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stringlengths
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stringlengths
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stringclasses
11 values
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stringlengths
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38
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17 values
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stringlengths
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244
10.1002_ejoc.201701463
[Sn](c1ccc(OC)cc1)(CCCC)(CCCC)CCCC
3
3
[0.42418137 0.59140627 0.57109837 0.63515626]
[0.09444664 0.66171881 0.90359469 0.70000003]
13C NMR
151 MHz
CDCl3
158.8 , 133.6 , 127.9 , 114.3 , 55.5 , 29.3 , 26.8 , 16.6 , 13.7
null
[(158.8, None, None), (133.6, None, None), (127.9, None, None), (114.3, None, None), (55.5, None, None), (29.3, None, None), (26.8, None, None), (16.6, None, None), (13.7, None, None)]
19
9
9
10.1002_ejoc.201701463
[N+](c1ccc([Sn](CCCC)(CCCC)CCCC)cc1)(=O)[O-]
4
4
[0.42197211 0.10058595 0.57330763 0.14726564]
[0.09499895 0.17402344 0.90249011 0.21269532]
1H NMR
600 MHz
CDCl3
8.13 (d, J = 8.5 Hz, 2H), 7.64 (d, J = 8.5 Hz, 2H), 1.58-1.50 (m, 6H), 1.36-1.31 (m, 6H), 1.17-1.07 (m, 6H), 0.89 (t, J = 7.3 Hz, 9H)
null
[('d', ['8.5Hz'], '2H', 8.13, 8.13), ('d', ['8.5Hz'], '2H', 7.64, 7.64), ('m', [], '6H', 1.58, 1.5), ('m', [], '6H', 1.36, 1.31), ('m', [], '6H', 1.17, 1.07), ('t', ['7.3Hz'], '9H', 0.89, 0.89)]
31
6
31
10.1002_ejoc.201701463
[N+](c1ccc([Sn](CCCC)(CCCC)CCCC)cc1)(=O)[O-]
4
4
[0.42197211 0.10058595 0.57330763 0.14726564]
[0.09499895 0.17402344 0.90249011 0.21269532]
13C NMR
151 MHz
CDCl3
153.5 , 148.3 , 137.2 , 122.1 , 29.1 , 27.4 , 13.8 , 10.0
null
[(153.5, None, None), (148.3, None, None), (137.2, None, None), (122.1, None, None), (29.1, None, None), (27.4, None, None), (13.8, None, None), (10.0, None, None)]
18
8
8
10.1002_ejoc.201701463
[Sn](c1ccccc1C)(CCCC)(CCCC)CCCC
4
4
[0.44516952 0.3902344 0.55121485 0.44414065]
[0.09389432 0.47031252 0.90249011 0.50781254]
1H NMR
600 MHz
CDCl3
7.40 (d, J = 8.3 Hz, 1H), 7.20 (dd, J = 17.3, 6.6 Hz, 2H), 7.14 (t, J = 7.5 Hz, 1H), 2.40 (s, 3H), 1.58-1.49 (m, 6H), 1.37-1.31 (m, 6H), 1.14-1.03 (m, 6H), 0.90 (t, J = 7.3 Hz, 9H)
null
[('d', ['8.3Hz'], '1H', 7.4, 7.4), ('dd', ['17.3Hz', '6.6Hz'], '2H', 7.2, 7.2), ('t', ['7.5Hz'], '1H', 7.14, 7.14), ('s', [], '3H', 2.4, 2.4), ('m', [], '6H', 1.58, 1.49), ('m', [], '6H', 1.37, 1.31), ('m', [], '6H', 1.14, 1.03), ('t', ['7.3Hz'], '9H', 0.9, 0.9)]
34
9
34
10.1002_ejoc.201701463
[Sn](c1ccccc1C)(CCCC)(CCCC)CCCC
4
4
[0.44516952 0.3902344 0.55121485 0.44414065]
[0.09389432 0.47031252 0.90249011 0.50781254]
13C NMR
151 MHz
CDCl3
144.8 , 142.2 , 136.7 , 129.0 , 128.4 , 125.0 , 29.3 , 27.5 , 25.2 , 13.8 , 10.2
null
[(144.8, None, None), (142.2, None, None), (136.7, None, None), (129.0, None, None), (128.4, None, None), (125.0, None, None), (29.3, None, None), (27.5, None, None), (25.2, None, None), (13.8, None, None), (10.2, None, None)]
19
11
11
10.1002_ejoc.201701463
[Sn](c1csc(C=O)c1)(CCCC)(CCCC)CCCC
4
4
[0.43025691 0.71171878 0.56502284 0.76171882]
[0.09389432 0.78828129 0.90359469 0.82734379]
1H NMR
600 MHz
CDCl3
9.99 (s, 1H), 7.79 (s, 1H), 7.72 (s, 1H), 1.54 (p, J = 7.8 Hz, 6H), 1.33 (q, J = 7.4 Hz, 6H), 1.14-1.05 (m, 6H), 0.89 (t, J = 7.3 Hz, 9H)
null
[('s', [], '1H', 9.99, 9.99), ('s', [], '1H', 7.79, 7.79), ('s', [], '1H', 7.72, 7.72), ('p', ['7.8Hz'], '6H', 1.54, 1.54), ('q', ['7.4Hz'], '6H', 1.33, 1.33), ('m', [], '6H', 1.14, 1.05), ('t', ['7.3Hz'], '9H', 0.89, 0.89)]
30
7
30
10.1002_ejoc.201701463
[Sn](c1csc(C=O)c1)(CCCC)(CCCC)CCCC
4
4
[0.43025691 0.71171878 0.56502284 0.76171882]
[0.09389432 0.78828129 0.90359469 0.82734379]
13C NMR
151 MHz
CDCl3
183.4 , 144.8 , 143.1 , 141.4 , 140.8 , 29.1 , 27.4 , 13.8 , 10.4
null
[(183.4, None, None), (144.8, None, None), (143.1, None, None), (141.4, None, None), (140.8, None, None), (29.1, None, None), (27.4, None, None), (13.8, None, None), (10.4, None, None)]
17
9
9
10.1002_ejoc.201701463
[Sn](c1ccc(C=O)s1)(CCCC)(CCCC)CCCC
5
5
[0.42307674 0.26171877 0.572203 0.29453127]
[0.09389432 0.32128906 0.90359469 0.36113284]
1H NMR
600 MHz
CDCl3
9.94 (s, 1H), 7.84 (d, J = 3.5 Hz, 1H), 7.26 (s, 1H), 1.60-1.54 (m, 6H), 1.34 (d, J = 7.3 Hz, 6H), 1.21-1.12 (m, 6H), 0.90 (t, J = 7.4 Hz, 9H)
null
[('s', [], '1H', 9.94, 9.94), ('d', ['3.5Hz'], '1H', 7.84, 7.84), ('s', [], '1H', 7.26, 7.26), ('m', [], '6H', 1.6, 1.54), ('d', ['7.3Hz'], '6H', 1.34, 1.34), ('m', [], '6H', 1.21, 1.12), ('t', ['7.4Hz'], '9H', 0.9, 0.9)]
30
7
30
10.1002_ejoc.201701463
[Sn](c1ccc(C=O)s1)(CCCC)(CCCC)CCCC
5
5
[0.42307674 0.26171877 0.572203 0.29453127]
[0.09389432 0.32128906 0.90359469 0.36113284]
13C NMR
151 MHz
CDCl3
182.1 , 149.3 , 136.8 , 136.3 , 29.0 , 27.3 , 13.8 , 11.2
null
[(182.1, None, None), (149.3, None, None), (136.8, None, None), (136.3, None, None), (29.0, None, None), (27.3, None, None), (13.8, None, None), (11.2, None, None)]
17
9
8
10.1002_ejoc.201701463
[Sn](c1ccc(C(C)=O)cc1)(CCCC)(CCCC)CCCC
5
5
[0.42141977 0.66171881 0.5749646 0.71875007]
[0.09389432 0.74453126 0.90138543 0.78125007]
1H NMR
600 MHz
CDCl3
7.87 (d, J = 8.1 Hz, 2H), 7.58 (d, J = 8.1 Hz, 2H), 2.59 (s, 3H), 1.60-1.48 (m, 6H), 1.36-1.30 (m, 6H), 1.15-1.03 (m, 6H), 0.89 (t, J = 7.3 Hz, 9H)
null
[('d', ['8.1Hz'], '2H', 7.87, 7.87), ('d', ['8.1Hz'], '2H', 7.58, 7.58), ('s', [], '3H', 2.59, 2.59), ('m', [], '6H', 1.6, 1.48), ('m', [], '6H', 1.36, 1.3), ('m', [], '6H', 1.15, 1.03), ('t', ['7.3Hz'], '9H', 0.89, 0.89)]
34
7
34
10.1002_ejoc.201701463
[Sn](c1ccc(C(C)=O)cc1)(CCCC)(CCCC)CCCC
5
5
[0.42141977 0.66171881 0.5749646 0.71875007]
[0.09389432 0.74453126 0.90138543 0.78125007]
13C NMR
151 MHz
CDCl3
198.7 , 150.4 , 136.8 , 127.2 , 29.2 , 27.5 , 26.7 , 13.8 , 9.8
null
[(198.7, None, None), (150.4, None, None), (136.8, None, None), (127.2, None, None), (29.2, None, None), (27.5, None, None), (26.7, None, None), (13.8, None, None), (9.8, None, None)]
20
10
9
10.1002_ejoc.201701463
[Sn](c1cccc([N+](=O)[O-])c1)(CCCC)(CCCC)CCCC
6
6
[0.44572186 0.10039063 0.55121485 0.16484376]
[0.09389432 0.19082033 0.90249011 0.22910157]
1H NMR
600 MHz
CDCl3
8.29 (s, 1H), 8.12 (d, J = 9.1 Hz, 1H), 7.76 (d, J = 7.1 Hz, 1H), 7.48 (t, J = 7.7 Hz, 1H), 1.54 (p, J = 8.3 Hz, 6H), 1.34 (q, J = 7.3 Hz, 6H), 1.18-1.08 (m, 6H), 0.89 (t, J = 7.3 Hz, 9H)
null
[('s', [], '1H', 8.29, 8.29), ('d', ['9.1Hz'], '1H', 8.12, 8.12), ('d', ['7.1Hz'], '1H', 7.76, 7.76), ('t', ['7.7Hz'], '1H', 7.48, 7.48), ('p', ['8.3Hz'], '6H', 1.54, 1.54), ('q', ['7.3Hz'], '6H', 1.34, 1.34), ('m', [], '6H', 1.18, 1.08), ('t', ['7.3Hz'], '9H', 0.89, 0.89)]
31
8
31
10.1002_ejoc.201701463
[Sn](c1cccc([N+](=O)[O-])c1)(CCCC)(CCCC)CCCC
6
6
[0.44572186 0.10039063 0.55121485 0.16484376]
[0.09389432 0.19082033 0.90249011 0.22910157]
13C NMR
151 MHz
CDCl3
147.9 , 145.1 , 142.6 , 130.6 , 128.6 , 123.1 , 29.1 , 27.4 , 13.8 , 10.0
null
[(147.9, None, None), (145.1, None, None), (142.6, None, None), (130.6, None, None), (128.6, None, None), (123.1, None, None), (29.1, None, None), (27.4, None, None), (13.8, None, None), (10.0, None, None)]
18
10
10
10.1002_ejoc.201701463
[Sn](c1cccc2ccccc12)(CCCC)(CCCC)CCCC
6
6
[0.44572186 0.50625001 0.55066256 0.56250004]
[0.09278968 0.58945315 0.90028075 0.62617192]
1H NMR
600 MHz
CDCl3
7.86-7.85 (m, 1H), 7.81 (d, J = 8.1 Hz, 1H), 7.78 (d, J = 8.0 Hz, 1H), 7.64 (d, J = 7.8 Hz, 1H), 7.49 (td, J = 6.4, 2.6 Hz, 2H), 7.44 (dd, J = 8.1, 6.6 Hz, 1H), 1.58 (dddd, J = 10.6, 8.4, 7.4, 5.8 Hz, 6H), 1.35 (q, J = 7.3 Hz, 6H), 1.25-1.18 (m, 6H), 0.89 (t, J = 7.3 Hz, 9H)
null
[('m', [], '1H', 7.86, 7.85), ('d', ['8.1Hz'], '1H', 7.81, 7.81), ('d', ['8.0Hz'], '1H', 7.78, 7.78), ('d', ['7.8Hz'], '1H', 7.64, 7.64), ('td', ['6.4Hz', '2.6Hz'], '2H', 7.49, 7.49), ('dd', ['8.1Hz', '6.6Hz'], '1H', 7.44, 7.44), ('dddd', ['10.6Hz', '8.4Hz', '7.4Hz', '5.8Hz'], '6H', 1.58, 1.58), ('q', ['7.3Hz'], '6H', ...
34
11
34
10.1002_ejoc.201701463
[Sn](c1cccc2ccccc12)(CCCC)(CCCC)CCCC
6
6
[0.44572186 0.50625001 0.55066256 0.56250004]
[0.09278968 0.58945315 0.90028075 0.62617192]
13C NMR
151 MHz
CDCl3
143.1 , 139.1 , 135.2 , 133.8 , 130.3 , 129.0 , 128.6 , 126.0 , 125.8 , 125.5 , 29.3 , 27.5 , 13.8 , 10.5
null
[(143.1, None, None), (139.1, None, None), (135.2, None, None), (133.8, None, None), (130.3, None, None), (129.0, None, None), (128.6, None, None), (126.0, None, None), (125.8, None, None), (125.5, None, None), (29.3, None, None), (27.5, None, None), (13.8, None, None), (10.5, None, None)]
22
14
14
10.1002_ejoc.201701463
CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1c(C(OCC)=O)cccc1
6
7
[0.43357079 0.85781251 0.56226124 0.91718754]
[0.093342 0.06982422 0.90028075 0.10654297]
1H NMR
600 MHz
CDCl3
8.10 (dd, J = 7.8, 1.3 Hz, 1H), 7.65 (dd, J = 7.2, 1.4 Hz, 1H), 7.48 (td, J = 7.3, 1.3 Hz, 1H), 7.37 (td, J = 7.5, 1.4 Hz, 1H), 4.37 (q, J = 7.1 Hz, 2H), 1.49 (dddd, J = 8.8, 7.9, 6.8, 3.5 Hz, 6H), 1.40 (t, J = 7.1 Hz, 3H), 1.34-1.29 (m, 6H), 1.11-1.00 (m, 6H), 0.87 (t, J = 7.3 Hz, 9H)
null
[('dd', ['7.8Hz', '1.3Hz'], '1H', 8.1, 8.1), ('dd', ['7.2Hz', '1.4Hz'], '1H', 7.65, 7.65), ('td', ['7.3Hz', '1.3Hz'], '1H', 7.48, 7.48), ('td', ['7.5Hz', '1.4Hz'], '1H', 7.37, 7.37), ('q', ['7.1Hz'], '2H', 4.37, 4.37), ('dddd', ['8.8Hz', '7.9Hz', '6.8Hz', '3.5Hz'], '6H', 1.49, 1.49), ('t', ['7.1Hz'], '3H', 1.4, 1.4), (...
36
10
36
10.1002_ejoc.201701463
CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1c(C(OCC)=O)cccc1
6
7
[0.43357079 0.85781251 0.56226124 0.91718754]
[0.093342 0.06982422 0.90028075 0.10654297]
13C NMR
151 MHz
CDCl3
168.75 , 147.23 , 137.14 , 135.93 , 131.76 , 129.75 , 128.00 , 61.30 , 29.35 , 27.60 , 14.53 , 13.86 , 11.24
null
[(168.75, None, None), (147.23, None, None), (137.14, None, None), (135.93, None, None), (131.76, None, None), (129.75, None, None), (128.0, None, None), (61.3, None, None), (29.35, None, None), (27.6, None, None), (14.53, None, None), (13.86, None, None), (11.24, None, None)]
21
13
13
10.1002_ejoc.201701463
[Sn](c1cccc(C(=O)OCC)c1)(CCCC)(CCCC)CCCC
7
7
[0.44185558 0.36171876 0.55342416 0.43164066]
[0.09389432 0.45781253 0.90249011 0.49531254]
1H NMR
600 MHz
CDCl3
8.14 (s, 1H), 7.96 (d, J = 7.8 Hz, 1H), 7.64 (d, J = 7.1 Hz, 1H), 7.38 (t, J = 7.5 Hz, 1H), 4.38 (q, J = 7.1 Hz, 2H), 1.59-1.50 (m, 6H), 1.40 (t, J = 7.1 Hz, 3H), 1.33 (q, J = 7.4 Hz, 6H), 1.14-1.04 (m, 6H), 0.89 (t, J = 7.3 Hz, 9H)
null
[('s', [], '1H', 8.14, 8.14), ('d', ['7.8Hz'], '1H', 7.96, 7.96), ('d', ['7.1Hz'], '1H', 7.64, 7.64), ('t', ['7.5Hz'], '1H', 7.38, 7.38), ('q', ['7.1Hz'], '2H', 4.38, 4.38), ('m', [], '6H', 1.59, 1.5), ('t', ['7.1Hz'], '3H', 1.4, 1.4), ('q', ['7.4Hz'], '6H', 1.33, 1.33), ('m', [], '6H', 1.14, 1.04), ('t', ['7.3Hz'], '9...
36
10
36
10.1002_ejoc.201701463
[Sn](c1cccc(C(=O)OCC)c1)(CCCC)(CCCC)CCCC
7
7
[0.44185558 0.36171876 0.55342416 0.43164066]
[0.09389432 0.45781253 0.90249011 0.49531254]
13C NMR
151 MHz
CDCl3
167.3 , 142.6 , 141.0 , 137.4 , 129.8 , 129.2 , 127.8 , 61.0 , 29.2 , 27.5 , 14.5 , 13.8 , 9.8
null
[(167.3, None, None), (142.6, None, None), (141.0, None, None), (137.4, None, None), (129.8, None, None), (129.2, None, None), (127.8, None, None), (61.0, None, None), (29.2, None, None), (27.5, None, None), (14.5, None, None), (13.8, None, None), (9.8, None, None)]
21
13
13
10.1002_ejoc.201701463
[Sn](c1ccc(C(=O)OCC)cc1)(CCCC)(CCCC)CCCC
7
7
[0.42141977 0.77460942 0.5749646 0.85625003]
[0.093342 0.88281257 0.90249011 0.92031251]
1H NMR
600 MHz
CDCl3
7.97 (d, J = 8.1 Hz, 2H), 7.55 (d, J = 8.1 Hz, 2H), 4.37 (d, J = 7.1 Hz, 2H), 1.60-1.50 (m, 6H), 1.39 (t, J = 7.1 Hz, 3H), 1.36-1.31 (m, 6H), 1.13-1.05 (m, 6H), 0.89 (t, J = 7.4 Hz, 9H)
null
[('d', ['8.1Hz'], '2H', 7.97, 7.97), ('d', ['8.1Hz'], '2H', 7.55, 7.55), ('d', ['7.1Hz'], '2H', 4.37, 4.37), ('m', [], '6H', 1.6, 1.5), ('t', ['7.1Hz'], '3H', 1.39, 1.39), ('m', [], '6H', 1.36, 1.31), ('m', [], '6H', 1.13, 1.05), ('t', ['7.4Hz'], '9H', 0.89, 0.89)]
36
8
36
10.1002_ejoc.201701463
[Sn](c1ccc(C(=O)OCC)cc1)(CCCC)(CCCC)CCCC
7
7
[0.42141977 0.77460942 0.5749646 0.85625003]
[0.093342 0.88281257 0.90249011 0.92031251]
13C NMR
151 MHz
CDCl3
167.2 , 149.6 , 136.5 , 130.1 , 128.5 , 61.0 , 29.2 , 27.5 , 14.5 , 13.8 , 9.8
null
[(167.2, None, None), (149.6, None, None), (136.5, None, None), (130.1, None, None), (128.5, None, None), (61.0, None, None), (29.2, None, None), (27.5, None, None), (14.5, None, None), (13.8, None, None), (9.8, None, None)]
21
11
11
10.1002_ejoc.201701463
[Sn](c1ccccc1[N+](=O)[O-])(CCCC)(CCCC)CCCC
8
8
[0.44516952 0.26230471 0.55121485 0.30800783]
[0.09389432 0.3355469 0.90359469 0.37382815]
1H NMR
600 MHz
CDCl3
8.31 (dd, J = 8.2, 1.2 Hz, 1H), 7.68 (dd, J = 7.2, 1.5 Hz, 1H), 7.61 (td, J = 7.2, 1.1 Hz, 1H), 7.49 (ddd, J = 8.3, 7.2, 1.6 Hz, 1H), 1.55-1.43 (m, 6H), 1.34-1.28 (m, 6H), 1.19-1.07 (m, 6H), 0.87 (t, J = 7.3 Hz, 9H)
null
[('dd', ['8.2Hz', '1.2Hz'], '1H', 8.31, 8.31), ('dd', ['7.2Hz', '1.5Hz'], '1H', 7.68, 7.68), ('td', ['7.2Hz', '1.1Hz'], '1H', 7.61, 7.61), ('ddd', ['8.3Hz', '7.2Hz', '1.6Hz'], '1H', 7.49, 7.49), ('m', [], '6H', 1.55, 1.43), ('m', [], '6H', 1.34, 1.28), ('m', [], '6H', 1.19, 1.07), ('t', ['7.3Hz'], '9H', 0.87, 0.87)]
31
8
31
10.1002_ejoc.201701463
[Sn](c1ccccc1[N+](=O)[O-])(CCCC)(CCCC)CCCC
8
8
[0.44516952 0.26230471 0.55121485 0.30800783]
[0.09389432 0.3355469 0.90359469 0.37382815]
13C NMR
151 MHz
CDCl3
153.8 , 140.4 , 137.8 , 133.5 , 129.3 , 124.2 , 29.2 , 27.5 , 13.8 , 11.2
null
[(153.8, None, None), (140.4, None, None), (137.8, None, None), (133.5, None, None), (129.3, None, None), (124.2, None, None), (29.2, None, None), (27.5, None, None), (13.8, None, None), (11.2, None, None)]
18
10
10
10.1002_ejoc.201701463
[Sn](c1ccc(F)cc1)(CCCC)(CCCC)CCCC
8
8
[0.43191387 0.57734379 0.56391821 0.62109375]
[0.09389432 0.64804693 0.90028075 0.68476567]
1H NMR
600 MHz
CDCl3
7.42 (dd, J = 8.5, 6.5 Hz, 2H), 7.07-6.99 (m, 2H), 1.56 (dt, J = 15.8, 7.7 Hz, 6H), 1.38-1.32 (m, 6H), 1.13-1.02 (m, 6H), 0.91 (t, J = 7.3 Hz, 9H)
null
[('dd', ['8.5Hz', '6.5Hz'], '2H', 7.42, 7.42), ('m', [], '2H', 7.07, 6.99), ('dt', ['15.8Hz', '7.7Hz'], '6H', 1.56, 1.56), ('m', [], '6H', 1.38, 1.32), ('m', [], '6H', 1.13, 1.02), ('t', ['7.3Hz'], '9H', 0.91, 0.91)]
31
6
31
10.1002_ejoc.201701463
[Sn](c1ccc(F)cc1)(CCCC)(CCCC)CCCC
8
8
[0.43191387 0.57734379 0.56391821 0.62109375]
[0.09389432 0.64804693 0.90028075 0.68476567]
13C NMR
151 MHz
CDCl3
163.4 (d, J = 246.4 Hz), 138.0 (d, J = 6.4 Hz), 136.8 (d, J = 3.9 Hz), 115.2 (d, J = 18.9 Hz), 29.2 , 27.5 , 13.8 , 9.8
null
[(163.4, 'd', 246.4), (138.0, 'd', 6.4), (136.8, 'd', 3.9), (115.2, 'd', 18.9), (29.2, None, None), (27.5, None, None), (13.8, None, None), (9.8, None, None)]
18
8
8
10.1002_ejoc.201701463
[Sn](c1ccc(F)cc1F)(CCCC)(CCCC)CCCC
8
9
[0.43136153 0.86484381 0.56391821 0.90859376]
[0.093342 0.07001953 0.90083309 0.10644532]
1H NMR
600 MHz
CDCl3
7.31 (ddd, J = 8.1, 7.3, 4.7 Hz, 1H), 6.87 (td, J = 8.3, 2.2 Hz, 1H), 6.74 (ddd, J = 9.4, 6.8, 2.3 Hz, 1H), 1.52 (q, J = 8.0 Hz, 6H), 1.36-1.30 (m, 6H), 1.16-1.05 (m, 6H), 0.89 (t, J = 7.3 Hz, 9H)
null
[('ddd', ['8.1Hz', '7.3Hz', '4.7Hz'], '1H', 7.31, 7.31), ('td', ['8.3Hz', '2.2Hz'], '1H', 6.87, 6.87), ('ddd', ['9.4Hz', '6.8Hz', '2.3Hz'], '1H', 6.74, 6.74), ('q', ['8.0Hz'], '6H', 1.52, 1.52), ('m', [], '6H', 1.36, 1.3), ('m', [], '6H', 1.16, 1.05), ('t', ['7.3Hz'], '9H', 0.89, 0.89)]
30
7
30
10.1002_ejoc.201701463
[Sn](c1ccc(F)cc1F)(CCCC)(CCCC)CCCC
8
9
[0.43136153 0.86484381 0.56391821 0.90859376]
[0.093342 0.07001953 0.90083309 0.10644532]
13C NMR
151 MHz
CDCl3
167.6 (dd, J = 235.7, 11.0 Hz) , 164.2 (dd, J = 247.8, 11.9 Hz) , 137.9 (dd, J = 17.9, 8.8 Hz), 121.9 (dd, J = 46.6, 3.6 Hz), 111.7 (dd, J = 19.4, 3.4 Hz), 102.9 (dd, J = 32.8, 23.6 Hz) , 29.1 , 27.4 , 13.8 , 10.1
null
[(167.6, 'dd', [235.7, 11.0]), (164.2, 'dd', [247.8, 11.9]), (137.9, 'dd', [17.9, 8.8]), (121.9, 'dd', [46.6, 3.6]), (111.7, 'dd', [19.4, 3.4]), (102.9, 'dd', [32.8, 23.6]), (29.1, None, None), (27.4, None, None), (13.8, None, None), (10.1, None, None)]
18
10
10
10.1002_ejoc.201701463
CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1ccc(C(=O)N)cc1
9
9
[0.42086746 0.36054688 0.5749646 0.42382816]
[0.093342 0.45078127 0.90359469 0.48671876]
1H NMR
600 MHz
CDCl3
7.73 (d, J = 8.0 Hz, 2H), 7.56 (d, J = 8.1 Hz, 2H), 5.89 (d, J = 216.9 Hz, 2H), 1.53 (p, J = 7.8 Hz, 6H), 1.33 (q, J = 7.4 Hz, 6H), 1.14-1.03 (m, 6H), 0.88 (t, J = 7.4 Hz, 9H)
null
[('d', ['8.0Hz'], '2H', 7.73, 7.73), ('d', ['8.1Hz'], '2H', 7.56, 7.56), ('d', ['216.9Hz'], '2H', 5.89, 5.89), ('p', ['7.8Hz'], '6H', 1.53, 1.53), ('q', ['7.4Hz'], '6H', 1.33, 1.33), ('m', [], '6H', 1.14, 1.03), ('t', ['7.4Hz'], '9H', 0.88, 0.88)]
33
7
33
10.1002_ejoc.201701463
CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1ccc(C(=O)N)cc1
9
9
[0.42086746 0.36054688 0.5749646 0.42382816]
[0.093342 0.45078127 0.90359469 0.48671876]
13C NMR
151 MHz
CDCl3
169.8 , 148.4 , 136.8 , 132.8 , 126.4 , 29.2 , 27.5 , 13.8 , 9.8
null
[(169.8, None, None), (148.4, None, None), (136.8, None, None), (132.8, None, None), (126.4, None, None), (29.2, None, None), (27.5, None, None), (13.8, None, None), (9.8, None, None)]
19
9
9
10.1002_ejoc.201701463
[Sn](c1ccc(C=O)cc1)(CCCC)(CCCC)CCCC
9
9
[0.42141977 0.76640628 0.57441231 0.80546878]
[0.093342 0.83281253 0.90304235 0.87031254]
1H NMR
600 MHz
CDCl3
10.00 (s, 1H), 7.79 (d, J = 8.0 Hz, 2H), 7.65 (d, J = 7.9 Hz, 2H), 1.60-1.50 (m, 6H), 1.38-1.31 (m, 6H), 1.17-1.05 (m, 6H), 0.90 (t, J = 7.3 Hz, 9H)
null
[('s', [], '1H', 10.0, 10.0), ('d', ['8.0Hz'], '2H', 7.79, 7.79), ('d', ['7.9Hz'], '2H', 7.65, 7.65), ('m', [], '6H', 1.6, 1.5), ('m', [], '6H', 1.38, 1.31), ('m', [], '6H', 1.17, 1.05), ('t', ['7.3Hz'], '9H', 0.9, 0.9)]
32
7
32
10.1002_ejoc.201701463
[Sn](c1ccc(C=O)cc1)(CCCC)(CCCC)CCCC
9
9
[0.42141977 0.76640628 0.57441231 0.80546878]
[0.093342 0.83281253 0.90304235 0.87031254]
13C NMR
151 MHz
CDCl3
192.8 , 152.7 , 137.1 , 136.2 , 128.6 , 29.2 , 27.4 , 13.7 , 10.0
null
[(192.8, None, None), (152.7, None, None), (137.1, None, None), (136.2, None, None), (128.6, None, None), (29.2, None, None), (27.4, None, None), (13.7, None, None), (10.0, None, None)]
19
9
9
10.1002_ejoc.201701463
[Sn](c1cccc(C(F)(F)F)c1)(CCCC)(CCCC)CCCC
10
10
[0.44516952 0.18828126 0.55121485 0.25195314]
[0.093342 0.27890627 0.90249011 0.31757813]
1H NMR
600 MHz
CDCl3
7.68 (s, 1H), 7.63 (d, J = 7.2 Hz, 1H), 7.53 (d, J = 7.8 Hz, 1H), 7.42 (t, J = 7.5 Hz, 1H), 1.57-1.51 (m, 6H), 1.36-1.32 (m, 6H), 1.12-1.07 (m, 6H), 0.89 (t, J = 7.3 Hz, 9H)
null
[('s', [], '1H', 7.68, 7.68), ('d', ['7.2Hz'], '1H', 7.63, 7.63), ('d', ['7.8Hz'], '1H', 7.53, 7.53), ('t', ['7.5Hz'], '1H', 7.42, 7.42), ('m', [], '6H', 1.57, 1.51), ('m', [], '6H', 1.36, 1.32), ('m', [], '6H', 1.12, 1.07), ('t', ['7.3Hz'], '9H', 0.89, 0.89)]
31
8
31
10.1002_ejoc.201701463
[Sn](c1cccnc1)(CCCC)(CCCC)CCCC
10
10
[0.44296026 0.54531251 0.55121485 0.58906254]
[0.09223736 0.61601565 0.90028075 0.65273439]
1H NMR
600 MHz
CDCl3
8.60 (s, 1H), 8.51 (s, 1H), 7.74 (d, J = 7.3 Hz, 1H), 7.25-7.17 (m, 1H), 1.60-1.50 (m, 6H), 1.36-1.31 (m, 6H), 1.15-1.05 (m, 6H), 0.89 (t, J = 7.3 Hz, 9H)
null
[('s', [], '1H', 8.6, 8.6), ('s', [], '1H', 8.51, 8.51), ('d', ['7.3Hz'], '1H', 7.74, 7.74), ('m', [], '1H', 7.25, 7.17), ('m', [], '6H', 1.6, 1.5), ('m', [], '6H', 1.36, 1.31), ('m', [], '6H', 1.15, 1.05), ('t', ['7.3Hz'], '9H', 0.89, 0.89)]
31
8
31
10.1002_ejoc.201701463
[Sn](c1cccnc1)(CCCC)(CCCC)CCCC
10
10
[0.44296026 0.54531251 0.55121485 0.58906254]
[0.09223736 0.61601565 0.90028075 0.65273439]
13C NMR
151 MHz
CDCl3
156.1 , 149.2 , 144.3 , 137.2 , 124.0 , 29.1 , 27.4 , 13.7 , 9.8
null
[(156.1, None, None), (149.2, None, None), (144.3, None, None), (137.2, None, None), (124.0, None, None), (29.1, None, None), (27.4, None, None), (13.7, None, None), (9.8, None, None)]
17
9
9
10.1002_ejoc.201701463
[Sn](c1ccccn1)(CCCC)(CCCC)CCCC
10
11
[0.44296026 0.85625003 0.55121485 0.90000006]
[0.09223736 0.06992188 0.90083309 0.10703125]
1H NMR
600 MHz
CDCl3
8.73 (d, J = 4.9 Hz, 1H), 7.51-7.45 (m, 1H), 7.40 (d, J = 7.4 Hz, 1H), 7.14-7.06 (m, 1H), 1.57 (dt, J = 15.6, 7.8 Hz, 6H), 1.36-1.31 (m, 6H), 1.18-1.08 (m, 6H), 0.88 (t, J = 7.3 Hz, 9H)
null
[('d', ['4.9Hz'], '1H', 8.73, 8.73), ('m', [], '1H', 7.51, 7.45), ('d', ['7.4Hz'], '1H', 7.4, 7.4), ('m', [], '1H', 7.14, 7.06), ('dt', ['15.6Hz', '7.8Hz'], '6H', 1.57, 1.57), ('m', [], '6H', 1.36, 1.31), ('m', [], '6H', 1.18, 1.08), ('t', ['7.3Hz'], '9H', 0.88, 0.88)]
31
8
31
10.1002_ejoc.201701463
[Sn](c1ccccn1)(CCCC)(CCCC)CCCC
10
11
[0.44296026 0.85625003 0.55121485 0.90000006]
[0.09223736 0.06992188 0.90083309 0.10703125]
13C NMR
151 MHz
CDCl3
150.7 , 133.4 , 132.5 , 122.1 , 29.2 , 27.5 , 13.8 , 10.0
null
[(150.7, None, None), (133.4, None, None), (132.5, None, None), (122.1, None, None), (29.2, None, None), (27.5, None, None), (13.8, None, None), (10.0, None, None)]
17
9
8
10.1002_ejoc.201701463
[Sn](c1ccsc1)(CCCC)(CCCC)CCCC
11
11
[0.45179734 0.31171876 0.54237777 0.36171876]
[0.09278968 0.38789063 0.90028075 0.42539065]
1H NMR
600 MHz
CDCl3
7.46 (dd, J = 4.7, 2.5 Hz, 1H), 7.34 (dd, J = 2.5, 0.9 Hz, 1H), 7.17 (d, J = 4.7 Hz, 1H), 1.59-1.52 (m, 6H), 1.37-1.32 (m, 6H), 1.08-1.04 (m, 6H), 0.90 (t, J = 7.4 Hz, 9H)
null
[('dd', ['4.7Hz', '2.5Hz'], '1H', 7.46, 7.46), ('dd', ['2.5Hz', '0.9Hz'], '1H', 7.34, 7.34), ('d', ['4.7Hz'], '1H', 7.17, 7.17), ('m', [], '6H', 1.59, 1.52), ('m', [], '6H', 1.37, 1.32), ('m', [], '6H', 1.08, 1.04), ('t', ['7.4Hz'], '9H', 0.9, 0.9)]
30
7
30
10.1002_ejoc.201701463
[Sn](c1ccsc1)(CCCC)(CCCC)CCCC
11
11
[0.45179734 0.31171876 0.54237777 0.36171876]
[0.09278968 0.38789063 0.90028075 0.42539065]
13C NMR
151 MHz
CDCl3
137.9 , 133.2 , 131.4 , 125.0 , 29.2 , 27.5 , 13.8 , 10.2
null
[(137.9, None, None), (133.2, None, None), (131.4, None, None), (125.0, None, None), (29.2, None, None), (27.5, None, None), (13.8, None, None), (10.2, None, None)]
16
8
8
10.1002_ejoc.201701463
[Sn](c1cccs1)(CCCC)(CCCC)CCCC
11
11
[0.44572186 0.62968753 0.55066256 0.66250001]
[0.09223736 0.6894532 0.90249011 0.72617193]
1H NMR
600 MHz
CDCl3
7.67 (d, J = 4.7 Hz, 1H), 7.33-7.27 (m, 1H), 7.23 (d, J = 3.2 Hz, 1H), 1.61 (p, J = 8.1, 7.4 Hz, 6H), 1.41-1.35 (m, 6H), 1.18-1.08 (m, 6H), 0.93 (t, J = 7.3 Hz, 9H)
null
[('d', ['4.7Hz'], '1H', 7.67, 7.67), ('m', [], '1H', 7.33, 7.27), ('d', ['3.2Hz'], '1H', 7.23, 7.23), ('p', ['8.1Hz', '7.4Hz'], '6H', 1.61, 1.61), ('m', [], '6H', 1.41, 1.35), ('m', [], '6H', 1.18, 1.08), ('t', ['7.3Hz'], '9H', 0.93, 0.93)]
30
7
30
10.1002_ejoc.201701463
[Sn](c1cccs1)(CCCC)(CCCC)CCCC
11
11
[0.44572186 0.62968753 0.55066256 0.66250001]
[0.09223736 0.6894532 0.90249011 0.72617193]
13C NMR
151 MHz
CDCl3
136.3 , 135.3 , 130.7 , 127.9 , 29.1 , 27.4 , 13.8 , 10.9
null
[(136.3, None, None), (135.3, None, None), (130.7, None, None), (127.9, None, None), (29.1, None, None), (27.4, None, None), (13.8, None, None), (10.9, None, None)]
16
8
8
10.1002_ejoc.201701463
[Sn](c1ccccc1Cl)(CCCC)(CCCC)CCCC
12
12
[0.44516952 0.1006836 0.55121485 0.14462891]
[0.09389432 0.17187502 0.90028075 0.20781251]
1H NMR
600 MHz
CDCl3
7.38 (dd, J = 7.1, 1.9 Hz, 1H), 7.35-7.32 (m, 1H), 7.25-7.22 (m, 1H), 7.20 (td, J = 7.2, 1.3 Hz, 1H), 1.55 (dddt, J = 8.8, 7.9, 6.1, 3.4 Hz, 6H), 1.37-1.32 (m, 6H), 1.19-1.10 (m, 6H), 0.89 (t, J = 7.3 Hz, 9H)
null
[('dd', ['7.1Hz', '1.9Hz'], '1H', 7.38, 7.38), ('m', [], '1H', 7.35, 7.32), ('m', [], '1H', 7.25, 7.22), ('td', ['7.2Hz', '1.3Hz'], '1H', 7.2, 7.2), ('dddt', ['8.8Hz', '7.9Hz', '6.1Hz', '3.4Hz'], '6H', 1.55, 1.55), ('m', [], '6H', 1.37, 1.32), ('m', [], '6H', 1.19, 1.1), ('t', ['7.3Hz'], '9H', 0.89, 0.89)]
31
8
31
10.1002_ejoc.201701463
[Sn](c1ccccc1Cl)(CCCC)(CCCC)CCCC
12
12
[0.44516952 0.1006836 0.55121485 0.14462891]
[0.09389432 0.17187502 0.90028075 0.20781251]
13C NMR
151 MHz
CDCl3
143.1 , 142.9 , 137.7 , 129.9 , 128.4 , 126.0 , 29.2 , 27.5 , 13.8 , 10.7
null
[(143.1, None, None), (142.9, None, None), (137.7, None, None), (129.9, None, None), (128.4, None, None), (126.0, None, None), (29.2, None, None), (27.5, None, None), (13.8, None, None), (10.7, None, None)]
18
10
10
10.1002_ejoc.201701463
Cc1ccc(-c2ccccc2)cc1
13
13
[0.42473371 0.29335939 0.572203 0.32539063]
[0.093342 0.35195314 0.90138543 0.39101564]
1H NMR
600 MHz
CDCl3
7.61 (d, J = 9.5 Hz, 2H), 7.52 (d, J = 8.1 Hz, 2H), 7.45 (t, J = 7.8 Hz, 2H), 7.35 (t, J = 7.4 Hz, 1H), 7.28 (d, J = 7.8 Hz, 2H), 2.43 (s, 3H)
null
[('d', ['9.5Hz'], '2H', 7.61, 7.61), ('d', ['8.1Hz'], '2H', 7.52, 7.52), ('t', ['7.8Hz'], '2H', 7.45, 7.45), ('t', ['7.4Hz'], '1H', 7.35, 7.35), ('d', ['7.8Hz'], '2H', 7.28, 7.28), ('s', [], '3H', 2.43, 2.43)]
12
6
12
10.1002_ejoc.201701463
Cc1ccc(-c2ccccc2)cc1
13
13
[0.42473371 0.29335939 0.572203 0.32539063]
[0.093342 0.35195314 0.90138543 0.39101564]
13C NMR
151 MHz
CDCl3
141.3 , 138.5 , 137.1 , 129.6 , 128.85 , 127.1 , 127.1 , 126.9 , 21.2
null
[(141.3, None, None), (138.5, None, None), (137.1, None, None), (129.6, None, None), (128.85, None, None), (127.1, None, None), (127.1, None, None), (126.9, None, None), (21.2, None, None)]
13
9
9
10.1002_ejoc.201701463
Cc1ccc(-c2ccccc2C)cc1
13
13
[0.42528602 0.54453127 0.572203 0.59140627]
[0.09499895 0.6171875 0.90138543 0.65468751]
1H NMR
600 MHz
CDCl3
7.33-7.28 (m, 8H), 2.47 (s, 3H), 2.35 (s, 3H)
null
[('m', [], '8H', 7.33, 7.28), ('s', [], '3H', 2.47, 2.47), ('s', [], '3H', 2.35, 2.35)]
14
8
14
10.1002_ejoc.201701463
Cc1ccc(-c2ccccc2C)cc1
13
13
[0.42528602 0.54453127 0.572203 0.59140627]
[0.09499895 0.6171875 0.90138543 0.65468751]
13C NMR
151 MHz
CDCl3
141.9 , 139.1 , 136.4 , 135.4 , 130.3 , 129.9 , 129.1 , 128.8 , 127.1 , 125.8 , 21.2 , 20.6
null
[(141.9, None, None), (139.1, None, None), (136.4, None, None), (135.4, None, None), (130.3, None, None), (129.9, None, None), (129.1, None, None), (128.8, None, None), (127.1, None, None), (125.8, None, None), (21.2, None, None), (20.6, None, None)]
14
12
12
10.1002_ejoc.201701463
COc1ccccc1-c1ccc(C)cc1
13
13
[0.42528602 0.78515632 0.572203 0.83515629]
[0.09499895 0.86093756 0.90469937 0.90156254]
1H NMR
600 MHz
CDCl3
7.46 (d, J = 6.9 Hz, 2H), 7.33 (t, J = 7.5 Hz, 2H), 7.25 (d, J = 7.3 Hz, 2H), 7.05 (t, J = 7.4 Hz, 1H), 7.00 (d, J = 8.1 Hz, 1H), 3.83 (s, 3H), 2.42 (s, 3H)
null
[('d', ['6.9Hz'], '2H', 7.46, 7.46), ('t', ['7.5Hz'], '2H', 7.33, 7.33), ('d', ['7.3Hz'], '2H', 7.25, 7.25), ('t', ['7.4Hz'], '1H', 7.05, 7.05), ('d', ['8.1Hz'], '1H', 7.0, 7.0), ('s', [], '3H', 3.83, 3.83), ('s', [], '3H', 2.42, 2.42)]
14
8
14
10.1002_ejoc.201701463
COc1ccccc1-c1ccc(C)cc1
13
13
[0.42528602 0.78515632 0.572203 0.83515629]
[0.09499895 0.86093756 0.90469937 0.90156254]
13C NMR
151 MHz
CDCl3
156.6 , 136.7 , 135.7 , 130.9 , 130.8 , 129.5 , 128.9 , 128.5 , 120.9 , 111.3 , 55.7 , 21.3
null
[(156.6, None, None), (136.7, None, None), (135.7, None, None), (130.9, None, None), (130.8, None, None), (129.5, None, None), (128.9, None, None), (128.5, None, None), (120.9, None, None), (111.3, None, None), (55.7, None, None), (21.3, None, None)]
14
12
12
10.1002_ejoc.201701463
Cc1ccc(-c2cccc([N+](=O)[O-])c2)cc1
14
14
[0.41258267 0.2125 0.58490636 0.26328127]
[0.09389432 0.28906252 0.90249011 0.328125 ]
1H NMR
600 MHz
CDCl3
8.44 (s, 1H), 8.17 (d, J = 9.5 Hz, 1H), 7.93-7.88 (m, 1H), 7.59 (t, J = 8.0 Hz, 1H), 7.53 (d, J = 8.1 Hz, 2H), 7.30 (d, J = 7.9 Hz, 2H), 2.42 (s, 3H)
null
[('s', [], '1H', 8.44, 8.44), ('d', ['9.5Hz'], '1H', 8.17, 8.17), ('m', [], '1H', 7.93, 7.88), ('t', ['8.0Hz'], '1H', 7.59, 7.59), ('d', ['8.1Hz'], '2H', 7.53, 7.53), ('d', ['7.9Hz'], '2H', 7.3, 7.3), ('s', [], '3H', 2.42, 2.42)]
11
7
11
10.1002_ejoc.201701463
Cc1ccc(-c2cccc([N+](=O)[O-])c2)cc1
14
14
[0.41258267 0.2125 0.58490636 0.26328127]
[0.09389432 0.28906252 0.90249011 0.328125 ]
13C NMR
151 MHz
CDCl3
148.9 , 143.0 , 138.7 , 135.9 , 132.9 , 130.0 , 129.8 , 127.1 , 121.8 , 21.3
null
[(148.9, None, None), (143.0, None, None), (138.7, None, None), (135.9, None, None), (132.9, None, None), (130.0, None, None), (129.8, None, None), (127.1, None, None), (121.8, None, None), (21.3, None, None)]
13
11
10
10.1002_ejoc.201701463
Cc1ccc(-c2cccc(C(F)(F)F)c2)cc1
14
14
[0.41423964 0.48164067 0.5826971 0.53164064]
[0.09389432 0.55781254 0.90359469 0.59531252]
1H NMR
600 MHz
CDCl3
7.83 (s, 1H), 7.76 (d, J = 7.6 Hz, 1H), 7.59 (d, J = 7.7 Hz, 1H), 7.54 (t, J = 7.7 Hz, 1H), 7.51 (d, J = 8.0 Hz, 2H), 7.29 (d, J = 7.9 Hz, 2H), 2.42 (s, 3H)
null
[('s', [], '1H', 7.83, 7.83), ('d', ['7.6Hz'], '1H', 7.76, 7.76), ('d', ['7.7Hz'], '1H', 7.59, 7.59), ('t', ['7.7Hz'], '1H', 7.54, 7.54), ('d', ['8.0Hz'], '2H', 7.51, 7.51), ('d', ['7.9Hz'], '2H', 7.29, 7.29), ('s', [], '3H', 2.42, 2.42)]
11
7
11
10.1002_ejoc.201701463
Cc1ccc(-c2cccc(C(F)(F)F)c2)cc1
14
14
[0.41423964 0.48164067 0.5826971 0.53164064]
[0.09389432 0.55781254 0.90359469 0.59531252]
13C NMR
151 MHz
CDCl3
142.1 , 138.1 , 137.0 , 131.3 (q, J = 32.2 Hz), 130.3 , 129.9 , 129.3 , 127.2 , 124.3 (q, J = 272.1 Hz ), 123.8 (q, J = 4.1 Hz), 21.3
null
[(142.1, None, None), (138.1, None, None), (137.0, None, None), (131.3, 'q', 32.2), (130.3, None, None), (129.9, None, None), (129.3, None, None), (127.2, None, None), (124.3, 'q', 272.1), (123.8, 'q', 4.1), (21.3, None, None)]
14
12
11
10.1002_ejoc.201701463
CCOC(=O)c1ccccc1-c1ccc(C)cc1
14
14
[0.42473371 0.75000007 0.572203 0.81406256]
[0.09278968 0.84140631 0.90138543 0.88046881]
1H NMR
600 MHz
CDCl3
7.81 (ddd, J = 7.7, 1.6, 0.5 Hz, 1H), 7.51 (td, J = 7.5, 1.4 Hz, 1H), 7.41-7.35 (m, 2H), 7.23-7.19 (m, 4H), 4.12 (q, J = 7.1 Hz, 2H), 2.40 (s, 3H), 1.05 (t, J = 7.1 Hz, 3H)
null
[('ddd', ['7.7Hz', '1.6Hz', '0.5Hz'], '1H', 7.81, 7.81), ('td', ['7.5Hz', '1.4Hz'], '1H', 7.51, 7.51), ('m', [], '2H', 7.41, 7.35), ('m', [], '4H', 7.23, 7.19), ('q', ['7.1Hz'], '2H', 4.12, 4.12), ('s', [], '3H', 2.4, 2.4), ('t', ['7.1Hz'], '3H', 1.05, 1.05)]
16
9
16
10.1002_ejoc.201701463
CCOC(=O)c1ccccc1-c1ccc(C)cc1
14
14
[0.42473371 0.75000007 0.572203 0.81406256]
[0.09278968 0.84140631 0.90138543 0.88046881]
13C NMR
151 MHz
CDCl3
169.0 , 142.5 , 138.7 , 137.0 , 131.5 , 131.2 , 130.8 , 129.7 , 128.8 , 128.4 , 127.0 , 61.0 , 21.3 , 13.9
null
[(169.0, None, None), (142.5, None, None), (138.7, None, None), (137.0, None, None), (131.5, None, None), (131.2, None, None), (130.8, None, None), (129.7, None, None), (128.8, None, None), (128.4, None, None), (127.0, None, None), (61.0, None, None), (21.3, None, None), (13.9, None, None)]
16
14
14
10.1002_ejoc.201701463
CCOC(=O)c1cccc(-c2ccc(C)cc2)c1
15
15
[0.40982107 0.23710939 0.58711562 0.31289064]
[0.09278968 0.33945315 0.90138543 0.37929689]
1H NMR
600 MHz
CDCl3
8.27 (td, J = 1.8, 0.5 Hz, 1H), 8.01 (ddd, J = 7.8, 1.7, 1.2 Hz, 1H), 7.77 (ddd, J = 7.7, 1.9, 1.1 Hz, 1H), 7.53 (d, J = 8.2 Hz, 2H), 7.50 (t, J = 7.8 Hz, 1H), 7.28 (d, J = 7.8 Hz, 2H), 4.41 (q, J = 7.1 Hz, 2H), 2.41 (s, 3H), 1.42 (t, J = 7.1 Hz, 3H)
null
[('td', ['1.8Hz', '0.5Hz'], '1H', 8.27, 8.27), ('ddd', ['7.8Hz', '1.7Hz', '1.2Hz'], '1H', 8.01, 8.01), ('ddd', ['7.7Hz', '1.9Hz', '1.1Hz'], '1H', 7.77, 7.77), ('d', ['8.2Hz'], '2H', 7.53, 7.53), ('t', ['7.8Hz'], '1H', 7.5, 7.5), ('d', ['7.8Hz'], '2H', 7.28, 7.28), ('q', ['7.1Hz'], '2H', 4.41, 4.41), ('s', [], '3H', 2.4...
16
9
16
10.1002_ejoc.201701463
CCOC(=O)c1ccc(-c2ccc(C)cc2)cc1
15
15
[0.40374556 0.55664066 0.59374349 0.62070318]
[0.09555127 0.64765629 0.90249011 0.68515631]
1H NMR
600 MHz
CDCl3
8.10 (d, J = 8.4 Hz, 2H), 7.65 (d, J = 8.4 Hz, 2H), 7.53 (d, J = 8.1 Hz, 2H), 7.28 (d, J = 7.9 Hz, 2H), 4.40 (q, J = 7.1 Hz, 2H), 2.41 (s, 3H), 1.42 (t, J = 7.1 Hz, 3H)
null
[('d', ['8.4Hz'], '2H', 8.1, 8.1), ('d', ['8.4Hz'], '2H', 7.65, 7.65), ('d', ['8.1Hz'], '2H', 7.53, 7.53), ('d', ['7.9Hz'], '2H', 7.28, 7.28), ('q', ['7.1Hz'], '2H', 4.4, 4.4), ('s', [], '3H', 2.41, 2.41), ('t', ['7.1Hz'], '3H', 1.42, 1.42)]
16
7
16
10.1002_ejoc.201701463
CCOC(=O)c1ccc(-c2ccc(C)cc2)cc1
15
15
[0.40374556 0.55664066 0.59374349 0.62070318]
[0.09555127 0.64765629 0.90249011 0.68515631]
13C NMR
151 MHz
CDCl3
166.7 , 145.6 , 138.2 , 137.3 , 130.2 , 129.8 , 129.1 , 127.2 , 126.9 , 61.1 , 21.3 , 14.5
null
[(166.7, None, None), (145.6, None, None), (138.2, None, None), (137.3, None, None), (130.2, None, None), (129.8, None, None), (129.1, None, None), (127.2, None, None), (126.9, None, None), (61.1, None, None), (21.3, None, None), (14.5, None, None)]
16
12
12
10.1002_ejoc.201701463
Cc1ccc(-c2ccc([N+](=O)[O-])cc2)cc1
15
16
[0.40098396 0.88984379 0.59705738 0.92109379]
[0.09389432 0.07001953 0.90249011 0.10820313]
1H NMR
600 MHz
CDCl3
8.28 (d, J = 8.8 Hz, 2H), 7.72 (d, J = 8.8 Hz, 2H), 7.53 (d, J = 8.1 Hz, 2H), 7.31 (d, J = 7.9 Hz, 2H), 2.43 (s, 3H)
null
[('d', ['8.8Hz'], '2H', 8.28, 8.28), ('d', ['8.8Hz'], '2H', 7.72, 7.72), ('d', ['8.1Hz'], '2H', 7.53, 7.53), ('d', ['7.9Hz'], '2H', 7.31, 7.31), ('s', [], '3H', 2.43, 2.43)]
11
5
11
10.1002_ejoc.201701463
Cc1ccc(-c2ccc([N+](=O)[O-])cc2)cc1
15
16
[0.40098396 0.88984379 0.59705738 0.92109379]
[0.09389432 0.07001953 0.90249011 0.10820313]
13C NMR
151 MHz
CDCl3
147.6 , 146.9 , 139.1 , 135.9 , 129.9 , 127.5 , 127.2 , 124.1 , 21.2
null
[(147.6, None, None), (146.9, None, None), (139.1, None, None), (135.9, None, None), (129.9, None, None), (127.5, None, None), (127.2, None, None), (124.1, None, None), (21.2, None, None)]
13
9
9
10.1002_ejoc.201701463
[N+](c1ccccc1-c1ccc(C)cc1)(=O)[O-]
16
16
[0.42473371 0.26230471 0.572203 0.31152344]
[0.09389432 0.33789066 0.90469937 0.37695316]
1H NMR
600 MHz
CDCl3
7.83 (d, J = 8.0 Hz, 1H), 7.60 (t, J = 7.6 Hz, 1H), 7.48-7.42 (m, 2H), 7.25-7.21 (m, 4H), 2.41 (s, 3H)
null
[('d', ['8.0Hz'], '1H', 7.83, 7.83), ('t', ['7.6Hz'], '1H', 7.6, 7.6), ('m', [], '2H', 7.48, 7.42), ('m', [], '4H', 7.25, 7.21), ('s', [], '3H', 2.41, 2.41)]
11
7
11
10.1002_ejoc.201701463
[N+](c1ccccc1-c1ccc(C)cc1)(=O)[O-]
16
16
[0.42473371 0.26230471 0.572203 0.31152344]
[0.09389432 0.33789066 0.90469937 0.37695316]
13C NMR
151 MHz
CDCl3
138.3 , 136.4 , 134.5 , 132.3 , 132.1 , 129.6 , 128.0 , 127.9 , 124.1 , 21.4
null
[(138.3, None, None), (136.4, None, None), (134.5, None, None), (132.3, None, None), (132.1, None, None), (129.6, None, None), (128.0, None, None), (127.9, None, None), (124.1, None, None), (21.4, None, None)]
13
11
10
10.1002_ejoc.201701463
Cc1ccc(-c2ccccn2)cc1
16
16
[0.42418137 0.53046879 0.572203 0.56640629]
[0.093342 0.59257815 0.90193777 0.63164065]
1H NMR
600 MHz
CDCl3
8.68 (d, J = 4.9 Hz, 1H), 7.91 (d, J = 8.1 Hz, 2H), 7.73-7.68 (m, 2H), 7.29 (d, J = 8.0 Hz, 2H), 7.19 (ddd, J = 6.6, 4.8, 2.0 Hz, 1H), 2.41 (s, 3H)
null
[('d', ['4.9Hz'], '1H', 8.68, 8.68), ('d', ['8.1Hz'], '2H', 7.91, 7.91), ('m', [], '2H', 7.73, 7.68), ('d', ['8.0Hz'], '2H', 7.29, 7.29), ('ddd', ['6.6Hz', '4.8Hz', '2.0Hz'], '1H', 7.19, 7.19), ('s', [], '3H', 2.41, 2.41)]
11
7
11
10.1002_ejoc.201701463
Cc1ccc(-c2ccccn2)cc1
16
16
[0.42418137 0.53046879 0.572203 0.56640629]
[0.093342 0.59257815 0.90193777 0.63164065]
13C NMR
151 MHz
CDCl3
157.5 , 149.6 , 139.0 , 136.8 , 136.7 , 129.6 , 126.9 , 121.9 , 120.3 , 21.3
null
[(157.5, None, None), (149.6, None, None), (139.0, None, None), (136.8, None, None), (136.7, None, None), (129.6, None, None), (126.9, None, None), (121.9, None, None), (120.3, None, None), (21.3, None, None)]
12
10
10
10.1002_ejoc.201701463
Cc1ccc(-c2cccnc2)cc1
16
16
[0.42528602 0.78554689 0.572203 0.82031257]
[0.093342 0.84687504 0.90304235 0.88750003]
1H NMR
600 MHz
CDCl3
8.84 (s, 1H), 8.56 (d, J = 4.7 Hz, 1H), 7.85 (d, J = 7.9 Hz, 1H), 7.48 (d, J = 8.1 Hz, 2H), 7.34 (dd, J = 7.9, 4.8 Hz, 1H), 7.28 (d, J = 7.8 Hz, 2H), 2.41 (s, 3H)
null
[('s', [], '1H', 8.84, 8.84), ('d', ['4.7Hz'], '1H', 8.56, 8.56), ('d', ['7.9Hz'], '1H', 7.85, 7.85), ('d', ['8.1Hz'], '2H', 7.48, 7.48), ('dd', ['7.9Hz', '4.8Hz'], '1H', 7.34, 7.34), ('d', ['7.8Hz'], '2H', 7.28, 7.28), ('s', [], '3H', 2.41, 2.41)]
11
7
11
10.1002_ejoc.201701463
Cc1ccc(-c2cccnc2)cc1
16
16
[0.42528602 0.78554689 0.572203 0.82031257]
[0.093342 0.84687504 0.90304235 0.88750003]
13C NMR
151 MHz
CDCl3
148.3 , 148.2 , 138.1 , 136.7 , 135.0 , 134.2 , 129.9 , 127.1 , 123.6 , 21.2
null
[(148.3, None, None), (148.2, None, None), (138.1, None, None), (136.7, None, None), (135.0, None, None), (134.2, None, None), (129.9, None, None), (127.1, None, None), (123.6, None, None), (21.2, None, None)]
12
10
10
10.1002_ejoc.201701463
Cc1ccc(-c2cncnc2)cc1
17
17
[0.42473371 0.23789065 0.57275534 0.27617189]
[0.09223736 0.30351564 0.90359469 0.34257815]
1H NMR
600 MHz
CDCl3
9.18 (s, 1H), 8.93 (s, 2H), 7.47 (d, J = 8.1 Hz, 2H), 7.35-7.30 (m, 2H), 2.42 (s, 3H)
null
[('s', [], '1H', 9.18, 9.18), ('s', [], '2H', 8.93, 8.93), ('d', ['8.1Hz'], '2H', 7.47, 7.47), ('m', [], '2H', 7.35, 7.3), ('s', [], '3H', 2.42, 2.42)]
10
5
10
10.1002_ejoc.201701463
Cc1ccc(-c2cncnc2)cc1
17
17
[0.42473371 0.23789065 0.57275534 0.27617189]
[0.09223736 0.30351564 0.90359469 0.34257815]
13C NMR
151 MHz
CDCl3
157.3 , 154.8 , 139.3 , 134.4 , 131.5 , 130.3 , 126.9 , 21.3
null
[(157.3, None, None), (154.8, None, None), (139.3, None, None), (134.4, None, None), (131.5, None, None), (130.3, None, None), (126.9, None, None), (21.3, None, None)]
11
8
8
10.1002_ejoc.201701463
Cc1ccc(-c2cnc(Cl)nc2)cc1
17
17
[0.40650716 0.49570315 0.59098189 0.53476565]
[0.09389432 0.56093751 0.90249011 0.60000001]
1H NMR
600 MHz
CDCl3
8.80 (s, 2H), 7.45 (d, J = 8.1 Hz, 2H), 7.33 (d, J = 7.8 Hz, 2H), 2.42 (s, 3H)
null
[('s', [], '2H', 8.8, 8.8), ('d', ['8.1Hz'], '2H', 7.45, 7.45), ('d', ['7.8Hz'], '2H', 7.33, 7.33), ('s', [], '3H', 2.42, 2.42)]
9
4
9
10.1002_ejoc.201701463
Cc1ccc(-c2cnc(Cl)nc2)cc1
17
17
[0.40650716 0.49570315 0.59098189 0.53476565]
[0.09389432 0.56093751 0.90249011 0.60000001]
13C NMR
151 MHz
CDCl3
160.0 , 157.4 , 139.7 , 133.1 , 130.4 , 130.1 , 126.9 , 21.4
null
[(160.0, None, None), (157.4, None, None), (139.7, None, None), (133.1, None, None), (130.4, None, None), (130.1, None, None), (126.9, None, None), (21.4, None, None)]
11
8
8
10.1002_ejoc.201701463
Cc1ccc(-c2ccc(N(C)C)cc2)cc1
17
17
[0.40429787 0.75390632 0.59098189 0.78515632]
[0.09389432 0.81093751 0.90249011 0.84843753]
1H NMR
600 MHz
CDCl3
7.51 (d, J = 8.7 Hz, 2H), 7.47 (d, J = 8.1 Hz, 2H), 7.22 (d, J = 8.1 Hz, 2H), 6.83 (d, J = 8.4 Hz, 2H), 3.00 (s, 6H), 2.39 (s, 3H)
null
[('d', ['8.7Hz'], '2H', 7.51, 7.51), ('d', ['8.1Hz'], '2H', 7.47, 7.47), ('d', ['8.1Hz'], '2H', 7.22, 7.22), ('d', ['8.4Hz'], '2H', 6.83, 6.83), ('s', [], '6H', 3.0, 3.0), ('s', [], '3H', 2.39, 2.39)]
17
6
17
10.1002_ejoc.201701463
Cc1ccc(-c2cccs2)cc1
18
18
[0.42970459 0.1640625 0.56667981 0.19902345]
[0.09278968 0.22539064 0.90359469 0.26210939]
1H NMR
600 MHz
CDCl3
7.55-7.52 (m, 2H), 7.29 (dd, J = 3.6, 1.1 Hz, 1H), 7.26 (dd, J = 5.1, 1.1 Hz, 1H), 7.21 (d, J = 7.9 Hz, 2H), 7.09 (dd, J = 5.1, 3.6 Hz, 1H), 2.39 (s, 3H)
null
[('m', [], '2H', 7.55, 7.52), ('dd', ['3.6Hz', '1.1Hz'], '1H', 7.29, 7.29), ('dd', ['5.1Hz', '1.1Hz'], '1H', 7.26, 7.26), ('d', ['7.9Hz'], '2H', 7.21, 7.21), ('dd', ['5.1Hz', '3.6Hz'], '1H', 7.09, 7.09), ('s', [], '3H', 2.39, 2.39)]
10
6
10
10.1002_ejoc.201701463
Cc1ccc(-c2cccs2)cc1
18
18
[0.42970459 0.1640625 0.56667981 0.19902345]
[0.09278968 0.22539064 0.90359469 0.26210939]
13C NMR
151 MHz
CDCl3
144.7 , 137.4 , 131.8 , 129.7 , 128.0 , 126.0 , 124.4 , 122.7 , 21.3
null
[(144.7, None, None), (137.4, None, None), (131.8, None, None), (129.7, None, None), (128.0, None, None), (126.0, None, None), (124.4, None, None), (122.7, None, None), (21.3, None, None)]
11
9
9
10.1002_ejoc.201701463
Cc1ccc(-c2ccsc2)cc1
18
18
[0.42915225 0.41875003 0.5694414 0.45000003]
[0.093342 0.4761719 0.90359469 0.51289067]
1H NMR
600 MHz
CDCl3
7.51 (d, J = 8.0 Hz, 2H), 7.42 (s, 1H), 7.38 (s, 2H), 7.22 (d, J = 7.9 Hz, 2H), 2.39 (s, 3H)
null
[('d', ['8.0Hz'], '2H', 7.51, 7.51), ('s', [], '1H', 7.42, 7.42), ('s', [], '2H', 7.38, 7.38), ('d', ['7.9Hz'], '2H', 7.22, 7.22), ('s', [], '3H', 2.39, 2.39)]
10
6
10
10.1002_ejoc.201701463
Cc1ccc(-c2ccsc2)cc1
18
18
[0.42915225 0.41875003 0.5694414 0.45000003]
[0.093342 0.4761719 0.90359469 0.51289067]
13C NMR
151 MHz
CDCl3
142.5 , 137.0 , 133.2 , 129.6 , 126.9 , 126.5 , 126.2 , 119.8 , 21.3
null
[(142.5, None, None), (137.0, None, None), (133.2, None, None), (129.6, None, None), (126.9, None, None), (126.5, None, None), (126.2, None, None), (119.8, None, None), (21.3, None, None)]
11
9
9
10.1002_ejoc.201701463
Cc1ccc(-c2csc(C=O)c2)cc1
18
18
[0.41865818 0.66953131 0.57551694 0.72421881]
[0.09278968 0.75039064 0.90469937 0.7910157 ]
1H NMR
600 MHz
CDCl3
9.97 (s, 1H), 8.01 (s, 1H), 7.81 (s, 1H), 7.48 (d, J = 8.0 Hz, 2H), 7.25 (d, J = 7.9 Hz, 2H), 2.39 (s, 3H)
null
[('s', [], '1H', 9.97, 9.97), ('s', [], '1H', 8.01, 8.01), ('s', [], '1H', 7.81, 7.81), ('d', ['8.0Hz'], '2H', 7.48, 7.48), ('d', ['7.9Hz'], '2H', 7.25, 7.25), ('s', [], '3H', 2.39, 2.39)]
10
6
10
10.1002_ejoc.201701463
Cc1ccc(-c2csc(C=O)c2)cc1
18
18
[0.41865818 0.66953131 0.57551694 0.72421881]
[0.09278968 0.75039064 0.90469937 0.7910157 ]
13C NMR
151 MHz
CDCl3
183.1 , 144.4 , 143.8 , 138.1 , 134.8 , 131.7 , 129.9 , 129.2 , 126.3 , 21.3
null
[(183.1, None, None), (144.4, None, None), (143.8, None, None), (138.1, None, None), (134.8, None, None), (131.7, None, None), (129.9, None, None), (129.2, None, None), (126.3, None, None), (21.3, None, None)]
12
10
10
10.1002_ejoc.201701463
Cc1ccc(-c2ccc(C=O)s2)cc1
19
19
[0.40595484 0.10078126 0.5882203 0.13593751]
[0.093342 0.16191407 0.90469937 0.20156251]
1H NMR
600 MHz
CDCl3
9.87 (s, 1H), 7.72 (d, J = 3.9 Hz, 1H), 7.56 (d, J = 8.2 Hz, 2H), 7.36 (d, J = 3.9 Hz, 1H), 7.23 (d, J = 9.1 Hz, 2H), 2.39 (s, 3H)
null
[('s', [], '1H', 9.87, 9.87), ('d', ['3.9Hz'], '1H', 7.72, 7.72), ('d', ['8.2Hz'], '2H', 7.56, 7.56), ('d', ['3.9Hz'], '1H', 7.36, 7.36), ('d', ['9.1Hz'], '2H', 7.23, 7.23), ('s', [], '3H', 2.39, 2.39)]
10
6
10
10.1002_ejoc.201701463
Cc1ccc(-c2ccc(C=O)s2)cc1
19
19
[0.40595484 0.10078126 0.5882203 0.13593751]
[0.093342 0.16191407 0.90469937 0.20156251]
13C NMR
151 MHz
CDCl3
182.9 , 154.8 , 142.1 , 139.9 , 137.6 , 130.4 , 130.0 , 126.5 , 123.7 , 21.5
null
[(182.9, None, None), (154.8, None, None), (142.1, None, None), (139.9, None, None), (137.6, None, None), (130.4, None, None), (130.0, None, None), (126.5, None, None), (123.7, None, None), (21.5, None, None)]
12
10
10
10.1002_ejoc.201701463
Cc1ccc(-c2ccccc2Cl)cc1
19
19
[0.42528602 0.35468751 0.572203 0.40507815]
[0.093342 0.43125002 0.90304235 0.46718751]
1H NMR
600 MHz
CDCl3
7.49 (d, J = 6.8 Hz, 1H), 7.37 (t, J = 8.4 Hz, 3H), 7.33 (t, J = 6.8 Hz, 1H), 7.30-7.27 (m, 3H), 2.44 (s, 3H)
null
[('d', ['6.8Hz'], '1H', 7.49, 7.49), ('t', ['8.4Hz'], '3H', 7.37, 7.37), ('t', ['6.8Hz'], '1H', 7.33, 7.33), ('m', [], '3H', 7.3, 7.27), ('s', [], '3H', 2.44, 2.44)]
11
7
11
10.1002_ejoc.201701463
Cc1ccc(-c2ccccc2Cl)cc1
19
19
[0.42528602 0.35468751 0.572203 0.40507815]
[0.093342 0.43125002 0.90304235 0.46718751]
13C NMR
151 MHz
CDCl3
140.6 , 137.5 , 136.7 , 132.7 , 131.5 , 130.0 , 129.4 , 128.9 , 128.45 , 126.9 , 21.4
null
[(140.6, None, None), (137.5, None, None), (136.7, None, None), (132.7, None, None), (131.5, None, None), (130.0, None, None), (129.4, None, None), (128.9, None, None), (128.45, None, None), (126.9, None, None), (21.4, None, None)]
13
11
11
10.1002_ejoc.201701463
Cc1ccc(-c2ccc(F)cc2)cc1
19
19
[0.41147804 0.62265631 0.5882203 0.65546879]
[0.09389432 0.68203126 0.90359469 0.71796879]
1H NMR
600 MHz
CDCl3
7.54 (dd, J = 8.6, 5.5 Hz, 2H), 7.48-7.43 (m, 2H), 7.28-7.25 (m, 2H), 7.13 (t, J = 8.7 Hz, 2H), 2.41 (s, 3H)
null
[('dd', ['8.6Hz', '5.5Hz'], '2H', 7.54, 7.54), ('m', [], '2H', 7.48, 7.43), ('m', [], '2H', 7.28, 7.25), ('t', ['8.7Hz'], '2H', 7.13, 7.13), ('s', [], '3H', 2.41, 2.41)]
11
5
11
10.1002_ejoc.201701463
Cc1ccc(-c2ccc(F)cc2)cc1
19
19
[0.41147804 0.62265631 0.5882203 0.65546879]
[0.09389432 0.68203126 0.90359469 0.71796879]
13C NMR
151 MHz
CDCl3
162.4 (d, J = 246.4 Hz), 137.5, 137.4 , 137.2 , 129.7 , 128.6 (d, J = 7.8 Hz), 127.0 , 115.7 (d, J = 21.2 Hz), 21.2
null
[(162.4, 'd', 246.4), (137.5, None, None), (137.4, None, None), (137.2, None, None), (129.7, None, None), (128.6, 'd', 7.8), (127.0, None, None), (115.7, 'd', 21.2), (21.2, None, None)]
13
9
9
10.1002_ejoc.201701463
Cc1ccc(-c2ccc(F)cc2F)cc1
19
20
[0.41147804 0.87421879 0.58711562 0.92421876]
[0.09389432 0.06972657 0.90138543 0.10654297]
1H NMR
600 MHz
CDCl3
7.44-7.38 (m, 3H), 7.29-7.27 (m, 2H), 6.99-6.89 (m, 2H), 2.43 (s, 3H)
null
[('m', [], '3H', 7.44, 7.38), ('m', [], '2H', 7.29, 7.27), ('m', [], '2H', 6.99, 6.89), ('s', [], '3H', 2.43, 2.43)]
10
6
10
10.1002_ejoc.201701463
Cc1ccc(-c2ccc(F)cc2F)cc1
19
20
[0.41147804 0.87421879 0.58711562 0.92421876]
[0.09389432 0.06972657 0.90138543 0.10654297]
13C NMR
151 MHz
CDCl3
162.2 (dd, J = 248.5, 11.7 Hz), 159.9 (dd, J = 250.2, 11.8 Hz), 137.7 , 132.2 , 131.4 (dd, J = 9.4, 5.0 Hz), 129.4 , 128.9 , 111.6 (dd, J = 21.0, 3.9 Hz), 104.3 (t, J=25.5 Hz), 21.3
null
[(162.2, 'dd', [248.5, 11.7]), (159.9, 'dd', [250.2, 11.8]), (137.7, None, None), (132.2, None, None), (131.4, 'dd', [9.4, 5.0]), (129.4, None, None), (128.9, None, None), (111.6, 'dd', [21.0, 3.9]), (104.3, 't', 25.5), (21.3, None, None)]
13
11
10
10.1002_ejoc.201701463
Cc1ccc(-c2ccc(C=O)cc2)cc1
20
20
[0.40540253 0.31171876 0.59263881 0.34726565]
[0.09278968 0.37421876 0.90469937 0.41132813]
1H NMR
600 MHz
CDCl3
10.05 (s, 1H), 7.94 (d, J = 8.1 Hz, 2H), 7.74 (d, J = 8.0 Hz, 2H), 7.55 (d, J = 7.9 Hz, 2H), 7.29 (d, J = 7.8 Hz, 2H), 2.42 (s, 3H)
null
[('s', [], '1H', 10.05, 10.05), ('d', ['8.1Hz'], '2H', 7.94, 7.94), ('d', ['8.0Hz'], '2H', 7.74, 7.74), ('d', ['7.9Hz'], '2H', 7.55, 7.55), ('d', ['7.8Hz'], '2H', 7.29, 7.29), ('s', [], '3H', 2.42, 2.42)]
12
6
12
10.1002_ejoc.201701463
Cc1ccc(-c2ccc(C=O)cc2)cc1
20
20
[0.40540253 0.31171876 0.59263881 0.34726565]
[0.09278968 0.37421876 0.90469937 0.41132813]
13C NMR
151 MHz
CDCl3
192.1 , 147.3 , 138.7 , 136.9 , 135.1 , 130.4 , 129.9 , 127.5 , 127.3 , 21.3
null
[(192.1, None, None), (147.3, None, None), (138.7, None, None), (136.9, None, None), (135.1, None, None), (130.4, None, None), (129.9, None, None), (127.5, None, None), (127.3, None, None), (21.3, None, None)]
14
10
10
10.1002_ejoc.201701463
CC(=O)c1ccc(-c2ccc(C)cc2)cc1
20
20
[0.40374556 0.56640629 0.59374349 0.60234378]
[0.09278968 0.62812504 0.90193777 0.66718754]
1H NMR
600 MHz
CDCl3
8.02 (d, J = 8.2 Hz, 2H), 7.67 (d, J = 8.2 Hz, 2H), 7.54 (d, J = 8.0 Hz, 2H), 7.28 (d, J = 7.9 Hz, 2H), 2.63 (s, 3H), 2.42 (s, 3H)
null
[('d', ['8.2Hz'], '2H', 8.02, 8.02), ('d', ['8.2Hz'], '2H', 7.67, 7.67), ('d', ['8.0Hz'], '2H', 7.54, 7.54), ('d', ['7.9Hz'], '2H', 7.28, 7.28), ('s', [], '3H', 2.63, 2.63), ('s', [], '3H', 2.42, 2.42)]
14
6
14
10.1002_ejoc.201701463
CC(=O)c1ccc(-c2ccc(C)cc2)cc1
20
20
[0.40374556 0.56640629 0.59374349 0.60234378]
[0.09278968 0.62812504 0.90193777 0.66718754]
13C NMR
151 MHz
CDCl3
197.9 , 145.8 , 138.4 , 137.1 , 135.7 , 129.8 , 129.0 , 127.2 , 127.1 , 26.7 , 21.3
null
[(197.9, None, None), (145.8, None, None), (138.4, None, None), (137.1, None, None), (135.7, None, None), (129.8, None, None), (129.0, None, None), (127.2, None, None), (127.1, None, None), (26.7, None, None), (21.3, None, None)]
15
11
11
10.1002_ejoc.201701463
Cc1ccc(-c2c3ccccc3cc3ccccc23)cc1
21
21
[0.42418137 0.28710939 0.57275534 0.37695316]
[0.093342 0.40390627 0.90304235 0.44140629]
1H NMR
600 MHz
CDCl3
8.49 (s, 1H), 8.05 (d, J = 8.5 Hz, 2H), 7.71 (d, J = 8.8 Hz, 2H), 7.48-7.44 (m, 2H), 7.40 (d, J = 7.8 Hz, 2H), 7.37-7.33 (m, 4H), 2.54 (s, 3H)
null
[('s', [], '1H', 8.49, 8.49), ('d', ['8.5Hz'], '2H', 8.05, 8.05), ('d', ['8.8Hz'], '2H', 7.71, 7.71), ('m', [], '2H', 7.48, 7.44), ('d', ['7.8Hz'], '2H', 7.4, 7.4), ('m', [], '4H', 7.37, 7.33), ('s', [], '3H', 2.54, 2.54)]
16
8
16
10.1002_ejoc.201701463
Cc1ccc(-c2c3ccccc3cc3ccccc23)cc1
21
21
[0.42418137 0.28710939 0.57275534 0.37695316]
[0.093342 0.40390627 0.90304235 0.44140629]
13C NMR
151 MHz
CDCl3
137.3 , 137.2 , 135.8 , 131.5 , 131.4 , 131.2 , 130.5 , 129.2 , 128.4 , 127.2 , 127.1 , 126.5 , 125.3 , 125.2 , 125.0 , 21.5
null
[(137.3, None, None), (137.2, None, None), (135.8, None, None), (131.5, None, None), (131.4, None, None), (131.2, None, None), (130.5, None, None), (129.2, None, None), (128.4, None, None), (127.2, None, None), (127.1, None, None), (126.5, None, None), (125.3, None, None), (125.2, None, None), (125.0, None, None), (21....
21
13
16
10.1002_ejoc.201701463
Cc1ccc(-c2c3ccccc3c(-c3ccc(C)cc3)c3ccccc23)cc1
21
21
[0.3766819 0.59609376 0.6197025 0.68671879]
[0.09278968 0.71328126 0.90138543 0.75234376]
1H NMR
600 MHz
CDCl3
7.75 (dd, J = 6.8, 3.3 Hz, 4H), 7.43 (d, J = 7.7 Hz, 4H), 7.39 (d, J = 7.8 Hz, 4H), 7.33 (dd, J = 6.9, 3.2 Hz, 4H), 2.56 (s, 6H)
null
[('dd', ['6.8Hz', '3.3Hz'], '4H', 7.75, 7.75), ('d', ['7.7Hz'], '4H', 7.43, 7.43), ('d', ['7.8Hz'], '4H', 7.39, 7.39), ('dd', ['6.9Hz', '3.2Hz'], '4H', 7.33, 7.33), ('s', [], '6H', 2.56, 2.56)]
22
5
22
10.1002_ejoc.201701463
Cc1ccc(-c2c3ccccc3c(-c3ccc(C)cc3)c3ccccc23)cc1
21
21
[0.3766819 0.59609376 0.6197025 0.68671879]
[0.09278968 0.71328126 0.90138543 0.75234376]
13C NMR
151 MHz
CDCl3
137.2 , 137.2 , 136.2 , 131.4 , 130.2 , 129.2 , 127.2 , 125.0 , 114.2 , 21.5
null
[(137.2, None, None), (137.2, None, None), (136.2, None, None), (131.4, None, None), (130.2, None, None), (129.2, None, None), (127.2, None, None), (125.0, None, None), (114.2, None, None), (21.5, None, None)]
28
9
10
10.1002_ejoc.201701463
CCOC(=O)c1ccc(-c2ccccc2OC)cc1
22
22
[0.41534426 0.36757814 0.5799355 0.43164066]
[0.09223736 0.45937501 0.90414703 0.52031253]
1H NMR
600 MHz
CDCl3
8.08 (d, J = 8.5 Hz, 2H), 7.60 (d, J = 8.5 Hz, 2H), 7.37-7.32 (m, 2H), 7.05 (td, J = 7.5, 1.1 Hz, 1H), 7.00 (d, J = 8.9 Hz, 1H), 4.40 (q, J = 7.1 Hz, 2H), 3.82 (s, 3H), 1.41 (t, J = 7.1 Hz, 3H)
null
[('d', ['8.5Hz'], '2H', 8.08, 8.08), ('d', ['8.5Hz'], '2H', 7.6, 7.6), ('m', [], '2H', 7.37, 7.32), ('td', ['7.5Hz', '1.1Hz'], '1H', 7.05, 7.05), ('d', ['8.9Hz'], '1H', 7.0, 7.0), ('q', ['7.1Hz'], '2H', 4.4, 4.4), ('s', [], '3H', 3.82, 3.82), ('t', ['7.1Hz'], '3H', 1.41, 1.41)]
16
9
16
10.1002_ejoc.201701463
CCOC(=O)c1ccc(-c2ccccc2OC)cc1
22
22
[0.41534426 0.36757814 0.5799355 0.43164066]
[0.09223736 0.45937501 0.90414703 0.52031253]
13C NMR
151 MHz
CDCl3
166.8 , 143.4 , 130.9 , 129.8 , 129.6 , 129.5 , 129.4 , 129.0 , 121.1 , 111.5 , 61.0 , 55.7 , 14.5
null
[(166.8, None, None), (143.4, None, None), (130.9, None, None), (129.8, None, None), (129.6, None, None), (129.5, None, None), (129.4, None, None), (129.0, None, None), (121.1, None, None), (111.5, None, None), (61.0, None, None), (55.7, None, None), (14.5, None, None)]
16
14
13
10.1002_ejoc.201701463
[N+](c1ccccc1-c1ccc(F)cc1)(=O)[O-]
22
22
[0.42252443 0.70039067 0.57275534 0.75039064]
[0.09168504 0.77695318 0.90469937 0.83906254]
1H NMR
600 MHz
CDCl3
7.86 (dd, J = 8.1, 1.3 Hz, 1H), 7.62 (td, J = 7.6, 1.3 Hz, 1H), 7.50 (ddd, J = 8.1, 7.4, 1.5 Hz, 1H), 7.42 (dd, J = 7.7, 1.4 Hz, 1H), 7.29 (dd, J = 8.8, 5.2 Hz, 2H), 7.12 (t, J = 8.7 Hz, 2H)
null
[('dd', ['8.1Hz', '1.3Hz'], '1H', 7.86, 7.86), ('td', ['7.6Hz', '1.3Hz'], '1H', 7.62, 7.62), ('ddd', ['8.1Hz', '7.4Hz', '1.5Hz'], '1H', 7.5, 7.5), ('dd', ['7.7Hz', '1.4Hz'], '1H', 7.42, 7.42), ('dd', ['8.8Hz', '5.2Hz'], '2H', 7.29, 7.29), ('t', ['8.7Hz'], '2H', 7.12, 7.12)]
8
6
8
10.1002_ejoc.201701463
[N+](c1ccccc1-c1ccc(F)cc1)(=O)[O-]
22
22
[0.42252443 0.70039067 0.57275534 0.75039064]
[0.09168504 0.77695318 0.90469937 0.83906254]
13C NMR
151 MHz
CDCl3
163.7 , 133.5 , 132.5 , 132.1 , 129.9 , 129.8 , 128.5 , 124.3 , 115.9 (d, J = 21.5 Hz)
null
[(163.7, None, None), (133.5, None, None), (132.5, None, None), (132.1, None, None), (129.9, None, None), (129.8, None, None), (128.5, None, None), (124.3, None, None), (115.9, 'd', 21.5)]
12
10
9
10.1002_ejoc.201701463
CCOC(=O)c1ccc(-c2ccc(F)cc2)cc1
23
23
[0.40153628 0.16445314 0.59374349 0.22871094]
[0.09223736 0.25546877 0.90359469 0.3433594 ]
1H NMR
600 MHz
CDCl3
8.10 (d, J = 8.4 Hz, 2H), 7.62-7.56 (m, 4H), 7.15 (t, J = 8.6 Hz, 2H), 4.40 (q, J = 7.1 Hz, 2H), 1.42 (t, J = 7.1 Hz, 3H)
null
[('d', ['8.4Hz'], '2H', 8.1, 8.1), ('m', [], '4H', 7.62, 7.56), ('t', ['8.6Hz'], '2H', 7.15, 7.15), ('q', ['7.1Hz'], '2H', 4.4, 4.4), ('t', ['7.1Hz'], '3H', 1.42, 1.42)]
13
6
13
10.1002_ejoc.201701463
CCOC(=O)c1ccc(-c2ccc(F)cc2)cc1
23
23
[0.40153628 0.16445314 0.59374349 0.22871094]
[0.09223736 0.25546877 0.90359469 0.3433594 ]
13C NMR
151 MHz
CDCl3
166.6 , 163.1 (d, J = 247.7 Hz), 144.62, 136.3 , 130.2 , 129.4 , 129.1 , 129.0 , 127.0 , 116.0 (d, J = 21.6 Hz), 61.1 , 14.5
null
[(166.6, None, None), (163.1, 'd', 247.7), (144.62, None, None), (136.3, None, None), (130.2, None, None), (129.4, None, None), (129.1, None, None), (129.0, None, None), (127.0, None, None), (116.0, 'd', 21.6), (61.1, None, None), (14.5, None, None)]
15
11
12
10.1002_ejoc.201701463
COc1ccc(-c2ccc([N+](=O)[O-])cc2)cc1
23
23
[0.39435614 0.49609379 0.60202828 0.52890627]
[0.09223736 0.55546878 0.90359469 0.61640629]
1H NMR
600 MHz
CDCl3
8.27 (d, J = 8.8 Hz, 2H), 7.69 (d, J = 8.8 Hz, 2H), 7.58 (d, J = 8.8 Hz, 2H), 7.02 (d, J = 8.8 Hz, 2H), 3.88 (s, 3H)
null
[('d', ['8.8Hz'], '2H', 8.27, 8.27), ('d', ['8.8Hz'], '2H', 7.69, 7.69), ('d', ['8.8Hz'], '2H', 7.58, 7.58), ('d', ['8.8Hz'], '2H', 7.02, 7.02), ('s', [], '3H', 3.88, 3.88)]
11
5
11
10.1002_ejoc.201701463
COc1ccc(-c2ccc([N+](=O)[O-])cc2)cc1
23
23
[0.39435614 0.49609379 0.60202828 0.52890627]
[0.09223736 0.55546878 0.90359469 0.61640629]
13C NMR
151 MHz
CDCl3
160.6 , 147.3 , 146.7 , 131.2 , 128.7 , 127.2 , 124.3 , 114.8 , 55.6
null
[(160.6, None, None), (147.3, None, None), (146.7, None, None), (131.2, None, None), (128.7, None, None), (127.2, None, None), (124.3, None, None), (114.8, None, None), (55.6, None, None)]
13
9
9