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2012-06-11
Thermal Stability of Thermoelectric Materials via In Situ Resistivity Measurements
An experimental setup for determining the electrical resistivity of several types of thermoelectric materials over the temperature range 20 < T < 550 C is described in detail. One resistivity measurement during temperature cycling is also explained for Cu0.01Bi2Te2.7Se0.3 while a second measurement is made on Yb0.35Co4Sb12 as a function of time at 400 C. Both measurements confirm that the materials are thermally stable for the temperature range and time period measured. Measurements made during temperature cycling show an irreversible decrease in the electrical resistivity of Cu0.01Bi2Te2.7Se0.3 when the measuring temperature exceeds the pressing temperature. Several other possible uses of such a system include but are not limited to studying the effects of annealing and/or oxidation as a function of both temperature and time.
1206.2094v1
2022-07-27
Terahertz microresonators for material characterisation
Terahertz (THz) technology is rapidly evolving, and the advancement of data and information processing devices is essential. Silicon THz microresonators provide perfect platforms to develop compact and integrated devices that could transform THz technology. Here we present a systematic study on the key figure of merit of silicon THz disc microresonators - the quality factor (Q-factor) - in dependence on the substrate's resistivity. Our results show that the Q-factor depends linearly on the resistivity and a variation in resistivity from 10k$\Omega$cm to 15k$\Omega$cm changes the Q-factor from 50k to 76k at 0.6THz. Moreover, we experimentally determine that the silicon material absorption is inversely proportional to the substrate's resistivity. In general, the presented methodology is ideally suited to precisely measure the material absorption of low-loss materials in the THz domain, which is challenging using conventional THz spectroscopy.
2207.13818v1
2023-03-24
Charge-density-wave resistive switching and voltage oscillations in ternary chalcogenide BaTiS3
Phase change materials, which show different electrical characteristics across the phase transitions, have attracted considerable research attention for their potential electronic device applications. Materials with metal-to-insulator or charge density wave (CDW) transitions such as VO2 and 1T-TaS2 have demonstrated voltage oscillations due to their robust bi-state resistive switching behavior with some basic neuronal characteristics. BaTiS3 is a small bandgap ternary chalcogenide that has recently reported the emergence CDW order below 245 K. Here, we report on the discovery of DC voltage / current-induced reversible threshold switching in BaTiS3 devices between a CDW phase and a room temperature semiconducting phase. The resistive switching behavior is consistent with a Joule heating scheme and sustained voltage oscillations with a frequency of up to 1 kHz has been demonstrated by leveraging the CDW phase transition and the associated negative differential resistance. Strategies of reducing channel sizes and improving thermal management may further improve the device performance. Our findings establish BaTiS3 as a promising CDW material for future energy-efficient electronics, especially for neuromorphic computing.
2303.14169v1
2016-02-24
Design and optimization of resistive anode for a two-dimensional imaging triple-GEM detector
The optimization of resistive anode for two dimensional imaging detectors which consists of a series of high resistive square pads surrounding by low resistive strips has been studied by both numerical simulations and experimental tests. It has been found that to obtain good detector performance, the resistance ratio of the pad to the strip should be larger than 5, the nonuniformity of the pad surface resistivity had better be less than $20\%$, a smaller pad width leads to a smaller spatial resolution and when the pad width is $6mm$, the spatial resolution ($\sigma$) can reach about $105{\mu}m$. Based on the study results, a 2-D GEM detector prototype with the optimized resistive anode is constructed and a good imaging performance is achieved.
1602.07438v1
2017-09-19
Considering non-uniform current distributions in magnetoresistive sensor designs and their implications for the resistance transfer function
Non-uniform current distributions of spin valves with disk shaped free layers are investigated. In the context of spin valves, the vortex state, which is the ground-state in many disk shaped magnetic bodies, allows for distinct parallel channels of high and low resistivity. The readout current is thus able to evade high resistivity regions in favor of low resistivity regions, giving rise to 'conductive inhomogeneities'. Therefore, the total resistance of the spin valve does not always correspond exactly to the total average magnetization of the free layer. In addition, the resistance transfer function can be significantly influenced by the spatial placement of the electrodes, giving rise to 'geometric inhomogeneities'. The resulting deviations from resistance to magnetization transfer function are investigated for different spin valve geometries and compared to measurements of comparable devices.
1709.06394v1
2023-09-19
Effects of plasma resistivity in three-dimensional full-F gyro-fluid turbulence simulations
A full-F, isothermal, electromagnetic, gyro-fluid model is used to simulate plasma turbulence in a COMPASS-sized, diverted tokamak. A parameter scan covering three orders of magnitude of plasma resistivity and two values for the ion to electron temperature ratio with otherwise fixed parameters is setup and analysed. Simulations are performed with a new version of the FELTOR code, which is fully parallelized on GPUs. Each simulation covers a couple of milliseconds. Two transport regimes for high and low plasma resistivities are revealed. Beyond a critical resistivity the mass and energy confinement reduces with increasing resistivity. Further, for high plasma resistivity the direction of parallel acceleration is swapped compared to low resistivity. The integration of exact conservation laws over the closed field line region allows for an identification of numerical errors within the simulations. The electron force balance and energy conservation show relative errors on the order of $10^{-3}$ while the particle conservation and ion momentum balance show errors on the order of $10^{-2}$. Relative fluctuations amplitudes increase from below $1\%$ in the core to $15\%$ in the edge and up to $40\%$ in the scrape-off layer. Finally, three-dimensional visualisations using ray tracing techniques are displayed and discussed. The field-alignment of turbulent fluctuations in density and parallel current becomes evident.
2309.10414v1
2016-11-09
TiO$_2$-based Memristors and ReRAM: Materials, Mechanisms and Models (a Review)
The memristor is the fundamental non-linear circuit element, with uses in computing and computer memory. ReRAM (Resistive Random Access Memory) is a resistive switching memory proposed as a non-volatile memory. In this review we shall summarise the state of the art for these closely-related fields, concentrating on titanium dioxide, the well-utilised and archetypal material for both. We shall cover material properties, switching mechanisms and models to demonstrate what ReRAM and memristor scientists can learn from each other and examine the outlook for these technologies.
1611.04456v1
2018-10-30
An alternative to the topological interpretation of the transverse resistivity anomalies in SrRuO3
We clarify the physical origin of anomalies in transverse resistivity often observed in exotic materials, such as SrRuO3, in which the Berry curvature is manifested in the transport properties. The previously attributed mechanism for the anomalies, the topological Hall effect (THE), is refuted by our thorough investigations as well as formulation of a model considering inhomogeneous magnetoelectric properties in the material. Our analyses fully explain every feature of the anomalies without resorting to the THE. The present results establish a fundamental understanding, which was previously overlooked, of magneto-transport properties in such exotic materials.
1810.12529v1
2004-11-26
The Acceleration Mechanism of Resistive MHD Jets Launched from Accretion Disks
We analyzed the results of non-linear resistive magnetohydrodynamical (MHD) simulations of jet formation to study the acceleration mechanism of axisymmetric, resistive MHD jets. The initial state is a constant angular momentum, polytropic torus threaded by weak uniform vertical magnetic fields. The time evolution of the torus is simulated by applying the CIP-MOCCT scheme extended for resistive MHD equations. We carried out simulations up to 50 rotation period at the innermost radius of the disk created by accretion from the torus. The acceleration forces and the characteristics of resistive jets were studied by computing forces acting on Lagrangian test particles. Since the angle between the rotation axis of the disk and magnetic field lines is smaller in resistive models than in ideal MHD models, magnetocentrifugal acceleration is smaller. The effective potential along a magnetic field line has maximum around $z \sim 0.5r_0$ in resistive models, where $r_0$ is the radius where the density of the initial torus is maximum. Jets are launched after the disk material is lifted to this height by pressure gradient force. Even in this case, the main acceleration force around the slow magnetosonic point is the magnetocentrifugal force. The power of the resistive MHD jet is comparable to the mechanical energy liberated in the disk by mass accretion. Joule heating is not essential for the formation of jets.
0411712v1
2016-10-30
Temperature and Humidity Dependence of Resistance in Nano-Diamond Powder
The electrical resistance of detonation nano-diamond powders was measured from liquid nitrogen temperature to room temperature and in relative humidity environments from around 10% to 100%. After sample exposures of several hours at 100% relative humidity at room temperature (around 295 K), when the temperature was reduced, the resistance increased to the upper measurement limit of our apparatus (120 M{\Omega}) at around 240 K. Upon warming, the resistance dropped back to the room temperature value, with some hysteresis. For sample exposures after several hours at 100% relative humidity at room temperature, as the relative humidity was reduced, the sample resistance increased to the upper range limit of the apparatus. As the relative humidity was then increased (all at room temperature), the resistance dropped. For samples exposed to low (~10%) relative humidity for several hours at room temperature, as the humidity was increased (at room temperature), the resistance decreased, and then increased when the humidity was reduced. The temperature behavior was markedly differ from that of powdered graphite and multi-walled carbon nano tubes.
1611.02242v2
2018-07-04
Gate controlled large resistance switching driven by charge density wave in 1T-TaS2/2H-MoS2 heterojunction
1T-TaS2 is a layered material that exhibits charge density wave (CDW) induced distinct electrical resistivity phases and has attracted a lot of attention for interesting device applications. However, such resistivity switching effects are often weak, and cannot be modulated by an external gate voltage - limiting their widespread usage. Using a back-gated 1T-TaS2/2H-MoS2 heterojunction, here we show that the usual resistivity switching in TaS2 due to different phase transitions is accompanied with a surprisingly strong modulation in the Schottky barrier height (SBH) at the TaS2/MoS2 interface - providing an additional knob to control the degree of the phase-transition-driven resistivity switching by an external gate voltage. In particular, the commensurate (C) to triclinic (T) phase transition results in an increase in the SBH owing to a collapse of the Mott gap in TaS2. The change in SBH allows us to estimate an electrical Mott gap opening of ~71 +/- 7 meV in the C phase of TaS2. On the other hand, the nearly-commensurate (NC) to incommensurate (IC) phase transition results in a suppression in the SBH, and the heterojunction shows a gate-controlled resistivity switching up to 17.3, which is ~14.5 times higher than that of standalone TaS2. The findings mark an important step forward showing a promising pathway to externally control as well as amplify the CDW induced resistivity switching. This will boost device applications that exploit these phase transitions, such as ultra-broadband photodetection, negative differential conductance, fast oscillator and threshold switching in neuromorphic circuits.
1807.01652v2
2008-10-08
Performance Analysis of 60nm gate length III-V InGaAs HEMTs: Simulations vs. experiments
An analysis of recent experimental data for high-performance In0.7Ga0.3As high electron mobility transistors (HEMTs) is presented. Using a fully quantum mechanical, ballistic model, we simulate In0.7Ga0.3As HEMTs with gate lengths of LG = 60nm, 85, and 135 nm and compare the result to the measured I-V characteristics including draininduced barrier lowering, sub-threshold swing, and threshold voltage variation with gate insulator thickness, as well as on-current performance. To first order, devices with three different oxide thicknesses and channel lengths can all be described by our ballistic model with appropriate values of parasitic series resistance. For high gate voltages, however, the ballistic simulations consistently overestimate the measured on-current, and they do not show the experimentally observed decrease in on-current with increasing gate length. With no parasitic series resistance at all, the simulated on-current of the LG = 60 nm device is about twice the measured current. According to the simulation, the estimated ballistic carrier injection velocity for this device is about 2.7 x 10^7 cm/s. Because of the importance of the semiconductor capacitance, the simulated gate capacitance is about 2.5 times less than the insulator capacitance. Possible causes of the transconductance degradation observed under high gate voltages in these devices are also explored. In addition to a possible gate-voltage dependent scattering mechanism, the limited ability of the source to supply carriers to the channel, and the effect of nonparabolicity are likely to play a role. The drop in on-current with increasing gate length is an indication that the devices operate below the ballistic limit.
0810.1540v1
2008-12-26
Flux quanta driven by high-density currents in low-impurity V3Si and LuNi2B2C: free flux flow and flux-core size effect
High density direct currents (DC) are used to drive flux quanta via the Lorentz force towards a highly ordered "free flux flow" (FFF) dynamic state, made possible by the weak-pinning environment of high-quality, single-crystal samples of two low-Tc superconducting compounds, V3Si and LuNi2B2C. We report the effect of the magnetic field-dependent fluxon core size on flux flow resistivity rho_f. Much progress has been made in minimizing the technical challenges associated with the use of high currents. Attainment of a FFF phase is indicated by the saturation at highest currents of flux-flow dissipation levels that are well below the normal state resistance and have field-dependent values. The field dependence of the corresponding rho_f is shown to be consistent with a prediction based on a model for the decrease of flux core size at higher fields in weak-coupling BCS s-wave materials.
0812.4715v4
2020-06-01
Radiation hardness of GaAs: Cr and Si sensors irradiated by electron beam
The interest in using the radiation detectors based on high resistive chromium-compensated GaAs (GaAs:Cr) in high energy physics and others applied fields has been growing steadily due to its numerous advantages over others classical materials. High radiation hardness at room temperature stands out and needs to be systematically investigated. In this paper an experimental study of the effect of 20.9 MeV electrons generated by the LINAC-200 accelerator on some properties of GaAs:Cr based sensors is presented. In parallel, Si sensors were irradiated at the same conditions, measured and analyzed in order to perform a comparative study. The target sensors were irradiated with the dose up to 1.5 MGy. The current-voltage characteristics, resistivity, charge collection efficiency and their dependences on the bias voltage and temperature were measured at different absorbed doses. An analysis of the possible microscopic mechanisms leading to the observed effects in GaAs:Cr sensors is presented in the article.
2006.01254v1
2021-02-04
Quantum Transport in Two-Dimensional WS$_2$ with High-Efficiency Carrier Injection Through Indium Alloy Contacts
Two-dimensional transition metal dichalcogenides (TMDCs) have properties attractive for optoelectronic and quantum applications. A crucial element for devices is the metal-semiconductor interface. However, high contact resistances have hindered progress. Quantum transport studies are scant as low-quality contacts are intractable at cryogenic temperatures. Here, temperature-dependent transfer length measurements are performed on chemical vapour deposition grown single-layer and bilayer WS$_2$ devices with indium alloy contacts. The devices exhibit low contact resistances and Schottky barrier heights (\sim10 k$\Omega$\si{\micro\metre} at 3 K and 1.7 meV). Efficient carrier injection enables high carrier mobilities ($\sim$190 cm$^2$V$^{-1}$s$^{-1}$) and observation of resonant tunnelling. Density functional theory calculations provide insights into quantum transport and properties of the WS$_2$-indium interface. Our results reveal significant advances towards high-performance WS$_2$ devices using indium alloy contacts.
2102.02489v1
2021-08-11
Single-domain perpendicular magnetization induced by the coherent O 2p-Ru 4d hybridized state in an ultra-high-quality SrRuO3 film
We investigated the Ru 4d and O 2p electronic structure and magnetic properties of an ultra-high-quality SrRuO3 film on SrTiO3 grown by machine-learning-assisted molecular beam epitaxy. The high itinerancy and long quantum lifetimes of the quasiparticles in the Ru 4d t2g-O 2p hybridized valence band are confirmed by observing the prominent well-screened peak in the Ru 3d core-level photoemission spectrum, the coherent peak near the Fermi energy in the valence band spectrum, and quantum oscillations in the resistivity. The element-specific magnetic properties and the hybridization between the Ru 4d and O 2p orbitals were characterized by Ru M2,3-edge and O K-edge soft X-ray absorption spectroscopy and X-ray magnetic circular dichroism measurements. The ultra-high-quality SrRuO3 film with the residual resistivity ratio of 86 shows the large orbital magnetic moment of oxygen ions induced by the strong orbital hybridization of the O 2p states with the spin-polarized Ru 4d t2g states. The film also shows single-domain perpendicular magnetization with an almost ideal remanent magnetization ratio of 0.97. These results provide detailed insights into the relevance between orbital hybridization and the perpendicular magnetic anisotropy in SrRuO3/SrTiO3 systems.
2108.04980v1
2009-08-03
Resistivity of Mn$_{1-x}$Fe$_x$Si single crystals: Evidence for quantum critical behavior
Resistivity measurements have been made on Mn$_{1-x}$Fe$_x$Si single crystals between 2 and 300K for $x$ = 0, 0.05, 0.08, 0.12 and 0.15. Fe doping is found to depress the magnetic ordering temperature from 30K for $x$ = 0 to below 2K for $x$ = 0.15. Although Fe doping results in a large increase of the low-temperature residual resistivity, the temperature dependence of the resistivity above the magnetic transition remains practically unaffected by increasing Fe content. An analysis of the temperature derivative of the resistivity provides strong evidence for the existence of a non-Fermi-liquid ground state near $x$ = 0.15 and thus for a quantum critical point tuned by Fe content.
0908.0294v1
2012-10-09
Effect of back-gate on contact resistance and on channel conductance in graphene-based field-effect transistors
We study the contact resistance and the transfer characteristics of back-gated field effect transistors of mono- and bi-layer graphene. We measure specific contact resistivity of ~7kohm*um2 and ~30kohm*um2 for Ni and Ti, respectively. We show that the contact resistance is a significant contributor to the total source-to-drain resistance and it is modulated by the back-gate voltage. We measure transfer characteristics showing double dip feature that we explain as the effect of doping due to charge transfer from the contacts causing minimum density of states for graphene under the contacts and in the channel at different gate voltage.
1210.2531v1
2013-07-01
Magnetic and transport parameters of LSMO and YBCO/LSMO films deposited on sapphire substrates
The La0.7Sr0.3MnO3 (LSMO) layers and YBa2Cu3O7-{\delta}/La0.7Sr0.3MnO3 (YBCO/LSMO) bilayers were grown by magnetron sputtering on sapphire (Al2O3 or ALO) substrates. Temperature dependences of resistance of single LSMO films, grown on ALO substrates were typical for polycrystalline manganite materials and the resistance decreased with decrease of the temperature at medium temperatures and increased at lower and higher temperatures. Deposition of a top YBCO layer led to a drastic increase of the sample resistance. These bilayers did not demonstrate a decreasing of the resistance with decrease of temperature. Temperature dependence of the resistance of these samples was interpreted in the framework of a phenomenological model of two intergrain conduction channels. In framework of this model, parameters of the samples were determined and discussed.
1307.0302v1
2015-01-27
Realization of a reversible switching in TaO2 polymorphs via Peierls distortion for resistance random access memory
Transition-metal-oxide based resistance random access memory is a promising candidate for next-generation universal non-volatile memories. Searching and designing appropriate new materials used in the memories becomes an urgent task. Here, a new structure with the TaO2 formula was predicted using evolutionary algorithms in combination with first-principles calculations. This new structure having a triclinic symmetry (T-TaO2) is both energetically and dynamically more favorable than the commonly believed rutile structure (R-TaO2). Our hybrid functional calculations show that T-TaO2 is a semiconductor with a band gap of 1.0 eV, while R-TaO2 is a metallic conductor. This large difference in electrical property makes TaO2 a potential candidate for resistance random access memory (RRAM). Furthermore, we have shown that T-TaO2 is actually a Peierls distorted R-TaO2 phase and the transition between these two structures is via a directional displacement of Ta atoms. The energy barrier for the reversible phase transition from R-TaO2 to T-TaO2 is 0.19 eV/atom and the other way around is 0.23 eV/atom, suggesting low power consumption for the resistance switch. The present findings provide a new mechanism for the resistance switch and will also stimulate experimental work to fabricate tantalum oxides based RRAM.
1501.06632v1
2015-02-09
Four-Probe Methods for Measuring the Resistivity of Samples in the Form of Rectangular Parallelepipeds
The problem of measuring the resistivity of isotropic samples of finite dimensions in the form of rectangular parallelepipeds using the four-probe technique was considered. Two variants of contact arrangements were studied: (1) four collinear probes are positioned on one side of a sample symmetrically with respect to the other sides, and (2) two probes on one side of a sample and two on the opposite side are placed precisely in opposite positions and symmetrically with respect to the other sides of the sample (the Schnabel method). Solutions of the problem of the electric field potential distribution in a sample for different positions of the current contacts were found. The solutions were obtained in the form of double series and methods of their summation are presented. The obtained results are extended to the case of measuring the resistivity of anisotropic samples when the resistivity tensor has two independent components. The results of using the developed technique for measuring the resistivity of such a highly anisotropic material as highly oriented pyrolitic graphite using the Schnabel method are presented.
1502.02600v1
2019-12-10
Resistance Drift in Ge2Sb2Te5 Phase Change Memory Line Cells at Low Temperatures and Its Response to Photoexcitation
Resistance drift in phase change materials is characterized in amorphous phase change memory line-cells from 300 K to 125 K range and is observed to follow the previously reported power-law behavior with drift coefficients in the 0.07 to 0.11 range in dark. While these drift coefficients measured in dark are similar to commonly observed drift coefficients (~0.1) at and above room temperature, measurements under light show a significantly lower drift coefficient (0.05 under illumination versus 0.09 in dark at 150K). Periodic on/off switching of light shows sudden decrease/increase of resistance, attributed to photo-excited carriers, followed by a very slow response (~30 minutes at 150 K) attributed to contribution of charge traps. Continuation of the resistance drift at low temperatures and the observed photo-response suggest that resistance drift in amorphous phase change materials is predominantly an electronic process.
1912.04480v2
2022-04-04
Inter- to Intra-Layer Resistivity Anisotropy of NdFeAs(O,H) with Various Hydrogen Concentrations
With molecular beam epitaxy and topotactic chemical reaction, we prepared NdFeAs(O,H) epitaxial thin films with various hydrogen concentrations on 5{\deg} vicinal cut MgO substrates. By measuring the resistivities along the longitudinal and transversal directions, the ab plane and the c axis resistivities (\{rho}_ab and \{rho}_c) were obtained. The resistivity anisotropy {\gamma}_\{rho}=\{rho}_c \ \{rho}_ab of NdFeAs(O,H) with various hydrogen concentrations was compared with that of NdFeAs(O,F). At the H concentrations which led to superconducting transition temperatures Tc over 40 K, {\gamma}_\r{ho} recorded ~100-150 at 50 K. On the other hand, a low {\gamma}_\{rho} value of 9 was observed with the mostly doped sample. The exponent \{beta} of the ab plane resistivity obtained by fitting a power law expression \{rho}_{ab}(T)=\{rho}_0+AT^\{beta} to the data was close to unity down to low temperature in the vicinity where the second antiferromagnetic phase locates, which may be related to the quantum critical point discussed at the over-doped side of the phase diagram.
2204.01554v1
2020-04-28
A Route to High-Toughness Battery Electrodes
There is increasing interest in materials that combine energy-storing functions with augmented mechanical properties, ranging from flexibility in bending to stretchability to structural properties. In the case of lithium-ion batteries, these mechanical functions could enable their integration in emerging technologies such as wearable, free-form electronics and ultimately as structural elements, for example, in transport applications. This work presents a method to produce flexible LiFePO4 LFP electrodes with an extraordinary combination of electrochemical and mechanical performance. Such electrodes exhibit an exceptionally high specific toughness, combined with superior rate capability and energy density, with respect to reference electrodes with typical metallic current collectors. These properties are a result of the strong adhesion of the active material particles to the high surface area carbon nanotube fiber fabric, used as a lightweight, tough, and highly conducting current collector. This strong adherence minimizes electrical resistance, mitigates interfacial failure, and increases ductility through heterogeneous strain after cohesive failure of the inorganic phase. As a result, these electrodes can withstand large deformations before fracture, and, even after fracture, they retain excellent electrochemical performance, approximately double that of unstretched, Al-supported LFP electrodes with equivalent loading.
2004.13350v1
2023-02-02
High-entropy silicide superconductors with W$_{5}$Si$_{3}$-type structure
We report the synthesis, crystal structure and physical properties of two new high-entropy silicides (HESs), namely (Nb$_{0.1}$Mo$_{0.3}$W$_{0.3}$Re$_{0.2}$Ru$_{0.1}$)$_{5}$Si$_{3}$ and (Nb$_{0.2}$Mo$_{0.3}$W$_{0.3}$Re$_{0.1}$Ru$_{0.1}$)$_{5}$Si$_{3}$. Structural analysis indicates that both HESs consist of a (nearly) single tetragonal W$_{5}$Si$_{3}$-type phase (space group $I$4/$mcm$) with a disordered cation distribution. Electrical resistivity, magnetic susceptibility and specific heat measurements show that (Nb$_{0.1}$Mo$_{0.3}$W$_{0.3}$Re$_{0.2}$Ru$_{0.1}$)$_{5}$Si$_{3}$ and (Nb$_{0.2}$Mo$_{0.3}$W$_{0.3}$Re$_{0.1}$Ru$_{0.1}$)$_{5}$Si$_{3}$ are weakly coupled bulk superconductors, which represent the first superconducting high-entropy nonoxide ceramics. In particular, these HESs have higher $T_{\rm c}$ values (3.2-3.3 K) compared with those of the binary counterparts, and their $B_{\rm c2}$(0)/$T_{\rm c}$ ratios are the largest among superconductors of the same structural type.
2302.00844v1
2024-01-15
Fatigue Behavior of High-Entropy Alloys
High-entropy alloys (HEAs) refer to alloys composed of five or more elements in equal or near-equal amounts or in an atomic concentration range of 5 to 35 atomic percent (at%). Different elemental ratios will affect the microstructures of HEAs and provide them with unique properties. Based on past research, HEAs have exhibited superior performance, relative to most conventional alloys, with respect to many properties, such as strength, toughness, corrosion resistance, magnetic behavior, etc. Among them, fatigue behavior has been a topic of focus, due to its importance in industrial applications. In this article, we summarized the research progress in the HEA-fatigue behavior in the past ten years, including experimental results and theoretical studies in subdivisions, such as high-cycle fatigue, low-cycle fatigue, fatigue-crack growth, fatigue mechanisms, etc. The influence of the processing and test methods on HEAs is described. The accuracy of several commonly used prediction models is also outlined. Finally, unresolved issues and suggestions on the direction of future research efforts are presented.
2401.07418v1
2024-01-26
Accelerated intermetallic phase amorphization in a Mg-based high-entropy alloy powder
We describe a novel mechanism for the synthesis of a stable high-entropy alloy powder from an otherwise immiscible Mg-Ti rich metallic mixture by employing high-energy mechanical milling. The presented methodology expedites the synthesis of amorphous alloy powder by strategically injecting entropic disorder through the inclusion of multi-principal elements in the alloy composition. Predictions from first principles and materials theory corroborate the results from microscopic characterizations that reveal a transition of the amorphous phase from a precursor intermetallic structure. This transformation, characterized by the emergence of antisite disorder, lattice expansion, and the presence of nanograin boundaries, signifies a departure from the precursor intermetallic structure. Additionally, this phase transformation is accelerated by the presence of multiple principal elements that induce severe lattice distortion and a higher configurational entropy. The atomic size mismatch of the dissimilar elements present in the alloy produces a stable amorphous phase that resists reverting to an ordered lattice even on annealing.
2401.15197v2
2024-03-28
High Mobility Charge Transport in a Multicarrier Altermagnet CrSb
A newly identified magnetic phase called altermagnet is being actively studied because of its unprecedented spin-dependent phenomena. Among the candidate materials, CrSb has a particularly high transition temperature and a large spin-splitting energy, but its transport properties have remained unexplored. In this study, we report the magnetotransport properties of CrSb measured on single crystals. We found that the Hall resistivity shows a nonlinear dependence on the magnetic field at low temperatures. From symmetry-based considerations, however, this behavior can not be attributed to an anomalous Hall effect, but to a multicarrier effect. A multicarrier fitting to the in-plane conductivity tensor revealed that there are carriers with high mobilities in CrSb, probably because of the presence of Weyl points in the electronic structure.
2403.19233v1
2014-02-26
MoS2 P-type Transistors and Diodes Enabled by High Workfunction MoOx Contacts
The development of low-resistance source/drain contacts to transition metal dichalcogenides (TMDCs) is crucial for the realization of high-performance logic components. In particular, efficient hole contacts are required for the fabrication of p-type transistors with MoS2, a model TMDC. Previous studies have shown that the Fermi level of elemental metals is pinned close to the conduction band of MoS2, thus resulting in large Schottky barrier heights for holes with limited hole injection from the contacts. Here, we show that substoichiometric molybdenum trioxide (MoOx, x<3), a high workfunction material, acts as an efficient hole injection layer to MoS2 and WSe2. In particular, we demonstrate MoS2 p-type field-effect transistors and diodes by using MoOx contacts. We also show drastic on-current improvement for p-type WSe2 FETs with MoOx contacts over devices made with Pd contacts, which is the prototypical metal used for hole injection. The work presents an important advance in contact engineering of TMDCs and will enable future exploration of their performance limits and intrinsic transport properties.
1402.6632v1
2015-03-23
Electron-Irradiation Induced Nanocrystallization of Pb(II) in Silica Gels Prepared in High Magnetic Field
In a previous study, structure of silica gels prepared in a high magnetic field was investigated. While a direct application of such anisotropic silica gels is for an optical anisotropic medium possessing chemical resistance, we show here their possibility of medium in materials processing. In this direction, for example, silica hydrogels have so far been used as media of crystal growth. In this paper, as opposed to the soft-wet state, dried silica gels have been investigated. We have found that lead (II) nanocrystallites were formed induced by electron irradiation to lead (II)-doped dried silica gels prepared in a high magnetic field such as B = 10 T. Hydrogels made from a sodium metasilicate solution doped with lead (II) acetate were prepared. The dried specimens were irradiated by electrons in a transmission electron microscope environment. Electron diffraction patterns indicated the crystallinity of lead (II) nanocrystallites depending on B. An advantage of this processing technique is that the crystallinity can be controlled through the strength of magnetic field B applied during gel preparation. Specific skills are not required to control the strength of magnetic field.
1503.06863v1
2017-04-07
Thermopower and thermal conductivity in the Weyl semimetal NbP
The Weyl semimetal NbP exhibits an extremely large magnetoresistance (MR) and an ultra-high mobility. The large MR originates from a combination of the nearly perfect compensation between electron- and hole-type charge carriers and the high mobility, which is relevant to the topological band structure. In this work we report on temperature- and field-dependent thermopower and thermal conductivity experiments on NbP. Additionally, we carried out complementary heat capacity, magnetization, and electrical resistivity measurements. We found a giant adiabatic magnetothermopower with a maximum of 800 $\mu$V/K at 50 K in a field of 9 T. Such large effects have been observed rarely in bulk materials. We suggest that the origin of this effect might be related to the high charge-carrier mobility. We further observe pronounced quantum oscillations in both thermal conductivity and thermopower. The obtained frequencies compare well with our heat capacity and magnetization data.
1704.02241v2
2020-10-29
Two-dimensional hole gas in organic semiconductors
A highly conductive metallic gas that is quantum mechanically confined at a solid-state interface is an ideal platform to explore nontrivial electronic states that are otherwise inaccessible in bulk materials. Although two-dimensional electron gas (2DEG) has been realized in conventional semiconductor interfaces, examples of two-dimensional hole gas (2DHG), which is the counter analogue of 2DEG, are still limited. Here, we report the observation of a 2DHG in solution-processed organic semiconductors in conjunction with an electric double-layer using ionic liquids. A molecularly flat single crystal of high mobility organic semiconductors serves as a defect-free interface that facilitates two-dimensional confinement of high-density holes. Remarkably low sheet resistance of 6 k$\Omega$ and high hole gas density of 10$^{14}$ cm$^{-2}$ result in a metal-insulator transition at ambient pressure. The measured degenerated holes in the organic semiconductors provide a broad opportunity to tailor low-dimensional electronic states using molecularly engineered heterointerfaces.
2010.15883v1
2021-07-29
Synergetic enhancement of power factor and suppression of lattice thermal conductivity via electronic structure modification and nanostructuring on Ni and B co-doped p-type Si-Ge alloy
For simultaneously achieving the high-power factor and low lattice thermal conductivity of Si-Ge based thermoelectric materials, we employed, in this study, constructively modifying the electronic structure near the chemical potential and nano-structuring by low temperature and high-pressure sintering on nano-crystalline powders. Nickel was doped to create the impurity states near the edge of the valence band for enhancing the power factor with boron for tuning the carrier concentration. The nanostructured samples with the nominal composition of Si0.65-xGe0.32Ni0.03Bx (x = 0.01, 0.02, 0.03, and 0.04) were synthesized by the mechanical alloying followed low-temperature and high-pressure sintering process. A large magnitude of Seebeck coefficient reaching 321 {\mu}VK-1 together with a small electrical resistivity of 4.49 m{\Omega}cm, leads to a large power factor of 2.3 Wm-1K-2 at 1000 K. With successfully reduced thermal conductivity down to 1.47 Wm-1K-1, a large value of ZT ~1.56 was obtained for Si0.65-xGe0.32Ni0.03B0.03 at 1000 K
2107.13778v1
2021-09-03
Growth and characterization of high-quality single-crystalline SnTe retaining cubic symmetry down to the lowest temperature studied
SnTe, an archetypical topological crystalline insulator, often shows a transition from a highly symmetric cubic phase to a rhombohedral structure at low temperatures. In order to achieve the highly symmetric cubic phase at low temperatures suitable for quantum behaviour, we have employed the modified Bridgman method to grow a high-quality single-crystalline sample of SnTe. Analysis of the crystal structure using Laue diffraction and rocking curve measurements show a very high degree of single crystallinity of the sample. Resistivity and the specific heat data do not show the signature of structural transition down to the lowest temperature studied. The magnetic susceptibility shows diamagnetic behaviour. All these properties manifest the behaviour of a typical bulk semiconductor with conducting surface states as expected in a topological material. Detailed powder x-ray diffraction measurements show cubic structure in the whole temperature range studied.
2109.01420v2
2021-11-22
High-entropy ceramics: propelling applications through disorder
Disorder enhances desired properties, as well as creating new avenues for synthesizing materials. For instance, hardness and yield stress are improved by solid-solution strengthening, a result of distortions and atomic size mismatches. Thermo-chemical stability is increased by the preference of chemically disordered mixtures for high-symmetry super-lattices. Vibrational thermal conductivity is decreased by force-constant disorder without sacrificing mechanical strength and stiffness. Thus, high-entropy ceramics propel a wide range of applications: from wear resistant coatings and thermal and environmental barriers to catalysts, batteries, thermoelectrics and nuclear energy management. Here, we discuss recent progress of the field, with a particular emphasis on disorder-enhanced properties and applications.
2111.11519v1
2022-11-08
Observation of room-temperature ferroelectricity in elemental Te nanowires
Ferroelectrics are essential in low-dimensional memory devices for multi-bit storage and high-density integration. A polar structure is a necessary premise for ferroelectricity, mainly existing in compounds. However, it is usually rare in elemental materials, causing a lack of spontaneous electric polarization. Here, we report an unexpected room-temperature ferroelectricity in few-chain Te nanowires. Out-of-plane ferroelectric loops and domain reversal are observed by piezoresponse force microscopy. Through density functional theory, we attribute the ferroelectricity to the ion-displacement created by the interlayer interaction between lone pair electrons. Ferroelectric polarization can induce a strong field effect on the transport along the Te chain, supporting a self-gated field-effect transistor. It enables a nonvolatile memory with high in-plane mobility, zero supply voltage, multilevel resistive states, and a high on/off ratio. Our work provides new opportunities for elemental ferroelectrics with polar structures and paves a way towards applications such as low-power dissipation electronics and computing-in-memory devices.
2211.04066v1
2009-07-17
Study of timing properties of single gap high-resistive bakelite RPC
The time resolution for several single gap (2 mm) prototype Resistive Plate Chambers (RPC) made of high resistive (bulk resistivity ~ 10^10 - 10^12 ohm cm), 2 mm thick matt finished bakelite paper laminates with silicone coating on the inner surfaces, has been measured. The time resolution for all the modules has been found to be ~ 2 ns at the plateau region.
0907.2982v1
2003-09-16
Metal-insulator transition in EuO
It is shown that the spectacular metal-insulator transition in Eu-rich EuO can be simulated within an extended Kondo lattice model. The different orders of magnitude of the jump in resistivity in dependence on the concentration of oxygen vacancies as well as the low-temperature resistance minimum in high-resistivity samples are reproduced quantitatively. The huge colossal magnetoresistance (CMR) is calculated and discussed.
0309369v2
2016-08-08
Quantum Criticality and DBI Magneto-resistance
We use the DBI action from string theory and holography to study the magneto-resistance at quantum criticality with hyperscaling violation. We find and analyze a rich class of scaling behaviors for the magneto-resistance. A special case describes the scaling results found in pnictides by Hayers et al. in~\cite{analytis}.
1608.02598v2
2023-09-19
Resistivity of the two-dimensional Bose-Hubbard model at weak coupling
We calculate the weak-coupling resistivity of the two-dimensional Bose Hubbard model, comparing with the more familiar fermionic case. At high temperature the resistivity is linear in $T$, while in the low temperature normal state it is exponentially suppressed. We explore the density dependence and calculate the momentum relaxation rate.
2309.10782v1
2018-09-24
Ionic Tuning of Cobaltites at the Nanoscale
Control of materials through custom design of ionic distributions represents a powerful new approach to develop future technologies ranging from spintronic logic and memory devices to energy storage. Perovskites have shown particular promise for ionic devices due to their high ion mobility and sensitivity to chemical stoichiometry. In this work, we demonstrate a solid-state approach to control of ionic distributions in (La,Sr)CoO$_{3}$ thin films. Depositing a Gd capping layer on the perovskite film, oxygen is controllably extracted from the structure, up-to 0.5 O/u.c. throughout the entire 36 nm thickness. Commensurate with the oxygen extraction, the Co valence state and saturation magnetization show a smooth continuous variation. In contrast, magnetoresistance measurements show no-change in the magnetic anisotropy and a rapid increase in the resistivity over the same range of oxygen stoichiometry. These results suggest significant phase separation, with metallic ferromagnetic regions and oxygen-deficient, insulating, non-ferromagnetic regions, forming percolated networks. Indeed, X-ray diffraction identifies oxygen-vacancy ordering, including transformation to a brownmillerite crystal structure. The unexpected transformation to the brownmillerite phase at ambient temperature is further confirmed by high-resolution scanning transmission electron microscopy which shows significant structural - and correspondingly chemical - phase separation. This work demonstrates room-temperature ionic control of magnetism, electrical resistivity, and crystalline structure in a 36 nm thick film, presenting new opportunities for ionic devices that leverage multiple material functionalities.
1809.08728v1
2020-02-17
Ductile and brittle crack-tip response in equimolar refractory high-entropy alloys
Understanding the strengthening and deformation mechanisms in refractory high-entropy alloys (HEAs), proposed as new high-temperature material, is required for improving their typically insufficient room-temperature ductility. Here, density-functional theory simulations and a continuum mechanics analysis were conducted to systematically investigate the competition between cleavage decohesion and dislocation emission from a crack tip in the body-centered cubic refractory HEAs HfNbTiZr, MoNbTaVW, MoNbTaW, MoNbTiV, and NbTiVZr. This crack-tip competition is evaluated for tensile loading and a totality of 15 crack configurations and slip systems. Our results predict that dislocation plasticity at the crack tip is generally unfavorable -- although the competition is close for some crack orientations, suggesting intrinsic brittleness and low crack-tip fracture toughness in these five HEAs at zero temperature. Fluctuations in local alloy composition, investigated for HfNbTiZr, can locally reduce the resistance to dislocation emission for a slip system relative to the configuration average of that slip system, but do not change the dominant crack-tip response. In the case of single-crystal MoNbTaW, where an experimental, room-temperature fracture-toughness value is available for a crack on a \{100\} plane, theoretical and experimental results agree favorably. Factors that may limit the agreement are discussed. We survey the effect of material anisotropy on preferred crack tip orientations, which are found to be alloy specific. Mixed-mode loadings are found to shift the competition in favor of cleavage or dislocation nucleation, depending on crack configuration and amplified by the effect of material anisotropy on crack tip stresses.
2002.07013v1
2019-08-22
Non-localized states and high hole mobility in amorphous germanium
Covalent amorphous semiconductors, such as amorphous silicon (a-Si) and germanium (a-Ge), are commonly believed to have localized electronic states at the top of the valence band and the bottom of the conduction band. Electrical conductivity is thought to be by the hopping mechanism through localized states. The carrier mobility of these materials is usually very low, in the order of ~10^-3 - 10^-2 cm^2/(Vs) at room temperature. In this study, we present the Hall effect characterization of a-Ge prepared by self-ion implantation of Ge ions. The a-Ge prepared by this method is highly homogenous and has a mass density within 98.5% of the crystalline Ge. The material exhibits an exceptionally high electrical conductivity and carrier mobility (~100 cm^2/(Vs)) for an amorphous semiconductor. The temperature-dependent resistivity of the material is very-well defined with two distinctive regions, extrinsic and intrinsic conductivity, as in crystalline Ge. These results are direct evidence for a largely-preserved band structure and non-localized states of the valence band in a-Ge, as proposed by Tauc et al. from optical characterization alone. This finding is not only significant for the understanding of electrical conductivity in covalent disordered semiconductors, but the exceptionally high mobility we have observed in amorphous Ge opens up device applications not previously considered for amorphous semiconductors.
1908.08246v1
2020-11-20
StressNet: Deep Learning to Predict Stress With Fracture Propagation in Brittle Materials
Catastrophic failure in brittle materials is often due to the rapid growth and coalescence of cracks aided by high internal stresses. Hence, accurate prediction of maximum internal stress is critical to predicting time to failure and improving the fracture resistance and reliability of materials. Existing high-fidelity methods, such as the Finite-Discrete Element Model (FDEM), are limited by their high computational cost. Therefore, to reduce computational cost while preserving accuracy, a novel deep learning model, "StressNet," is proposed to predict the entire sequence of maximum internal stress based on fracture propagation and the initial stress data. More specifically, the Temporal Independent Convolutional Neural Network (TI-CNN) is designed to capture the spatial features of fractures like fracture path and spall regions, and the Bidirectional Long Short-term Memory (Bi-LSTM) Network is adapted to capture the temporal features. By fusing these features, the evolution in time of the maximum internal stress can be accurately predicted. Moreover, an adaptive loss function is designed by dynamically integrating the Mean Squared Error (MSE) and the Mean Absolute Percentage Error (MAPE), to reflect the fluctuations in maximum internal stress. After training, the proposed model is able to compute accurate multi-step predictions of maximum internal stress in approximately 20 seconds, as compared to the FDEM run time of 4 hours, with an average MAPE of 2% relative to test data.
2011.10227v1
2022-05-16
Single Crystalline 2D Material Nanoribbon Networks for Nanoelectronics
The last decade has seen a flurry of studies related to graphene nanoribbons owing to their potential applications in the quantum realm. However, little experimental work has been reported towards nanoribbons of other 2D materials due to the absence of synthesis routes. Here, we propose a universal approach to synthesize high-quality networks of nanoribbons from arbitrary 2D materials while maintaining high crystallinity, sufficient yield, narrow size distribution, and straight-forward device integrability. The wide applicability of this technique is demonstrated by fabricating MoS2, WS2, WSe2, and graphene nanoribbon field effect transistors that inherently do not suffer from interconnection resistances. By relying on self-assembled and self-aligned organic nanostructures as masks, we demonstrate the possibility of controlling the predominant crystallographic direction of the nanoribbon's edges. Electrical characterization shows record mobilities and very high ON currents for various TMDCs despite extreme width scaling. Lastly, we explore decoration of nanoribbon edges with plasmonic particles paving the way towards the development of nanoribbon-based plasmonic sensing and opto-electronic devices.
2205.09507v1
2023-04-18
Controllable Strain-driven Topological Phase Transition and Dominant Surface State Transport in High-Quality HfTe5 Samples
Controlling materials to create and tune topological phases of matter could potentially be used to explore new phases of topological quantum matter and to create novel devices where the carriers are topologically protected. It has been demonstrated that a trivial insulator can be converted into a topological state by modulating the spin-orbit interaction or the crystal lattice. However, there are limited methods to controllably and efficiently tune the crystal lattice and at the same time perform electronic measurements at cryogenic temperatures. Here, we use large controllable strain to demonstrate the topological phase transition from a weak topological insulator phase to a strong topological insulator phase in high-quality HfTe5 samples. After applying high strain to HfTe5 and converting it into a strong topological insulator, we found that the sample's resistivity increased by more than two orders of magnitude (24,000%) and that the electronic transport is dominated by the topological surface states at cryogenic temperatures. Our findings show that HfTe5 is an ideal material for engineering topological properties, and it could be generalized to study topological phase transitions in van der Waals materials and heterostructures. These results can pave the way to create novel devices with applications ranging from spintronics to fault-tolerant topologically protected quantum computers.
2304.09072v1
2016-12-17
Electric Properties of Dirac Fermions Captured into 3D Nanoporous Graphene Networks
Graphene, as a promising material of post-silicon electronics, opens a new paradigm for the novel electronic properties and device applications. On the other hand, the 2D feature of graphene makes it technically challenging to be integrated into 3D transistors with a sufficient processor capacity. Although there are many attempts to assemble 2D graphene into 3D structures, the characteristics of massless Dirac fermions cannot be well preserved in these materials for transistor applications. Here we report a high-performance graphene transistor by utilizing 3D nanoporous graphene which is comprised of an interconnected single graphene sheet and a commodious open porosity to infuse an ionic liquid for a tunable electronic state by applying electric fields. The 3D nanoporous graphene transistor, with high carrier mobility of 5000-7500 cm$^2$V$^{-1}$s$^{-1}$, exhibits two to three orders of magnitude higher electric conductance and capacitance than those of 2D graphene devices, along with preserved ambipolor electronic nature of Dirac cones. Moreover, the 3D graphene networks with Dirac fermions turn out to exhibit a unique nonlinear Hall resistance in a wide range of the gate voltages. The high quality 3D nanoporous graphene EDLT may open a new field for utilizing Dirac fermions in 3D network structures for various fundamental and practical applications.
1612.05716v1
2017-11-24
Stability of Thin Film Refractory Plasmonic Materials Taken to High Temperatures in Air
Materials such as W, TiN, and SrRuO3 (SRO) have been suggested as promising alternatives to Au and Ag in plasmonic applications owing to their refractory properties. However, investigation of the reproducibility of the optical properties after thermal cycling at high operational temperatures is so far lacking. Here, thin films of W, Mo, Ti, TiN, TiON, Ag, Au, and SrRuO3 are investigated to assess their viability for robust refractory plasmonic applications. Films ranging in thickness from 50 - 180 nm are deposited on MgO and Si substrates by RF magnetron sputtering and, in the case of SrRuO3, pulsed laser deposition, prior to characterisation by means of AFM, XRD, spectroscopic ellipsometry, and DC resistivity. Measurements are conducted before and after annealing in air at temperatures ranging from 300 - 1000{\deg} C for one hour, to establish the maximum cycling temperature and potential longevity at temperature for each material. It is found that SrRuO3 retains metallic behaviour after annealing at 800{\deg} C, however, importantly, the optical properties of TiN and TiON are degraded as a result of oxidation. Nevertheless, both TiN and TiON may be better suited than Au or SRO for high temperature applications operating under vacuum conditions.
1711.08923v1
2016-03-17
Transport evidence for the three-dimensional Dirac semimetal phase in ZrTe5
Topological Dirac semimetal is a newly discovered class of materials and has attracted intense attentions. This material can be viewed as a three-dimensional (3D) analogue of graphene and has linear energy dispersion in bulk, leading to a range of exotic transport properties. Here we report direct quantum transport evidence of 3D Dirac semimetal phase of layered material ZrTe5 by angular dependent magnetoresistance measurements under high magnetic fields up to 31 Tesla. We observed very clear negative longitudinal magnetoresistance induced by chiral anomaly under the condition of the magnetic field aligned only along the current direction. Pronounced Shubnikov-de Hass (SdH) quantum oscillations in both longitudinal magnetoresistance and transverse Hall resistance were observed, revealing anisotropic light cyclotron masses and high mobility of the system. In particular, a nontrivial {\pi}-Berry phase in the SdH gives clear evidence for 3D Dirac semimetal phase. Furthermore, we observed clear Landau Level splitting under high magnetic field, suggesting possible splitting of Dirac point into Weyl points due to broken time reversal symmetry. Our results indicate that ZrTe5 is an ideal platform to study 3D massless Dirac and Weyl fermions in a layered compound.
1603.05351v2
2022-06-16
Scalable Composites Benefiting from Transition-Metal Oxides as Cathode Materials for Efficient Lithium-Sulfur Batteries
Composite materials achieved by including transition-metal oxides with different structures and morphologies in sulfur are suggested as scalable cathodes for high-energy lithium-sulfur (Li-S) batteries. The composites contain 80 wt.% sulfur and 20 wt.% of either MnO2 or TiO2, leading to a sulfur content in the electrode of 64 wt.% and revealing a reversible, fast, and lowly polarized conversion process in the cell with limited interphase resistance. The S-TiO2 composite exhibits an excellent rate capability between C/10 and 2C, and a cycle life extended over 400 cycles at 2C, owing to the effects of the nanometric TiO2 additive in boosting the reaction kinetics. Instead, the micrometric sized particles of MnO2 partially limit the electrochemical activity of S-MnO2 to the current rate of 1C. Nevertheless, both S-MnO2 and S-TiO2 withstand a sulfur loading up to values approaching 6 mgcm-2, and deliver an areal capacit ranging from about 4.5 to 5.5 mAhcm-2 at C/5. The excellent performances of the metal oxide-sulfur electrodes, even at high active material loading, and the possible scalability of the synthetic pathway adopted in the work suggest that the composites are viable cathodes for next-generation Li-S batteries with high energy density and efficient electrochemical process.
2206.14569v1
2024-01-25
Spatially Resolved High Voltage Kelvin Probe Force Microcopy: A Novel Avenue for Examining Electrical Phenomena at Nanoscale
Kelvin probe microscopy (KPFM) is a well-established scanning probe technique, used to measure surface potential accurately; it has found extensive use in the study of a range of materials phenomena. In its conventional form, KPFM frustratingly precludes imaging samples or scenarios where large surface potential exists or large surface potential gradients are created outside the typical +/-10V window. If the potential regime measurable via KPFM could be expanded, to enable precise and reliable metrology, through a high voltage KPFM (HV-KPFM) adaptation, it could open up pathways towards a range of novel experiments, where the detection limit of regular KPFM has so far prevented the use of the technique. In this work, HV-KPFM has been realised and shown to be capable of measuring large surface potential and potential gradients with accuracy and precision. The technique has been employed to study a range of materials (positive temperature coefficient of resistivity ceramics, charge storage fluoropolymers and pyroelectrics) where accurate spatially resolved mapping of surface potential within high voltage regime facilitates novel physical insight. The results demonstrate that HV-KPFM can be used as an effective tool to fill in existing gaps in surface potential measurements while also opening routes for novel studies in materials physics.
2401.14124v1
2024-02-05
High Strain Engineering of a Suspended WSSe Monolayer Membrane by Indentation and Measured by Tip-enhanced Photoluminescence
Straintronics involves the manipulation and regulation of the electronic characteristics of 2D materials through the use of macro- and nano-scale strain engineering. In this study, we utilized an atomic force microscope (AFM) coupled with an optical system to perform indentation measurements and tip-enhanced photoluminescence (TEPL), allowing us to extract the local optical response of a suspended monolayer membrane of ternary WSSe at various levels of deformation, up to strains of 10%. The photoluminescence signal is modelled considering the deformation, stress distribution and strain dependence of the WSSe band structure. We observe an additional TEPL signal that exhibits significant variation under strain, with 64 meV per percent of elongation. This peak is linked to the highly strained 2D material lying right underneath the tip. We discuss the amplification of the signal and its relation to the excitonic funnelling effect in a more comprehensive model. We will also compare the diffusion caused by Auger recombination against the radiative excitonic decay. We use TEPL to examine and comprehend the local physics of 2D semi-conducting materials subjected to extreme mechanical strain. Chemical vapour deposition-fabricated 2D ternaries possess high strain resistance, comparable to the benchmark MoS2, and a high Young's modulus of 273 GPa.
2402.03061v1
2019-08-11
Magnetotransport as diagnostic of spin reorientation: kagome ferromagnet as a case study
While in most ferro or antiferromagnetic materials there is a unique crystallographic direction, including crystallographically equivalent directions, in which the moments like to point due to spin-orbit coupling, in some, the direction of the spin reorients as a function of a certain physical parameter such as temperature, pressure etc. Fe3Sn2 is a kagome ferromagnet with an onset of ferromagnetism below 650 K, and undergoes a spin reorientation near 150 K. While it is known that the moments in Fe3Sn2 point perpendicular to the kagome plane at high temperatures and parallel to the kagome plane at low temperatures, how the distribution of the magnetic domains in the two different spin orientations evolve throughout the spin reorientation is not well known. Furthermore, while there have been various reports on the magnetotransport properties in the Hall configuration, the angular dependence of magnetoresistance has not been studied so far. In this paper, we have examined the spin reorientation by using anisotropic magnetoresistivity in detail, exploiting the dependence of the resistivity on the direction between magnetization and applied current. We are able to determine the distribution of the magnetic domains as a function of temperature between 360 K to 2 K and the reorientation transition to peak at 120 K. We discover that both out of plane and in plane phases coexist at temperatures around the spin reorientation, indicative of a first order transition. Although the volume of the magnetic domains in the different phases sharply changes at the spin reorientation transition, the electronic structure for a specific magnetization is not influenced by the spin reorientation. In contrast, we observe an electronic transition around 40 K, hitherto unreported, and reflected in both the zero-field resistivity and anisotropic resistivity.
1908.03927v1
2021-11-22
Shape-Dependent Multi-Weight Magnetic Artificial Synapses for Neuromorphic Computing
In neuromorphic computing, artificial synapses provide a multi-weight conductance state that is set based on inputs from neurons, analogous to the brain. Additional properties of the synapse beyond multiple weights can be needed, and can depend on the application, requiring the need for generating different synapse behaviors from the same materials. Here, we measure artificial synapses based on magnetic materials that use a magnetic tunnel junction and a magnetic domain wall. By fabricating lithographic notches in a domain wall track underneath a single magnetic tunnel junction, we achieve 4-5 stable resistance states that can be repeatably controlled electrically using spin orbit torque. We analyze the effect of geometry on the synapse behavior, showing that a trapezoidal device has asymmetric weight updates with high controllability, while a straight device has higher stochasticity, but with stable resistance levels. The device data is input into neuromorphic computing simulators to show the usefulness of application-specific synaptic functions. Implementing an artificial neural network applied on streamed Fashion-MNIST data, we show that the trapezoidal magnetic synapse can be used as a metaplastic function for efficient online learning. Implementing a convolutional neural network for CIFAR-100 image recognition, we show that the straight magnetic synapse achieves near-ideal inference accuracy, due to the stability of its resistance levels. This work shows multi-weight magnetic synapses are a feasible technology for neuromorphic computing and provides design guidelines for emerging artificial synapse technologies.
2111.11516v2
2014-11-04
Tackling drug resistant infection outbreaks of global pandemic Escherichia coli ST131 using evolutionary and epidemiological genomics
High-throughput molecular screening is required to investigate the origin and diffusion of antimicrobial resistance in pathogen outbreaks. The most frequent cause of human infection is Escherichia coli, which is dominated by sequence type 131 (ST131), a set of rapidly radiating pandemic clones. The highly infectious clades of ST131 originated firstly by a mutation enhancing virulence and adhesion. Secondly, single-nucleotide polymorphisms occurred enabling fluoroquinolone-resistance, which is near-fixed in all ST131. Thirdly, broader resistance through beta-lactamases has been gained and lost frequently, symptomatic of conflicting environmental selective effects. This flexible approach to gene exchange is worrying and supports the proposition that ST131 will develop an even wider range of plasmid and chromosomal elements promoting antimicrobial resistance. To stymie ST131, deep genome sequencing is required to understand the origin, evolution and spread of antimicrobial resistance genes. Phylogenetic methods that decipher past events can predict future patterns of virulence and transmission based on genetic signatures of adaptation and gene exchange. Both the effect of partial antimicrobial exposure and cell dormancy caused by variation in gene expression may accelerate the development of resistance. High-throughput sequencing can decode measurable evolution of cell populations within patients associated with systems-wide changes in gene expression during treatments. A multi-faceted approach can enhance assessment of antimicrobial resistance in E. coli ST131 by examining transmission dynamics between hosts to achieve a goal of pre-empting resistance before it emerges by optimising antimicrobial treatment protocols.
1411.0905v3
2014-09-25
Recycled nylon fibers as cement mortar reinforcement
We investigate engineering applications of recycled nylon fibers obtained from waste fishing nets, focusing our attention on the use of recycled nylon fibers as tensile reinforcement of cementitious mortars. We begin by characterizing the tensile behavior of both unconditioned and alkali-cured recycled nylon fibers obtained through manual cutting of waste fishing net filaments, with the aim of assessing the resistance of such materials to chemical attacks. Special attention is also given to evaluating the workability of fresh mortar and the possible impacts of contaminants released by waste fishing nets into the environment. Next, we deal with compression and bending tests on cementitious mortars reinforced with recycled nylon fibers, and establish comparisons with the experimental behavior of the unreinforced material and with results given in existing literature. In our analysis of different weight fractions and aspect ratios of the reinforcing fibers, we observe marked increases in the tensile strength (up to +35%) and toughness (up to 13 times greater) of the nylon reinforced mortar, as compared with the unreinforced material. The presented results emphasize the high environmental and mechanical potential of recycled nylon fibers for the reinforcement of sustainable cement mortars.
1409.7258v4
2019-05-14
Ohmic contact engineering in few-layer black Phosphorus field effect transistors
Achieving good quality Ohmic contacts to van der Waals materials is a challenge, since at the interface between metal and van der Waals material, different conditions can occur, ranging from the presence of a large energy barrier between the two materials to the metallization of the layered material below the contacts. In black phosphorus (bP), a further challenge is its high reactivity to oxygen and moisture, since the presence of uncontrolled oxidation can substantially change the behavior of the contacts. In this study, we investigate the influence of the metal used for the contacts to bP against the variability between different flakes and different samples, using three of the most used metals as contacts: Chromium, Titanium, and Nickel. Using the transfer length method, from an analysis of ten devices, both at room temperature and at low temperature, Ni results to be the best metal for Ohmic contacts to bP, providing the lowest contact resistance and minimum scattering between different devices. Moreover, we investigate the gate dependence of the current-voltage characteristics of these devices. In the accumulation regime, we observe good linearity for all metals investigated.
1905.05649v1
2019-06-24
Conductivity of Dirac-like surface states in correlated honeycomb transition metal oxide Mott insulators
The search for materials with novel and unusual electronic properties is at the heart of condensed matter physics as well as the basis to develop conceptual new technologies. In this context, the correlated honeycomb transition metal oxides attract large attention for both, being a possible experimental realization of the theoretically predicted magnetic Kitaev exchange and the theoretical prospect of topological nontriviality. The Mott insulating sodium iridate is prototypical among these materials with the promising prospect to bridge the field of strongly correlated systems with topology, finally opening a path to a wide band gap material with exotic surface properties. Here, we report a profound study of the electronic properties of ultra-high-vacuum cleaved surfaces combining transport measurements with scanning tunneling techniques, showing that multiple conductive channels with differing nature are simultaneously apparent in this material. Most importantly, a V-shaped density of states and a low sheet resistance, in spite of a large defect concentration, point towards a topologically protected surface conductivity contribution. By incorporating the issue of the addressability of electronic states in the tunneling process, we develop a framework connecting previous experimental results as well as theoretical considerations.
1906.09809v2
2020-07-22
Impact of Li$_{2.9}$B$_{0.9}$S$_{0.1}$O$_{3.1}$ glass additive on the structure and electrical properties of the LATP-based ceramics
The existing solid electrolytes for lithium ion batteries suffer from low total ionic conductivity, which restricts its usefulness for the lithium-ion battery technology. Among them, the NASICON-based materials, such as Li1.3Al0.3Ti1.7(PO4)3 (LATP) exhibit low total ionic conductivity due to highly resistant grain boundary phase. One of the possible approaches to efficiently enhance their total ionic conductivity is the formation of a composite material. Herein, the Li2.9B0.9S0.1O3.1 glass, called LBSO hereafter, was chosen as an additive material to improve the ionic properties of the ceramic Li1.3Al0.3Ti1.7(PO4)3 base material. The properties of this Li1.3Al0.3Ti1.7(PO4)3-xLi2.9B0.9S0.1O3.1 (0 < x < 0.3) system have been studied by means of high temperature X-ray diffractometry (HTXRD), 7Li, 11B, 27Al and 31P magic angle spinning nuclear magnetic resonance spectroscopy (MAS NMR), thermogravimetry (TG), scanning electron microscopy (SEM), impedance spectroscopy (IS) and density methods. We show here that the introduction of the foreign LBSO phase enhances their electric properties. This study reveals several interesting correlations between the apparent density, the microstructure, the composition, the sintering temperature and the ionic conductivity. Moreover, the electrical properties of the composites will be discussed in the terms of the brick-layer model (BLM). The highest value of {\sigma}tot = 1.5 x 10-4 Scm-1 has been obtained for LATP-0.1LBSO material sintered at 800{\deg}C.
2007.11244v2
2020-12-16
Anisotropic phonon-mediated electronic transport in chiral Weyl semimetals
Discovery and observations of exotic, quantized optical and electrical responses have sparked renewed interest in nonmagnetic chiral crystals. Within this class of materials, six group V transition metal ditetrelides, that is, XY$_2$ (X = V, Nb, Ta and Y = Si, Ge), host composite Weyl nodes on high-symmetry lines, with Kramers-Weyl fermions at time-reversal invariant momenta. In addition, at least two of these materials, NbGe$_2$ and NbSi$_2$, exhibit superconducting transitions at low temperatures. The interplay of strong electron-phonon interaction and complex Fermi surface topology present an opportunity to study both superconductivity and hydrodynamic electron transport in these systems. Towards this broader question, we present an ab initio theoretical study of the electronic transport and electron-phonon scattering in this family of materials, with a particular focus on NbGe$_2$ vs. NbSi$_2$, and the other group V ditetrelides. We shed light on the microscopic origin of NbGe$_2$'s large and anisotropic room temperature resistivity and contextualize its strong electron-phonon scattering with a presentation of other relevant scattering lifetimes, both momentum-relaxing and momentum-conserving. Our work explores the intriguing possibility of observing hydrodynamic electron transport in these chiral Weyl semimetals.
2012.09207v1
2022-08-15
Valley-coherent quantum anomalous Hall state in AB-stacked MoTe2/WSe2 bilayers
Moir\'e materials provide fertile ground for the correlated and topological quantum phenomena. Among them, the quantum anomalous Hall (QAH) effect, in which the Hall resistance is quantized even under zero magnetic field, is a direct manifestation of the intrinsic topological properties of a material and an appealing attribute for low-power electronics applications. The QAH effect has been observed in both graphene and transition metal dichalcogenide (TMD) moir\'e materials. It is thought to arise from the interaction-driven valley polarization of the narrow moir\'e bands. Here, we show surprisingly that the newly discovered QAH state in AB-stacked MoTe2/WSe2 moir\'e bilayers is not valley-polarized but valley-coherent. The layer- and helicity-resolved optical spectroscopy measurement reveals that the QAH ground state possesses spontaneous spin (valley) polarization aligned (anti-aligned) in two TMD layers. In addition, saturation of the out-of-plane spin polarization in both layers occurs only under high magnetic fields, supporting a canted spin texture. Our results call for a new mechanism for the QAH effect and highlight the potential of TMD moir\'e materials with strong electronic correlations and spin-orbit interactions for exotic topological states.
2208.07452v1
2022-09-26
Evaluating Effects of Geometry and Material Composition on Production of Transversely Shaped Beams from Diamond Field Emission Array Cathodes
Field emission cathodes (FECs) are attractive for the next generation of injectors due to their ability to provide high current density bright beams with low intrinsic emittance. One application of FECs worthy of special attention is to provide transversely shaped electron beams for emittance exchange that translates a transverse electron beam pattern into a longitudinal pattern. FECs can be fabricated in a desired pattern and produce transversely shaped beams without the need for complex masking or laser schemes. However, reliable and consistent production of transversely shaped beams is affected by material properties of the FEC. This paper reports the results of testing two diamond field emitter array (DFEA) FECs with the same lithography pattern and emitter geometry but different material and tip characteristics. Although both cathodes were able to sustain gradients of 44 MV/m and produce maximum output integral charge of 0.5 nC per radiofrequency (rf) pulse, their emission patterns were quite different. One cathode did not produce a patterned beam while the other one did. Differences in field emission characteristics and patterned beam production were explained by the differences in the tip geometry and the cathode material properties. The main practical takeaway was found to be that the tip sharpness was not a prerequisite for good patterned beam production. Instead, other material characteristics, such as the ballast resistance, determined cathode performance.
2209.13047v1
2023-04-13
Effect of hirtisation on the roughness and fatigue performance of porous titanium lattice structures
Additive manufacturing (AM) has enabled the fabrication of extremely complex components such as porous metallic lattices, which have applications in aerospace, automotive, and in particular biomedical devices. The fatigue resistance of these materials is currently an important limitation however, due to manufacturing defects such as semi-fused particles and weld lines. Here Hirtisation$^\circledR$ is used for post-processing of Ti-6Al-4V lattices, reducing the strut surface roughness (Sa) from 12 to 6 $\mu$m, removing all visible semi-fused particles. The evenness of this treatment in lattices with $\rho /\rho_{s}$ up to 18.3% and treatment depth of 6.5 mm was assessed, finding no evidence of reduced effectiveness on internal surfaces. After normalising to quasi-static mechanical properties to account for material losses during hirtisation (34-37% reduction in strut diameter), the fatigue properties show a marked improvement due to the reduction in surface roughness. Normalised high cycle fatigue strength ($\sigma_{f,10^{6}}/\sigma_{y}$) increased from around 0.1 to 0.16-0.21 after hirtisation, an average increase of 80%. For orthopaedic implant devices where matching the stiffness of surrounding bone is crucial, the $\sigma_{f}/E$ ratio is a key metric. After hirtisation the $\sigma_{f}/E$ ratio increased by 90%, enabling design of stiffness matched implant materials with greater fatigue strength. This work demonstrates that hirtisation is an effective method for improving the surface roughness of porous lattice materials, thereby enhancing their fatigue performance.
2304.06621v1
2024-03-15
An inflated dynamic Laplacian to track the emergence and disappearance of semi-material coherent sets
Lagrangian methods continue to stand at the forefront of the analysis of time-dependent dynamical systems. Most Lagrangian methods have criteria that must be fulfilled by trajectories as they are followed throughout a given finite flow duration. This key strength of Lagrangian methods can also be a limitation in more complex evolving environments. It places a high importance on selecting a time window that produces useful results, and these results may vary significantly with changes in the flow duration. We show how to overcome this drawback in the tracking of coherent flow features. Finite-time coherent sets (FTCS) are material objects that strongly resist mixing in complicated nonlinear flows. Like other materially coherent objects, by definition they must retain their coherence properties throughout the specified flow duration. Recent work [Froyland and Koltai, CPAM, 2023] introduced the notion of semi-material FTCS, whereby a balance is struck between the material nature and the coherence properties of FTCS. This balance provides the flexibility for FTCS to come and go, merge and separate, or undergo other changes as the governing unsteady flow experiences dramatic shifts. The purpose of this work is to illustrate the utility of the inflated dynamic Laplacian introduced in [Froyland and Koltai, CPAM, 2023] in a range of dynamical systems that are challenging to analyse by standard Lagrangian means, and to provide an efficient meshfree numerical approach for the discretisation of the inflated dynamic Laplacian.
2403.10360v1
2024-03-20
Tailoring Physical Properties of Crystals through Synthetic Temperature Control: A Case Study for new Polymorphic NbFeTe2 phases
Growth parameters play a significant role in the crystal quality and physical properties of layered materials. Here we present a case study on a van der Waals magnetic NbFeTe2 material. Two different types of polymorphic NbFeTe2 phases, synthesized at different temperatures, display significantly different behaviors in crystal symmetry, electronic structure, electrical transport, and magnetism. While the phase synthesized at low temperature showing behavior consistent with previous reports, the new phase synthesized at high temperature, has completely different physical properties, such as metallic resistivity, long-range ferromagnetic order, anomalous Hall effect, negative magnetoresistance, and distinct electronic structures. Neutron diffraction reveals out-of-plane ferromagnetism below 70K, consistent with the electrical transport and magnetic susceptibility studies. Our work suggests that simply tuning synthetic parameters in a controlled manner could be an effective route to alter the physical properties of existing materials potentially unlocking new states of matter, or even discovering new materials.
2403.13596v1
2022-07-06
Proposal for semiconductor-free negative differential resistance tunnel diode with ultra-high peak-to-valley current ratio
The negative differential resistance (NDR) tunnel diodes are promising alternative devices for beyond-CMOS computing as they offer several potential applications when integrated with transistors. We propose a novel semiconductor-free NDR tunnel diode concept that exhibits an ultra-high peak-to-valley current ratio (PVCR) value. Our proposed NDR diode consists of two cold metal electrodes separated by a thin insulating tunnel barrier. The NDR effect stems from the unique electronic band structure of the cold metal electrodes, i.e., the width of the isolated metallic bands around the Fermi level as well as the energy gaps separating higher- and lower-lying bands determine the current-voltage ($I$-$V$) characteristics and the PVCR value of the tunnel diode. By proper choice of the cold metal electrode materials, either a conventional N-type or ${\Lambda}$-type NDR effect can be obtained. Two-dimensional (2D) materials offer a unique platform for the realization of proposed NDR tunnel diodes. To demonstrate the proof of concept we employ the nonequilibrium Green function method combined with density functional theory to calculate the $I$-$V$ characteristic of the lateral (AlI$_2$/MgI$_2$/AlI$_2$) and vertical (NbS$_2$/h-BN/NbS$_2$) heterojunction tunnel diodes based on 2D cold metals. For the lateral tunnel diode, we obtain a ${\Lambda}$-type NDR effect with an ultra-high PVCR value of 10$^{16}$ at room temperature, while the vertical tunnel diode exhibits a conventional N-type NDR effect with a smaller PVCR value of about 10$^4$. The proposed concept provides a semiconductor-free solution for NDR devices to achieve desired $I$-$V$ characteristics with ultra-high PVCR values for memory and logic applications.
2207.02593v2
2001-02-12
Temperature- and magnetic-field-dependent resistivity of MgB2 sintered at high temperature and high pressure condition
We report the temperature- and magnetic-field-dependent resistivity of MgB2 sintered at high temperature and high pressure condition. The superconducting transition width for the resistivity measurement was about 0.4 K, and the low-field magnetization showed a sharp superconducting transition with a transition width of about 1 K. The resistivity in the normal state roughly followed T^2 behavior with smaller residual resistivity ratio (RRR) of 3 over broad temperature region above 100 K rather than reported T^3 behavior with larger RRR value of ~ 20 in the samples made at lower pressures. Also, the resistivity did not change appreciably with the applied magnetic field, which was different from previous report. These differences were discussed with the microscopic and structural change due to the high-pressure sintering.
0102215v4
2017-03-01
Size Dependence of Nanoscale Wear of Silicon Carbide
Nanoscale, single-asperity wear of single-crystal silicon carbide (sc-SiC) and nanocrystalline silicon carbide (nc-SiC) is investigated using single-crystal diamond nanoindenter tips and nanocrystalline diamond atomic force microscopy (AFM) tips under dry conditions, and the wear behavior is compared to that of single-crystal silicon with both thin and thick native oxide layers. We discovered a transition in the relative wear resistance of the SiC samples compared to that of Si as a function of contact size. With larger nanoindenter tips (tip radius around 370 nm), the wear resistances of both sc-SiC and nc-SiC are higher than that of Si. This result is expected from the Archard's equation because SiC is harder than Si. However, with the smaller AFM tips (tip radius around 20 nm), the wear resistances of sc-SiC and nc-SiC are lower than that of Si, despite the fact that the contact pressures are comparable to those applied with the nanoindenter tips, and the plastic zones are well-developed in both sets of wear experiments. We attribute the decrease in the relative wear resistance of SiC compared to that of Si to a transition from a wear regime dominated by the materials' resistance to plastic deformation (i.e., hardness) to a regime dominated by the materials' resistance to interfacial shear. This conclusion is supported by our AFM studies of wearless friction, which reveal that the interfacial shear strength of SiC is higher than that of Si. The contributions of surface roughness and surface chemistry to differences in interfacial shear strength are also discussed.
1703.01181v1
2022-02-09
Scalable $\rm Al_2O_3-TiO_2$ Conductive Oxide Interfaces as Defect Reservoirs for Resistive Switching Devices
Resistive switching devices herald a transformative technology for memory and computation, offering considerable advantages in performance and energy efficiency. Here we employ a simple and scalable material system of conductive oxide interfaces and leverage their unique properties for a new type of resistive switching device. For the first time, we demonstrate an $\rm Al_2O_3-TiO_2$ based valence-change resistive switching device, where the conductive oxide interface serves both as the back electrode and as a reservoir of defects for switching. The amorphous-polycrystalline $\rm Al_2O_3-TiO_2$ conductive interface is obtained following the technological path of simplifying the fabrication of the two-dimensional electron gases (2DEGs), making them more scalable for practical mass integration. We combine physical analysis of the device chemistry and microstructure with comprehensive electrical analysis of its switching behavior and performance. We pinpoint the origin of the resistive switching to the conductive oxide interface, which serves as the bottom electrode and as a reservoir of oxygen vacancies. The latter plays a key role in valence-change resistive switching devices. The new device, based on scalable and complementary metal-oxide-semiconductor (CMOS) technology-compatible fabrication processes, opens new design spaces towards increased tunability and simplification of the device selection challenge.
2202.04477v2
2019-04-07
Phase field modelling of crack propagation in functionally graded materials
We present a phase field formulation for fracture in functionally graded materials (FGMs). The model builds upon homogenization theory and accounts for the spatial variation of elastic and fracture properties. Several paradigmatic case studies are addressed to demonstrate the potential of the proposed modelling framework. Specifically, we (i) gain insight into the crack growth resistance of FGMs by conducting numerical experiments over a wide range of material gradation profiles and orientations, (ii) accurately reproduce the crack trajectories observed in graded photodegradable copolymers and glass-filled epoxy FGMs, (iii) benchmark our predictions with results from alternative numerical methodologies, and (iv) model complex crack paths and failure in three dimensional functionally graded solids. The suitability of phase field fracture methods in capturing the crack deflections intrinsic to crack tip mode-mixity due to material gradients is demonstrated. Material gradient profiles that prevent unstable fracture and enhance crack growth resistance are identified: this provides the foundation for the design of fracture resistant FGMs. The finite element code developed can be downloaded from www.empaneda.com/codes.
1904.08749v1
2009-05-13
Reliability of resistivity quantification for shallow subsurface water processes
The reliability of surface-based electrical resistivity tomography (ERT) for quantifying resistivities for shallow subsurface water processes is analysed. A method comprising numerical simulations of water movement in soil and forward-inverse modeling of ERT surveys for two synthetic data sets is presented. Resistivity contrast, e.g. by changing water content, is shown to have large influence on the resistivity quantification. An ensemble and clustering approach is introduced in which ensembles of 50 different inversion models for one data set are created by randomly varying the parameters for a regularisation based inversion routine. The ensemble members are sorted into five clusters of similar models and the mean model for each cluster is computed. Distinguishing persisting features in the mean models from singular artifacts in individual tomograms can improve the interpretation of inversion results. Especially in the presence of large resistivity contrasts in high sensitivity areas, the quantification of resistivities can be unreliable. The ensemble approach shows that this is an inherent problem present for all models inverted with the regularisation based routine. The results also suggest that the combination of hydrological and electrical modeling might lead to better results.
0905.2117v1
2009-06-17
Resistive MHD jet simulations with large resistivity
Axisymmetric resistive MHD simulations for radially self-similar initial conditions are performed, using the NIRVANA code. The magnetic diffusivity could occur in outflows above an accretion disk, being transferred from the underlying disk into the disk corona by MHD turbulence (anomalous turbulent diffusivity), or as a result of ambipolar diffusion in partially ionized flows. We introduce, in addition to the classical magnetic Reynolds number Rm, which measures the importance of resistive effects in the induction equation, a new number Rb, which measures the importance of the resistive effects in the energy equation. We find two distinct regimes of solutions in our simulations. One is the low-resistivity regime, in which results do not differ much from ideal-MHD solutions. In the high-resistivity regime, results seem to show some periodicity in time-evolution, and depart significantly from the ideal-MHD case. Whether this departure is caused by numerical or physical reasons is of considerable interest for numerical simulations and theory of astrophysical outflows and is currently investigated.
0906.3254v1
2011-12-29
Magnetospheric Accretion and Ejection of Matter in Resistive Magnetohydrodynamic Simulations
The ejection of matter in the close vicinity of a young stellar object is investigated, treating the accretion disk as a gravitationally bound reservoir of matter. By solving the resistive MHD equations in 2D axisymmetry using our version of the Zeus-3D code with newly implemented resistivity, we study the effect of magnetic diffusivity in the magnetospheric accretion-ejection mechanism. Physical resistivity was included in the whole computational domain so that reconnection is enabled by the physical as well as the numerical resistivity. We show, for the first time, that quasi-stationary fast ejecta of matter, which we call {\em micro-ejections}, of small mass and angular momentum fluxes, can be launched from a purely resistive magnetosphere. They are produced by a combination of pressure gradient and magnetic forces, in presence of ongoing magnetic reconnection along the boundary layer between the star and the disk, where a current sheet is formed. Mass flux of micro-ejection increases with increasing magnetic field strength and stellar rotation rate, and is not dependent on the disk to corona density ratio and amount of resistivity.
1112.6226v2
2016-10-17
Nonlinear Resistivity for Magnetohydrodynamical Models
A new formulation of the plasma resistivity that arises from the collisional momentum-transfer rate between electrons and ions is presented. The resistivity computed herein is shown to depend not only on the temperature and density but also on all other polynomial velocity-space moments of the distribution function, such as the pressure tensor and heat flux vector. The exact expression for the collisional momentum-transfer rate is determined, and is used to formulate the nonlinear anisotropic resistivity. The new formalism recovers the Spitzer resistivity, as well as the concept of thermal force if the heat flux is assumed to be proportional to a temperature gradient. Furthermore, if the pressure tensor is related to viscous stress, the latter enters the expression for the resistivity. The relative importance of the nonlinear term(s) with respect to the well-established electron inertia and Hall terms is also examined. The subtle implications of the nonlinear resistivity, and its dependence on the fluid variables, are discussed in the context of magnetized plasma environments and phenomena such as magnetic reconnection.
1610.05193v2
2020-03-09
Quantum mechanical current-to-voltage conversion with quantum Hall resistance array
Accurate measurement of the electric current requires a stable and calculable resistor for an ideal current to voltage conversion. However, the temporal resistance drift of a physical resistor is unavoidable, unlike the quantum Hall resistance directly linked to the Planck constant h and the elementary charge e. Lack of an invariant high resistance leads to a challenge in making small current measurements below 1 muA with an uncertainty better than one part in 106. In this work, we demonstrate a current to voltage conversion in the range from a few nano amps to one microamp with an invariant quantized Hall array resistance. The converted voltage is directly compared with the Josephson voltage reference in the framework of Ohm's law. Markedly distinct from the classical conversion, which relies on an artifact resistance reference, this current-to-voltage conversion does not demand timely resistance calibrations. It improves the precision of current measurement down to 8 10 -8 at 1 muA.
2003.04464v1
2021-02-11
Suppressing evolution through environmental switching
Ecology and evolution under changing environments are important in many subfields of biology with implications for medicine. Here, we explore an example: the consequences of fluctuating environments on the emergence of antibiotic resistance, which is an immense and growing problem. Typically, high doses of antibiotics are employed to eliminate the infection quickly and minimize the time under which resistance may emerge. However, this strategy may not be optimal. Since competition can reduce fitness and resistance typically has a reproductive cost, resistant mutants' fitness can depend on their environment. Here we show conditions under which environmental varying fitness can be exploited to prevent the emergence of resistance. We develop a stochastic Lotka-Volterra model of a microbial system with competing phenotypes: a wild strain susceptible to the antibiotic, and a mutant strain that is resistant. We investigate the impact of various pulsed applications of antibiotics on population suppression. Leveraging competition, we show how a strategy of environmental switching can suppress the infection while avoiding resistant mutants. We discuss limitations of the procedure depending on the microbe and pharmacodynamics and methods to ameliorate them.
2102.05813v2
2023-12-08
Electron-hole collision-limited resistance of gapped graphene
Collisions between electrons and holes can dominate the carrier scattering in clean graphene samples in the vicinity of charge neutrality point. While electron-hole limited resistance in pristine gapless graphene is well-studied, its evolution with induction of band gap $E_g$ is less explored. Here, we derive the functional dependence of electron-hole limited resistance of gapped graphene $\rho_{eh}$ on the ratio of gap and thermal energy $E_g/kT$. At low temperatures and large band gaps, the resistance grows linearly with $E_g/kT$, and possesses a minimum at $E_g \approx 2.5 kT$. This contrast to the Arrhenius activation-type behaviour for intrinsic semiconductors. Introduction of impurities restores the Arrhenius law for resistivity at low temperatures and/or high doping densities. The hallmark of electron-hole collision effects in graphene resistivity at charge neutrality is the crossover between exponential and power-law resistivity scalings with temperature.
2312.05066v1
2019-03-18
Experimental and Theoretical Investigation on the Possible Half-metallic Behaviour of Equiatomic Quaternary Heusler Alloys: CoRuMnGe and CoRuVZ (Z = Al, Ga)
In this report, structural, electronic, magnetic and transport properties of quaternary Heusler alloys CoRuMnGe and CoRuVZ (Z = Al, Ga) are investigated. All the three alloys are found to crystallize in cubic structure. CoRuMnGe exhibits L2$_1$ structure whereas, the other two alloys have B2-type disorder. For CoRuMnGe and CoRuVGa, the experimental magnetic moments are in close agreement with the theory as well as those predicted by the Slater-Pauling rule, while for CoRuVAl, a relatively large deviation is seen. The reduction in the moment in case of CoRuVAl possibly arises due to the anti-site disorder between Co and Ru sites as well as V and Al sites. Among these alloys, CoRuMnGe has the highest T$\mathrm{_C}$ of 560 K. Resistivity variation with temperature reflects the half-metallic nature in CoRuMnGe alloy. CoRuVAl shows metallic character in both paramagnetic and ferromagnetic states, whereas the temperature dependence of resistivity for CoRuVGa is quite unusual. In the last system, $\rho$ vs. T curve shows an anomaly in the form of a maximum and a region of negative temperature coefficient of resistivity (TCR) in the magnetically ordered state. The ab initio calculations predict nearly half-metallic ferromagnetic state with high spin polarization of 91, 89 and 93 \% for CoRuMnGe, CoRuVAl and CoRuVGa respectively. To investigate the electronic properties of the experimentally observed structure, the Co-Ru swap disordered structures of CoRuMnGe alloy are also simulated and it is found that the disordered structures retain half-metallic nature, high spin polarization with almost same magnetic moment as in the ideal structure. Nearly half-metallic character, high T$\mathrm{_C}$ and high spin polarization make CoRuMnGe alloy promising for room temperature spintronic applications.
1903.07265v2
2021-05-06
High-sensitivity of initial SrO growth on the residual resistivity in epitaxial thin films of SrRuO$_3$ on SrTiO$_3$ (001)
The growth of SrRuO$_3$ (SRO) thin film with high-crystallinity and low residual resistivity (RR) is essential to explore its intrinsic properties. Here, utilizing the adsorption-controlled growth technique, the growth condition of initial SrO layer on TiO$_2$-terminated SrTiO$_3$ (STO) (001) substrate was found to be crucial for achieving a low RR in the resulting SRO film grown afterward. The optimized initial SrO layer shows a $c$(2 x 2) superstructure that was characterized by electron diffraction, and a series of SRO films with different thicknesses ($t$s) were then grown. The resulting SRO films exhibit excellent crystallinity with orthorhombic-phase down to $t \approx$ 4.3 nm, which was confirmed by high resolution X-ray measurements. From azimuthal X-ray scan for SRO orthorhombic (021) reflection, we uncover four structural domains with a dominant domain of orthorhombic SRO [001] along cubic STO [010] direction. The dominant domain population depends on $t$, STO miscut angle (${\alpha}$), and miscut direction (${\beta}$), giving a volume fraction of about 92 $\%$ for $t \approx$ 26.6 nm and (${\alpha}$, ${\beta}$) ~ (0.14$^{\rm o}$, 5$^{\rm o}$). On the other hand, metallic and ferromagnetic properties were well preserved down to $t \approx$ 1.2 nm. Residual resistivity ratio (RRR = ${\rho}$(300 K)/${\rho}$(5 K)) reduces from 77.1 for $t \approx$ 28.5 nm to 2.5 for $t \approx$ 1.2 nm, while ${\rho}$(5 K) increases from 2.5 $\mu\Omega$cm for $t \approx$ 28.5 nm to 131.0 $\mu\Omega$cm for $t \approx$ 1.2 nm. The ferromagnetic onset temperature ($T_c\prime$) of around 151 K remains nearly unchanged down to $t \approx$ 9.0 nm and decreases to 90 K for $t \approx$ 1.2 nm. Our finding thus provides a practical guideline to achieve high crystallinity and low RR in ultra-thin SRO films by simply adjusting the growth of initial SrO layer.
2105.02404v1
2021-12-01
Synthesis and study of (Na, Zr) and (Ca, Zr) phosphate-molybdates and phosphate-tungstates: Thermal expansion behavior, radiation test and hydrolytic stability
Thermal expansion behavior at high temperatures of synthesized Na$_{1-x}$Zr$_2$(PO$_4$)$_{3-x}$(XO$_4$)$_x$, and Ca$_{1-x}$Zr$_2$(PO$_4$)$_{3-x}$(XO$_4$)$_x$, X = Mo, W compounds has been investigated. Ceramics with relatively high density (more than 97.5%) were produced by Spark Plasma Sintering (SPS) of submicron powders obtained by sol-gel synthesis. The study of strength characteristics has revealed that hardness the ceramics are greater than 5 GPa, and minimum fracture toughness factor was 1 MPa*m$^{1/2}$. It was found that ceramics have a high hydrolytic resistance in the static regime -- the minimum leaching rates for the Mo- and W-containing specimens were $31\times10^{-6}$ and $3.36\times 10^{-6}$ g/(cm$^2$*day), respectively. The ceramics had a high resistance to the irradiation by Xe$^{+26}$ multiple-charged ions with the energy 167 MeV up to the fluences in the range 1*10$^{12}$ - 6*10$^{13}$ cm$^{-2}$. The Mo-containing Na$_{0.5}$Zr$_2$(PO$_4$)$_{2.5}$(XO$_4$)$_{0.5}$ ceramics were shown to have a higher radiation resistance that the phosphate-tungstates.
2112.00373v1
2021-02-22
High T$_C$ ferromagnetic inverse Heusler alloys: A comparative study of Fe$_2$RhSi and Fe$_2$RhGe
We report the results of experimental investigations on structural, magnetic, resistivity, caloric properties of Fe$_2$RhZ (Z=Si,Ge) along with \textit{ab-initio} band structure calculations using first principle simulations. Both these alloys are found to crystallize in inverse Heusler structure but with disorder in tetrahedral sites between Fe and Rh. Fe$_2$RhSi has saturation moment of 5.00 $\mu_B$ and while its counterpart has 5.19 $\mu_B$. Resistivity measurement reveals metallic nature in both of them. Theoretical simulations using generalized gradient approximation(GGA) predict inverse Heusler structure with ferromagnetic ordering as ground state for both the alloys. However it underestimates the experimentally observed moments. GGA+$U$ approach, with Hubbard $U$ values estimated from density functional perturbation theory helps to improve the comparison of the experimental results. Fe$_2$RhSi is found to be half metallic ferromagnet while Fe$_2$RhGe is not. Varying $U$ values on Fe and Rh sites does not change the net moment much in Fe$_2$RhSi, unlike in Fe$_2$RhGe. Relatively small exchange splitting of orbitals in Fe$_2$RhGe compared to that of Fe$_2$RhSi is the reason for not opening the band gap in the minority spin channel in the former. High ordering temperature and moment make Fe$_2$RhSi useful for spintronics applications.
2102.10967v1
1995-11-10
Contrasting Dynamic Spin Susceptibility Models and their Relation to High Temperature Superconductivity
We compare the normal-state resistivities $\rho$ and the critical temperatures $T_c$ for superconducting $d_{x^2-y^2}$ pairing due to antiferromagnetic (AF) spin fluctuation exchange in the context of the two phenomenological dynamical spin susceptibility models, recently proposed by Millis, Monien, and Pines (MMP) and Monthoux and Pines (MP) and, respectively, by Radtke, Ullah, Levin, and Norman (RULN), for the cuprate high-$T_c$ materials. Assuming comparable electronic bandwidths and resistiviies in both models, we show that the RULN model gives a much lower d-wave $T_c$ ($\lsim20$K) than the MMP model (with $T_c\sim100$K). We demonstrate that these profound differences in the $T_c$'s arise from fundamental differences in the spectral weight distributions of the two model susceptibilities and are {\it{not}} primarily caused by differences in the calculational techniques employed by MP and RULN. The MMP model, claimed to fit NMR data in YBCO, exhibits substantial amounts of spin fluctuation spectral weight up to an imposed cut-off of 400meV, whereas, in the RULN model, claimed to fit YBCO neutron scattering data, the weight is narrowly peaked and effectively cut-off by 100meV. Further neutron scattering experiments, to explore the spectral weight distribution at all wavevectors over a sufficiently large excitation energy range, will thus be of crucial importance to resolve the question whether AF spin fluctuation exchange provides a viable mechanism to account for high-$T_c$ superconductivity. The large high-frequency boson spectral weight, needed to generate both a high d-wave $T_c$ and a low normal-state resistivity, also implies large values, of order unity, for the Migdal smallness parameter, thus casting serious doubt on the validity of the very
9511051v1
2011-11-14
High Field (14Tesla) Magneto Transport of Sm/PrFeAsO
We report high field magneto transport of Sm/PrFeAsO. Below spin density wave transition (TSDW), the magneto-resistance (MR) of Sm/PrFeAsO is positive and increasing with decreasing temperature. The MR of SmFeAsO, is found 16%, whereas the same is 21.5% in case of PrFeAsO, at 2.5 K under applied magnetic field of 14 Tesla (T). In case of SmFeAsO, the variation of isothermal MR with field below 20 K is nonlinear at lower magnetic fields (< 2 Tesla) and the same is linear at moderately higher magnetic fields (H \geq 3.5 T). On the other hand PrFeAsO shows almost linear MR at all temperatures below 20 K. The anomalous behavior of MR being exhibited in PrFeAsO is originated from Dirac cone states. The stronger interplay of Fe and Pr ordered moments is responsible for this distinct behavior. PrFeAsO also shows a hump in resistivity (R-T) with possible conduction band (FeAs) mediated ordering of Pr moments at around 12 K. However the same is absent in SmFeAsO even down to 2 K. Our results of high field magneto-transport of up to 14 Tesla brings about clear distinction between ground states of SmFeAsO and PrFeAsO.
1111.3143v2
2013-02-25
On the specifics of the electrical conductivity anomalies in PVC nanocomposites
A qualitative model describing the "anomalous" features of the conductivity of polymer nanocomposites, in particular, switching to the conducting state in relatively thick (tens of microns or more) of flexible PVC films is considered. In previously published experimental results, change of conductivity by 10 or more orders of magnitude occurred both in the absence of external influences (spontaneously), and under the influence of an applied electric field, as well as other initiating factors (such as uniaxial pressure) . In a model of hopping conduction mechanism it is shown, that switching in the conduction states under the action of external field significantly (by orders of magnitude) below threshold can be associated with a high-resistance state instability that results from the sequence of "shorting" (reversible soft breakdown) of narrow insulating gaps between regions with relatively high conductivity. Increasing the field strength in the remaining insulating gaps ultimately leads to the formation of a conducting channel between the external electrodes and switching conductivity of the composite film sample in a state of high conductivity. This cascade model is essentially based on the transition from the usual description of the charge tunneling through single independent insulating gap to take into account correlations between adjacent gaps. In the frame of developed model other "anomalies" such as exponential dependence of the resistance on the sample thickness, pressure, and other influences can be qualitative explained. An analogy of the model with a cascading breakdown of avalanche transistors is also considered.
1302.5993v1
2016-12-15
The properties of ultrapure delafossite metals
Although they were first synthesized in chemistry laboratories nearly fifty years ago, the physical properties of the metals PdCoO2, PtCoO2 and PdCrO2 have only more recently been studied in detail. The delafossite structure contains triangular co-ordinated atomic layers, and electrical transport in the delafossite metals is strongly two-dimensional. Their most notable feature is their in-plane conductivity, which is amazingly high for oxide metals. At room temperature, the conductivity of non-magnetic PdCoO2 and PtCoO2 is higher per carrier than those of any alkali metal and even the most conductive elements, copper and silver. At low temperatures the best crystals have resistivities of a few n{\Omega}cm, corresponding to mean free paths of tens of microns. PdCrO2 is a frustrated antiferromagnetic metal, with magnetic scattering contributing to the resistivity at high temperatures and small gaps opening in the Fermi surface below the N\'eel temperature. There is good evidence that electronic correlations are weak in the Pd/Pt layers but strong in the Co/Cr layers; indeed the Cr layer in PdCrO2 is thought to be a Mott insulator. The delafossite metals therefore act like natural heterostructures between strongly correlated and nearly free electron sub-systems. Combined with the extremely high conductivity, they provide many opportunities to study electrical transport and other physical properties in new regimes. The purpose of this review is to describe current knowledge of these fascinating materials and set the scene for what is likely to be a considerable amount of future research.
1612.04948v1
2017-10-05
Dual-wavelength Photo-Hall effect spectroscopy of deep levels in high resistive CdZnTe with negative differential photoconductivity
Photo-Hall effect spectroscopy was used in the study of deep levels in high resistive CdZnTe. The monochromator excitation in the photon energy range 0.65-1.77 eV was complemented by a laser diode high-intensity excitation at selected photon energies. A single sample characterized by multiple unusual features like negative differential photoconductivity and anomalous depression of electron mobility was chosen for the detailed study involving measurements at both the steady and dynamic regimes. We revealed that the Hall mobility and photoconductivity can be both enhanced and suppressed by an additional illumination at certain photon energies. The anomalous mobility decrease was explained by an excitation of the inhomogeneously distributed deep level at the energy Ev+1.0 eV enhancing thus potential non-uniformities. The appearance of negative differential photoconductivity was interpreted by an intensified electron occupancy of that level by a direct valence band-to-level excitation. Modified Shockley-Read-Hall theory was used for fitting experimental results by a model comprising five deep levels. Properties of the deep levels and their impact on the device performance were deduced.
1710.01945v1
2020-02-25
Hydrogenated amorphous silicon detectors for particle detection, beam flux monitoring and dosimetry in high-dose radiation environment
Hydrogenated amorphous silicon (a-Si:H) has remarkable radiation resistance properties and can be deposited on a lot of different substrates. A-Si:H based particle detectors have been built since mid 1980s as planar p-i-n or Schottky diode structures; the thickness of these detectors ranged from 1 to 50 micron. However MIP detection using planar structures has always been problematic due to the poor S/N ratio related to the high leakage current at high depletion voltage and the low charge collection efficiency. The usage of 3D detector architecture can be beneficial for the possibility to reduce inter-electrode distance and increase the thickness of the detector for larger charge generation compared to planar structures. Such a detector can be used for future hadron colliders for its radiation resistance and also for X-ray imaging. Furthermore the possibility of a-Si:H deposition on flexible materials (like kapton) can be exploited to build flexible and thin beam flux measurement detectors and x-ray dosimeters.
2002.10848v1
2021-01-29
Wide-range epitaxial strain control of electrical and magnetic properties in high-quality SrRuO3 films
Epitaxial strain in 4d ferromagnet SrRuO3 films is directly linked to the physical properties through the strong coupling between lattices, electrons, and spins. It provides an excellent opportunity to tune the functionalities of SrRuO3 in electronic and spintronic devices. However, a thorough understanding of the epitaxial strain effect in SrRuO3 has remained elusive due to the lack of systematic studies. This study demonstrates wide-range epitaxial strain control of electrical and magnetic properties in high-quality SrRuO3 films. The epitaxial strain was imposed by cubic or pseudocubic perovskite substrates having a lattice mismatch of -1.6 to 2.3% with reference to bulk SrRuO3. The Poisson ratio, which describes the two orthogonal distortions due to the substrate clamping effect, is estimated to be 0.33. The Curie temperature (TC) and residual resistivity ratios of the series of films are higher than or comparable to the highest reported values for SrRuO3 on each substrate, confirming the high crystalline quality of the films. A TC of 169 K is achieved in a tensile-strained SrRuO3 film on the DyScO3 (110) substrate, which is the highest value ever reported for SrRuO3. The TC (146-169 K), magnetic anisotropy (perpendicular or in-plane magnetic easy axis), and metallic conduction (residual resistivity at 2 K of 2.10 - 373 {\mu}{\Omega}cm) of SrRuO3 are widely controlled by epitaxial strain. These results provide guidelines to design SrRuO3-based heterostructures for device applications.
2101.12376v1
2020-05-16
Pressure-induced Topological and Structural Phase Transitions in an Antiferromagnetic Topological Insulator
Recently, natural van der Waals heterostructures of (MnBi2Te4)m(Bi2Te3)n have been theoretically predicted and experimentally shown to host tunable magnetic properties and topologically nontrivial surface states. In this work, we systematically investigate both the structural and electronic responses of MnBi2Te4 and MnBi4Te7 to external pressure. In addition to the suppression of antiferromagnetic order, MnBi2Te4 is found to undergo a metal-semiconductor-metal transition upon compression. The resistivity of MnBi4Te7 changes dramatically under high pressure and a non-monotonic evolution of \r{ho}(T) is observed. The nontrivial topology is proved to persists before the structural phase transition observed in the high-pressure regime. We find that the bulk and surface states respond differently to pressure, which is consistent with the non-monotonic change of the resistivity. Interestingly, a pressure-induced amorphous state is observed in MnBi2Te4, while two high pressure phase transitions are revealed in MnBi4Te7. Our combined theoretical and experimental research establishes MnBi2Te4 and MnBi4Te7 as highly tunable magnetic topological insulators, in which phase transitions and new ground states emerge upon compression.
2005.08015v1
2020-08-03
Solute hydrogen and deuterium observed at the near atomic scale in high-strength steel
Observing solute hydrogen (H) in matter is a formidable challenge, yet, enabling quantitative imaging of H at the atomic-scale is critical to understand its deleterious influence on the mechanical strength of many metallic alloys that has resulted in many catastrophic failures of engineering parts and structures. Here, we report on the APT analysis of hydrogen (H) and deuterium (D) within the nanostructure of an ultra-high strength steel with high resistance to hydrogen embrittlement. Cold drawn, severely deformed pearlitic steel wires (Fe-0.98C-0.31Mn-0.20Si-0.20Cr-0.01Cu-0.006P-0.007S wt.%, {\epsilon}=3.1) contains cementite decomposed during the pre-deformation of the alloy and ferrite. We find H and D within the decomposed cementite, and at some interfaces with the surrounding ferrite. To ascertain the origin of the H/D signal obtained in APT, we explored a series of experimental workflows including cryogenic specimen preparation and cryogenic-vacuum transfer from the preparation into a state-of-the-art atom probe. Our study points to the critical role of the preparation, i.e. the possible saturation of H-trapping sites during electrochemical polishing, how these can be alleviated by the use of an outgassing treatment, cryogenic preparation and transfer prior to charging. Accommodation of large amounts of H in the under-stoichiometric carbide likely explains the resistance of pearlite against hydrogen embrittlement.
2008.00684v1
2021-07-01
Singular angular magnetoresistance and sharp resonant features in a high-mobility metal with open orbits, ReO3
We report high-resolution angular magnetoresistance (AMR) experiments performed on crystals of ReO$_3$ with high mobility (90,000 cm$^2$/Vs at 2 K) and extremely low residual resistivity (5-8 n$\Omega$cm). The Fermi surface, comprised of intersecting cylinders, supports open orbits. The resistivity $\rho_{xx}$ in a magnetic field $B$ = 9 T displays a singular pattern of behavior. With $\bf E\parallel \hat{x}$ and $\bf B$ initially $\parallel\bf\hat{z}$, tilting $\bf B$ in the longitudinal $k_z$-$k_x$ plane leads to a steep decrease in $\rho_{xx}$ by a factor of 40. However, if $\bf B$ is tilted in the transverse $k_y$-$k_z$ plane, $\rho_{xx}$ increases steeply by a factor of 8. Using the Shockley tube integral approach, we show that, in ReO$_3$, the singular behavior results from the rapid conversion of closed to open orbits, resulting in opposite signs for AMR in orthogonal planes. The floor values of $\rho_{xx}$ in both AMR scans are identified with specific sets of open and closed orbits. Also, the "completion angle" $\gamma_c$ detected in the AMR is shown to be an intrinsic geometric feature that provides a new way to measure the Fermi radius $k_F$. However, additional sharp resonant features which appear at very small tilt angles in the longitudinal AMR scans are not explained by the tube integral approach.
2107.00742v1
2021-07-07
Development and validation of electrical-insulating Al2O3 coatings for high-temperature liquid PbLi applications
Electrical-insulating coatings are of great importance for liquid-metal breeder/coolant based systems relevant to fusion power plants. In specific to Pb-16Li eutectic, a candidate breeder material, such coatings are being actively investigated for their criticality in addressing various functionalities. For such applications, a candidate coating must be demonstrated for its compatibility with corrosive media, high operational temperatures and integrity of electrical-insulation over long durations without substantial degradation. At present, no relevant in-situ insulation resistance (IR) data is available for performance assessment of coated substrates within PbLi environment. To address this shortfall, an experimental study was performed at IPR towards application of high-purity alumina coatings on SS-316L substrates and further rigorous validation in static PbLi environment. The adopted coating process required a low-temperature heat treatment (< 430C) and could yield average coating thicknesses in the range of 100-500 micron. Coated samples were validated for their electrical insulation integrity in static PbLi over two test campaigns for continuous durations of over 700 h and 1360 h, including thermal cycling, at operational temperature between 300C-400C. Estimated volumetric electrical-resistivity remained of the order of 109-1011 ohm-cm without significant degradation. In-situ estimations of thermal derating factors establish excellent electrical-insulation characteristics after long term exposure to liquid PbLi. This paper presents details of utilized coating application methods, coating thickness estimations, liquid-metal test set-up, insulation performance and critical observations from SEM/EDX and XRD analysis on the tested samples.
2107.03244v1
2021-09-26
Tomographic Volumetric Additive Manufacturing of Silicon Oxycarbide Ceramics
Ceramics are highly technical materials with properties of interest for multiple industries. Precisely because of their high chemical, thermal, and mechanical resistance, ceramics are difficult to mold into complex shapes. A possibility to make convoluted ceramic parts is to use preceramic polymers (PCP) in liquid form. The PCP resin is first solidified in a desired geometry and then transformed into ceramic compounds through a pyrolysis step that preserves the shape. Light-based additive manufacturing (AM) is a promising route to achieve solidification of the PCP resin. Different approaches, such as stereolithography, have already been proposed but they all rely on a layer-by-layer printing process which sets limitations on the printing speed and object geometry. Here, we report on the fabrication of complex 3D centimeter-scale ceramic parts by using tomographic volumetric printing which is fast, high resolution and offers a lot of freedom in terms of geometrical design compared to state-of-the-art AM techniques. First, we formulated a photosensitive preceramic resin that was solidified by projecting light patterns from multiple angles. Then, the obtained 3D printed parts were converted into ceramics by pyrolyzing them in a furnace. We demonstrate the strength of this approach through the fabrication of dense microcomponents exhibiting overhangs and hollow geometries without the need of supporting structures, and characterize their resistance to high heat and harsh chemical treatments.
2109.12680v1
2022-11-16
Characterisation of Gamma-irradiated MCz-Silicon Detectors with a High-$K$ Negative Oxide as Field Insulator
The high-luminosity operation of the Tracker in the Compact Muon Solenid (CMS) detector at the Large Hadron Collider (LHC) experiment calls for the development of silicon-based sensors. This involves implementation of AC-coupling to micro-scale pixel sensor areas to provide enhanced isolation of radiation-induced leakage currents. The motivation of this study is the development of AC-pixel sensors with negative oxides (such as aluminium oxide - Al$_2$O$_3$ and hafnium oxide - HfO$_2$) as field insulators that possess good dielectric strength and provide radiation hardness. Thin films of Al$_2$O$_3$ and HfO$_2$ grown by atomic layer deposition (ALD) method were used as dielectrics for capacitive coupling. A comparison study based on dielectric material used in MOS capacitors indicate HfO$_2$ as a better candidate since it provides higher sensitivity (where, the term sensitivity is defined as the ratio of the change in flat-band voltage to dose) to negative charge accumulation with gamma irradiation. Further, space charge sign inversion was observed for sensors processed on high resistivity p-type Magnetic Czochralski silicon (MCz-Si) substrates that were irradiated with gamma rays up to a dose of 1 MGy. The inter-pixel resistance values of heavily gamma irradiated AC-coupled pixel sensors suggest that high-$K$ negative oxides as field insulators provide a good electrical isolation between the pixels.
2211.09158v2
2023-07-12
Extrinsic Anomalous Hall effect in Mn Doped GeSnTe Semiconductors in the Bad Metal Hopping Regime
We present high field magnetotransport studies of Ge1-x-y(SnxMny)Te bulk multiferroics with diamagnetic Sn and paramagnetic Mn concentration x = 0.38 to 0.79 and y = 0.02 to 0.086, respectively. The zero field resistivity, {\rho}(T) takes significant contribution from defects below T = 20 K however, a mixed scattering contribution from dynamic disorder and unusual sources is estimated from T = 20 K to 300 K. The carrier mobility shows anomalous temperature dependence from T0.2 to T0.5 which hints towards possible presence of polaronic effects resulting from coupling of holes with phonons. This anomalous behavior cannot be understood in terms of pure phononic scattering mechanism at high temperature. From point of view of high field results, the transverse component of magnetoresistivity manifests anomalous Hall effect originating from extrinsic scattering sources, particularly the side jump mechanism reveals a larger contribution. We also find that the correlation between the transverse and longitudinal conductivities follow the universal scaling law {\sigma}xy ~ {\sigma}xxn where n = 1.6 in the low conductivity limit. The values n = 1.5 to 1.8 obtained for the present GSMT alloys justify the bad metal hopping regime since the results fall in the low conductivity ferromagnetic family with {\sigma}xx ~ 104 ohmcm-1. The interpretation of the n = 1.6 scaling in the low conductivity regime is thus far not fully understood. However, the anomalous Hall resistivity scaling with modified relation by Tian et al is indicative of the dominant side jump scattering along with noticeable role of skew scattering.
2307.06271v1
2012-10-07
Tailoring Magnetism of Perpendicularly Magnetized MnxGa Epitaxial Films on GaAs for Practical Applications
MnxGa films with high perpendicular anisotropy, coercivity and energy product have great application potential in ultrahigh-density perpendicular recording, permanent magnets, spin-transfer-torque memory and oscillators, magneto-resistance sensors and ferromagnetic metal/semiconductor heterostructure devices. Here we present a comprehensive diagram of effective magnetism-tailoring of perpendicularly magnetized MnxGa films grown on III-V semiconductor GaAs by using molecular-beam epitaxy for the first time, by systematically investigating the wide-range composition and detailed post-growth annealing effects. We show that the (001)-orientated MnxGa films with L10 or D022 ordering could be crystallized on GaAs in a very wide composition range from x=0.76 to 2.6. L10-ordered MnxGa films show robust magnetization, high remanent ratio, giant perpendicular anisotropy, high intrinsic and extrinsic coercivity, and large energy product, which make this kind of material favorable for perpendicular magnetic recording, high-performance spintronic devices and permanent magnet applications. In contrast, D022-ordered films exhibit lower perpendicular anisotropy and weaker magnetism. Post-growth annealing MnxGa films studies reveal high thermal-stability up to 450 oC, and effective tailoring of magnetic properties can be realized by prolonging annealing at 450 oC. These results would be helpful for understanding this kind of material and designing new spintronic devices for specific practical applications.
1210.2062v3
2012-11-14
The Critical Current Density of an SNS Josephson-Junction
The critical current density (Jc) through a superconductor in high magnetic fields is controlled by the inclusions and microstructure of the material that hold fluxons stationary to keep the resistance zero and is described using Ginzburg-Landau (G-L) theory. Although the functional form of Jc for superconducting-normal-superconducting (SNS) Josephson-Junctions (J-Js) is known in the low field limit, includes the local properties of the junctions and has been confirmed experimentally in many systems, there are no general solutions for Jc of J-Js in high fields. Scaling laws describe the functional form (magnetic field, temperature and strain dependence) of Jc for polycrystalline superconductors in high fields but do not include local grain boundary properties. They are derived by considering isolated pinning sites where at criticality fluxons either depin or free fluxons shear past pinned fluxons as part of the flux line lattice. However, visualisation of solutions to the Time Dependent Ginzburg-Landau (TDGL) equations for polycrystalline materials have shown that fluxons cross the superconductor by flowing along the grain boundaries. Here we derive clean- and dirty- limit analytic equations for of SNS J-Js in high fields and verify them using computational solutions to TDGL theory. We consider SNS J-Js to be the basic building blocks for grain boundaries in polycrystalline materials since they provide flux-flow channels. The J-Js description provides a mathematical framework that includes the utility of scaling laws together with our microscopic understanding of barriers to supercurrent flow and helps identify the grain boundary engineering that can improve in low temperature polycrystalline superconductors used in high magnetic field applications.
1211.3255v2
2013-09-08
Nanoscale resolution scanning thermal microscopy with thermally conductive nanowire probes
Scanning thermal microscopy (SThM) - a type of scanning probe microscopy that allows mapping thermal transport and temperatures in nanoscale devices, is becoming a key approach that may help to resolve heat dissipation problems in modern processors and develop new thermoelectric materials. Unfortunately, performance of current SThM implementations in measurement of high thermal conductivity materials continues to me limited. The reason for these limitations is two-fold - first, SThM measurements of high thermal conductivity materials need adequate high thermal conductivity of the probe apex, and secondly, the quality of thermal contact between the probe and the sample becomes strongly affected by the nanoscale surface corrugations of the studied sample. In this paper we develop analytical models of the SThM approach that can tackle these complex problems - by exploring high thermal conductivity nanowires as a tip apex, and exploring contact resistance between the SThM probe and studied surface, the latter becoming particularly important when both tip and surface have high thermal conductivities. We develop analytical model supported by the finite element analysis simulations and by the experimental tests of SThM prototype using carbon nanotube (CNT) at the tip apex as a heat conducting nanowire. These results elucidate vital relationships between the performance of the probe in SThM from one side and thermal conductivity, geometry of the probe and its components from the other, providing pathway for overcoming current limitations of SThM.
1309.2010v1
2019-09-13
Electric field and current induced electroforming modes in NbOx
Electroforming is used to initiate the memristive response in metal/oxide/metal devices by creating a filamentary conduction path in the oxide film. Here we use a simple photoresist-based detection technique to map the spatial distribution of conductive filaments formed in Nb/NbOx/Pt devices, and correlate these with current-voltage characteristics and in-situ thermoreflectance measurements to identify distinct modes of electroforming in low and high conductivity NbOx films. In low conductivity films the filaments are randomly distributed within the oxide film, consistent with a field-induced weakest-link mechanism, while in high conductivity films they are concentrated in the center of the film. In the latter case the current-voltage characteristics and in-situ thermoreflectance imaging show that electroforming is associated with current bifurcation into regions of low and high current density. This is supported by finite element modelling of the current distribution and shown to be consistent with predictions of a simple core-shell model of the current distribution. These results clearly demonstrate two distinct modes of electroforming in the same materials system and show that the dominant mode depends on the conductivity of the film, with field-induced electroforming dominant in low conductivity films and current-bifurcation induced electroforming dominant in high conductivity films. Finally, we demonstrate S-type and snap-back negative differential resistance in the high conductivity films and explain this behavior in terms of two-zone model.
1909.06443v2
2000-05-25
Critical Resistivity along the Quantum Hall Liquid--Insulator Transition Line
The critical resistivity measured along the quantum Hall liquid--insulator transition line indicates a pronounced peak at a critical filling factor close to 1, which marks the crossover from the high to low magnetic field regime in the phase diagram. The origin of this behavior is explained in the framework of classical transport in a puddle network model. The proposed scenario is also consistent with the behavior of the critical Hall resistance along the transition line. In addition, a formula is suggested as a fit for isotherms ($\rho_{xx}$ vs. $\nu$) in the moderately high field regime, which exhibits a violation of duality symmetry as the critical resistivity is evelated from the `universal' value $h/e^2$.
0005436v1