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} | ['gnd:4326464-5', 'gnd:4147194-5', 'gnd:4279983-1'] | ['Calciumsilicate', 'Zementherstellung', 'Nachhaltigkeit'] | ['bau'] | [['Villiers, Johan P. R.', 'Stemmermann, P.']] | [['(firstid)GBV:874372089', '(ppn)874372089', '(doi)10.25673/1885']] | [''] | [['(classificationName=linseach:mapping)cet', '(classificationName=bk, id=106421085)56.45 - Baustoffkunde', '(classificationName=bk, id=10641657X)58.10 - Verfahrenstechnik: Allgemeines', '(classificationName=ddc-dbn)540', '(classificationName=linseach:mapping)arc', '(classificationName=linseach:mapping)bau']] | ['Fremdionenstabilisierte Dicalciumsilikate : Synthese und hydraulische Reaktion'] | [['The cement industry has a global share of about 8 % on the CO2 emission. Therefore, there is increased demand for research on new sustainable binding materials as well as on clinker substitute products. A newly developed binding material based on hydraulic calcium hydrosilicates is Celitement. Therefore this work aims on the production and characterization of calcium silicates. The investigation focuses on the phase C2S. Due to the incorporation of foreign ions the high temperature modifications (α’H- and α-C2S) can be stabilized. Hydration studies under standard conditions show that C2S converted into the C-S-H phase within 100 hours. The hydraulic reactivity under hydrothermal conditions was studied by means of XRD in situ using the beamline SUL-X at the synchrotron radiation facility in Karlsruhe as well as ex situ in laboratory autoclaves. The hydrothermal treatment of the C2S samples produced α-C2SH, suitable for the production of Celitement.', 'dicalcium silicate; foreign ions; stabilization; high temperature modifications; hydrothermal hydration; synchrotron; alpha-dicalciumsilicate hydrate (α-C2SH); cement; Celitement', 'Dicalciumsilikat; Fremdionen; Stabilisierung; Hochtemperaturmodifikationen; hydrothermale Hydratation; Synchrotron; alpha-Dicalciumsilikathydrat (α-C2SH); Zement; Celitement', 'Da die Zementindustrie einen Anteil von 8% am weltweiten CO2-Ausstoß verursacht, ist die Produktion von nachhaltigem Zement in den Fokus von Forschung und Entwicklung gerückt. Eines dieser neuartig entwickeltes Bindemittel ist das, auf hydraulischen Calciumhydrosilikaten basierende Produkt Celitement. Im Rahmen dieser Arbeit wurden daher reaktive Calciumsilikate hergestellt und charakterisiert. Hauptaugenmerk lag dabei auf dem C2S. Durch den Einbau von Fremdionen gelang es, die Hochtemperaturmodifikationen (α’H- und α-C2S) zu stabilisieren. Hydratationsversuche unter Standardbedingungen zeigten einen Umsatz nach 100 Stunden in die C-S-H Phase. Die hydraulischen Reaktivitäten unter hydrothermalen Bedingungen wurden in situ an der Beamline SUL-X der Strahlenquelle für Synchrotronstrahlung in Karlsruhe sowie ex situ in Laborautoklaven untersucht. Durch die hydrothermale Behandlung der C2S-Phasen konnte α C2SH hergestellt werden, das für die Produktion von Celitement geeignet ist.']] | ['2016'] | ['http://id.loc.gov/vocabulary/iso639-1/de'] | ['commercial licence'] | [[{'@id': 'gnd:4326464-5'}, {'@id': 'gnd:4147194-5'}, {'@id': 'gnd:4279983-1'}]] | ['gnd:1150432454', 'gnd:2024276-1', 'gnd:4147194-5', 'gnd:4279983-1', 'gnd:4326464-5', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A874372089'] | ['Pöllmann, Herbert', 'Martin-Luther-Universität Halle-Wittenberg', 'Calciumsilicate', 'Zementherstellung', 'Nachhaltigkeit'] | 1 |
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"Das Reibauftragschwei\u00dfverfahren ist eine relativ neue und vielversprechende Technologie zur Oberfl\u00e4chenmodifikation technischer Komponenten. Hierbei k\u00f6nnen Beschichtungen zur lokalen Eigenschafts\u00e4nderung oder zu Reparaturzwecken erzeugt werden. Das Hauptmerkmal dieses Verfahrens, im Vergleich zu konventionellen Beschichtungsmethoden, ist, dass die Schichten in der Festphase aufgetragen werden. Durch die eingebrachte massive plastische Verformung des Werkstoffes \u00e4ndert sich die Mikrostruktur und es entsteht ein vollst\u00e4ndig rekristallisiertes Gef\u00fcge. Die Korngr\u00f6\u00dfe der entstandenen Schichten ist im Regelfall kleiner als die des Ausgangsmaterials, was zu verbesserten mechanischen Eigenschaften f\u00fchrt. Weil das Reibauftragschwei\u00dfen ein relativ neues Verfahren ist, sind einige der m\u00f6glichen Materialkombinationen in artgleichen und artfremden Paarungen noch unerforscht. Aufgrund dessen, dass Titanlegierungen als Ausgangswerkstoff kostspielig sind, sind neue Technologien, welche die Produktionskosten reduzieren k\u00f6nnen, von gro\u00dfem Interesse. Mit dem Reibauftragschwei\u00dfen bietet sich ein Beschichtungsverfahren an, welches auch modernen Anspr\u00fcchen an die Umweltvertr\u00e4glichkeit gerecht wird. Das Ziel der vorliegenden Arbeit war es, Schichten aus Titanlegierungen mittels Reibauftragschwei\u00dfen aufzutragen. Daf\u00fcr wurde die Prozessentwicklung f\u00fcr die Werkstoffe Ti-6Al-4V und Ti-Gr.1 realisiert. Titanlegierungen weisen ein komplexes Umformverhalten bei hohen Temperaturen auf, insbesondere, wenn sie sowohl den alpha-beta-, als auch den beta-Phasenbereich beim Umformen durchlaufen. Hierbei sind Dehnratenempfindlichkeit und Flie\u00dfinstabilit\u00e4t charakteristisch f\u00fcr Titanlegierungen, was die Verarbeitung beim Reibauftragschwei\u00dfen erschweren kann. Diese Schwierigkeiten wurden durch die systematische Erarbeitung geeigneter Prozessparameter und einer zielf\u00fchrenden Prozesssteuerung \u00fcberwunden. Es wurde ein breites Parameterfenster etabliert, innerhalb dessen zwei verschiedene Regimes der Drehzahlen gefunden wurden, zwischen denen sich das Materialverhalten deutlich unterscheidet. Das niedrige Drehzahl-Regime weist dabei Ver\u00e4nderungen in der Prozesstemperatur auf, welche die Flie\u00dfeigenschaften des Werkstoffs beeinflussen, was wiederum zu einer Wulstbildung an den Schichten f\u00fchrt. Die Mikrostruktur in diesem Regime offenbart feine, dynamisch rekristallisierte K\u00f6rner. Dazu gegens\u00e4tzlich weist das hohe Drehzahl-Regime eine h\u00f6here resultierende Temperatur auf, die in diesem Bereich nicht variiert. Die konstante Temperatur f\u00fchrt zu einem stabilen Materialflie\u00dfverhalten und erm\u00f6glicht damit eine dementsprechend wulstfreie Realisierung von Schichten. Allerdings f\u00fchren diese hohen Temperaturen zu einem Anstieg in der Korngr\u00f6\u00dfe. Die in Bezug auf die Korngr\u00f6\u00dfe unterschiedlich entwickelte Mikrostruktur zeigte keinen Einfluss auf das Schwingungsverschlei\u00dfverhalten der Schichten. Die Verschlei\u00dfeigenschaften der Schichten und des Grundwerkstoffs erwiesen sich als vergleichbar. Im Zuge von Mikroflachzug-Tests offenbarten die Schichten eine erh\u00f6hte Festigkeit mit leichten Einbu\u00dfen in der Duktilit\u00e4t, was ein charakteristisches Verhalten f\u00fcr dynamisch rekristallisierte Werkstoffe bei Vorhandensein von Restverformung ist. Somit konnte gezeigt werden, dass das Reibauftragschwei\u00dfen als Reparaturmethode f\u00fcr Titan- Bauteile, grunds\u00e4tzlich in Betracht gezogen werden kann."
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} | ['gnd:4185562-0', 'gnd:4053870-9'] | ['Schweißen', 'Titanlegierung'] | ['mas'] | ['gnd:1133309526'] | [['(doi)10.15480/882.1338', '(ppn)875851010', '(firstid)GBV:875851010']] | [''] | [['Titanium', '(classificationName=bk, id=106420070)52.82 - Fügetechnik', '(classificationName=linseach:mapping)mas', '(classificationName=ddc-dbn)670', 'Friction surfacing', '(classificationName=ddc)620: Ingenieurwissenschaften']] | ['Friction surfacing of titanium grade 1 and Ti-6Al-4V'] | [['The friction surfacing process is a relatively novel and promising surface modification technology, by which coatings can be deposited as a protection or surface repair method. The main feature of this process, compared with other technologies, is that the coatings are deposited in solid state phase. Therefore, the induced massive deformation alters the initial microstructure of the materials, resulting in a fully recrystallised microstructure of the coatings. Typically, the grain size of the coating is smaller than that of the raw material, which leads to improved mechanical properties. Since the process is a relatively new technology, several possible material combinations in similar or dissimilar configurations are unexplored. Titanium alloys are rather expensive. Therefore, new technologies are required to keep the production cost at an acceptable level and offer an additional cladding process that is environmental friendly. The aim of the current work was to deposit coatings from the titanium alloys by friction surfacing. Process development for Ti-6Al-4V alloy and Ti-Gr.1 as coating materials to be deposited by friction surfacing was carried out. At high temperatures titanium alloys exhibit complex deformation behaviour, particularly when passing through the alpha-beta phase transformation and in the beta phase state. Strain rate sensitivity and flow instabilities are characteristics of Ti-based materials that may hinder the deposition process. These difficulties were overcome by the selection of an adequate process control method and a systematic choice of process parameter combinations. A broad range of parameter sets for titanium depositions has been established, whereby two different acting rotational speed regimes were observed. The low rotational speed regime revealed variations in the process temperature, which influenced the material flow behaviour leading to flash generation at the coating. The microstructure in this regime consists of refined dynamically recrystallised grains. In contrast, the high rotational speed regime revealed a higher resulting temperature, which did not vary in this range. This constant temperature led to stable material flow behaviour and flash-free coatings were deposited. However, the high temperature influenced the grain size of the coatings resulting in coarse grains. Still, these differences in the grain size did not influence the fretting wear behaviour of the coatings. The investigation of fretting wear experiments exposed a similar behaviour of friction surfacing coatings and the base material. In micro tensile tests the coatings exhibited an increase in strength but a decrease in ductility, which is typical for dynamically recrystallised materials, which contain residual deformation. Therefore, it could be shown that friction surfacing can be considered as a repair method for titanium parts.', 'Das Reibauftragschweißverfahren ist eine relativ neue und vielversprechende Technologie zur Oberflächenmodifikation technischer Komponenten. Hierbei können Beschichtungen zur lokalen Eigenschaftsänderung oder zu Reparaturzwecken erzeugt werden. Das Hauptmerkmal dieses Verfahrens, im Vergleich zu konventionellen Beschichtungsmethoden, ist, dass die Schichten in der Festphase aufgetragen werden. Durch die eingebrachte massive plastische Verformung des Werkstoffes ändert sich die Mikrostruktur und es entsteht ein vollständig rekristallisiertes Gefüge. Die Korngröße der entstandenen Schichten ist im Regelfall kleiner als die des Ausgangsmaterials, was zu verbesserten mechanischen Eigenschaften führt. Weil das Reibauftragschweißen ein relativ neues Verfahren ist, sind einige der möglichen Materialkombinationen in artgleichen und artfremden Paarungen noch unerforscht. Aufgrund dessen, dass Titanlegierungen als Ausgangswerkstoff kostspielig sind, sind neue Technologien, welche die Produktionskosten reduzieren können, von großem Interesse. Mit dem Reibauftragschweißen bietet sich ein Beschichtungsverfahren an, welches auch modernen Ansprüchen an die Umweltverträglichkeit gerecht wird. Das Ziel der vorliegenden Arbeit war es, Schichten aus Titanlegierungen mittels Reibauftragschweißen aufzutragen. Dafür wurde die Prozessentwicklung für die Werkstoffe Ti-6Al-4V und Ti-Gr.1 realisiert. Titanlegierungen weisen ein komplexes Umformverhalten bei hohen Temperaturen auf, insbesondere, wenn sie sowohl den alpha-beta-, als auch den beta-Phasenbereich beim Umformen durchlaufen. Hierbei sind Dehnratenempfindlichkeit und Fließinstabilität charakteristisch für Titanlegierungen, was die Verarbeitung beim Reibauftragschweißen erschweren kann. Diese Schwierigkeiten wurden durch die systematische Erarbeitung geeigneter Prozessparameter und einer zielführenden Prozesssteuerung überwunden. Es wurde ein breites Parameterfenster etabliert, innerhalb dessen zwei verschiedene Regimes der Drehzahlen gefunden wurden, zwischen denen sich das Materialverhalten deutlich unterscheidet. Das niedrige Drehzahl-Regime weist dabei Veränderungen in der Prozesstemperatur auf, welche die Fließeigenschaften des Werkstoffs beeinflussen, was wiederum zu einer Wulstbildung an den Schichten führt. Die Mikrostruktur in diesem Regime offenbart feine, dynamisch rekristallisierte Körner. Dazu gegensätzlich weist das hohe Drehzahl-Regime eine höhere resultierende Temperatur auf, die in diesem Bereich nicht variiert. Die konstante Temperatur führt zu einem stabilen Materialfließverhalten und ermöglicht damit eine dementsprechend wulstfreie Realisierung von Schichten. Allerdings führen diese hohen Temperaturen zu einem Anstieg in der Korngröße. Die in Bezug auf die Korngröße unterschiedlich entwickelte Mikrostruktur zeigte keinen Einfluss auf das Schwingungsverschleißverhalten der Schichten. Die Verschleißeigenschaften der Schichten und des Grundwerkstoffs erwiesen sich als vergleichbar. Im Zuge von Mikroflachzug-Tests offenbarten die Schichten eine erhöhte Festigkeit mit leichten Einbußen in der Duktilität, was ein charakteristisches Verhalten für dynamisch rekristallisierte Werkstoffe bei Vorhandensein von Restverformung ist. Somit konnte gezeigt werden, dass das Reibauftragschweißen als Reparaturmethode für Titan- Bauteile, grundsätzlich in Betracht gezogen werden kann.']] | ['2016'] | ['http://id.loc.gov/vocabulary/iso639-1/en'] | ['open access'] | [[{'@id': 'gnd:4185562-0'}, {'@id': 'gnd:4053870-9'}]] | ['gnd:10184290-9', 'gnd:1133309526', 'gnd:2067664-5', 'gnd:4053870-9', 'gnd:4185562-0', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A875851010'] | ['Technische Universität Hamburg-Harburg, Institut für Werkstoffphysik und -technologie', 'Huber, Norbert', 'Technische Universität Hamburg-Harburg', 'Schweißen', 'Titanlegierung'] | 15 |
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} | ['gnd:4167928-3', 'gnd:4065317-1', 'gnd:4162299-6'] | ['Wellenleiter', 'Ionenstrahlätzen', 'Lithiumniobat'] | ['phy'] | ['Technische Informationsbibliothek (TIB)'] | [['(ppn)877741859', '(firstid)GBV:877741859']] | [''] | [['(classificationName=linseach:mapping)phy', '(classificationName=ddc)535.2', '(classificationName=ddc-dbn)530', '(classificationName=bk, id=106407449)33.38 - Quantenoptik, nichtlineare Optik']] | ['Micro and nanostructured lithium niobate for integrated nonlinear optics'] | ['The efficiency of nonlinear interaction processes in lithium niobate (LN) can be significantly enhanced by a confinement of the optical fields to waveguide or resonator modes. The functionalities of the optical elements strongly depend on their specific layout and can be implemented only with a sophisticated microstructure technology. This thesis, therefore, contributes to the advancement and development of existing patterning approaches and their application to the realization of microstructured waveguides and resonators. Especially the full potential of ion beam enhanced etching (IBEE) of LN is explored by the realization of advanced structures such as photonic crystals. Furthermore, a modified IBEE process which is based on KOH instead of HF is established after studying the etching behavior of ion beam irradiated LN in different hydroxide solutions for a broad range of experimental conditions. Substituting HF by KOH makes thin film LN substrates fully compatible with IBEE because KOH does not etch the intermediate silicon dioxide layer. IBEE is used in combination with electron beam lithography for large area patterning. In particular, it is used for the realization of nanoscale ridge waveguides and photonic crystal waveguides that are sufficiently long for the observation of propagation effects with a scanning near field optical microscope. In addition to IBEE, direct patterning of photonic structures by focused ion beam (FIB) is suitable for prototyping of small areas. The impact of gallium ion contaminations from the FIB milling, which remain in the substrate and impair the dimensional accuracy, is investigated. FIB patterning is eventually used to realize microdisk and photonic crystal resonators. Their linear and nonlinear optical characterization is presented, particularly the resonantly enhanced second harmonic generation from a photonic crystal resonator.'] | ['2016'] | ['http://id.loc.gov/vocabulary/iso639-1/en'] | ['open access'] | [[{'@id': 'gnd:4167928-3'}, {'@id': 'gnd:4065317-1'}, {'@id': 'gnd:4162299-6'}]] | ['gnd:112211561X', 'gnd:36164-1', 'gnd:4065317-1', 'gnd:4162299-6', 'gnd:4167928-3', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A877741859'] | ['Geiß, Reinhard', 'Friedrich-Schiller-Universität Jena', 'Wellenleiter', 'Ionenstrahlätzen', 'Lithiumniobat'] | 22 |
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} | ['gnd:4046699-1', 'gnd:4009840-0', 'gnd:4586449-4'] | ['Chemische Analyse', 'Polymere', 'MALDI-MS'] | ['che'] | ['Technische Informationsbibliothek (TIB)'] | [['(firstid)GBV:879182563', '(ppn)879182563']] | [''] | [['(classificationName=bk, id=106417525)35.80 - Makromolekulare Chemie', '(classificationName=ddc)547.8', '(classificationName=linseach:mapping)che', '(classificationName=bk, id=106417312)35.26 - Massenspektrometrie']] | ['Characterization of macromolecular systems by mass spectrometry and hyphenated techniques'] | ['The focus of this thesis was to gain in-depth structural information of synthetic polymers by the application of several combined techniques. The second chapter provides an overview about the influence of the polymer architecture on its characterization by mass spectrometry and complementary methods. In the third chapter, we demonstrate the use of MS, more specifically MALDI-ToF MS, which provides molar masses and dispersity values for poly(furfuryl glycidyl ether) (PFGE). The second example is the study of poly(N-isopropyl acrylamide) (PNiPAm) copolymers with glyco-monomers with specific combinations of matrices and cationization agents. The fourth chapter will combine three different examples regarding linear, star-shaped and hybrid polymers, which were analyzed by advanced techniques. The linear copolymers were analyzed by separating them according to their chemical heterogeneity using liquid absorption chromatography at critical conditions (LACCC) of poly(2-ethyl-2-oxazoline) (PEtOx), followed by automated spotting onto a MALDI target, which was subsequently analyzed by MALDI. Secondly, star-shaped polymers: [poly(ethylene oxide) (PEO)-b-PEtOx]8 were monitored firstly by using LACCC of linear PEO as first separation dimension and furthermore injected onto an SEC column confirming the molar mass. Lastly, a hybrid PEO star-shaped polymer was investigated using MALDI to verify the complete functionality of the core with PEO arms. Finally, the last chapter will focus on the creation of a software to obtain information regarding average composition, overcoming isotopic, overlapping peaks and isobaric species from MS spectra. Moreover, the quantitative studies were carried out by correction of the mass discrimination and isotopic abundance. Consequently, advanced analytical techniques such as different ionization techniques within MS, a range of chromatographic hyphenation and computational methods are implemented for elucidating the complexity of synthetic polymers.'] | ['2017'] | ['http://id.loc.gov/vocabulary/iso639-1/en'] | ['commercial licence'] | [[{'@id': 'gnd:4046699-1'}, {'@id': 'gnd:4009840-0'}, {'@id': 'gnd:4586449-4'}]] | ['gnd:1124709509', 'gnd:36164-1', 'gnd:4009840-0', 'gnd:4046699-1', 'gnd:4586449-4', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A879182563'] | ['Crotty, Sarah Charlotte', 'Friedrich-Schiller-Universität Jena', 'Chemische Analyse', 'Polymere', 'MALDI-MS'] | 5 |
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"The asset management is an indispensable and pre-conditional condition for its long-term existence and successful foundation work, especially for charitable foundations. Against the backdrop of the low-interest phase, which has now been going on for years, many board members are forced to open up more complex and risk-protected forms of investment, beyond the conservative or even secondary investment opportunities.The work examines, in particular, the extent to which the liability of the board of trustees must be appropriate and points out guidelines for asset management in foundations. The protection of the foundation as an autonomous fortune is of particular importance for dogmatic as well as for practical reasons. The work questions, among other things, the ways of reducing the liability risks of foundations, which is the subject of the foundation law as well as by the legislature, and calls on the greater professionalization of the decision-makers in the foundation, especially for the great majority of small and small foundations.",
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} | ['gnd:4022378-4', 'gnd:4158442-9', 'gnd:4121202-2'] | ['Gruppe', 'Entscheidungsprozess', 'Gruppenentscheidung'] | ['sow'] | ['Technische Informationsbibliothek (TIB)'] | [['(ppn)880286105', '(firstid)GBV:880286105']] | [''] | [['(classificationName=linseach:mapping)pae', '(classificationName=bk, id=106413104)77.64 - Gruppendynamik', '(classificationName=ddc)150', '(classificationName=linseach:mapping)sow', '(classificationName=ddc-dbn)150']] | ['Verzerrter Recall als potentielles Hindernis für Synergie bei Gruppenentscheidungen'] | [['In hidden profile decision-making tasks, groups often fall short of their potential to make a better decision than each individual group member. Several reasons for this phenomenon have already been established, such as biases regarding both the content of the group discussion and the individual evaluation of information relevant to the decision. This thesis looks into a further aspect of individual information processing where biases could be detrimental to the quality of group decisions: The individual recall of information relevant to the task at hand. Specifically, two biases are propos...', 'In Hidden Profiles gelingt es Gruppen häufig nicht, ihr Potenzial, bessere Entscheidungen als jedes ihrer Mitglieder zu treffen, zu erfüllen. Für dieses Phänomen wurden bereits verschiedene Ursachen ermittelt. Dazu gehören insbesondere Verzerrungen im Inhalt der Gruppendiskussion sowie der Bewertung von entscheidungsrelevanten Informationen durch die Gruppenmitglieder. In der vorliegenden Arbeit wird nun ein weiterer Aspekt individueller Informationsverarbeitung untersucht, dessen Verzerrung einen nachteiligen Einfluss auf die Entscheidungsqualität von Diskussionsgruppen haben könnte: der i...']] | ['2016'] | ['http://id.loc.gov/vocabulary/iso639-1/de'] | ['open access'] | [[{'@id': 'gnd:4022378-4'}, {'@id': 'gnd:4158442-9'}, {'@id': 'gnd:4121202-2'}]] | ['gnd:4022378-4', 'gnd:4121202-2', 'gnd:4158442-9', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A880286105'] | ['Gruppe', 'Entscheidungsprozess', 'Gruppenentscheidung'] | 25 |
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} | ['gnd:4156024-3', 'gnd:4041456-5', 'gnd:4022005-9'] | ['Grenzschicht', 'Navier-Stokes-Gleichung', 'Gas-Flüssigkeit-System'] | ['mat'] | ['Technische Informationsbibliothek (TIB)'] | [['(doi)10.6094/UNIFR/11679', '(ppn)880443847', '(firstid)BSZ:483458651', '(contract)FRUB-opus-11679']] | [''] | [['(classificationName=linseach:mapping)phy', '(classificationName=msc)35Q53', '(classificationName=msc)35Q35', '(classificationName=msc)76D05', '(classificationName=msc)35-02', '(classificationName=ddc)510', '(classificationName=msc)76T10', '(classificationName=linseach:mapping)mat', '(classificationName=ddc-dbn)510', '(classificationName=msc)76-02']] | ['Sharp-Interface limit for the Navier-Stokes-Korteweg equations'] | [['Abstract: Liquid-vapour flows can be described by two different types of mathematical models: known as diffuse- and sharp-interface models, respectively. The difference between them lies in the representation of the interfacial layer where phase transitions occur. While in diffuse-interface models this region has a small, but positive, thickness, in sharp-interface models an infinitesimally thin hypersurface is used instead. The diffuse-interface model can be related to the associated sharp-interface model by taking the limit where the thickness of the interfacial region tends to zero. We will call this the sharp-interface limit of the diffuse-interface model.Here, we investigate the sharp-interface limit for the Navier-Stokes-Korteweg model, which is an extension of the compressible Navier-Stokes equations.This diffuse-interface model for liquid-vapour flows was already proposed by the Dutch mathematician Diederik Johannes Korteweg in 1901.By means of compactness arguments, we show that solutions of the Navier-Stokes-Korteweg equations converge to solutions of a physically meaningful free-boundary problem. Assuming that an associated energy functional converges in a suitable sense, we obtain the sharp-interface limit at the level of weak solutions', 'Abstract: Flüssigkeits-Gas-Gemische können durch zwei unterschiedliche Arten von mathematischen Modellen beschrieben werden: diffuse und scharfe Grenzschicht-Modelle. Diese unterscheiden sich in der Darstellung der Grenzschicht in der Phasenübergänge stattfinden. Während dieser Bereich in diffusen Grenzschicht-Modellen eine kleine, positive Dicke besitzt, wird er in scharfen Grenzschicht-Modellen durch eine unendlich dünne Hyperfläche dargestellt. Um den Zusammenhang zwischen einem diffusen und einem scharfen Grenzschicht-Modell zu untersuchen, betrachtet man den Grenzwert für eine im Unendlichen verschwindende Grenzschichtdicke. Dieser wird als singulärer Grenzwert bezeichnet.Im Rahmen dieser Arbeit wird der singuläre Grenzwert des Navier-Stokes-Korteweg-Modells, einer Erweiterung der kompressiblen Navier-Stokes-Gleichungen, durchgeführt.Dieses diffuse Grenzschicht-Modell wurde bereits 1901 von dem niederländischen Mathematiker Diederik Johannes Korteweg vorgeschlagen.Mittels Kompaktheitsmethoden wird bewiesen, dass Lösungen der Navier-Stokes-Korte-weg-Gleichungen gegen Lösungen eines physikalisch sinnvollen freien Randwertproblems konvergieren. Unter der Annahme, dass ein zugehöriges Energiefunktional in einem geeigneten Sinn konvergiert, wird der Übergang zum singulären Grenzwert für schwache Lösungen durchgeführt']] | ['2017'] | ['http://id.loc.gov/vocabulary/iso639-1/en'] | ['open access'] | [[{'@id': 'gnd:4156024-3'}, {'@id': 'gnd:4041456-5'}, {'@id': 'gnd:4022005-9'}]] | ['gnd:1125456744', 'gnd:4022005-9', 'gnd:4041456-5', 'gnd:4156024-3', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A880443847'] | ['Daube, Johannes', 'Grenzschicht', 'Navier-Stokes-Gleichung', 'Gas-Flüssigkeit-System'] | 16 |
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} | ['gnd:7751254-6', 'gnd:4132693-3'] | ['Politische Institution', 'Verhaltensökonomie'] | ['oek'] | ['Technische Informationsbibliothek (TIB)'] | [['(ppn)880454806', '(firstid)GBV:880454806']] | [''] | [['Volkswirtschaft', '(classificationName=ddc-dbn)330', 'Verhaltensökonomik', 'Politisches System', '(classificationName=linseach:mapping)oek', '(classificationName=bk, id=106416332)83.00 - Volkswirtschaft: Allgemeines', 'Institutionelle Infrastruktur']] | ['Strategic communication, voting and political institutions : essays in behavioral political economy'] | ['Explaining how political institutions shape human behavior is one of the big challenges of social sciences. This thesis uses game theory, behavioral economics and the tools of experimental economics to study two topics in particular: information aggregation and legitimacy of institutions. While political decisions are most accurate when based on aggregated information, individuals with heterogeneous preferences over political issues often have no incentives to share their private information sincerely. The first two chapters investigate whether individuals - instead of strategic lying - resort to telling the truth as a simple heuristic in complex collective decisions and whether the desire to show one’s own expertise induces sincere communication. The last chapter studies how a political institution’s legitimacy influences the extent and efficacy of third-party punishment. The evidence presented in this thesis shows that individuals differ largely in their ability to lie strategically, they are more likely to tell the truth when they can signal their expertise in a prestigious knowledge area, and sanctions of a democratically legitimized institution are milder and more effective. Relaxing the standard assumptions of full rationality and self-interested preferences, and integrating cognitive constraints and behavioral motives such as image concerns and legitimacy in economic models is thus key to understanding political behavior.'] | ['2017'] | ['http://id.loc.gov/vocabulary/iso639-1/en'] | ['open access'] | [[{'@id': 'gnd:7751254-6'}, {'@id': 'gnd:4132693-3'}]] | ['gnd:1093235373', 'gnd:36164-1', 'gnd:4132693-3', 'gnd:7751254-6', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A880454806'] | ['Marcin, Isabel', 'Friedrich-Schiller-Universität Jena', 'Politische Institution', 'Verhaltensökonomie'] | 19 |
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} | ['gnd:4193873-2', 'gnd:4141899-2', 'gnd:4185549-8'] | ['Alkohole', 'Titandioxid', 'Fotokatalyse'] | ['che'] | [['gnd:131454617', 'gnd:171963172']] | [['(firstid)GBV:880580402', '(ppn)880580402']] | [''] | [['(classificationName=bk, id=106417266)35.17 - Katalyse', '(classificationName=linseach:mapping)che', '(classificationName=bk, id=106407791)35.16 - Photochemie', '(classificationName=ddc-dbn)540']] | ['Photokatalytische Oxidation niedermolekularer Alkohole'] | ['Photokatalyse, Titandioxid, niedermolekulare Alkohole, HPLC-Analyse, NASH-Methode. - Photocatalysis, titanium dioxide, low molecular weight alcohols, HPLC-analysis, NASH-analysis'] | ['2017'] | ['http://id.loc.gov/vocabulary/iso639-1/de'] | ['open access'] | [[{'@id': 'gnd:4193873-2'}, {'@id': 'gnd:4141899-2'}, {'@id': 'gnd:4185549-8'}]] | ['gnd:131454617', 'gnd:171963172', 'gnd:4141899-2', 'gnd:4185549-8', 'gnd:4193873-2', 'gnd:64681-7', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A880580402'] | ['Renz, Franz', 'Bahnemann, Detlef', 'Alkohole', 'Titandioxid', 'Fotokatalyse', 'Gottfried Wilhelm Leibniz Universität Hannover'] | 5 |
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} | ['gnd:4207952-4', 'gnd:4045539-7', 'gnd:4300564-0'] | ['Pflanzen', 'Tandem-Massenspektrometrie', 'Sekundärmetabolit'] | ['che'] | ['Technische Informationsbibliothek (TIB)'] | [['(ppn)880811382', '(firstid)GBV:880811382']] | [''] | [['(classificationName=ddc)547.7', '(classificationName=ddc-dbn)570', '(classificationName=linseach:mapping)che', '(classificationName=bk, id=106417312)35.26 - Massenspektrometrie']] | ['Tissue and population-level diversity in plant secondary metabolism : a systematic exploration using MS/MS structural analysis'] | ['Plants are amazing synthetic chemists that create diversified secondary metabolites which play myriad ecological roles for their survival and reproductive fitness in nature. The structural complexity of secondary metabolism has severely hampered its functional analysis. The potential of MS-based metabolomics and of the large-scale acquisition of tandem MS (MS/MS) spectra is limited by the absence of straightforward classification and visualization pipelines so that secondary metabolite and the underlying pathway interpretations can be easily made. From a mechanistic standpoint, secondary metabolism diversity attributes to the occurrence of multiplicity of genes in plant genomes. Yet the majorities of metabolic gene functions remain however unknown. In this thesis, I developed a workflow to systematically explore the diversity of secondary metabolism in Nicotiana attenuata – a metabolically rich ecological model plant. I first characterize the metabolic space of this model plant using the large-scale acquisition of MS/MS spectral information in a data-independent manner and the computational re-assembly of non-redundant MS/MS spectra. The resulting MS signatures were then aligned and visualized to rapidly formulate structural hypotheses. Using natural variation, I examined the correlations among jasmonate signaling and large-scale defense metabolism. The resulting correlation maps uncovered new metabolic layers in a plant’s jasmonate-mediated defensive arsenal. In the tissue-level exploration of secondary metabolite diversity, Transciptomic and metabolomic information and their variance as analyzed by information theory were used for the predictions of tissue-specific function of genes responsible for the metabolic signatures.'] | ['2017'] | ['http://id.loc.gov/vocabulary/iso639-1/en'] | ['open access'] | [[{'@id': 'gnd:4207952-4'}, {'@id': 'gnd:4045539-7'}, {'@id': 'gnd:4300564-0'}]] | ['gnd:1124709711', 'gnd:36164-1', 'gnd:4045539-7', 'gnd:4207952-4', 'gnd:4300564-0', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A880811382'] | ['Li, Dapeng', 'Friedrich-Schiller-Universität Jena', 'Pflanzen', 'Tandem-Massenspektrometrie', 'Sekundärmetabolit'] | 5 |
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} | ['gnd:4384866-7', 'gnd:4314752-5'] | ['Zirkumstellare Hülle', 'Kosmischer Staub'] | ['rest'] | ['Technische Informationsbibliothek (TIB)'] | [['(firstid)GBV:880854782', '(ppn)880854782']] | [''] | [['(classificationName=linseach:mapping)rest', '(classificationName=bk, id=10640699X)39.43 - Interstellare Materie', '(classificationName=ddc-dbn)520', '(classificationName=ddc)523.113']] | ['Collisional modelling of resolved debris discs'] | ["Debris discs are optically thin circumstellar discs that comprise solids in a broad range of sizes, from (sub)micron-sized dust grains up to kilometre-sized planetesimals. The dust component of debris discs is short-lived and continuously replenished through collisional attrition between planetesimals in reservoirs analogous to the Solar system's asteroid and Kuiper belts. Together with planets, debris discs are believed to be the end product of the star and planet formation process. In this thesis, collisional modelling is employed, which simulates the long-term collisional evolution from planetesimals to dust. The calculated dust distributions are used for the comparison with observational data. This powerful technique reveals properties of the underlying dust-producing planetesimal belts which are not directly discernible by observations. The code ACE of the Jena AIU group predicts the evolution of rotationally-symmetric debris discs. ACE calculates collisions between ensembles of circumstellar objects and considers the influence of stellar gravity as well as stellar radiative and corpuscular forces. The code is applied to the systems HIP 17439, AU Mic, and q1 Eri, where the outer part of a debris disc is spatially resolved at multiple wavelengths. All three systems show hints for warm and cold dust populations. The modelling addresses the question of what might be their origin. Two scenarios are considered: a Solar system-like architecture with two planetesimal belts as in-situ sources of dust (Scenario I), and an outer planetesimal belt from which dust is transported inwards by Poynting-Robertson and stellar wind drag (Scenario II). While Scenario I seems to be the most plausible for q1 Eri, Scenario II is preferred for AU Mic. However, no strict conclusion can be drawn for HIP 17439, where both scenarios are possible. More than two planetesimal belts or even a radially extended planetesimal belt cannot be excluded either."] | ['2017'] | ['http://id.loc.gov/vocabulary/iso639-1/de'] | ['open access'] | [[{'@id': 'gnd:4384866-7'}, {'@id': 'gnd:4314752-5'}]] | ['gnd:1124709053', 'gnd:36164-1', 'gnd:4314752-5', 'gnd:4384866-7', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A880854782'] | ['Schüppler, Christian', 'Friedrich-Schiller-Universität Jena', 'Zirkumstellare Hülle', 'Kosmischer Staub'] | 24 |
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"Nanoporous gold (npg), a bicontinuous network of nanoscale gold ligaments and pores, displays tunable mechanical behavior through the variation of internal length-scales. However, it is severely limited by its lack of ductility in tension. By infiltrating the porous structure with epoxy, a composite material with enhanced tensile ductility and ow stress is achieved. The present work aims at a three-fold investigation of micromechanical behavior, mechanisms of deformation and failure of the npg-epoxy composite, focusing on 3D microstructural characterization, finite element simulation and micromechanical testing. In order to understand the composite microstructure, high resolution 3D reconstructions of the npg ligament network were achieved with focused ion beam (FIB) based tomography, taking advantage of epoxy infiltration on FIB machining of porous media. It is assumed that the infiltration of epoxy does not significantly alter the geometry of the npg network. Samples of varying structural length-scales were used, with mean ligament diameters in the range of tens to hundreds of nanometers, as achieved through isothermal annealing of npg. Quantitative analyses of the 3D reconstructions were carried out in terms of metric properties (e.g., relative density, ligament diameter distribution and specific surface area), topological properties (e.g., connectivity density), and directional properties (e.g., directional tortuosity). Importantly, representative volumes (RVs) were identified, which reflects the global structural properties of the material. It was found that npg coarsens in a nearly self-similar manner. This allows the identification of structural parameters, which can be used to describe the mechanical behavior of the global npg structure over varying length scales. FEM simulations applied to meshed RVs of the 3D reconstructions strongly suggest that the effective relative density of the load bearing ligament structure is the critical structural parameter in determining the mechanical behavior of npg structural geometry, rather than the solid relative density alone, as is often assumed. After infiltration with epoxy, the densification during deformation of npg-epoxy composites is strongly suppressed. This leads to a strongly enhanced strength compared to pure npg. However, the dependence of the yield strength on the mean ligament size is much weaker in the composite structure as compared to pure npg. The size effects in pure npg have been commonly attributed to dislocation activities within the gold ligaments, whereas in the composite material the influence of the interface on the motion of the dislocations and the epoxy chains must be considered. The interfacial behavior leads to a strengthening effect in the composites but weakens the size effects. The comparisons of the elastic moduli from the analytical models predictions, the experiments and the FEM simulations demonstrated the influences of the connectivity, the effective relative density of the load bearing ligament structure, the directional tortuosity of the ligaments and the interface on the elastic behavior of the npg-epoxy composites. Interfacial failure was experimentally observed under compression and tension. The tension-compression asymmetry investigation revealed that the npg-epoxy composite is stronger in compression than in tension. These various observations point to the important roles that the hard phase, i.e., the interconnected ligament network, the soft phase, i.e., the continuous epoxy, and the interface between them play on the mechanical behavior of npg-epoxy composites.",
"Nanopor\u00f6ses Gold (NPG), ein bikontinuierliches Netzwerk aus nanoskaligen Goldligamenten und Poren, weist durch Variation der inneren L\u00e4ngenskalen ein abstimmbares mechanisches Verhalten auf. Allerdings ist es schwerwiegend eingeschr\u00e4nkt durch seinen Mangel an Verformbarkeit unter Zugspannung. Durch Infiltration der por\u00f6sen Struktur mit Epoxid erh\u00e4lt man ein Kompositmaterial mit verbesserter Zugverformbarkeit und Flie\u00dfspannung. Die vorliegende Arbeit strebt eine dreifache Untersuchung des mikromechanischen Verhaltens, der Verformungsmechanismen und des mechanischen Versagens von NPG-Epoxid Kompositen an, durch Fokussierung auf 3D Mikrostrukturcharakterisierung, Finite Elemente Simulation (FEM) und mikromechanische Pr\u00fcfung. Um die Kompositmikrostruktur zu verstehen wurden hochaufgel\u00f6ste 3D Rekonstruktionen mit auf fokussierten Ionenstrahlen (focused ion beam, FIB) basierter Tomographie hergestellt, m\u00f6glich gemacht durch den positiven Effekt der Infiltration mit Epoxid auf die Bearbeitung por\u00f6ser Medien mit FIB. Dabei wird angenommen, dass die Epoxidinfiltration die Geometrie des NPG Netzwerks nicht signifikant \u00e4ndert. Proben mit unterschiedlichen strukturellen L\u00e4ngen wurden verwendet, d.h. mit mittleren Ligamentdurchmessern im Bereich von einigen 10 bis mehrere 100 nm, erreicht durch isothermes Anlassen. Es wurden quantitative Analysen der 3D Rekonstruktionen durchgef\u00fchrt hinsichtlich der metrischen Eigenschaften (z.B. relative Dichte, Verteilungen der Ligamentdurchmesser und spezifische Oberfl\u00e4che), topologischen Eigenschaften (z.B. Konnektivit\u00e4tsdichten) und richtungsabh\u00e4ngigen Eigenschaften (z.B. Richtungstortuosit\u00e4t). Von gro\u00dfer Wichtigkeit war die Identifikation von repr\u00e4sentativen Volumen (RV), die die globalen Struktureigenschaften des Materials reflektieren. Es wurde herausgefunden, dass NPG nahezu selbst\u00e4hnlich vergr\u00f6bert. Dies erlaubt die Identifizierung struktureller Gr\u00f6\u00dfen, die zur Beschreibung des mechanischen Verhaltens globaler NPG Strukturen \u00fcber variierende L\u00e4ngenskalen verwendet werden k\u00f6nnen. FEM Simulationen angewendet auf vermaschte RV der 3D Rekonstruktionen weisen stark darauf hin, dass die effektive relative Dichte der lasttragenden Ligamentstruktur die kritische Gr\u00f6\u00dfe in der Bestimmung des mechanischen Verhaltens der NPG Strukturgeometrie ist, eher als die relative Dichte der festen Phase wie oft angenommen. Nach der Infiltration mit Epoxid ist die Verdichtung von NPG-Epoxid Kompositen unter Verformung stark unterdr\u00fcckt. Dies f\u00fchrt zu einer stark verbesserten Festigkeit im Vergleich zu reinem NPG. Allerdings ist die Abh\u00e4ngigkeit der Flie\u00dfgrenze von der mittleren Ligamentgr\u00f6\u00dfe viel schw\u00e4cher in der Kompositstruktur verglichen mit reinem NPG. Die Gr\u00f6\u00dfeneffekte in reinem NPG sind \u00fcblicherweise Versetzungsaktivit\u00e4ten in den Goldligamenten zugeordnet worden, wogegen im Kompositmaterial der Einfluss der Grenzfl\u00e4che auf die Versetzungsbewegung und die Epoxidketten in Betracht gezogen werden muss. Das Grenzfl\u00e4chenverhalten f\u00fchrt zu einem Verst\u00e4rkungseffekt in den Kompositen aber schw\u00e4cht die Gr\u00f6\u00dfeneffekte ab. Die Vergleiche der Elastizit\u00e4tsmoduln aus den Vorhersagen der analytischen Modelle, den Experimenten und der FEM Simulationen demonstrierten die Einfl\u00fcsse der Konnektivit\u00e4t, der effektiven relativen Dichte der lasttragenden Ligamentstruktur, der Richtungstortuosit\u00e4t der Ligamente und der Grenzfl\u00e4che auf das elastische Verhalten der NPG-Epoxid Komposite. Grenzfl\u00e4chenversagen wurde experimentell beobachtet unter Kompression und Zug. Die Untersuchung der Zug-Druck Asymmetrie zeigte, dass das NPG-Epoxid Komposit st\u00e4rker unter Druck als unter Zug ist. Diese unterschiedlichen Beobachtungen zeigen die wichtigen Rollen auf, die die harte Phase, also das verkn\u00fcpfte Ligamentnetzwerk, die weiche Phase, d.h. das kontinuierliche Epoxid, und die Grenzfl\u00e4che zwischen ihnen f\u00fcr das mechanische Verhalten von NPG-Epoxid Komposite spielen."
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However, it is severely limited by its lack of ductility in tension. By infiltrating the porous structure with epoxy, a composite material with enhanced tensile ductility and ow stress is achieved. The present work aims at a three-fold investigation of micromechanical behavior, mechanisms of deformation and failure of the npg-epoxy composite, focusing on 3D microstructural characterization, finite element simulation and micromechanical testing. In order to understand the composite microstructure, high resolution 3D reconstructions of the npg ligament network were achieved with focused ion beam (FIB) based tomography, taking advantage of epoxy infiltration on FIB machining of porous media. It is assumed that the infiltration of epoxy does not significantly alter the geometry of the npg network. Samples of varying structural length-scales were used, with mean ligament diameters in the range of tens to hundreds of nanometers, as achieved through isothermal annealing of npg. Quantitative analyses of the 3D reconstructions were carried out in terms of metric properties (e.g., relative density, ligament diameter distribution and specific surface area), topological properties (e.g., connectivity density), and directional properties (e.g., directional tortuosity). Importantly, representative volumes (RVs) were identified, which reflects the global structural properties of the material. It was found that npg coarsens in a nearly self-similar manner. This allows the identification of structural parameters, which can be used to describe the mechanical behavior of the global npg structure over varying length scales. FEM simulations applied to meshed RVs of the 3D reconstructions strongly suggest that the effective relative density of the load bearing ligament structure is the critical structural parameter in determining the mechanical behavior of npg structural geometry, rather than the solid relative density alone, as is often assumed. After infiltration with epoxy, the densification during deformation of npg-epoxy composites is strongly suppressed. This leads to a strongly enhanced strength compared to pure npg. However, the dependence of the yield strength on the mean ligament size is much weaker in the composite structure as compared to pure npg. The size effects in pure npg have been commonly attributed to dislocation activities within the gold ligaments, whereas in the composite material the influence of the interface on the motion of the dislocations and the epoxy chains must be considered. The interfacial behavior leads to a strengthening effect in the composites but weakens the size effects. The comparisons of the elastic moduli from the analytical models predictions, the experiments and the FEM simulations demonstrated the influences of the connectivity, the effective relative density of the load bearing ligament structure, the directional tortuosity of the ligaments and the interface on the elastic behavior of the npg-epoxy composites. Interfacial failure was experimentally observed under compression and tension. The tension-compression asymmetry investigation revealed that the npg-epoxy composite is stronger in compression than in tension. These various observations point to the important roles that the hard phase, i.e., the interconnected ligament network, the soft phase, i.e., the continuous epoxy, and the interface between them play on the mechanical behavior of npg-epoxy composites.', 'Nanoporöses Gold (NPG), ein bikontinuierliches Netzwerk aus nanoskaligen Goldligamenten und Poren, weist durch Variation der inneren Längenskalen ein abstimmbares mechanisches Verhalten auf. Allerdings ist es schwerwiegend eingeschränkt durch seinen Mangel an Verformbarkeit unter Zugspannung. Durch Infiltration der porösen Struktur mit Epoxid erhält man ein Kompositmaterial mit verbesserter Zugverformbarkeit und Fließspannung. Die vorliegende Arbeit strebt eine dreifache Untersuchung des mikromechanischen Verhaltens, der Verformungsmechanismen und des mechanischen Versagens von NPG-Epoxid Kompositen an, durch Fokussierung auf 3D Mikrostrukturcharakterisierung, Finite Elemente Simulation (FEM) und mikromechanische Prüfung. Um die Kompositmikrostruktur zu verstehen wurden hochaufgelöste 3D Rekonstruktionen mit auf fokussierten Ionenstrahlen (focused ion beam, FIB) basierter Tomographie hergestellt, möglich gemacht durch den positiven Effekt der Infiltration mit Epoxid auf die Bearbeitung poröser Medien mit FIB. Dabei wird angenommen, dass die Epoxidinfiltration die Geometrie des NPG Netzwerks nicht signifikant ändert. Proben mit unterschiedlichen strukturellen Längen wurden verwendet, d.h. mit mittleren Ligamentdurchmessern im Bereich von einigen 10 bis mehrere 100 nm, erreicht durch isothermes Anlassen. Es wurden quantitative Analysen der 3D Rekonstruktionen durchgeführt hinsichtlich der metrischen Eigenschaften (z.B. relative Dichte, Verteilungen der Ligamentdurchmesser und spezifische Oberfläche), topologischen Eigenschaften (z.B. Konnektivitätsdichten) und richtungsabhängigen Eigenschaften (z.B. Richtungstortuosität). Von großer Wichtigkeit war die Identifikation von repräsentativen Volumen (RV), die die globalen Struktureigenschaften des Materials reflektieren. Es wurde herausgefunden, dass NPG nahezu selbstähnlich vergröbert. Dies erlaubt die Identifizierung struktureller Größen, die zur Beschreibung des mechanischen Verhaltens globaler NPG Strukturen über variierende Längenskalen verwendet werden können. FEM Simulationen angewendet auf vermaschte RV der 3D Rekonstruktionen weisen stark darauf hin, dass die effektive relative Dichte der lasttragenden Ligamentstruktur die kritische Größe in der Bestimmung des mechanischen Verhaltens der NPG Strukturgeometrie ist, eher als die relative Dichte der festen Phase wie oft angenommen. Nach der Infiltration mit Epoxid ist die Verdichtung von NPG-Epoxid Kompositen unter Verformung stark unterdrückt. Dies führt zu einer stark verbesserten Festigkeit im Vergleich zu reinem NPG. Allerdings ist die Abhängigkeit der Fließgrenze von der mittleren Ligamentgröße viel schwächer in der Kompositstruktur verglichen mit reinem NPG. Die Größeneffekte in reinem NPG sind üblicherweise Versetzungsaktivitäten in den Goldligamenten zugeordnet worden, wogegen im Kompositmaterial der Einfluss der Grenzfläche auf die Versetzungsbewegung und die Epoxidketten in Betracht gezogen werden muss. Das Grenzflächenverhalten führt zu einem Verstärkungseffekt in den Kompositen aber schwächt die Größeneffekte ab. Die Vergleiche der Elastizitätsmoduln aus den Vorhersagen der analytischen Modelle, den Experimenten und der FEM Simulationen demonstrierten die Einflüsse der Konnektivität, der effektiven relativen Dichte der lasttragenden Ligamentstruktur, der Richtungstortuosität der Ligamente und der Grenzfläche auf das elastische Verhalten der NPG-Epoxid Komposite. Grenzflächenversagen wurde experimentell beobachtet unter Kompression und Zug. Die Untersuchung der Zug-Druck Asymmetrie zeigte, dass das NPG-Epoxid Komposit stärker unter Druck als unter Zug ist. Diese unterschiedlichen Beobachtungen zeigen die wichtigen Rollen auf, die die harte Phase, also das verknüpfte Ligamentnetzwerk, die weiche Phase, d.h. das kontinuierliche Epoxid, und die Grenzfläche zwischen ihnen für das mechanische Verhalten von NPG-Epoxid Komposite spielen.']] | ['2017'] | ['http://id.loc.gov/vocabulary/iso639-1/en'] | ['open access'] | [[{'@id': 'gnd:1076028772'}, {'@id': 'gnd:4062670-2'}]] | ['gnd:10194308-8', 'gnd:1076028772', 'gnd:1138805939', 'gnd:2067664-5', 'gnd:4062670-2', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A880948493'] | ['Technische Universität Hamburg-Harburg, Institut für Keramische Hochleistungswerkstoffe', 'Werkstoffmechanik', 'Lilleodden, Erica', 'Technische Universität Hamburg-Harburg', 'Verbundwerkstoff'] | 7 |
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"Nanoporous gold (npg), a bicontinuous network of nanoscale gold ligaments and pores, displays tunable mechanical behavior through the variation of internal length-scales. However, it is severely limited by its lack of ductility in tension. By infiltrating the porous structure with epoxy, a composite material with enhanced tensile ductility and ow stress is achieved. The present work aims at a three-fold investigation of micromechanical behavior, mechanisms of deformation and failure of the npg-epoxy composite, focusing on 3D microstructural characterization, finite element simulation and micromechanical testing. In order to understand the composite microstructure, high resolution 3D reconstructions of the npg ligament network were achieved with focused ion beam (FIB) based tomography, taking advantage of epoxy infiltration on FIB machining of porous media. It is assumed that the infiltration of epoxy does not significantly alter the geometry of the npg network. Samples of varying structural length-scales were used, with mean ligament diameters in the range of tens to hundreds of nanometers, as achieved through isothermal annealing of npg. Quantitative analyses of the 3D reconstructions were carried out in terms of metric properties (e.g., relative density, ligament diameter distribution and specific surface area), topological properties (e.g., connectivity density), and directional properties (e.g., directional tortuosity). Importantly, representative volumes (RVs) were identified, which reflects the global structural properties of the material. It was found that npg coarsens in a nearly self-similar manner. This allows the identification of structural parameters, which can be used to describe the mechanical behavior of the global npg structure over varying length scales. FEM simulations applied to meshed RVs of the 3D reconstructions strongly suggest that the effective relative density of the load bearing ligament structure is the critical structural parameter in determining the mechanical behavior of npg structural geometry, rather than the solid relative density alone, as is often assumed. After infiltration with epoxy, the densification during deformation of npg-epoxy composites is strongly suppressed. This leads to a strongly enhanced strength compared to pure npg. However, the dependence of the yield strength on the mean ligament size is much weaker in the composite structure as compared to pure npg. The size effects in pure npg have been commonly attributed to dislocation activities within the gold ligaments, whereas in the composite material the influence of the interface on the motion of the dislocations and the epoxy chains must be considered. The interfacial behavior leads to a strengthening effect in the composites but weakens the size effects. The comparisons of the elastic moduli from the analytical models predictions, the experiments and the FEM simulations demonstrated the influences of the connectivity, the effective relative density of the load bearing ligament structure, the directional tortuosity of the ligaments and the interface on the elastic behavior of the npg-epoxy composites. Interfacial failure was experimentally observed under compression and tension. The tension-compression asymmetry investigation revealed that the npg-epoxy composite is stronger in compression than in tension. These various observations point to the important roles that the hard phase, i.e., the interconnected ligament network, the soft phase, i.e., the continuous epoxy, and the interface between them play on the mechanical behavior of npg-epoxy composites.",
"Nanopor\u00f6ses Gold (NPG), ein bikontinuierliches Netzwerk aus nanoskaligen Goldligamenten und Poren, weist durch Variation der inneren L\u00e4ngenskalen ein abstimmbares mechanisches Verhalten auf. Allerdings ist es schwerwiegend eingeschr\u00e4nkt durch seinen Mangel an Verformbarkeit unter Zugspannung. Durch Infiltration der por\u00f6sen Struktur mit Epoxid erh\u00e4lt man ein Kompositmaterial mit verbesserter Zugverformbarkeit und Flie\u00dfspannung. Die vorliegende Arbeit strebt eine dreifache Untersuchung des mikromechanischen Verhaltens, der Verformungsmechanismen und des mechanischen Versagens von NPG-Epoxid Kompositen an, durch Fokussierung auf 3D Mikrostrukturcharakterisierung, Finite Elemente Simulation (FEM) und mikromechanische Pr\u00fcfung. Um die Kompositmikrostruktur zu verstehen wurden hochaufgel\u00f6ste 3D Rekonstruktionen mit auf fokussierten Ionenstrahlen (focused ion beam, FIB) basierter Tomographie hergestellt, m\u00f6glich gemacht durch den positiven Effekt der Infiltration mit Epoxid auf die Bearbeitung por\u00f6ser Medien mit FIB. Dabei wird angenommen, dass die Epoxidinfiltration die Geometrie des NPG Netzwerks nicht signifikant \u00e4ndert. Proben mit unterschiedlichen strukturellen L\u00e4ngen wurden verwendet, d.h. mit mittleren Ligamentdurchmessern im Bereich von einigen 10 bis mehrere 100 nm, erreicht durch isothermes Anlassen. Es wurden quantitative Analysen der 3D Rekonstruktionen durchgef\u00fchrt hinsichtlich der metrischen Eigenschaften (z.B. relative Dichte, Verteilungen der Ligamentdurchmesser und spezifische Oberfl\u00e4che), topologischen Eigenschaften (z.B. Konnektivit\u00e4tsdichten) und richtungsabh\u00e4ngigen Eigenschaften (z.B. Richtungstortuosit\u00e4t). Von gro\u00dfer Wichtigkeit war die Identifikation von repr\u00e4sentativen Volumen (RV), die die globalen Struktureigenschaften des Materials reflektieren. Es wurde herausgefunden, dass NPG nahezu selbst\u00e4hnlich vergr\u00f6bert. Dies erlaubt die Identifizierung struktureller Gr\u00f6\u00dfen, die zur Beschreibung des mechanischen Verhaltens globaler NPG Strukturen \u00fcber variierende L\u00e4ngenskalen verwendet werden k\u00f6nnen. FEM Simulationen angewendet auf vermaschte RV der 3D Rekonstruktionen weisen stark darauf hin, dass die effektive relative Dichte der lasttragenden Ligamentstruktur die kritische Gr\u00f6\u00dfe in der Bestimmung des mechanischen Verhaltens der NPG Strukturgeometrie ist, eher als die relative Dichte der festen Phase wie oft angenommen. Nach der Infiltration mit Epoxid ist die Verdichtung von NPG-Epoxid Kompositen unter Verformung stark unterdr\u00fcckt. Dies f\u00fchrt zu einer stark verbesserten Festigkeit im Vergleich zu reinem NPG. Allerdings ist die Abh\u00e4ngigkeit der Flie\u00dfgrenze von der mittleren Ligamentgr\u00f6\u00dfe viel schw\u00e4cher in der Kompositstruktur verglichen mit reinem NPG. Die Gr\u00f6\u00dfeneffekte in reinem NPG sind \u00fcblicherweise Versetzungsaktivit\u00e4ten in den Goldligamenten zugeordnet worden, wogegen im Kompositmaterial der Einfluss der Grenzfl\u00e4che auf die Versetzungsbewegung und die Epoxidketten in Betracht gezogen werden muss. Das Grenzfl\u00e4chenverhalten f\u00fchrt zu einem Verst\u00e4rkungseffekt in den Kompositen aber schw\u00e4cht die Gr\u00f6\u00dfeneffekte ab. Die Vergleiche der Elastizit\u00e4tsmoduln aus den Vorhersagen der analytischen Modelle, den Experimenten und der FEM Simulationen demonstrierten die Einfl\u00fcsse der Konnektivit\u00e4t, der effektiven relativen Dichte der lasttragenden Ligamentstruktur, der Richtungstortuosit\u00e4t der Ligamente und der Grenzfl\u00e4che auf das elastische Verhalten der NPG-Epoxid Komposite. Grenzfl\u00e4chenversagen wurde experimentell beobachtet unter Kompression und Zug. Die Untersuchung der Zug-Druck Asymmetrie zeigte, dass das NPG-Epoxid Komposit st\u00e4rker unter Druck als unter Zug ist. Diese unterschiedlichen Beobachtungen zeigen die wichtigen Rollen auf, die die harte Phase, also das verkn\u00fcpfte Ligamentnetzwerk, die weiche Phase, d.h. das kontinuierliche Epoxid, und die Grenzfl\u00e4che zwischen ihnen f\u00fcr das mechanische Verhalten von NPG-Epoxid Komposite spielen."
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} | ['gnd:1076028772', 'gnd:4062670-2'] | ['Werkstoffmechanik', 'Verbundwerkstoff'] | ['phy'] | [['Technische Informationsbibliothek (TIB)', {'@id': 'gnd:1138805939'}]] | [['(ppn)880948493', '(firstid)GBV:880948493', '(doi)10.15480/882.1354']] | [''] | [['Composites', '3D microstructure analysis', '(classificationName=linseach:mapping)fer', '(classificationName=bk, id=106418769)51.32 - Werkstoffmechanik', 'Focused ion beam tomography', '(classificationName=ddc-dbn)620', '(classificationName=linseach:mapping)phy', '(classificationName=ddc)620: Ingenieurwissenschaften', 'Nanomechanics', 'FEM simulation', '(classificationName=bk, id=106416707)51.75 - Verbundwerkstoffe, Schichtstoffe', 'Nanoporous gold']] | ['Micromechanical and three-dimensional microstructural characterization of nanoporous gold-epoxy composites'] | [['Nanoporous gold (npg), a bicontinuous network of nanoscale gold ligaments and pores, displays tunable mechanical behavior through the variation of internal length-scales. However, it is severely limited by its lack of ductility in tension. By infiltrating the porous structure with epoxy, a composite material with enhanced tensile ductility and ow stress is achieved. The present work aims at a three-fold investigation of micromechanical behavior, mechanisms of deformation and failure of the npg-epoxy composite, focusing on 3D microstructural characterization, finite element simulation and micromechanical testing. In order to understand the composite microstructure, high resolution 3D reconstructions of the npg ligament network were achieved with focused ion beam (FIB) based tomography, taking advantage of epoxy infiltration on FIB machining of porous media. It is assumed that the infiltration of epoxy does not significantly alter the geometry of the npg network. Samples of varying structural length-scales were used, with mean ligament diameters in the range of tens to hundreds of nanometers, as achieved through isothermal annealing of npg. Quantitative analyses of the 3D reconstructions were carried out in terms of metric properties (e.g., relative density, ligament diameter distribution and specific surface area), topological properties (e.g., connectivity density), and directional properties (e.g., directional tortuosity). Importantly, representative volumes (RVs) were identified, which reflects the global structural properties of the material. It was found that npg coarsens in a nearly self-similar manner. This allows the identification of structural parameters, which can be used to describe the mechanical behavior of the global npg structure over varying length scales. FEM simulations applied to meshed RVs of the 3D reconstructions strongly suggest that the effective relative density of the load bearing ligament structure is the critical structural parameter in determining the mechanical behavior of npg structural geometry, rather than the solid relative density alone, as is often assumed. After infiltration with epoxy, the densification during deformation of npg-epoxy composites is strongly suppressed. This leads to a strongly enhanced strength compared to pure npg. However, the dependence of the yield strength on the mean ligament size is much weaker in the composite structure as compared to pure npg. The size effects in pure npg have been commonly attributed to dislocation activities within the gold ligaments, whereas in the composite material the influence of the interface on the motion of the dislocations and the epoxy chains must be considered. The interfacial behavior leads to a strengthening effect in the composites but weakens the size effects. The comparisons of the elastic moduli from the analytical models predictions, the experiments and the FEM simulations demonstrated the influences of the connectivity, the effective relative density of the load bearing ligament structure, the directional tortuosity of the ligaments and the interface on the elastic behavior of the npg-epoxy composites. Interfacial failure was experimentally observed under compression and tension. The tension-compression asymmetry investigation revealed that the npg-epoxy composite is stronger in compression than in tension. These various observations point to the important roles that the hard phase, i.e., the interconnected ligament network, the soft phase, i.e., the continuous epoxy, and the interface between them play on the mechanical behavior of npg-epoxy composites.', 'Nanoporöses Gold (NPG), ein bikontinuierliches Netzwerk aus nanoskaligen Goldligamenten und Poren, weist durch Variation der inneren Längenskalen ein abstimmbares mechanisches Verhalten auf. Allerdings ist es schwerwiegend eingeschränkt durch seinen Mangel an Verformbarkeit unter Zugspannung. Durch Infiltration der porösen Struktur mit Epoxid erhält man ein Kompositmaterial mit verbesserter Zugverformbarkeit und Fließspannung. Die vorliegende Arbeit strebt eine dreifache Untersuchung des mikromechanischen Verhaltens, der Verformungsmechanismen und des mechanischen Versagens von NPG-Epoxid Kompositen an, durch Fokussierung auf 3D Mikrostrukturcharakterisierung, Finite Elemente Simulation (FEM) und mikromechanische Prüfung. Um die Kompositmikrostruktur zu verstehen wurden hochaufgelöste 3D Rekonstruktionen mit auf fokussierten Ionenstrahlen (focused ion beam, FIB) basierter Tomographie hergestellt, möglich gemacht durch den positiven Effekt der Infiltration mit Epoxid auf die Bearbeitung poröser Medien mit FIB. Dabei wird angenommen, dass die Epoxidinfiltration die Geometrie des NPG Netzwerks nicht signifikant ändert. Proben mit unterschiedlichen strukturellen Längen wurden verwendet, d.h. mit mittleren Ligamentdurchmessern im Bereich von einigen 10 bis mehrere 100 nm, erreicht durch isothermes Anlassen. Es wurden quantitative Analysen der 3D Rekonstruktionen durchgeführt hinsichtlich der metrischen Eigenschaften (z.B. relative Dichte, Verteilungen der Ligamentdurchmesser und spezifische Oberfläche), topologischen Eigenschaften (z.B. Konnektivitätsdichten) und richtungsabhängigen Eigenschaften (z.B. Richtungstortuosität). Von großer Wichtigkeit war die Identifikation von repräsentativen Volumen (RV), die die globalen Struktureigenschaften des Materials reflektieren. Es wurde herausgefunden, dass NPG nahezu selbstähnlich vergröbert. Dies erlaubt die Identifizierung struktureller Größen, die zur Beschreibung des mechanischen Verhaltens globaler NPG Strukturen über variierende Längenskalen verwendet werden können. FEM Simulationen angewendet auf vermaschte RV der 3D Rekonstruktionen weisen stark darauf hin, dass die effektive relative Dichte der lasttragenden Ligamentstruktur die kritische Größe in der Bestimmung des mechanischen Verhaltens der NPG Strukturgeometrie ist, eher als die relative Dichte der festen Phase wie oft angenommen. Nach der Infiltration mit Epoxid ist die Verdichtung von NPG-Epoxid Kompositen unter Verformung stark unterdrückt. Dies führt zu einer stark verbesserten Festigkeit im Vergleich zu reinem NPG. Allerdings ist die Abhängigkeit der Fließgrenze von der mittleren Ligamentgröße viel schwächer in der Kompositstruktur verglichen mit reinem NPG. Die Größeneffekte in reinem NPG sind üblicherweise Versetzungsaktivitäten in den Goldligamenten zugeordnet worden, wogegen im Kompositmaterial der Einfluss der Grenzfläche auf die Versetzungsbewegung und die Epoxidketten in Betracht gezogen werden muss. Das Grenzflächenverhalten führt zu einem Verstärkungseffekt in den Kompositen aber schwächt die Größeneffekte ab. Die Vergleiche der Elastizitätsmoduln aus den Vorhersagen der analytischen Modelle, den Experimenten und der FEM Simulationen demonstrierten die Einflüsse der Konnektivität, der effektiven relativen Dichte der lasttragenden Ligamentstruktur, der Richtungstortuosität der Ligamente und der Grenzfläche auf das elastische Verhalten der NPG-Epoxid Komposite. Grenzflächenversagen wurde experimentell beobachtet unter Kompression und Zug. Die Untersuchung der Zug-Druck Asymmetrie zeigte, dass das NPG-Epoxid Komposit stärker unter Druck als unter Zug ist. Diese unterschiedlichen Beobachtungen zeigen die wichtigen Rollen auf, die die harte Phase, also das verknüpfte Ligamentnetzwerk, die weiche Phase, d.h. das kontinuierliche Epoxid, und die Grenzfläche zwischen ihnen für das mechanische Verhalten von NPG-Epoxid Komposite spielen.']] | ['2017'] | ['http://id.loc.gov/vocabulary/iso639-1/en'] | ['open access'] | [[{'@id': 'gnd:1076028772'}, {'@id': 'gnd:4062670-2'}]] | ['gnd:10194308-8', 'gnd:1076028772', 'gnd:1138805939', 'gnd:2067664-5', 'gnd:4062670-2', 'https://www.tib.eu/de/suchen/id/TIBKAT%3A880948493'] | ['Technische Universität Hamburg-Harburg, Institut für Keramische Hochleistungswerkstoffe', 'Werkstoffmechanik', 'Lilleodden, Erica', 'Technische Universität Hamburg-Harburg', 'Verbundwerkstoff'] | 22 |
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