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train_100
What is described in this image?
Figure 1. 1H NMR spectra of MIC (A) and UPy (B) in DMSO-d6.
train_101
What is described in this image?
FIG. 7. TEM images of graphene oxide-epoxy nanocomposites at 0.5% GO loading (a) at low and (b) high magnification.
train_102
What is described in this image?
Fig. 12.3 Schematic representation of TLC chamber
train_103
What is described in this image?
Table 3 Peak temperatures at various heating rates of peak 1 and peak 2 in SLM built sample DSC scans.
train_104
What is described in this image?
Fig. 6. MDSC traces of Liprol™ 270-MDI PU and Liprol™ 320-MDI PU.
train_105
What is described in this image?
Table 2 Chemical composition of investigated glass (wt%).
train_106
What is described in this image?
Fig. 1 e The ionic conductivity of polymer electrolytes with different weight fraction of BmImBr.
train_107
What is described in this image?
Table 1 Phase transition temperatures, hysteresis and optical properties
train_108
What is described in this image?
Table 1. Processing parameters used for PHB extrusion and injection.
train_109
What is described in this image?
Table 2 Percentage of reacted and unreacted OH groups on the diols
train_110
What is described in this image?
Fig. 3. X-Ray powder diffraction pattern of two Ga2O3 films annealed at 900 C in O2 or N2 flow (samples 146g5 and 146g6 in Table 1).
train_111
What is described in this image?
FIG. 2. (a) Thermopower (α) peak in Cu2Se (blue circles) and Cu1.97Ag.03Se (green squres). The increase in thermopower, shown with a critical exponent fit, is clearly associated with the continuous phase transition. Between 390 K and 410 K, there is a significant increase in the measured thermopower above that predicte...
train_112
What is described in this image?
Figure 10. Effect of heating rate on the glass transition temperature and relaxation time as functions of annealing time. (A) Experimentally observed (DSC onset) Tg. (B) Simulation based prediction (Tg*, eq 8). (C) Evolution of relaxation time during heating at 2 °C/min, as a function of annealing time. (D) Evolution o...
train_113
What is described in this image?
Figure 5. Double logarithmic plot of the conversion C vs. time curves above tc for (a) TXþNMDEA, (b) TX-OCH2COOH, and (c) TX-SCH2COOH photoinitiators, respectively. The exponents were determined from the slope of the straight lines.
train_114
What is described in this image?
Figure 3. Temperature for the tan δ peak positions (Tg1 andTg2) versus the logarithm of frequency.
train_115
What is described in this image?
Table 3 Interatomic distance r, temperature factor b, and the number of interactions n of models obtained by the least-squares fits in Fig. 7 for water in Ph-PMO, together with those for water confined in MCM-41 C14 [5]. The estimated standard deviations in r and n are ±0.01 Å and ±0.2, respectively.
train_116
What is described in this image?
Table 1. Curing Characteristics of Samples Containing the Different Loadings of ESO
train_117
What is described in this image?
Fig. 9 Infrared spectra of felodipine/PVP/VA solid dispersion showing (a) the NH stretching region (3150–3450 cm 1) and (b) the carbonyl stretching region (1550–1800 cm 1). Percentages represent the weight percentage of PVP/VA in the solid dispersion.
train_118
What is described in this image?
Fig. 3. Stressestrain curves for polyurethane films from different vegetable oil polyols.
train_119
What is described in this image?
Fig. 2—(a) Fe-C equilibrium diagram with the critical carbon range between 0.09 and 0.17 wt pctC, and (b) influence of alloying elements on the Fe-C system.
train_120
What is described in this image?
Table 4 Experimentally measured specific heat values (heating).
train_121
What is described in this image?
Figure 2. Flash DSC heating scans demonstrating the calculation of the limiting fictive temperature (Tf′) for the 160 nm thick film on Krytox oil (top) and the 71 nm thick film on Krytox oil (bottom); the scans were performed on heating at 800 K/s after cooling at either 0.1 and 100 K/s. Curves were rotated to be horiz...
train_122
What is described in this image?
Fig. 3. 3D AFM micrographs with RMS roughness of starch bioplastic (A) Starch bioplastic (160 X), (B) Starch Bioplastic (1800 X), (C) Presence of granules (650 X), (D) Presence of void (1600 X), (E)–(F) Presence of crack (6500 X).
train_123
What is described in this image?
FIG. 2. The reaction mechanism for synthesis of smart polymers. Color images available online at www.liebertpub.com/tec
train_124
What is described in this image?
Table 1 Glass transition temperatures (Tg) of NaxEMIm(1 x)TFSI and NaxBMIm(1 x)TFSI for molar fractions x ¼ 0, 0.1, 0.2, and Sat (saturated sample).
train_125
What is described in this image?
Table 1 Dynamic parameters of DPPC in absence and presence of NBD-PC
train_126
What is described in this image?
Fig. 2. X-ray diffraction patterns of ZrW2O8 at 25, 150 and 2208C. Both the patterns at 25 and 1508C can be indexed as cubic symmetry. The pattern at 2208C can also be indexed as cubic symmetry, however, several peaks such as 111, 221, 310 and so on disappear.
train_127
What is described in this image?
Fig. 10. Material properties use
train_128
What is described in this image?
Fig. 2. The DSC thermograms during cooling process for HL lignite with different moisture contents of: (a) 50.22%; (b) 42.37%; (c) 40.16%; (d) 37.49%; (e) 33.13%; (f) 31.93%; (g) 30.92%; (h) 29.56%; (i) 27.84%; (j) 27.63%; (k) 24.55%; (l) 21.16%; (m) 17.42%.
train_129
What is described in this image?
FIG. 6. Square root of the transition width of the thermal glass transition versus Tg.
train_130
What is described in this image?
Fig. 7. OTP heat capacity measured by FDSC at different scanning rates.
train_131
What is described in this image?
Fig. 6. Evaluation of the specific heat of a pharmaceutical sample run in a pan with a pierced lid. Curve a: original total heat flow; curve b: baseline corrected heat flow; curve c: remnant water content in the sample; curve d: apparent specific heat; curve e: specific heat of the dry sample.
train_132
What is described in this image?
Fig. 5. Alternating DSC scan (Mettler±Toledo STARe system) through the glass-transition region of a fully cured epoxy resin of sample mass 20.15 mg using the following conditions: qav 18C/min; AT 18C; and per 1 min [28].
train_133
What is described in this image?
Table 2 Characteristic temperatures of phase transitions of investigated steel grades obtained during heating and calculated making use of FactSage software
train_134
What is described in this image?
Figure 1. (a) Schematics of the fabrication of the PMMA/DCNTA nanocomposite. (b) Pictures of pristine CNTA and DCNTA. SEM images of the pristine CNT array (c) and PMMA/DCNTA (d). The Mw of PMMA is 15 kg/mol, and the scale bar is 1 μm.
train_135
What is described in this image?
Table 2 WAXD and DSC data of non-equimolar PLLA/PDLA blends prepared by low temperature approach at processing temperature of 160 C.a
train_136
What is described in this image?
Table 1. Gel Times at 25°C and reactivity of resins activated (0.5% Cobalt octoate) e catalyzed with MEKP and AAP (1%) in presence or not of the inhibitor (0.5%)
train_137
What is described in this image?
Fig. 2. The schematic diagram of the thermal conductivity test.
train_138
What is described in this image?
Fig. 8. Melting peak temperatures of neat POM and POM samples containing 1.4, 3.4, 4.5 and 5.4 mass% of dioxalane at a heating rate of 150 ◦C/min after various cooling rates (from 5 to 300 ◦C/min): (a) uncorrected data and (b) data ( k
train_139
What is described in this image?
Table 2 Antibacterial activity of polysaccharides from olive leaves.
train_140
What is described in this image?
Fig. 2. From left to right, the pictures taken at room temperature for lactic acid (melting point 326 K), lactic acid:choline chloride at molar ratio 2:1 (melting point 206 K) and choline chloride (decomposition temperature 575 K).
train_141
What is described in this image?
Fig. 5. Fractography images of: (a) TAGS-80, (b) TAGS-85, and (c) Ge0.87Pb0.13Te + 3% Bi2Te3, following mechanical compression testing.
train_142
What is described in this image?
Figure 6. (a) UV vis diffuse reflectance spectra and (b) PL spectra of h-MoO3 hexagonal prisms and a-MoO3 nanoplate-based rods.
train_143
What is described in this image?
Figure 5 FTIR-PAS spectrum of carbonyl band in PLA : PS 50 : 50 blend.
train_144
What is described in this image?
Fig. 5. The stability assessment of lutein, LPP and LPTP in the dark at 80 C (A), under UV light at 25 C (B) and in flowing oxygen in the dark at 25 C (C).
train_145
What is described in this image?
Figure 8. Crystal growth rate corrected for thermodynamic driving force, plotted against the undercooled melt viscosity in a log−log format for a subset of the compounds.
train_146
What is described in this image?
Figure 12. Schematic of the melting and crystallization rates as a function of supercooling and superheating. The equilibrium melting temperature is Tm.
train_147
What is described in this image?
Figure 9. Weight loss of treated PLA and plasticized PLA with: (a) PLA/TEC; (b) PLA/ATBC at various concentrations after heating at 100 °C and 135 °C.
train_148
What is described in this image?
Fig. 2. MALDI-TOF spectrum of methoxylated soybean oil polyol.
train_149
What is described in this image?
Figure 4. Through-plane small-angle X-ray scattering profiles of PIL (a) block and (b) random copolymers (containing TFSI counteranions). Numbers on graph correspond to PIL composition (mol %). Data in (a) are vertically offset for clarity.
train_150
What is described in this image?
FIG. 1 (color online). Top: Schematic representation of the glass-transition temperature gradient in the vicinity of a particle, with a cutoff at Tmax g . The volume Vimm represents the immobilized protons at the surface of the particle, corresponding to a thickness e0, Vg the volume on which the Tg gradient is applied...
train_151
What is described in this image?
Table 2. Lattice parameters for ‘as-received’ and ‘retrieved’ NiTi wires.
train_152
What is described in this image?
Fig. 1. Structures of (A) DPPC, (B) C6-NBD-PC and (C) C12-NBD
train_153
What is described in this image?
Fig. 3. TGA analysis of PMMA/paraffin microcapsules, paraffin and PMMA.
train_154
What is described in this image?
Figure 14. DSC traces of PU obtained by polymerization of HMODAz (5/5′) derived from methyl oleate (run 4 (vii), Table 1), PU obtained by polymerization of HODEAz (8) derived from ricinoleic acid (run 9, Table 1), and PU obtained by polymerization of MHHDC (10) derived from ricinoleic acid (run 2, Table 2).
train_155
What is described in this image?
Fig. 7. Melting point depression T for 18.2 nm CPG from DSC heating scans at 0.05 K/min as a function of the water-to-CPG ratio. The symbols are for Tpk ( ), Ton ( ), and Ton-pk ( ) methods.
train_156
What is described in this image?
Table 3 Calculated theoretical reaction enthalpy.
train_157
What is described in this image?
Figure 3. Differential scanning calorimetry curves of hydroxyapatite, showing the endo- and exothermic peaks at onset temperatures of 480.0 ± 0.3 K during heating and cooling, respectively. Note that the temperature at which the heat anomaly was observed agreed well with that at which the superstructure reflection disa...
train_158
What is described in this image?
TABLE 2 Parameters of the Relaxation Model, Evaluated from the T1 Temperature Dependence in the Solid Phases of 5CB
train_159
What is described in this image?
Fig. 7. DSC curves of the nanocomposites.
train_160
What is described in this image?
Fig. 10. (a) Representative adhesive Araldite® 2015 tensile stress–strain curves after different exposure time; (b) Normalized mechanical properties as a function of exposure time.
train_161
What is described in this image?
Fig. 3. Second derivative of amide A band from FTIR spectra of films based on mixtures of fish gelatin (G) and lignin (L1000 and L2400) at the ratio 85% gelatin: 15% lignin (w/w). Single gelatin film, G; compound films with lignin, GeL1000 and GeL2400.
train_162
What is described in this image?
Figure 7. Deconvolution of DSC profile into the duplicated melting or crystallization contributions indicated by different lines for the nucleation-crystallized sample. The observed and fitted profiles are represented by solid and dotted lines.
train_163
What is described in this image?
Fig. 6. CD spectra of RL9 (A), RW9 (B) and R9 (C) in 10 mM sodium phosphate buffer (solid line), DMPC LUVs (hatched line) and DMPG (dotted line) at P/L ratio of 1/25 measured at 20 °C.
train_164
What is described in this image?
Figure 8. Boson peak frequency ωbos plots as a function of temperature for the (TeO2)0.7(ZnO)0.3 glass with (full symbols) and without (open symbols) subtraction of the quasi-elastic scattering component. The inset shows a plot of the frequency ωmin as a function of temperature for the (TeO2)0.7(ZnO)0.3 glass, where ωm...
train_165
What is described in this image?
Table 1 shows the glycosidic linkage composition of the three alactomannans. Partially methylated alditol acetates analyzed by C/MS revealed a polysaccharide containing nonreducing terminal nits of Manp (0.35%, 0.30% and 0.13%) and Galp (17.23%, 20.92% nd 34.02%) as well as 4-Manp (59.15%, 53.18% and 24.73%), 4,6- anp ...
train_166
What is described in this image?
Fig. 4. DSC thermogram at a heating rate of 10 C/min.
train_167
What is described in this image?
Fig. 7 WAXD curves of AnP3, AnP3P, AnP4 and AnP4P: (a) pressed sample; (b) annealed sample; (c) pressed sample; (d) annealed sample.
train_168
What is described in this image?
Fig. 8. Temperature evolution of experimental infrared spectra.
train_169
What is described in this image?
Figure 3. FTIR spectra of (a) eda600, (b) uncured poly(BA-eda600), (c) poly(BA-eda600) cured at 150 C for 2 h, and (d) poly(BA-eda600) cured at 180 C for 2 h.
train_170
What is described in this image?
Table 2a List of infrared wave numbers and vibrational mode for PEO, LiCF3SO3 and EC.
train_171
What is described in this image?
Table 2. VFT Fit Parameters for The Temperature Dependence of τs
train_172
What is described in this image?
Fig. 14. Comparison of dissolution profiles of ITZ HMEs and PMs using various polymers – (a) ITZ HMEs and PMs (30:70) in SGF, (b) ITZ HMEs and PMs (50:50) in SGF, (c) ITZ HMEs (30:70) in SIF and (d) ITZ HMEs (50:50) in SIF. No release of ITZ was observed from pure ITZ sample and PMs of ITZ in SIF.
train_173
What is described in this image?
Fig. 7.2 Schematic representation of emission spectra in atomic emission spectroscopy
train_174
What is described in this image?
Fig. 1. Plots of conductivity and viscosity with LiBOB concentration.
train_175
What is described in this image?
Table 1 Particle sizes and DSC peaks for VO2 nanobumps.
train_176
What is described in this image?
Fig. 8. Comparison of CO2/N2 separation performance of polyurethane–silica nanocomposite membranes with Robeson’s upper bound line.
train_177
What is described in this image?
Fig. 6. Backscattered electron images of the FeCoNi(CuAl)0.8 alloys: (a) as-cast; (b) annealed at 573 K; (c) annealed at 623 K; (d) annealed at 673 K.
train_178
What is described in this image?
Table 2: Technical specifications of Differential scanning calorimetry
train_179
What is described in this image?
Fig. 3. DSC curves of PHB/soda lignin.
train_180
What is described in this image?
Table 4 Transformation characteristics determined after deconvolution.
train_181
What is described in this image?
Table 1 Compositional dependence of crystallization parameters Tc , Tg , Tm , (Tc − Tg) and crystallization enthalpy ( Hc) of Ga15Se85−xAgx from non-isothermal DSC experiments at a heating rate of 15 K/min.
train_182
What is described in this image?
Figure 11. Kissinger analysis on Tpa on reheating.
train_183
What is described in this image?
Fig. 10. Comparison of the residual tensile strength variation with temperature reported here and that reported by Bai and Keller [8] and Robert and Benmokrane [9].
train_184
What is described in this image?
Fig. 4. DSC curves of MMG samples.
train_185
What is described in this image?
Fig. 7. Relative concentrations of the four binders at 318.15 K (45 °C): (a) OX direction; (b) OY direction.
train_186
What is described in this image?
Fig. 6 Views of Si sample after DSC test: a photograph of solidified Si sample connected with alumina lid (upside down position of the lid), b 3D-CT image of alumina crucible coated with h-BN spray and covered with uncoated alumina lid showing Si drop solidified on the lid
train_187
What is described in this image?
Fig. 5 The thermogram of pure SOPC sample
train_188
What is described in this image?
Fig. 1. Temperature dependence of the heat ¯ow of a DGEBA/ DDM network containing 20 wt% PES after di erent curing times at 373 K (heating rate: 10 K/min) measured by conventional DSC. The curing times are 0 min (sample weight: 27.9 mg), 30 min (sample weight: 27.1 mg), 60 min (sample weight: 37.7 mg) and 200 min (samp...
train_189
What is described in this image?
Table 9 Fit parameters of the DSCN(T) for experimental curves of 6 mg of PHBVH after calibration at the onset for the given sample mass and rate (the error margins are from the nonlinear fitting), *nonlinear least squares error out of the bounds due to indeterminate high α value
train_190
What is described in this image?
Fig. 3. Tensile properties as a function of PC/PLA wt. ratio; compared with neat PLA and PC.
train_191
What is described in this image?
Fig. 7. Food-mass based latent heat obtained during P-scan tests as compared to the reference data of pure water from Bridgman (1912).
train_192
What is described in this image?
Figure 1. Chemical structures of azo-arm compounds.
train_193
What is described in this image?
FIG. 3. Temperature dependences of lattice parameters of Aurivillius compounds: Bi5Ti3FeO15 a ; Bi6Ti3Fe2O18 b ; the tetragonal phase of Bi5Ti3FeO15 c ; and the tetragonal phase of Bi6Ti3Fe2O18 d . The data of tetragonal phases are represented as 2atet and 2Vtet for comparison.
train_194
What is described in this image?
Fig. 11. (a) The Ti–Ni binary phase diagram; (b) Schematic illustration of phase transformations between austenite and martensite upon loading and unloading, and heating and cooling.
train_195
What is described in this image?
Fig. 7 TGA of epoxy/POSS composites with different inorganic contents at 10 °C/min in a nitrogen atmosphere
train_196
What is described in this image?
Table 2 Color properties and transmittance of films.
train_197
What is described in this image?
Table 1 List of ATR-FTIR vibrational modes of CMC and PVA.
train_198
What is described in this image?
Fig. 5. Temperature dependencies of the relative Gibbs free energy curves for the three modifications solid x1, solid x2, and liquid phase.
train_199
What is described in this image?
Fig. 9. Temperature evolution of experimental spectra-correlations (X axis-temperature [K], Y-axis-wavenumbers (cm 1), gray rectangle – area of phase transition).