques for faulty Alloy models which leverages multiple test formulas. AlloyFL is also the first set of fault localization techniques at the AST node granularity. We implements in AlloyFL both spectrum-based and mutation-based fault localization techniques, as well as techniques that are based on Alloy's built-in unsat core. We introduce new metrics to measure the accuracy of AlloyFL and systematically evaluate AlloyFL on 38 real faulty models and 9000 mutant models. The results show that the mutation-based fault localization techniques are significantly more accurate than other types of techniques.
1807.08707v1
2019-04-09
Band structure of Ge$_{1-x}$Sn$_{x}$alloy: a full-zone 30-band $k$$\cdot$$p$ model
A full-zone 30-band $k$$\cdot$$p$ model is developed as an efficient and reliable tool to compute electronic band structure in Ge$_{1-x}$Sn$_{x}$ alloy. The model was first used to reproduce the electronic band structures in Ge and $\alpha$-Sn obtained with empirical tight binding and \textit{ab initio} methods. Input parameters for the 30-band $k$$\cdot$$p$ model are carefully calibrated against prior empirical predications and experimental data. Important material properties such as effective mass for electrons and holes, Luttinger parameters, and density of states are obtained for Ge$_{1-x}$Sn$_{x}$ alloy with the composition range $0<x<0.3$. The 30-band $k$$\cdot$$p$ model that requires far less computing resources is a necessary capability for optimization of sophisticated devices made from Ge$_{1-x}$Sn$_{x}$ alloy with a large parameter space to explore.
1904.04415v1
2019-04-15
Mid-infrared (3-8 μm) $\text{Ge}_{1-y}\text{Sn}_y$ alloys (0.15 < $y$ < 0.30): synthesis, structural, and optical properties
$\text{Ge}_{1-y}\text{Sn}_y$ alloys with compositions in the 0.15 < $y$ < 0.30 range have been grown directly on Si substrates using a chemical vapor deposition approach that allows for growth temperatures as high as 290 $^{\circ}$C. The films show structural properties that are consistent with results from earlier materials with much lower Sn concentrations. These include the lattice parameter and the Ge-Ge Raman frequency, which are found to depend linearly on composition. The simplicity of the structures, directly grown on Si, makes it possible to carry out detailed optical studies. Sharp absorption edges are found, reaching 8 $\mu$m near $y$ =0.3. The compositional dependence of edge energies shows a cubic deviation from the standard quadratic alloy expression. The cubic term may dramatically impact the ability of the alloys to cover the long-wavelength (8-12 $\mu$m) mid-IR atmospheric window.
1904.07201v2
2019-10-29
Icosahedral quasicrystal, 1/1 and 2/1 approximants in Zn-based ternary alloys containing Au and Yb/Tb
In a narrow composition range centered at Zn74.5Au10.5Yb15.0, Tsai-type icosahedral quasicrystal is formed in alloys quenched from 880 C. This quasicrystal belongs to the primitive type with the 6-dimensional lattice parameter a6D=7.378 A. The quasicrystal was not formed in the slowly cooled specimen, and was considered a metastable phase. The stable phase is a 2/1 approximant of the lattice parameter a2/1=23.271 A. This approximant forms exclusively in Zn76.0Au9.0Yb15.0 alloy annealed at 530 C. In addition, Zn70.5Au15.5Tb14.0 alloy annealed at 505 C forms a Tsai-type 1/1 approximant (a1/1=14.343 A). These new Zn-based phases observed in this study correspond to the quasicrystal-related phases in binary Cd-lanthanoid systems, and show the possibility of isostructural substitution of Cd by Zn/Au.
1910.13078v1
2012-09-25
Automatic Unbounded Verification of Alloy Specifications with Prover9
Alloy is an increasingly popular lightweight specification language based on relational logic. Alloy models can be automatically verified within a bounded scope using off-the-shelf SAT solvers. Since false assertions can usually be disproved using small counter-examples, this approach suffices for most applications. Unfortunately, it can sometimes lead to a false sense of security, and in critical applications a more traditional unbounded proof may be required. The automatic theorem prover Prover9 has been shown to be particularly effective for proving theorems of relation algebras [7], a quantifier-free (or point-free) axiomatization of a fragment of relational logic. In this paper we propose a translation from Alloy specifications to fork algebras (an extension of relation algebras with the same expressive power as relational logic) which enables their unbounded verification in Prover9. This translation covers not only logic assertions, but also the structural aspects (namely type declarations), and was successfully implemented and applied to several examples.
1209.5773v1
2014-06-01
The application of radiation diffuse scattering to the calculation of phase diagrams of F.C.C. substitutional alloys
By using quantitative information about the radiation diffuse-scattering intensity of the disordered f.c.c. substitutional alloy the Fourier component of mixing energies of atoms may be estimated. We have to use the measurement data of the diffuse-scattering intensities at the corresponding reciprocal-space points k of the disordered phase and then determine the parameter w(k). The statistical thermodynamics of the nonideal solid solution is determined by these energy parameters {w(k)}. Therefore, one can obtain the configuration free energy of an alloy, F = U - TS (U - internal energy, S - entropy), and then determine its fundamental thermodynamic characteristics, including not only its phase diagram, but also the concentration-dependent order-disorder transformation temperature, temperature and concentration long-range order parameter dependences, chemical activity, heat capacity etc. Some thermodynamic properties are calculated within the framework of the statistical-thermodynamic approach for f.c.c.-Ni-Fe alloy. The diffuse-scattering intensity values are taken from data in the literature.
1406.0161v1
2018-02-19
Borderline Magnetism: How Does Adding Magnesium to Paramagnetic CeCo$_3$ Make a 450 K Ferromagnet with Large Magnetic Anisotropy?
A recent experimental study (Phys. Rev. Appl. 9, 024023, 2018) on paramagnetic CeCo$_3$ finds that Magnesium alloying induces a ferromagnetic transition with intrinsic properties large enough for permanent magnet applications. Here we explain these surprising results \textit{via} a first principles study of the electronic structure and magnetism of Magnesium-alloyed CeCo$_3$. We find the origin of this Magnesium-induced ferromagnetic transition to be Stoner physics - the substantial increase in the Fermi-level density-of-states $N(E_F)$ with Mg alloying. Our calculations suggest that both Ce and Co atoms are important for generating large magnetic anisotropy suggesting the viability of Co-3$d$, and Ce-4$f$ interaction for the generation of magnetic anisotropy in magnetic materials. These results offer a new route to the discovery of ferromagnetic materials and provide fundamental insight into the magnetic properties of these alloys
1802.06747v2
2018-10-31
Voltage effects on the stability of Pd ensembles in Pd-Au/Au(111) surface alloys
The catalytic performance of multimetallic electrodes is often attributed to a beneficial combination of ligand, strain, and ensemble effects. Understanding the influence of the electrochemical environment on the stability of the alloy surface structure is thus a crucial component to the design of highly active and durable electrocatalysts. In this work, we study the effects of an applied voltage to electrocatalytic Pd-Au/Au(111) surface alloys in contact with a model continuum electrolyte. Using planewave density functional theory, two-dimensional cluster expansions are parameterized and used to simulate dilute Pd-Au surface alloys under electrochemical conditions via Metropolis Monte Carlo within an extended canonical ensemble. While Pd monomers are stable at all potentials considered, different extents of surface electrification are observed to promote the formation of Pd dimers and trimers, as well as clusters of Pd monomers. We find that the relative proportion of monomer, dimer, and trimer surface fractions is in good agreement with in situ scanning tunneling microscopy measurements. The further development and refinement of the approaches described herein may serve as a useful aid in the development of next-generation electrocatalysts.
1812.11018v1
2019-02-01
Metallic glasses for biodegradable implants
Metallic glasses are excellent candidates for biomedical implant applications due to their inherent strength and corrosion resistance. Use of metallic glasses in structural applications is limited, however, because bulk dimensions are challenging to achieve. Glass-forming ability (GFA) varies strongly with alloy composition and becomes more difficult to predict as the number of chemical species in a system increases. Here we present a theoretical model - implemented in the AFLOW framework - for predicting GFA based on the competition between crystalline phases, and apply it to biologically relevant binary and ternary systems. Elastic properties are estimated based on the rule of mixtures for alloy systems that are predicted to be bulk glass-formers. Focusing on Ca- and Mg-based systems for use in biodegradable orthopedic support applications, we suggest alloys in the AgCaMg and AgMgZn families for further study; and alloys based on the compositions: Ag$_{0.33}$Mg$_{0.67}$, Cu$_{0.5}$Mg$_{0.5}$, Cu$_{0.37}$Mg$_{0.63}$ and Cu$_{0.25}$Mg$_{0.5}$Zn$_{0.25}$.
1902.00485v1
2019-02-25
Anomalous local distortion in BCC refractory high-entropy alloys
Whereas exceptional mechanical and radiation performances have been found in the emergent medium- and high-entropy alloys (MEAs and HEAs), the importance of their complex atomic environment, reflecting diversity in atomic size and chemistry, to defect transport has been largely unexplored at the atomic level. Here we adopt a local structure approach based on the atomic pair distribution function measurements in combination with density functional theory calculations to investigate a series of body-centered cubic (BCC) MEAs and HEAs. Our results demonstrate that all alloys exhibit local lattice distortions (LLD) to some extent, but an anomalous LLD, merging of the first and second atomic shells, occurs only in the Zr- and/or Hf-containing MEAs and HEAs. In addition, through the ab-initio simulations we show that charge transfer among the elements profoundly reduce the size mismatch effect. The observed competitive coexistence between LLD and charge transfer not only demonstrates the importance of the electronic effects on the local environments in MEAs and HEAs, but also provides new perspectives to in-depth understanding of the complicated defect transport in these alloys.
1902.09279v1
2019-06-17
Phase selection and microstructure of slowly solidified Al-Cu-Fe alloys
The search for effective methods to fabricate bulk single-phase quasicrystalline Al-Cu-Fe alloys is currently an important task. Crucial to solving this problem is to understand mechanisms of phase formation in this system. Here we study crystallization sequence during solidification as well as the conditions of solid phase formation in slowly solidified Al-Cu-Fe alloys in a wide range of compositions. Concentration dependencies of undercoolability were also constructed by differential thermal analysis method. These experimental results are compared with data on chemical short-range order in the liquid state determined from \textit{ab initio} molecular dynamic simulations. We observe that main features of interatomic interaction in the Al-Cu-Fe alloys are similar for both liquid and solid states and they change in the vicinity of i-phase composition. In the concentration region, where the i-phase forms from the melt, both the undercoolability and the crystallization character depend on the temperature of the melts before cooling.
1906.06941v1
2020-04-01
Ab initio study of band gap properties in novel metastable BC8/ST12 Si$_x$Ge$_{1-x}$ alloys
The cubic $Ia\bar{3}$ (BC8) and tetragonal $P4_32_12$ (ST12) high pressure modifications of Si and Ge are attractive candidates for applications in optoelectronic, thermoelectric or plasmonic devices. Si$_x$Ge$_{1-x}$ alloys in BC8/ST12 modifications could help overcome the indirect and narrow band gaps of the pure phases and enable tailoring for specific use-cases. Such alloys have experimentally been found to be stable at ambient conditions after release from high pressure synthesis, however their fundamental properties are not known. In this work, we employ {\it ab initio} calculations based on density functional theory (DFT) to investigate the electronic properties of these compounds as a function of composition $x$. We obtain the effective band structures of intermediate alloys by constructing special quasi random structures (SQS) and unfolding their band structure to the corresponding primitive cell. Furthermore, we show that the indirect band gap of the ST12 Ge end-member can be tuned to become direct at $x_\text{Si} \approx 0.16$. Finally, our investigations also demonstrate that the BC8 modification, on the other hand, is insensitive to compositional changes and is a narrow direct band gap semiconductor only in the case of pure Si.
2004.00461v1
2020-04-05
Bulk nanostructured AlCoCrFeMnNi chemically complex alloy synthesized by laser-powder bed fusion process
We report the synthesis of a bulk nanostructured alloy using the laser-powder bed fusion process. The equiatomic AlCoCrFeMnNi chemically complex alloy forms a nanoscale modulated structure, which is homogeneously distributed in the as-built condition. The nanostructure consisted of Al & Ni-rich ordered (B2) and Cr & Fe-rich disordered (A2) BCC phases. The two phases form an interconnected phase-network with coherent interface boundaries. Atom-probe-tomography and aberration-corrected scanning transmission electron microscopy analysis of the spatial distribution of the modulated structure suggests the occurrence of nano-scale spinodal decomposition. These results introduce a direct synthesis of bulk nanostructured alloys with promising geometric flexibility.
2004.02309v1
2020-04-08
Ti-alloying of BaZrS3 chalcogenide perovskite for photovoltaics
BaZrS3, a prototypical chalcogenide perovskite, has been shown to possess a direct band gap, an exceptionally strong near band edge light absorption, and good carrier transport. Coupled with its great stability, non-toxicity with earth abundant elements, it is thus a promising candidate for thin film solar cells. However, its reported band gap in the range of 1.7-1.8 eV is larger than the optimal value required to reach the Shockley-Queisser limit of a single junction solar cell. Here we report the synthesis of Ba(Zr1-xTix)S3 perovskite compounds with a reduced band gap. It is found that Ti alloying is extremely effective in band gap reduction of BaZrS3: a mere 4 at% alloying decreases the band gap from 1.78 to 1.51 eV, resulting in a theoretical maximum power conversion efficiency of 32%. Higher Ti-alloying concentration is found to destabilize the distorted chalcogenide perovskite phase.
2004.04261v1
2020-04-18
Seeking for low thermal conductivity atomic configurations in $\rm{Si_{0.5}Ge_{0.5}}$ alloys with Bayesian Optimization
The emergence of data-driven science has opened up new avenues for understanding the thermophysical properties of materials. For decades, alloys are known to possess very low thermal conductivity, but the extreme thermal conductivity can be achieved by alloying has never been identified. In this work, we combine the Bayesian optimization with a high throughput thermal conductivity calculation to search for the lowest thermal conductivity atomic configuration of $\rm{Si_{0.5}Ge_{0.5}}$ alloy. It is found layered structures are most beneficial for reducing the thermal conductivity among all atomic configurations, which is attributed to the strong branch-folding effect. Furthermore, the roles of interface roughness and layer thicknesses in producing the lowest thermal conductivity are investigated. Through another comprehensive search using Bayesian optimization, the layered structure with smooth interfaces and optimized layer thickness arrangement is identified as the optimal structure with the lowest thermal conductivity.
2004.08654v1
2020-05-26
Localization of electronic states resulting from electronic topological transitions in the Mo$_{1-x}$Re$_x$ alloys: A photoemission study
We present the results of resonant photoemission spectroscopy experiments on the Mo$_{1-x}$Re$_{x}$ alloy compositions spanning over two electronic topological transitions (ETT) at the critical concentrations $x_{C1}$ = 0.05 and $x_{C2}$ = 0.11. The photoelectrons show an additional resonance ($R3$) in the constant initial state (CIS) spectra of the alloys along with two resonances ($R1$ and $R2$) which are similar to those observed in molybdenum. All the resonances show Fano-like line shapes. The asymmetry parameter $q$ of the resonances $R1$ and $R3$ of the alloys is observed to be large and negative. Our analysis suggests that the origin of large negative q is associated with phonon assisted inter band scattering between the Mo-like states and the narrow band that appeared due to the ETT.
2005.12835v1
2020-05-26
Machine learning formation enthalpies of intermetallics
Developing fast and accurate methods to discover intermetallic compounds is relevant for alloy design. While density-functional-theory (DFT)-based methods have accelerated design of binary and ternary alloys by providing rapid access to the energy and properties of the stable intermetallics, they are not amenable for rapidly screening the vast combinatorial space of multi-principal element alloys (MPEAs). Here, a machine-learning model is presented for predicting the formation enthalpy of binary intermetallics and used to identify new ones. The model uses easily accessible elemental properties as descriptors and has a mean absolute error (MAE) of 0.025 eV/atom in predicting the formation enthalpy of stable binary intermetallics reported in the Materials Project database. The model further predicts stable intermetallics to form in 112 binary alloy systems that do not have any stable intermetallics reported in the Materials Project database. DFT calculations confirm one such stable intermetallic identified by the model, NbV2 to be on the convex hull. The model trained with binary intermetallics can also predict ternary intermetallics with similar accuracy as DFT, which suggests that it could be extended to identify compositionally complex intermetallics that may form in MPEAs.
2005.13046v1
2020-05-28
Robustness of helical magnetic structure under external pressure in Fe-doped MnNiGe alloy
We have investigated the detailed magnetic structure of a Fe-doped MnNiGe alloy of nominal composition MnNi$_{0.75}$Fe$_{0.25}$Ge by ambient and high pressure (6 kbar) neutron powder diffraction study. The alloy undergoes a martensitic phase transition between 230 K and 275 K. The low-temperature martensite phase orders antiferromagnetically with helical modulation of Mn-spins. At 1.5 K, the incommensurate propagation vector $\bf k$ is found to be (0.1790(1),0,0), and it remains almost unchanged with temperature under ambient condition. The Application of external pressure ($P$) reduces the martensitic transition temperature and results in a significant change in the incommensurate magnetic propagation vector. At 10 K, with 6 kbar of external pressure, the incommensurate magnetic structure of the alloy stabilizes with $\bf k$ = (0.1569(1),0,0). Interestingly, the strong temperature dependence of $\bf k$ in the presence of external $P$ has also been observed.
2005.13909v1
2020-05-28
A new high-throughput method using additive manufacturing for alloy design and heat treatment optimization
Many alloys made by Additive Manufacturing (AM) require careful design of post-heat treatment as an indispensable step of microstructure engineering to further enhance the performance. We developed a high-throughput approach by fabricating a long-bar sample heat-treated under a monitored gradient temperature zone for phase transformation study to accelerate the post-heat treatment development of AM alloys. This approach has been proven efficient in determining the aging temperature with peak hardness. We observed that the precipitation strengthening is predominant for the studied superalloy by laser powder bed fusion, and the grain size variation is insensitive on temperature between 605 and 825 Celcius. This new approach can be applied to post-heat treatment optimization of other materials made by AM, and further assist new alloy development.
2005.14092v2
2020-08-14
Atomistic study of grain-boundary segregation and grain-boundary diffusion in Al-Mg alloys
Mg grain boundary (GB) segregation and GB diffusion can impact the processing and properties of Al-Mg alloys. Yet, Mg GB diffusion in Al has not been measured experimentally or predicted by simulations. We apply atomistic computer simulations to predict the amount and the free energy of Mg GB segregation, and the impact of segregation on GB diffusion of both alloy components. At low temperatures, Mg atoms segregated to a tilt GB form clusters with highly anisotropic shapes. Mg diffuses in Al GBs slower than Al itself, and both components diffuse slowly in comparison with Al GB self-diffusion. Thus, Mg segregation significantly reduces the rate of mass transport along GBs in Al-Mg alloys. The reduced atomic mobility can be responsible for the improved stability of the microstructure at elevated temperatures.
2008.06145v2
2020-08-24
Enhancement of Spin-charge Conversion in Dilute Magnetic Alloys by Kondo Screening
We derive a kinetic theory capable of dealing both with large spin-orbit coupling and Kondo screening in dilute magnetic alloys. We obtain the collision integral non-perturbatively and uncover a contribution proportional to the momentum derivative of the impurity scattering S-matrix. The latter yields an important correction to the spin diffusion and spin-charge conversion coefficients, and fully captures the so-called side-jump process without resorting to the Born approximation (which fails for resonant scattering), or to otherwise heuristic derivations. We apply our kinetic theory to a quantum impurity model with strong spin-orbit, which captures the most important features of Kondo-screened Cerium impurities in alloys such as La$_{1-x}$Cu$_6$. We find 1) a large zero-temperature spin Hall conductivity that depends solely on the Fermi wave number and 2) a transverse spin diffusion mechanism that modifies the standard Fick's diffusion law. Our predictions can be readily verified by standard spin-transport measurements in metal alloys with Kondo impurities.
2008.10185v2
2021-03-23
Dark-bright excitons mixing in alloyed InGaAs self-assembled quantum dots
Quantum dots are arguably one of the best platforms for optically accessible spin based qubits. The paramount demand of extended qubit storage time can be met by using quantum-dot-confined dark exciton: a longlived electron-hole pair with parallel spins. Despite its name the dark exciton reveals weak luminescence that can be directly measured. The origins of this optical activity remain largely unexplored. In this work, using the atomistic tight-binding method combined with configuration-interaction approach, we demonstrate that atomic-scale randomness strongly affects oscillator strength of dark excitons confined in self-assembled cylindrical InGaAs quantum dots with no need for faceting or shape-elongation. We show that this process is mediated by two mechanisms: mixing dark and bright configurations by exchange interaction, and equally important appearance of non-vanishing optical transition matrix elements that otherwise correspond to nominally forbidden transitions in a non-alloyed case. The alloy randomness has essential impact on both bright and dark exciton states, including their energy, emission intensity, and polarization angle. We conclude that, due to the atomic-scale alloy randomness, finding dots with desired dark exciton properties may require exploration of a large ensemble, similarly to how dots with low bright exciton splitting are selected for entanglement generation.
2103.12356v1
2021-03-27
Structure-Composition-Property Relationships in Antiperovskite Nitrides: Guiding a Rational Alloy Design
The alloy strategy through A- or X-site is a common method for experimental preparation of high-performance and stable lead-based perovskite solar cells. As one of the important candidates for lead-free and stable photovoltaic absorber, the inorganic antiperovskite family has recently been reported to exhibit excellent optoelectronic properties. However, the current reports on the design of antiperovskite alloys are rare. In this work, we investigated the previously overlooked electronic property (e.g., conduction band convergence), static dielectric constant, and exciton binding energy in inorganic antiperovskite nitrides by first-principles calculations. Then, we reveal a linear relationship between tolerance factor and various physical quantities. Guided by the established structure-composition-property relationship in six antiperovskite nitrides X3NA (X2+ = Mg2+, Ca2+, Sr2+; A3- = P3-, As3-, Sb3-, Bi3-), for the first time, we design a promising antiperovskite alloy Mg3NAs0.5Bi0.5 with the quasi-direct band gap of 1.402 eV. Finally, we make a comprehensive comparison between antiperovskite nitrides and conventional halide perovskites for pointing out the future direction for device applications.
2103.14944v2
2022-03-01
Towards quantitative inference of nanoscale defects in irradiated metals and alloys
Quantifying the population of nanoscale defects that are formed in metals and alloys exposed to extreme radiation environments remains a pressing challenge in materials science. These defects both fundamentally alter material properties and seed long-timescale performance degradation, which often limits the lifespan of engineering systems. Unlike ceramic and semiconducting materials, these defects in metals and alloys are not spectroscopically active, forcing characterization to rely on indirect measurements from which the distribution of nanoscale defects may be inferred. In this mini-review, different experimental methodologies which have been employed for defect inference are highlighted to capture the current state of the art. Future directions in this area are proposed, which, by combining data streams from multiple and complementary characterization methods in concert with multi-scale modeling and simulation, will enable the ultimate goal of quantifying the full spectrum of defects in irradiated metals and alloys.
2203.00760v2
2022-03-12
Convolutional neural networks enable high-fidelity prediction of path-dependent diffusion barrier spectra in multi-principal element alloys
The emergent multi-principal element alloys (MPEAs) provide a vast compositional space to search for novel materials for technological advances. However, how to efficiently identify optimal compositions from such a large design space for targeted properties is a grand challenge in material science. Here we developed a convolutional neural network (CNN) model that can accurately and efficiently predict path-dependent vacancy migration energy barriers, which are critical to diffusion behaviors and many high-temperature properties, of MPEAs at any compositions and with different chemical short-range orders within a given alloy system. The success of the CNN model makes it promising for developing a database of diffusion barriers for different MPEA systems, which would accelerate alloy screening for the discovery of new compositions with desirable properties. Besides, the length scale of local configurations relevant to migration energy barriers is uncovered, and the implications of this success to other aspects of materials science are discussed.
2203.06503v3
2022-03-16
Simple machine-learned interatomic potentials for complex alloys
Developing data-driven machine-learning interatomic potentials for materials containing many elements becomes increasingly challenging due to the vast configuration space that must be sampled by the training data. We study the learning rates and achievable accuracy of machine-learning interatomic potentials for many-element alloys with different combinations of descriptors for the local atomic environments. We show that for a five-element alloy system, potentials using simple low-dimensional descriptors can reach meV/atom-accuracy with modestly sized training datasets, significantly outperforming the high-dimensional SOAP descriptor in data efficiency, accuracy, and speed. In particular, we develop a computationally fast machine-learned and tabulated Gaussian approximation potential (tabGAP) for Mo-Nb-Ta-V-W alloys with a combination of two-body, three-body, and a new simple scalar many-body density descriptor based on the embedded atom method.
2203.08458v2
2022-03-19
Multiscale simulation of powder-bed fusion processing of metallic alloys
We present a computational framework for the simulations of powder-bed fusion of metallic alloys, which combines: (1) CalPhaD calculations of temperature-dependent alloy properties and phase diagrams, (2) macroscale finite element (FE) thermal simulations of the material addition and fusion, and (3) microscopic phase-field (PF) simulations of solidification in the melt pool. The methodology is applied to simulate the selective laser melting (SLM) of an Inconel 718 alloy using realistic processing parameters. We discuss the effect of temperature-dependent properties and the importance of accounting for different properties between the powder bed and the dense material in the macroscale thermal simulations. Using a two-dimensional longitudinal slice of the thermal field calculated via FE simulations, we perform an appropriately-converged PF solidification simulation at the scale of the entire melt pool, resulting in a calculation with over one billion grid points, yet performed on a single cluster node with eight graphics processing units (GPUs). These microscale simulations provide new insight into the grain texture selection via polycrystalline growth competition under realistic SLM conditions, with a level of detail down to individual dendrites.
2203.10370v1