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2022-04-26
Nonreciprocal electrical transport in multiferroic semiconductor (Ge,Mn)Te
We have investigated the nonreciprocal electrical transport, that is a nonlinear resistance effect depending on the current direction, in multiferroic Rashba semiconductor (Ge,Mn)Te. Due to coexistence of ferromagnetic and ferroelectric orders, (Ge,Mn)Te provides a unique platform for exploring the nonreciprocal electrical transport in a bulk form. (Ge,Mn)Te thin films shows a large nonreciprocal resistance compared to GeTe, the nonmagnetic counterpart with the same crystal structure. The magnetic-field-angle dependence of the nonreciprocal resistance is maximized when magnetic field is orthogonal to both current and electric polarization, in accord with the symmetry argument. From the analysis of temperature and magnetic field dependence, we deduce that inelastic scatterings of electrons mediated by magnons dominantly contribute to the observed nonreciprocal response. Furthermore, the nonreciprocal resistance is significantly enhanced by lowering hole density. The Fermi level dependence is attributed to the deformation of the Rashba band in which the spin-momentum locked single Fermi surface appears by exchange field from the in-plane magnetization. The present study provides a key insight to the mechanisms of novel transport phenomena caused by the interplay of ferroelectric and ferromagnetic orders in a semiconductor.
2204.12427v1
2022-08-17
Transport properties of dipole skyrmions in amorphous FeGd multilayers
The transport response of dipole skyrmions in amorphous centrosymmetric Fe/Gd multilayer is investigated by temperature and field-dependent resistivity measurements collected in three current and magnetic field configurations. It is shown that a dipole skyrmion lattice phase may form at certain temperatures leading to a unique signature of the polar longitudinal resistivity. This signature differs from the conventional field-varying parabolic response associated with stripe phases, which transition to a disordered skyrmion phase under applied fields. Transport measurements under different field history protocols reveal that the anomaly in the polar longitudinal resistivity appears under specific field history reversal processes. Our experimental results are reproduced using micromagnetic simulations that show the anomaly in the polar longitudinal resistivity is related to a domain wall reconfiguration that occurs as the domain morphology transitions from disordered stripes to a skyrmion lattice under applied perpendicular fields.
2208.08487v1
2023-01-18
Synthesizing $2h/e^2$ resistance plateau at the first Landau level confined in a quantum point contact
A comprehensive understanding of quantum Hall edge transmission, especially the hole-conjugate of a Laughlin state such as a $2/3$ state, is critical for advancing fundamental quantum Hall physics and enhancing the design of quantum Hall edge interferometry. In this study, we report a robust intermediate $2h/e^2$ resistance quantization in a quantum point contact (QPC) when the bulk is set at the fractional filling $2/3$ quantum Hall state. Our results suggest the occurrence of two equilibration processes. First, the co-propagating $1/3$ edges moving along a soft QPC arm confining potential fully equilibrate and act as a single $2/3$ edge mode. Second, the $2/3$ edge mode is further equilibrated with an integer $1$ edge mode formed in the QPC. The complete mixing between them results in a diagonal resistance value quantized at $2h/e^2$. Similar processes occur for a bulk filling $5/3$, leading to an intermediate $(2/3)h/e^2$ resistance quantization.
2301.07488v2
2024-02-28
Impact of etches on thin-film single-crystal niobium resonators
A single crystal niobium thin film was grown using molecular beam epitaxy on a c-plane sapphire wafer. Several samples were fabricated into dc resistivity test devices and coplanar waveguide resonator chips using the same microfabrication procedures and solvent cleans. The samples were then subject to different acid cleaning treatments using different combinations of piranha, hydrofluoric acid, and buffered oxide etch solutions. The different samples expressed changes in dc resistivity in the normal and superconducting states such that the low temperature resistivities changed by more than 100\%, and the residual resistivity ratio dropped by a factor of 2. The internal quality factor of coplanar waveguide resonators measured near 5~GHz also showed significant variation at single photon powers ranging from 1.4$\times 10^6$ to less than 60$\times 10^3$. These changes correlate with the formation of surface crystallites that appear to be hydrocarbons. All observations are consistent with hydrogen diffusing into the niobium film at levels below the saturation threshold that is needed to observe niobium hydrides.
2402.18051v1
2024-05-02
Optimization of reactively sputtered Mn3GaN films based on resistivity measurements
Mn-based nitrides with antiperovskite structures have several properties that can be utilised for antiferromagnetic spintronics. Their magnetic properties depend on the structural quality, composition and doping of the cubic antiperovskite structure. Such nitride thin films are usually produced by reactive physical vapour deposition, where the deposition rate of N can only be controlled by the N2 gas flow. We show that the tuning of the N content can be optimised using low temperature resistivity measurements, which serve as an indicator of the degree of structural disorder. Several Mn3GaNx films were prepared by reactive magnetron sputtering under different N2 gas flows. Under optimised conditions, we obtain films that exhibit a metal-like temperature dependence, a vanishing logarithmic increase in resistivity towards zero, the highest resistivity ratio and a lattice contraction of 0.4 % along the growth direction when heated above that of the N\'eel temperature in agreement with the bulk samples.
2405.01203v1
2004-02-04
A simple estimate of the electron hopping energy in the Bechgaard salts
Starting from a previously derived theoretical expression for the electrical conductivity of the Bechgaard salts,and experimental data on the resistivity of these materials,it is shown how a valueof the electron hopping energy can be determined.Values obtained in this way are in agreement with estimates made by more complicated methods.
0402127v1
2019-09-12
Gallium Nitride FET Model
We have presented an analytical physics-based compact model of GaN power FET, which can accurately describe the I-V characteristics in all operation modes. The model considers the source-drain resistance, different interface trap densities and self-heating effects.
1909.05702v1
2019-09-18
A current-voltage characteristic of photoresistance. A plane case
The formation of photo-electron current in the volume of semi-conductor material is investigated in this article. A plane case when a material is uniformly illuminated by light is considered. The current-voltage characteristic of a photo resistance is obtained in analytical form.
1909.09135v1
2019-10-04
The Test of Topological Property of YbB6
Topological insulator is a recently discovered class of material with topologically protected surface state. YbB6 is predicted to be moderately correlated Z2 topological insulator similar to SmB6. Here, I experimentally test the resistance property of bulk YbB6 to verify its topological property. By changing the thickness of YbB6, I found out that although the data curves did not completely conform to the theory of topology, the experimental observation to the overall trend showed a similar topological phenomenon.
1910.02056v1
2020-01-25
Exfoliation of Two-Dimensional Nanosheets of Metal Diborides
The metal diborides are a class of ceramic materials with crystal structures consisting of hexagonal sheets of boron atoms alternating with planes of metal atoms held together with mixed character ionic/covalent bonds. Many of the metal diborides are ultrahigh temperature ceramics like HfB$_2$, TaB$_2$, and ZrB$_2$, which have melting points above 3000$^\circ$C, high mechanical hardness and strength at high temperatures, and high chemical resistance, while MgB$_2$ is a superconductor with a transition temperature of 39 K. Here we demonstrate that this diverse family of non-van der Waals materials can be processed into stable dispersions of two-dimensional (2D) nanosheets using ultrasonication-assisted exfoliation. We generate 2D nanosheets of the metal diborides AlB$_2$, CrB$_2$, HfB$_2$, MgB$_2$, NbB$_2$, TaB$_2$, TiB$_2$, and ZrB$_2$, and use electron and scanning probe microscopies to characterize their structures, morphologies, and compositions. The exfoliated layers span up to micrometers in lateral dimension and reach thicknesses down to 2-3 nm, while retaining their hexagonal atomic structure and chemical composition. We exploit the convenient solution-phase dispersions of exfoliated CrB$_2$ nanosheets to incorporate them directly into polymer composites. In contrast to the hard and brittle bulk CrB$_2$, we find that CrB$_2$ nanocomposites remain very flexible and simultaneously provide increases in the elastic modulus and the ultimate tensile strength of the polymer. The successful liquid-phase production of 2D metal diborides enables their processing using scalable low-temperature solution-phase methods, extending their use to previously unexplored applications, and reveals a new family of non-van der Waals materials that can be efficiently exfoliated into 2D forms.
2001.09237v1
2005-10-07
Collective Spin and Charge Excitations in (Sr,La)_{14-x}Ca_xCu_{24}O_{41} Quantum Spin Ladders
We study magnetic and electronic properties of two-leg ladder materials. We observed a two-magnon (2M) resonance which we analyze in terms of symmetry, relaxation and resonance properties. Our findings were contrasted to 2M Raman measurements in other magnetic crystals. This comparison made us suggest that the spin-spin correlations in a self-doped two leg ladder may have a modulated component besides the exponential decay characteristic of a spin liquid ground state. We found that the 2M intensity resonates at the Mott gap energy. Interplane Sr substitution for Ca introduces strong disorder leading to inhomogeneous broadening of the 2M resonance. The doped holes in the spin liquid ground state further dilute the magnetic correlations, suppressing the spectral weight of this excitation. At high Ca concentrations are superconducting under pressure and hole pairing was proposed to be a robust feature of doped ladders. The measured dielectric response in the microwave region, the low energy Raman data, the non-linear transport properties along with soft x-ray scattering allowed us to conclude that the ground state for a wide range of Ca concentrations (x < 12) is characterized by charge density wave correlations. This state seems to be driven not by phonons but by Coulomb forces and many-body effects. We highlighted the similarity in the finite frequency Raman response as opposed to the very different behavior of the DC resistivity between undoped and doped ladders. We found that at high Ca concentrations the carrier relaxation is characterized by the same large activation energy (~2000 K) as in the self-doped compound. This observation prompted us to suggest an unconventional metallic transport driven by collective electronic response.
0510193v1
2009-02-13
Nanoscale Electronic Inhomogeneity in In2Se3 Nanoribbons Revealed by Microwave Impedance Microscopy
Driven by interactions due to the charge, spin, orbital, and lattice degrees of freedom, nanoscale inhomogeneity has emerged as a new theme for materials with novel properties near multiphase boundaries. As vividly demonstrated in complex metal oxides and chalcogenides, these microscopic phases are of great scientific and technological importance for research in high-temperature superconductors, colossal magnetoresistance effect, phase-change memories, and domain switching operations. Direct imaging on dielectric properties of these local phases, however, presents a big challenge for existing scanning probe techniques. Here, we report the observation of electronic inhomogeneity in indium selenide (In2Se3) nanoribbons by near-field scanning microwave impedance microscopy. Multiple phases with local resistivity spanning six orders of magnitude are identified as the coexistence of superlattice, simple hexagonal lattice and amorphous structures with 100nm inhomogeneous length scale, consistent with high-resolution transmission electron microscope studies. The atomic-force-microscope-compatible microwave probe is able to perform quantitative sub-surface electronic study in a noninvasive manner. Finally, the phase change memory function in In2Se3 nanoribbon devices can be locally recorded with big signal of opposite signs.
0902.2255v1
2009-10-01
Template engineering of Co-doped BaFe2As2 single-crystal thin films
Understanding new superconductors requires high-quality epitaxial thin films to explore intrinsic electromagnetic properties, control grain boundaries and strain effects, and evaluate device applications. So far superconducting properties of ferropnictide thin films appear compromised by imperfect epitaxial growth and poor connectivity of the superconducting phase. Here we report novel template engineering using single-crystal intermediate layers of (001) SrTiO3 and BaTiO3 grown on various perovskite substrates that enables genuine epitaxial films of Co-doped BaFe2As2 with high transition temperature (zero resistivity Tc of 21.5K), small transition widths (delta Tc = 1.3K), superior Jc of 4.5 MA/cm2 (4.2K, self field) and strong c-axis flux pinning. Implementing SrTiO3 or BaTiO3 templates to match the alkaline earth layer in the Ba-122 with the alkaline earth-oxygen layer in the templates opens new avenues for epitaxial growth of ferropnictides on multi-functional single crystal substrates. Beyond superconductors, it provides a framework for growing heteroepitaxial intermetallic compounds on various substrates by matching interfacial layers between templates and thin film overlayers.
0910.0268v1
2009-11-19
Large transport critical currents of powder-in-tube Sr0.6K0.4Fe2As2/Ag superconducting wires and tapes
We report significant transport critical currents firstly achieved in Sr0.6K0.4Fe2As2 wires and tapes with a Tc = 34 K, which were fabricated through an in-situ powder-in-tube process. Silver was used as a chemical addition as well as a sheath material. Transport measurements were performed by a standard four-probe resistive method. All the wire and tape samples have shown transport properties. Critical current density Jc was enhanced upon silver addition, and at 4.2 K, a best Jc of ~1200 A/cm^2 (Ic = 9 A) was achieved for 20 % silver added tapes, which is the highest in iron-based wires and tapes so far. The Jc is almost field independent between 1 T and 10 T, exhibiting a strong vortex pinning. Such a high transport critical current density is attributed to the absence of reaction layer between the silver sheath and superconducting core, as well as an improved connectivity between grains. We also identify a weak-link behavior from the creep drop of Jc at low fields and a hysteretic phenomenon. Finally, we found that compared to Fe, Ta and Nb tubes, Ag was the best sheath material for the fabrication of high-performance 122 type pnictide wires and tapes.
0911.3701v1
2010-10-05
Hierarchical formation of bulgeless galaxies: Why outflows have low angular momentum
Using high resolution, fully cosmological smoothed particle hydro-dynamical simulations of dwarf galaxies in a Lambda cold dark matter Universe, we show how baryons attain a final angular momentum distribution which allows pure disc galaxies to form. Blowing out substantial amounts of gas through supernovae and stellar winds, which is well supported observationally, is a key ingredient in forming bulgeless discs. We outline why galactic outflows preferentially remove low angular momentum material, and show that this is a natural result when structure forms in a cold dark matter cosmology. The driving factors are a) the mean angular momentum of accreted material increases with time, b) lower potentials at early times, c) the existence of an extended reservoir of high angular momentum gas which is not within star forming regions, meaning that only gas from the inner region (low angular momentum gas) is expelled and d) the tendency for outflows to follow the path of least resistance which is perpendicular to the disc. We also show that outflows are enhanced during mergers, thus expelling much of the gas which has lost its angular momentum during these events, and preventing the formation of "classical", merger driven bulges in low mass systems. Stars formed prior to such mergers form a diffuse, extended stellar halo component.
1010.1004v3
2014-02-13
On the spheroidized carbide dissolution and elemental partitioning in a high carbon bearing steel 100Cr6
We report on the characterization of high carbon bearing steel 100Cr6 using electron microscopy and atom probe tomography in combination with multi-component diffusion simulations (DICTRA). Scanning electron micrographs show that around 14 vol.% spheroidized carbides are formed during soft annealing and only 3 vol.% remain after dissolution into the austenitic matrix by austenitization at 1123 K (850 {\deg}C) for 300 s. The spheroidized particles are identified as (Fe, Cr)3C by transmission electron microscopy. Atom probe analyses reveal the redistribution and partitioning behaviors of elements, i.e. C, Si, Mn, Cr, Fe in both, the spheroidized carbides and the bainitic matrix in the sample isothermally heat-treated at 773 K (500 {\deg}C) after austenitization. A homogeneous distribution of C and gradual gradient of Cr was detected within the spheroidized carbides. Due to its limited diffusivity in (Fe, Cr)3C, Cr exhibits a maximum concentration at the surface of spheroidized carbides (16 at.%) and decreases gradually from surface towards the core down to a level of about 2 at.%. The atom probe results also indicate that the partially dissolved spheroidized carbides during austenitization may serve as nucleation sites for intermediate temperature cementite within bainite, which results in a relatively softer surface and harder core in spheroidized particles. This microstructure may contribute to the good wear resistance and fatigue properties
1402.3315v1
2014-05-23
Proof-of-principle of a new geometry for sampling calorimetry using inorganic scintillator plates
A novel geometry for a sampling calorimeter employing inorganic scintillators as an active medium is presented. To overcome the mechanical challenges of construction, an innovative light collection geometry has been pioneered, that minimises the complexity of construction. First test results are presented, demonstrating a successful signal extraction. The geometry consists of a sampling calorimeter with passive absorber layers interleaved with layers of an active medium made of inorganic scintillating crystals. Wavelength-shifting (WLS) fibres run along the four long, chamfered edges of the stack, transporting the light to photodetectors at the rear. To maximise the amount of scintillation light reaching the WLS fibres, the scintillator chamfers are depolished. It is shown herein that this concept is working for cerium fluoride (CeF$_3$) as a scintillator. Coupled to it, several different types of materials have been tested as WLS medium. In particular, materials that might be sufficiently resistant to the High-Luminosity Large Hadron Collider radiation environment, such as cerium-doped Lutetium-Yttrium Orthosilicate (LYSO) and cerium-doped quartz, are compared to conventional plastic WLS fibres. Finally, an outlook is presented on the possible optimisation of the different components, and the construction and commissioning of a full calorimeter cell prototype is presented.
1405.6202v1
2015-02-10
Emergence of the minority hole with high mobility on the electrical transport in the Fe-pnictides Ba(Fe$_{1-x}$Mn$_x$As)$_2$
In Fe pnictide (Pn) superconducting materials, neither Mn- nor Cr- doping to the Fe site induces superconductivity, even though hole carriers are generated. This is in strong contrast with the superconductivity appearing when holes are introduced by alkali metal substitution on the insulating blocking layers. We investigate in detail the effects of Mn doping on magneto-transport properties in Ba(Fe$_{1-x}$Mn$_x$As)$_2$ for elucidating the intrinsic reason. The negative Hall coefficient for $x$ = 0 estimated in the low magnetic field ($B$) regime gradually increases as $x$ increases, and its sign changes to a positive one at $x$ = 0.020. Hall resistivities as well as simultaneous interpretation using the magnetoconductivity tensor including both longitudinal and transverse transport components clarify that minority holes with high mobility are generated by the Mn doping via spin density wave (SDW) transition at low temperatures, while original majority electrons and holes residing in the parabolic-like Fermi surfaces (FSs) of the semimetallic Ba(FeAs)$_2$ are negligibly affected. Present results indicate that the mechanism of hole doping in Ba(Fe$_{1-x}$Mn$_x$As)$_2$ is greatly different from that of the other superconducting FePns family.
1502.02845v3
2015-08-16
Surface States Engineering of Metal/MoS2 Contacts Using Sulfur Treatment for Reduced Contact Resistance and Variability
Variability and lack of control in the nature of contacts between metal/MoS2 interface is a major bottleneck in the realisation of high-performance devices based on layered materials for several applications. In this letter, we report on the reduction in Schottky barrier height at metal/MoS2 interface by engineering the surface states through sulphur treatment. Electrical characteristics for back-gated MoS2 field effect transistor structures were investigated for two high work-function metal contacts Ni and Pd. Contacts on MoS2 treated with sulphur exhibited significant improvements in Ohmic nature with concomitant reduction in variability compared to those on untreated MoS2 films leading to a 2x increase in extracted mobility. X-ray Photoelectron Spectroscopy (XPS) measurements, Raman Spectroscopy and comparison of threshold voltages indicated absence of additional doping or structural changes due to sulphur treatment. The Schottky barrier heights were extracted from temperature-dependent transfer characteristics based on the thermionic current model. A reduction in barrier height of 80 and 135 meV extracted for Ni/MoS2 and Pd/MoS2 contacts respectively is hence attributed to the increase in surface states (or stronger Fermi level pinning) due to sulphur treatment. The corresponding charge neutrality levels at metal/MoS2 interface, were extracted to be 0.16 eV (0.17 eV) below the conduction band before (after) Sulphur treatment. This first report of surface states engineering in MoS2 leading to superior contacts is expected to significantly benefit the entire class of devices based on layered 2D materials.
1508.03795v2
2016-06-28
Method for Transferring High-Mobility CVD-Grown Graphene with Perfluoropolymers
The transfer of graphene grown by chemical vapor deposition (CVD) using amorphous polymers represents a widely implemented method for graphene-based electronic device fabrication. However, the most commonly used polymer, poly(methyl methacrylate) (PMMA), leaves a residue on the graphene that limits the mobility. Here we report a method for graphene transfer and patterning that employs a perfluoropolymer---Hyflon---as a transfer handle and to protect graphene against contamination from photoresists or other polymers. CVD-grown graphene transferred this way onto LaAlO$_3$/SrTiO$_3$ heterostructures is atomically clean, with high mobility (~30,000 cm$^2$V$^{-1}$s$^{-1}$) near the Dirac point at 2 K and clear, quantized Hall and magneto-resistance. Local control of the LaAlO$_3$/SrTiO$_3$ interfacial metal-insulator transition---through the graphene---is preserved with this transfer method. The use of perfluoropolymers such as Hyflon with CVD-grown graphene and other 2D materials can readily be implemented with other polymers or photoresists.
1606.08802v1
2016-10-31
High Electric Field Carrier Transport and Power Dissipation in Multilayer Black Phosphorus Field Effect Transistor with Dielectric Engineering
This study addresses high electric field transport in multilayer black phosphorus (BP) field effect transistors (FETs) with self-heating and thermal spreading by dielectric engineering. Interestingly, we found that multilayer BP device on a SiO2 substrate exhibited a maximum current density of 3.3 x 10E10 A/m2 at an electric field of 5.58 MV/m, several times higher than multilayer MoS2. Our breakdown thermometry analysis revealed that self-heating was impeded along BP-dielectric interface, resulting in a thermal plateau inside the channel and eventual Joule breakdown. Using a size-dependent electro-thermal transport model, we extracted an interfacial thermal conductance of 1-10 MW/m2 K for the BP-dielectric interfaces. By using hBN as a dielectric material for BP instead of thermally resistive SiO2 (about 1.4 W/m K), we observed a 3 fold increase in breakdown power density and a relatively higher electric field endurance together with efficient and homogenous thermal spreading because hBN had superior structural and thermal compatibility with BP. We further confirmed our results based on micro-Raman spectroscopy and atomic force microscopy, and observed that BP devices on hBN exhibited centrally localized hotspots with a breakdown temperature of 600K, while the BP device on SiO2 exhibited a hotspot in the vicinity of the electrode at 520K.
1610.09951v1
2017-02-02
High-Pressure Synthesis and Characterization of $β$-GeSe - A Semiconductor with Six-Rings in an Uncommon Boat Conformation
Two-dimensional materials have significant potential for the development of new devices. Here we report the electronic and structural properties of $\beta$-GeSe, a previously unreported polymorph of GeSe, with a unique crystal structure that displays strong two-dimensional structural features. $\beta$-GeSe is made at high pressure and temperature and is stable under ambient conditions. We compare it to its structural and electronic relatives $\alpha$-GeSe and black phosphorus. The $\beta$ form of GeSe displays a boat conformation for its Ge-Se six-ring, while the previously known $\alpha$ form, and black phosphorus, display the more common chair conformation for their six-rings. Electronic structure calculations indicate that $\beta$-GeSe is a semiconductor, with an approximate bulk band gap of $\Delta~\approx$ 0.5 eV, and, in its monolayer form, $\Delta~\approx$ 0.9 eV. These values fall between those of $\alpha$-GeSe and black phosphorus, making $\beta$-GeSe a promising candidate for future applications. The resistivity of our $\beta$-GeSe crystals measured in-plane is on the order of $\rho \approx$ 1 $\Omega$cm, while being essentially temperature independent.
1702.00715v1
2017-09-21
Effect of nanostructure on thermoelectric properties of La$_{0.7}$Sr$_{0.3}$MnO$_{3}$ in 300-600 K range
In oxide materials, nanostructuring effect has been found very promising approach for the enhancement of \textit{figure-of-merit}, \textit{ZT}. In the present work, we have synthesized La$_{0.7}$Sr$_{0.3}$MnO$_{3}$ (LSMO) compound using sol-gel method and samples of crystallite size of 34, 41, and 49 nm were obtained by giving different heat treatment. Seebeck coefficient ($\alpha$), electrical resistivity ($\rho$), and thermal conductivity ($\kappa$) measurements were carried out in 300-600 K temperature range. The systematic change in the values of $\alpha$ from $\sim$ -19 $\mu$V/K to $\sim$ -24 $\mu$V/K and drastic reduction in the values of $\kappa$ from $\sim$0.88 W/mK to $\sim$0.23 W/mK are observed as crystallite size is reduced from 49 nm to 34 nm at $\sim$600 K. Also, fall in the values of $\rho$ in the paramagnetic (PM) insulator phase (400-600 K) are effectively responsible for the increasing trend in the values of \textit{ZT} at high temperature. For the crystallite size of 41 nm, value of \textit{ZT} at 600 K was found to be $\sim$0.017, which can be further increased up to $\sim$0.045 around 650 K temperature. The predicted value of \textit{ZT} suggests that LSMO can be suitable oxide material for thermoelectric applications at high temperature.
1709.07205v2
2017-12-17
Short range order in the quantum XXZ honeycomb lattice material BaCo$_2$(PO$_4$)$_2$
We present observations of highly frustrated quasi two-dimensional (2D) magnetic correlations in the honeycomb lattice layers of the S$_{eff}$ = 1/2 compound $\gamma$-BaCo$_2$(PO$_4$)$_2$ ($\gamma$-BCPO). Specific heat shows a broad peak comprised of two weak kink features at $T_{N1} \sim$ 6 K and $T_{N2} \sim$ 3.5 K, the relative weights of which can be modified by sample annealing. Neutron powder diffraction measurements reveal short range quasi-2D order that is established below $T_{N1}$ and $T_{N2}$, at which two separate, incompatible, short range magnetic orders onset: commensurate antiferromagnetic correlations with correlation length $\xi_c = 60\pm2$ \AA \ ($T_{N1}$) and in quasi-2D helical domains with $\xi_h = 350 \pm 11$ \AA \ ($T_{N2}$). The ac magnetic susceptibility response lacks frequency dependence, ruling out spin freezing. Inelastic neutron scattering data on $\gamma$-BCPO is compared with linear spin wave theory, and two separate parameter regions of the XXZ $J_1$-$J_2$-$J_3$ model with ferromagnetic nearest-neighbor exchange $J_1$ are favored, both near regions of high classical degeneracy. High energy coherent excitations ($\sim 10$ meV) persist up to at least 40 K, suggesting strong in-plane correlations persist above $T_N$. These data show that $\gamma$-BCPO is a rare highly frustrated, quasi-2D S$_{eff}$ = 1/2 honeycomb lattice material which resists long range magnetic order and spin freezing.
1712.06208v2
2018-02-22
Touch Sensors with Overlapping Signals: Concept Investigation on Planar Sensors with Resistive or Optical Transduction
Traditional methods for achieving high localization accuracy on tactile sensors usually involve a matrix of miniaturized individual sensors distributed on the area of interest. This approach usually comes at a price of increased complexity in fabrication and circuitry, and can be hard to adapt to non-planar geometries. We propose a method where sensing terminals are embedded in a volume of soft material. Mechanical strain in this material results in a measurable signal between any two given terminals. By having multiple terminals and pairing them against each other in all possible combinations, we obtain a rich signal set using few wires. We mine this data to learn the mapping between the signals we extract and the contact parameters of interest. Our approach is general enough that it can be applied with different transduction methods, and achieves high accuracy in identifying indentation location and depth. Moreover, this method lends itself to simple fabrication techniques and makes no assumption about the underlying geometry, potentially simplifying future integration in robot hands.
1802.08209v2
2018-11-27
Unifying Description of Competing Orders in Two Dimensional Quantum Magnets
Quantum magnets provide the simplest example of strongly interacting quantum matter, yet they continue to resist a comprehensive understanding above one spatial dimension (1D). In 1D, a key ingredient to progress is Luttinger liquid theory which provides a unified description. Here we explore a promising analogous framework in two dimensions, the Dirac spin liquid (DSL), which can be constructed on several different lattices. The DSL is a version of Quantum Electrodynamics ( QED$_3$) with four flavors of Dirac fermions coupled to photons. Importantly, its excitations also include magnetic monopoles that drive confinement. By calculating the complete action of symmetries on monopoles on the square, honeycomb, triangular and kagom\`e lattices, we answer previously open key questions. We find that the stability of the DSL is enhanced on the triangular and kagom\`e lattices as compared to the bipartite (square and honeycomb) lattices. We obtain the universal signatures of the DSL on the triangular and kagom\`e lattices, including those that result from monopole excitations, which serve as a guide to numerics and to experiments on existing materials. Interestingly, the familiar 120 degree magnetic orders on these lattices can be obtained from monopole proliferation. Even when unstable, the Dirac spin liquid unifies multiple ordered states which could help organize the plethora of phases observed in strongly correlated two-dimensional materials.
1811.11186v2
2017-03-18
The Effect of Temperature on Cu-K-In-Se Thin Films
Films of Cu-K-In-Se were co-evaporated at varied K/(K+Cu) compositions and substrate temperatures (with constant (K+Cu)/In ~ 0.85). Increased Na composition on the substrate's surface and decreased growth temperature were both found to favor Cu1-xKxInSe2 (CKIS) alloy formation, relative to mixed-phase CuInSe2 + KInSe2 formation. Structures from X-ray diffraction (XRD), band gaps, resistivities, minority carrier lifetimes and carrier concentrations from time-resolved photoluminescence were in agreement with previous reports, where low K/(K+Cu) composition films exhibited properties promising for photovoltaic (PV) absorbers. Films grown at 400-500 C were then annealed to 600 C under Se, which caused K loss by evaporation in proportion to initial K/(K+Cu) composition. Similar to growth temperature, annealing drove CKIS alloy consumption and CuInSe2 + KInSe2 production, as evidenced by high temperature XRD. Annealing also decomposed KInSe2 and formed K2In12Se19. At high temperature the KInSe2 crystal lattice gradually contracted as temperature and time increased, as well as just time. Evaporative loss of K during annealing could accompany the generation of vacancies on K lattice sites, and may explain the KInSe2 lattice contraction. This knowledge of Cu-K-In-Se material chemistry may be used to predict and control minor phase impurities in Cu(In,Ga)(Se,S)2 PV absorbers-where impurities below typical detection limits may have played a role in recent world record PV efficiencies that utilized KF post-deposition treatments.
1703.06366v1
2019-02-26
Bonding and oxidation protection of Ti${_2}$AlC and Cr${_2}$AlC for a Ni-based Superalloy
Alumina forming, oxidation and thermal shock resistant MAX phases are of a high interest for high temperature applications. Herein we report, on bonding and resulting interactions between a Ni-based superalloy, NSA, and two alumina forming MAX phases. The diffusion couples Cr${_2}$AlC/Inconel-718/Ti${_2}$AlC were assembled and heated to 1000 or 1100{\deg}C in a vacuum hot press under loads corresponding to stresses of either 2 MPa or 20 MPa. The resulting interfaces were examined using X-ray diffraction, scanning electron microscopy and energy-dispersive X-ray spectroscopy. Good bonding between Cr${_2}$AlC and NSA was achieved after hot pressing at 1000{\deg}C and a contact pressure of only 2 MPa; in the case of Ti${_2}$AlC a higher temperature (1100{\deg}C) and pressure (20 MPa) were needed. In both cases, a diffusion bond was realized with no evidence of interfacial damage or cracking after cooling to room temperature. Twenty thermal cycles from room temperature to 1000{\deg}C showed that Ti${_2}$AlC is a poor oxidation barrier for Inconel-718. However, in the case of Cr${_2}$AlC no cracks, delamination nor surface degradation were observed, suggesting that this material could be used to protect Inconel-718 from oxidation.
1902.10001v2
2020-04-22
Deformation of micrometer and mm-sized Fe2.4wt.%Si single- and bi-crystals with a high angle grain boundary at room temperature
Plasticity in body-centred cubic (BCC) metals, including dislocation interactions at grain boundaries, is much less understood than in face-centred cubic (FCC) metals. At low temperatures additional resistance to dislocation motion due to the Peierls barrier becomes important, which increases the complexity of plasticity. Iron-silicon steel is an interesting, model BCC material since the evolution of the dislocation structure in specifically-oriented grains and at particular grain boundaries have far-reaching effects not only on the deformation behaviour but also on the magnetic properties, which are important in its final application as electrical steel. In this study, two different orientations of micropillars (1, 2, 4 microns in diameter) and macropillars (2500 microns) and their corresponding bi crystals are analysed after compression experiments with respect to the effect of size on strength and dislocation structures. Using different experimental methods, such as slip trace analysis, plane tilt analysis and cross-sectional EBSD, we show that direct slip transmission occurs, and different slip systems are active in the bi-crystals compared to their single-crystal counterparts. However, in spite of direct transmission and a very high transmission factor, dislocation pile-up at the grain boundary is also observed at early stages of deformation. Moreover, an effect of size scaling with the pillar size in single crystals and the grain size in bi-crystals is found, which is consistent with investigations elsewhere in FCC metals.
2004.10598v2
2022-02-01
Strong Edge Stress in Molecularly Thin Organic$-$Inorganic Hybrid Ruddlesden$-$Popper Perovskites and Modulations of Their Edge Electronic Properties
Organic$-$inorganic hybrid Ruddlesden$-$Popper perovskites (HRPPs) have gained much attention for optoelectronic applications due to their high moisture resistance, good processibility under ambient conditions, and long functional lifetimes. Recent success in isolating molecularly thin hybrid perovskite nanosheets and their intriguing edge phenomena have raised the need for understanding the role of edges and the properties that dictate their fundamental behaviours. In this work, we perform a prototypical study on the edge effects in ultrathin hybrid perovskites by considering monolayer (BA)$_2$PbI$_4$ as a representative system. Based on first-principles simulations of nanoribbon models, we show that in addition to significant distortions of the octahedra network at the edges, strong edge stresses are also present in the material. Structural instabilities that arise from the edge stress could drive the relaxation process and dominate the morphological response of edges in practice. A clear downward shift of the bands at the narrower ribbons, as indicative of the edge effect, facilitates the separation of photo-excited carriers (electrons move towards the edge and holes move towards the interior part of the nanosheet). Moreover, the desorption energy of the organic molecule can also be much lower at the free edges, making it easier for functionalization and/or substitution events to take place. The findings reported in this work elucidate the underlying mechanisms responsible for edge states in HRPPs and will be important in guiding the rational design and development of high-performance layer$-$edge devices.
2202.00296v1
2016-03-11
Quantum Critical Behavior in a Concentrated Ternary Solid Solution
Quantum critical behavior has been associated with some of the most exotic emergent states of matter including high-temperature superconductivity. Much of the research into quantum critical point (QCP) physics has been hampered by the lack of model systems simple enough to be analyzed by theory. Here, we show that the concentrated solid solution fcc alloys, including the so-called high-entropy alloys, are ideal model systems to study the effects of chemical disorder on emergent properties near a quantum critical region. The face centered cubic (fcc) alloy NiCoCrx with x near 1 is found to be close to the Cr concentration where the ferromagnetic transition temperature, Tc, goes to 0. Near this composition these alloys exhibit a resistivity linear in temperature to 2 K, a linear magnetoresistance, an excess -TlnT contribution to the low temperature heat capacity and excess low temperature entropy. All of the low temperature electrical, magnetic and thermodynamic properties of the alloys with compositions near x near 1 are not typical of a Fermi liquid and suggest strong magnetic fluctuations associated with a quantum critical region. The limit of extreme chemical disorder in these simple fcc materials thus provides a novel and unique platform to study quantum critical behavior in a highly tunable system.
1603.03781v1
2019-03-09
Dry transfer method for suspended graphene on lift-off-resist: simple ballistic devices with Fabry-Pérot interference
We demonstrate a fabrication scheme for clean suspended structures using chemical-vapor-deposition-grown graphene and a dry transfer method on lift-off-resist-coated substrates to facilitate suspended graphene nanoelectronic devices for technology applications. It encompasses the demands for scalable fabrication as well as for ultra-fast response due to weak coupling to environment. The fabricated devices exhibited initially a weak field-effect response with substantial positive ($p$) doping which transformed into weak negative ($n$) doping upon current annealing at the temperature of 4 Kelvin. With increased annealing current, $n$-doping gradually decreased while the Dirac peak position approached zero in gate voltage. An ultra-low residual charge density of $9\times10^8 \mathrm{ \ cm^{-2}}$ and a mobility of $1.9 \times 10^5 \mathrm{\ cm^2/Vs}$ were observed. Our samples display clear Fabry-P\'{e}rot (FP) conductance oscillation which indicates ballistic electron transport. The spacing of the FP oscillations are found to depend on the charge density in a manner that agrees with theoretical modeling based on Klein tunneling of Dirac particles. The ultra-low residual charge, the FP oscillations with density dependent period, and the high mobility prove excellent quality of our suspended graphene devices. Owing to its simplicity, scalability and robustness, this fabrication scheme enhances possibilities for production of suspended, high-quality, two-dimensional-material structures for novel electronic applications.
1903.03780v1
2019-12-11
Quantum oscillations and electronic structures in large Chern number semimetal RhSn
We report the magnetoresistance, Hall effect, de Haas-van Alphen (dHvA) oscillations and the electronic structures of single crystal RhSn, which is a typical material of CoSi family holding a large Chern number. The large unsaturated magnetoresistance is observed with B//[001]. The Hall resistivity curve indicates that RhSn is a multi-band system with high mobility. Evident quantum oscillations have been observed, from which the light effective masses are extracted. Ten fundamental frequencies are extracted after the fast Fourier transform analysis of the dHvA oscillations with B//[001] configuration. The two low frequencies F$_1$ and F$_2$ do not change obviously and the two high frequencies F$_9$ and F$_{10}$ evolve into four when B rotates from B//[001] to B//[110], which is consistent with the band structure in the first-principles calculations with spin-orbit coupling (SOC). The extracted Berry phases of the relative pockets show a good agreement with the Chern number $\pm4$ (with SOC) in the first-principles calculations. Above all, our studies indicate that RhSn is an ideal platform to study the unconventional chiral fermions and the surface states.
1912.05148v1
2019-12-11
Bulk and Two-dimensional Silver and Copper Monohalides: A Unique Class of Materials with Modest Ionicity/Covalency and Ferroelasticity/Multiferroicity
Silver and copper monohalides can be viewed as a class of compounds in the neutral zone between predominantly covalent and ionic compounds, thereby exhibiting neither strong ionicity nor strong covalency. We show ab initio calculation evidence that silver and copper monohalides entail relatively low transition barriers between the non-polar rock-salt phase and the polar zinc-blende phase, due largely to their unique chemical nature of modest iconicity or covalency. Notably, the low transition barriers endow both monohalides with novel mechanical and electronic properties, i.e., coupled ferroelasticity and ferroelectricity with large polarizations and relatively low switching barriers at ambient conditions. Several halides even possess very similar lattice constants and structures as the prevailing semiconductors such as silicon, thereby enabling epitaxial growth on silicon. Moreover, based on extensive structural search, we find that the most stable two-dimensional (2D) polymorphs of the monolayer halides are close or even greater in energy than their bulk counterparts, a feature not usually seen in the family of rock-salt or zinc-blende semiconductors. The low transition barrier between zinc-blende phase and 2D phase is predicted. Moreover, several 2D monolayer halides also exhibit multiferroicity with coupled ferroelasticity or ferroelectricity, thereby rendering their potential applications as high-density integrated memories for efficient data reading and writing. Their surfaces, covered by halides, also provide oxidation resistance and give low cleave energy from layered structure, suggesting high likelihood of experimental synthesis of these 2D polymorphs.
1912.05172v1
2015-04-14
Carrier Transport at the Metal-MoS2 Interface
This study illustrates the nature of electronic transport and its transition from one mechanism to another between a metal electrode and MoS2 channel interface in a field effect transistor (FET) device. Interestingly, measurements of the contact resistance (Rc) as a function of temperature indicate a transition in the carrier transport across the energy barrier from a thermionic emission at a high temperature to tunneling at a low temperature. Furthermore, at a low temperature, the nature of the tunneling behavior is ascertained by the current-voltage dependency that helps us feature direct tunneling at a low bias and Fowler-Nordheim tunneling at a high bias for a Pd-MoS2 contact due to the effective barrier shape modulation by biasing. In contrast, only direct tunneling is observed for a Cr-MoS2 contact over the entire applied bias range. In addition, simple analytical calculations were carried out to extract Rc at the gating range, and the results are consistent with the experimental data. Our results describe the transition in carrier transport mechanisms across a metal-MoS2 interface, and this information provides guidance for the design of future flexible, transparent electronic devices based on 2-dimensional materials.
1504.03466v1
2018-12-28
Nanoscale Self-Healing Mechanisms in Shape Memory Ceramics
Shape memory (SM) ceramics, such as yttria-stabilized tetragonal zirconia (YSTZ), are a unique family of SM materials that offer unique properties including ultra-high operating temperature, and high resistance to chemical corrosion and oxidation. However, formation of defects is usually observed in SM ceramics during manufacturing and/or by mechanical deformation. To fully take advantage of the SM properties of these ceramics, it is necessary to fully understand the nano-structural evolution of defects under external stimuli. In this study, defect closure behaviors in YSTZ nanopillars are investigated by atomistic simulations. Two characteristic orientations of [011-] and [001] are selected to represent the dominant deformation mechanisms of phase transformation and dislocation migration, respectively. With the presence of crack and void, the strength and yield strain of nanopillars are noted to decrease significantly, especially for [011-]-oriented YSTZ nanopillars. Volume expansion associated with the tetragonal to monoclinic phase transformation is observed to promote healing of crack and void. Atom stress analyses reveal stress concentrations along the newly formed monoclinic phase bands. A critical crack width is identified, less than which the crack can be fully closed in compression. Size effect study reveals that an increase in nanopillar size has a positive effect on crack self-healing behavior. For [001]-oriented YSTZ nanopillars, dislocation migration leads to formations of an amorphous phase, which also assist the crack and void closure process. The revealed crack/void healing mechanisms may provide a path for mitigating internal defects that influences the mechanical properties and deformation mechanisms of SM ceramics.
1812.11136v1
2019-06-24
Melting of vortex lattice in magnetic superconductor $\mathrm{Rb}\mathrm{Eu}\mathrm{Fe}_{4}\mathrm{As}_{4}$
The iron-based superconductors are characterized by strong fluctuations due to high transition temperatures and small coherence lengths. We investigate fluctuation behavior in the magnetic iron-pnictide superconductor $\mathrm{Rb}\mathrm{Eu}\mathrm{Fe}_{4}\mathrm{As}_{4}$ by calorimetry and transport. We find that the broadening of the specific-heat transition in magnetic fields is very well described by the lowest-Landau-level scaling. We report calorimetric and transport observations for vortex-lattice melting, which is seen as a sharp drop of the resistivity and a step of the specific heat at the magnetic-field-dependent temperature. The melting line in the temperature/magnetic-field plane lies noticeably below the upper-critical-field line and its location is in quantitative agreement with theoretical predictions without fitting parameters. Finally, we compare the melting behavior of $\mathrm{Rb}\mathrm{Eu}\mathrm{Fe}_{4}\mathrm{As}_{4}$ with other superconducting materials showing that thermal fluctuations of vortices are not as prevalent as in the high-temperature superconducting cuprates, yet they still noticeably influence the properties of the vortex matter.
1906.10236v2
2020-01-23
Magnetic-field-induced robust zero Hall plateau state in MnBi$_2$Te$_4$ Chern insulator
The intrinsic antiferromagnetic topological insulator MnBi2Te4 provides an ideal platform for exploring exotic topological quantum phenomena. Recently, the Chern insulator and axion insulator phases have been realized in few-layer MnBi2Te4 devices at low magnetic field regime. However, the fate of MnBi2Te4 in high magnetic field has never been explored in experiment. In this work, we report transport studies of exfoliated MnBi2Te4 flakes in pulsed magnetic fields up to 61.5 T. In the high-field limit, the Chern insulator phase with Chern number C = -1 evolves into a robust zero Hall resistance plateau state. Nonlocal transport measurements and theoretical calculations demonstrate that the charge transport in the zero Hall plateau state is conducted by two counter-propagating edge states that arise from the combined effects of Landau levels and large Zeeman effect in strong magnetic fields. Our result demonstrates the intricate interplay among intrinsic magnetic order, external magnetic field, and nontrivial band topology in MnBi2Te4.
2001.08401v2
2020-04-14
Highly Conducting Spaced TiO$_2$ Nanotubes Enable Defined Conformal Coating with Nanocrystalline Nb$_2$O$_5$ and High Performance Supercapacitor Applications
In this work, we report on the electrochemical behavior of nitrided spaced TiO$_2$ nanotubes conformally coated with a nanocrystalline Nb$_2$O$_5$ layer and find for these hierarchical structures an excellent supercapacitor performance. Highly aligned conductive 1D electrodes were obtained by a three step process: i) growth of self-organized nanotubes with defined and adjustable intertube spacing, ii) conformal Nb$_2$O$_5$ decoration in the tube interspace (while providing full electrolyte access to the entire active area), and iii) high temperature nitridation. Key is the growth of a nanotube array with regular tube-to-tube interspacing that enables an optimized decoration with secondary materials such as Nb$_2$O$_5$. We observe an increase in electrode capacitance from 158 $\mu$F cm-2 for bare TiO$_2$ NTs, to 1536 $\mu$F cm-2 for TiO$_2$/Nb$_2$O$_5$ NTs, to finally 37 mF cm-2 for Nb$_2$O$_5$ decorated and then nitrided nanotubes. This drastic increase can be ascribed firstly to the defined spacing established between the tube arrays that then allows for a conformal coating with a secondary active coating. Secondly, nitridation causes a drastic increase of the electron conductivity of the entire scaffold and thus reduces resistive losses.
2005.01603v1
2020-10-13
High-pressure synthesis of Ba$_2$RhO$_4$, a rhodate analogue of the layered perovskite Sr-ruthenate
A new layered perovskite-type oxide Ba$_2$RhO$_4$ was synthesized by a high-pressure technique with the support of convex-hull calculations. The crystal and electronic structure were studied by both experimental and computational tools. Structural refinements for powder x-ray diffraction data showed that Ba$_2$RhO$_4$ crystallizes in a K$_2$NiF$_4$-type structure, isostructural to Sr$_2$RuO$_4$ and Ba$_2$IrO$_4$. Magnetic, resistivity, and specific heat measurements for polycrystalline samples of Ba$_2$RhO$_4$ indicate that the system can be characterized as a correlated metal. Despite the close similarity to its Sr$_2$RuO$_4$ counterpart in the electronic specific heat coefficient and the Wilson ratio, Ba$_2$RhO$_4$ shows no signature of superconductivity down to 0.16 K. Whereas the Fermi surface topology has reminiscent pieces of Sr$_2$RuO$_4$, an electron-like e$_g$-($d_{x^2-y^2}$) band descends below the Fermi level, making of this compound unique also as a metallic counterpart of the spin-orbit-coupled Mott insulator Ba$_2$IrO$_4$.
2010.06556v1
2021-02-15
Magic thickness of 25 Å makes periodic metal-insulator transitions
Novel quantum phenomena, including high-temperature superconductivity, topological properties, and charge/spin density waves, appear in low-dimensional conductive materials. It is possible to artificially create low-dimensional systems by fabricating ultrathin films, quantum wires, or quantum dots with flat interfaces. Some experiments have been performed on ultrathin compounds of strongly correlated electron systems. However, since it is technically difficult to control multiple elements precisely, most of the properties of artificially fabricated low-dimensional compounds fall into uncharted territory. Here we show that extraordinary metal-insulator transitions that oscillate depending on the scale occur in CaRuO_3 films with a thickness of around several unit cells. We grow high-crystalline CaRuO_3 ultrathin films, whose surface roughness is controlled at 199 pm, by molecular beam epitaxy. We observe that resistivity oscillates with a magic thickness of 25 {\AA}, which changes by 3 and 9 orders of magnitude at room temperature and at low temperature, respectively. These changes are much larger than quantum size effects. We also confirm the same periodicity with photoelectron spectroscopy by etching the ultrathin film. Considering the large energy, periodicity and anisotropy, we conclude that the oscillating transitions originate from the commensurability of Mott insulation triggered by Peierls instability arising from a dual restriction on the dimensions in wavenumber space and real space. We have shown the possibility of producing new functional materials by controlling film thickness on electron correlated compounds at the picometer level.
2102.07323v1
2021-06-17
Synthesis of Murunskite Single Crystals: A Bridge Between Cuprates and Pnictides
Numerous contemporary investigations in condensed matter physics are devoted to high temperature (high-$T_c$ ) cuprate superconductors. Despite its unique effulgence among research subjects, the enigma of the high-$T_c$ mechanism still persists. One way to advance its understanding is to discover and study new analogous systems. Here we begin a novel exploration of the natural mineral murunskite, K$_2$FeCu$_3$S$_4$, as an interpolation compound between cuprates and ferropnictides, the only known high-$T_c$ superconductors at ambient pressure. Because in-depth studies can be carried out only on single crystals, we have mastered the synthesis and growth of high quality specimens. Similar to the cuprate parent compounds, these show semiconducting behavior in resistivity and optical transmittance, and an antiferromagnetic ordering at 100 K. Spectroscopy (XPS) and calculations (DFT) concur that the sulfur 3$p$ orbitals are partially open, making them accessible for charge manipulation, which is a prerequisite for superconductivity in analogous layered structures. DFT indicates that the valence band is more cuprate-like, while the conduction band is more pnictide-like. With appropriate doping strategies, this parent compound promises exciting future developments.
2106.09555v1
2021-09-14
Creep properties and deformation mechanisms of single-crystalline $γ^\prime$-strengthened superalloys in dependence of the Co/Ni ratio
Co-base superalloys are considered as promising high temperature materials besides the well-established Ni-base superalloys. However, Ni appears to be an indispensable alloying element also in Co-base superalloys. To address the influence of the base elements on the deformation behavior, high-temperature compressive creep experiments were performed on a single crystal alloy series that was designed to exhibit a varying Co/Ni ratio and a constant Al, W and Cr content. Creep tests were performed at 900 {\deg}C and 250 MPa and the resulting microstructures and defect configurations were characterized via electron microscopy. The minimum creep rates differ by more than one order of magnitude with changing Co/Ni ratio. An intermediate CoNi-base alloy exhibits the overall highest creep strength. Several strengthening contributions like solid solution strengthening of the $\gamma$ phase, effective diffusion coefficients or stacking fault energies were quantified. Precipitate shearing mechanisms differ significantly when the base element content is varied. While the Ni-rich superalloys exhibit SISF and SESF shearing, the Co-rich alloys develop extended APBs when the $\gamma^\prime$ phase is cut. This is mainly attributed to a difference in planar fault energies, caused by a changing segregation behavior. As result, it is assumed that the shearing resistivity and the occurring deformation mechanisms in the $\gamma^\prime$ phase are crucial for the creep properties of the investigated alloy series.
2109.06767v1
2022-06-29
Tailoring of rhenium oxidation state in ReOx thin films during reactive HiPIMS deposition process and following annealing
Bulk rhenium trioxide (ReO3) has an unusually high electrical conductivity and, being nanosized, has promising catalytic properties. However, the production of pure ReO3 thin films is challenging due to the difficulty to stabilize rhenium in a 6+ oxidation state. Here we present a novel approach for the deposition of ReOx (x = 1.6-2.9) thin films using reactive high power impulse magnetron sputtering (r-HiPIMS) from a metallic rhenium target in a mixed Ar/O2 atmosphere. The thin films were deposited in the gas-sustained self-sputtering regime, observed during r-HiPIMS process according to current waveforms. The influence of the substrate temperature, the oxygen-to-argon flow ratio and post-annealing at 250 {\deg}C in the air for 3 h on the properties of the films were studied. The as-deposited films have an X-ray amorphous structure (a-ReOx) when deposited at room temperature while a nano-crystalline \b{eta}-ReO2 phase when deposited at elevated temperatures (150 or 250 {\deg}C). The amorphous a-ReOx can be converted into the crystalline ReO3 with a lattice parameter of 3.75 {\AA} upon annealing in the air. The surface morphology of the films is dense without detectable voids when elevated substrate temperatures are used. Various Re oxidation states are observed on the surface of the films in different ratios depending on the deposition parameters. All samples exhibit electrical resistivity on the order of 10-3 Ohmxcm and optical properties typical for thin metallic films.
2206.14665v1
2022-06-02
A mechanically strong and ductile soft magnet with extremely low coercivity
Soft magnetic materials (SMMs) serve in electrical applications and sustainable energy supply, allowing magnetic flux variation in response to changes in applied magnetic field, at low energy loss1. The electrification of transport, households and manufacturing leads to an increase in energy consumption due to hysteresis losses2. Therefore, minimizing coercivity, which scales these losses, is crucial3. Yet, meeting this target alone is not enough: SMMs in electrical engines must withstand severe mechanical loads, i.e., the alloys need high strength and ductility4. This is a fundamental design challenge, as most methods that enhance strength introduce stress fields that can pin magnetic domains, thus increasing coercivity and hysteretic losses5. Here, we introduce an approach to overcome this dilemma. We have designed a Fe-Co-Ni-Ta-Al multicomponent alloy with ferromagnetic matrix and paramagnetic coherent nanoparticles (~91 nm size, ~55% volume fraction). They impede dislocation motion, enhancing strength and ductility. Their small size, low coherency and small magnetostatic energy create an interaction volume below the magnetic domain wall width, leading to minimal domain wall pinning, thus maintaining the soft magnetic properties. The alloy has a tensile strength of 1336 MPa at 54% tensile elongation, extremely low coercivity of 78 A/m (<1 Oe), moderate saturation magnetization of 100 Am2/kg, and high electrical resistivity of 103 {\mu}{\Omega} u Ohm cm.
2207.05686v1
2022-07-26
Cr$_3$X$_4$ (X=Se, Te) monolayers as new platform to realize robust spin filter, spin diode and spin valve
Two-dimensional ferromagnetic (FM) half-metals are promising candidates for advanced spintronic devices with small-size and high-capacity. Motivated by recent report on controlling synthesis of FM Cr$_3$Te$_4$ nanosheet, herein, to explore the potential application in spintronics, we designed spintronic devices based on Cr$_3$X$_4$ (X=Se, Te) monolayers and investigated their spin transport properties. We found that Cr$_3$Te$_4$ monolayer based device shows spin filtering and dual spin diode effect when applying bias voltage, while Cr$_3$S$_4$ monolayer is an excellent platform to realize a spin valve. The different transport properties are primarily ascribed to the semiconducting spin channel, which is close to and away from the Fermi level in Cr$_3$Te$_4$ and Cr$_3$Se$_4$ monolayers, respectively. Interestingly, the current in monolayer Cr$_3$Se$_4$ based device also displays a negative differential resistance effect (NDRE) and a high magnetoresistance ratio (up to 2*10$^3$). Moreover, we found thermally induced spin filtering effect and NDRE in Cr$_3$Se$_4$ junction when applying temperature gradient instead of bias voltage. These theoretical findings highlight the potential of Cr$_3$X$_4$ (X=Se, Te) monolayers in spintronic applications and put forward realistic materials to realize nanosale spintronic device.
2207.12679v1
2022-10-26
Ion-beam Assisted Sputtering of Titanium Nitride Thin Films
Titanium nitride is a material of interest for many superconducting devices such as nanowire microwave resonators and photon detectors. Thus, controlling the growth of TiN thin films with desirable properties is of high importance. In previous work on niobium nitride, ion beam-assisted sputtering (IBAS) reduced nitrogen sensitivity during deposition in tandem with an increase in nominal critical temperature. We have deposited thin films of titanium nitride by both, the conventional method of DC reactive magnetron sputtering and the IBAS method and compare their superconducting critical temperatures Tc as functions of thickness, sheet resistance, and nitrogen flow rate. We perform electrical and structural characterizations by electric transport and X-ray diffraction measurements. Compared to the conventional method of reactive sputtering, the IBAS technique has demonstrated a 10% increase in nominal critical temperature and 33% reduced sensitivity to nitrogen flow, without noticeable variation in the lattice structure. Additionally, we explore the behavior of superconducting Tc in ultra-thin films. Trends in films grown at high nitrogen concentrations follow predictions of mean-field theory in disordered films and show suppression of superconducting Tc due to geometric effects, while nitride films grown at low nitrogen concentrations strongly deviate from the theoretical models.
2210.15065v3
2023-02-14
MgF$_2$ as an effective additive for improving ionic conductivity of ceramic solid electrolytes
As typical solid-state electrolytes (SSEs), {Na}$_{1+x}${Zr}$_2${Si}$_{x}${P}$_{3-x}${O}$_{12}$ NASICONs provide an ideal platform for solid-state batteries (SSBs) that display higher safety and accommodate higher energy densities. The critical points for achieving SSBs with higher efficiencies are to improve essentially the ionic conductivity and to reduce largely the interfacial resistance between SSEs and cathode materials, which would necessitate extremely high level of craftsmanship and high-pressure equipment. An alternative to higher-performance and lower-cost SSBs is additive manufacturing. Here, we report on an effective additive, MgF$_2$, which was used in synthesizing NASICONs, resulting in SSEs with fewer defects and higher performance. With an addition of mere 1 wt$\%$ MgF$_2$ additive, the total room-temperature ionic conductivity of the NASICON electrolyte reaches up to 2.03 mS cm$^{-1}$, improved up to $\sim$ 181.3$\%$, with an activation energy of 0.277 eV. Meanwhile, the stability of the Na plating/stripping behavior in symmetric cells increases from 236 to 654 h. We tried to reveal the microscopic origins of the higher ionic conductivity of MgF$_2$-doped NASICONs by comprehensive in-house characterizations. Our study discovers a novel MgF$_2$ additive and provides an efficient way to prepare higher-performance SSEs, making it possible to fabricate lower-cost SSBs in industries.
2302.07264v1
2023-07-03
Low temperature dynamic polaron liquid in a manganite exhibiting colossal magnetoresistance
Polarons - fermionic charge carriers bearing a strong companion lattice deformation - exhibit a natural tendency for self-localization due to the recursive interaction between electrons and the lattice. While polarons are ubiquitous in insulators, how they evolve in transitions to metallic and superconducting states in quantum materials remains an open question. Here, we use resonant inelastic x-ray scattering (RIXS) to track the electron-lattice coupling in the colossal magneto-resistive bi-layer manganite La$_{1.2}$Sr$_{1.8}$Mn$_2$O$_7$ across its metal-to-insulator transition. The response in the insulating high-temperature state features harmonic emissions of a dispersionless oxygen phonon at small energy transfer. Upon cooling into the metallic state, we observe a drastic redistribution of spectral weight from the region of these harmonic emissions to a broad high energy continuum. In concert with theoretical calculations, we show that this evolution implies a shift in electron-lattice coupling from static to dynamic lattice distortions that leads to a distinct polaronic ground state in the low temperature metallic phase - a dynamic polaron liquid.
2307.00718v3
2023-09-24
FeCo Nanowire-Strontium Ferrite Powder Composites for Permanent Magnets with High-Energy Products
Due to the issues associated with rare-earth elements, there arises a strong need for magnets with properties between those of ferrites and rare-earth magnets that could substitute the latter in selected applications. Here, we produce a high remanent magnetization composite bonded magnet by mixing FeCo nanowire powders with hexaferrite particles. In the first step, metallic nanowires with diameters between 30 and 100 nm and length of at least 2 {\mu}m are fabricated by electrodeposition. The oriented as-synthesized nanowires show remanence ratios above 0.76 and coercivities above 199 kA/m and resist core oxidation up to 300 {\deg}C due to the existence of a > 8 nm thin oxide passivating shell. In the second step, a composite powder is fabricated by mixing the nanowires with hexaferrite particles. After the optimal nanowire diameter and composite composition are selected, a bonded magnet is produced. The resulting magnet presents a 20% increase in remanence and an enhancement of the energy product of 48% with respect to a pure hexaferrite (strontium ferrite) magnet. These results put nanowire-ferrite composites at the forefront as candidate materials for alternative magnets for substitution of rare earths in applications that operate with moderate magnet performance.
2309.13724v1
2023-11-01
Transport and electrical properties of cryogenic thermoelectric FeSb2: the effect of isoelectronic and hole doping
Thermoelectric materials operating at cryogenic temperatures are in high demand for efficient cooling and power generation in applications ranging from superconductors to quantum computing. The narrow band-gap semiconductor FeSb2, known for its colossal Seebeck coefficient, holds promise for such applications, provided its thermal conductivity value can be reduced. This study investigates the impact of isoelectronic substitution (Bi) and hole doping (Pb) at the Sb site on the transport properties of FeSb2, with a particular focus on thermal conductivity (\k{appa}). Polycrystalline FeSb2 powder, along with Bi- and Pb-doped samples, were synthesized using a simple co-precipitation approach, followed by thermal treatment in an H2 atmosphere. XRD and SEM analysis confirms the formation of the desired phase pre- and post-consolidation using spark plasma sintering (SPS). The consolidation process resulted in a high compaction density and the formation of submicrometer-sized grains, as substantiated by electron backscattered diffraction (EBSD) analysis. Substituting 1% of Bi and Pb at the Sb site successfully suppressed the thermal conductivity (\k{appa}) from ~15 W/m-K in pure FeSb2 to ~10 and ~8.7 W/m-K, respectively. Importantly, resistivity measurements revealed a metal-to-insulator transition at around 6.5 K in undoped FeSb2 and isoelectronically Bi-substituted FeSb2, suggesting the existence of metallic surface states and provides valuable evidence for the perplexing topological behavior exhibited by FeSb2.
2311.00326v1
2023-12-13
Computational design of NDR tunnel diodes with high peak-to-valley current ratio based on two-dimensional cold metals: The case of NbSi$_2$N$_4$/HfSi$_2$N$_4$/NbSi$_2$N$_4$ lateral heterojunction diode
Cold metals have recently gained attention as a promising platform for innovative devices, such as tunnel diodes with negative differential resistance (NDR) and field-effect transistors with subthreshold swings below the thermionic limit. Recently discovered two-dimensional (2D) MA$_2$Z$_4$ (M = Ti, Zr, Hf, Nb, Ta; A = Si, Ge; Z = N, P) compounds exhibit both cold metallic and semiconducting behavior. In this work, we present a computational study of lateral heterojunction tunnel diodes based on 2D NbSi$_2$N$_4$ and HfSi$_2$N$_4$ compounds. Employing density functional theory combined with a nonequilibrium Green function method, we investigate the current-voltage ($I$-$V$) characteristics of lateral tunnel diodes with varying barrier thicknesses in both zigzag and armchair orientations. We find that tunnel diodes in the zigzag orientation exhibit significantly higher peak current densities, while those in the armchair orientation display larger peak-to-valley current ratios (PVCRs) compared to the zigzag orientation. Our findings suggest that MA$_2$Z$_4$ materials are promising candidates for realizing NDR tunnel diodes with high PVCR values, which could have potential applications in memory, logic circuits, and other electronic devices.
2312.08473v2
2024-01-29
Increasing the Collection Efficiency in Selenium Thin-Film Solar Cells Using a Closed-Space Annealing Strategy
Elemental selenium is a promising wide-bandgap ($E_\mathrm{G}\approx$ 1.95 eV) photovoltaic material for the next generation of thin-film solar cells. To realize high-efficiency selenium solar cells, it is crucial to optimize the crystallization process of the selenium thin-film photoabsorber. However, the high vapor pressure of selenium restricts the processing conditions to a compromise between the growth of large crystal grains and the formation of pinholes. In this study, we introduce a closed-space annealing (CSA) strategy designed to suppress the sublimation of selenium, enabling thermal annealing processes at higher temperatures and for longer periods of time. As a result, we consistently improve carrier collection and the overall photovoltaic device performance in our selenium solar cells. By characterizing the carrier dynamics in our devices, we conclude that the observed improvements result from a reduction in charge transfer resistance rather than an increase in carrier diffusion length. The CSA strategy is a promising method for controlling surface morphology and roughness without reducing crystal grain sizes, which paves the way for further advancements in the efficiency and reproducibility of selenium thin-film solar cells.
2401.15936v1
2024-02-10
Cylindrical compression of thin wires by irradiation with a Joule-class short pulse laser
Equation of state measurements at Jovian or stellar conditions are currently conducted by dynamic shock compression driven by multi-kilojoule multi-beam nanosecond-duration lasers. These experiments require precise design of the target and specific tailoring of the spatial and temporal laser profiles to reach the highest pressures. At the same time, the studies are limited by the low repetition rate of the lasers. Here, we show that by the irradiation of a thin wire with single beam Joule-class short-pulse laser, a converging cylindrical shock is generated compressing the wire material to conditions relevant for the above applications. The shockwave was observed using Phase Contrast Imaging employing a hard X-ray Free Electron Laser with unprecedented temporal and spatial sensitivity. The data collected for Cu wires is in agreement with hydrodynamic simulations of an ablative shock launched by a highly-impulsive and transient resistive heating of the wire surface. The subsequent cylindrical shockwave travels towards the wire axis and is predicted to reach a compression factor of 9 and pressures above 800 Mbar. Simulations for astrophysical relevant materials underline the potential of this compression technique as a new tool for high energy density studies at high repetition rates.
2402.06983v1
2024-03-04
Quantum Hall Transport Measurements of Lateral p-n Junctions Formed via Precise Spatial Photodoping of Graphene/hBN Heterostructures
Heterostructures composed of 2-dimensional (2D) materials are spatially dope in-operando to modify devices for custom functionalities, such as lateral p-n-p junctions. After optically photodoping an hBN/Graphene/hBN heterostructure, detailed magnetotransport measurements including quantum Hall transport show several clear electronic regimes. In the p+-p-p+ and n-n+-n configurations, we see clear quantization of the longitudinal resistance. Using the Landauer-Buttiker model we elucidate the nature of the electrostatic profile at the interface between the doped regions. In the p-n-p configuration, due to the heavily graded junction profile that completely separates the p- and n-Landau level edge states from interacting, an "insulating" state is observed that is not common and has not been measured in previous quantum Hall transport measurements of graphene pnJ devices in high magnetic fields. This insulating state is promising as the basis for a high-performance graphene switching device with a good ON/OFF ratio. In principle, these doping and measurement techniques can be applied to any other 2D heterostructure encapsulated within an hBN sandwich to understand the quality of the electrostatic interface between doped regions.
2403.01998v1
2020-12-05
A15 Nb$_3$Si -- A "high" Tc superconductor synthesized at a pressure of one megabar and metastable at ambient conditions
A15 Nb$_3$Si is, until now, the only high temperature superconductor produced at high pressure (~110 GPa) that has been successfully brought back to room pressure conditions in a metastable condition. Based on the current great interest in trying to create metastable-at-room-pressure high temperature superconductors produced at high pressure, we have restudied explosively compressed A15 Nb$_3$Si and its production from tetragonal Nb$_3$Si. First, diamond anvil cell pressure measurements up to 88 GPa were performed on explosively compressed A15 Nb$_3$Si material to trace Tc as a function of pressure. Tc is suppressed to ~ 5.2 K at 88 GPa. Then, using these Tc (P) data for A15 Nb$_3$Si, pressures up to 92 GPa were applied at room temperature (which increased to 120 GPa at 5 K) on tetragonal Nb$_3$Si. Measurements of the resistivity gave no indication of any A15 structure production, i.e., no indications of the superconductivity characteristic of A15 Nb$_3$Si. This is in contrast to the explosive compression (up to P~110 GPa) of tetragonal Nb$_3$Si, which produced 50-70% A15 material, Tc = 18 K at ambient pressure, in a 1981 Los Alamos National Laboratory experiment. Our theoretical calculations show that A15 Nb$_3$Si has an enthalpy vs the tetragonal structure that is 0.07 eV/atom smaller at 100 GPa, implying that the accompanying high temperature (1000 deg C) caused by explosive compression is necessary to successfully drive the reaction kinetics of the tetragonal -> A15 Nb$_3$Si structural transformation. Annealing experiments on the A15 explosively compressed material reaching time scales of 39 years are consistent with this viewpoint.
2012.02905v2
2006-03-17
Second Core Formation and High Speed Jets: Resistive MHD Nested Grid Simulations
The stellar core formation and high speed jets driven by the formed core are studied by using three-dimensional resistive MHD nested grid simulations. Starting with a Bonnor-Ebert isothermal cloud rotating in a uniform magnetic field, we calculate the cloud evolution from the molecular cloud core (n = 10^6 cm^-3, r_c = 4.6 times 10^4 AU) to the stellar core (n \simeq 10^23 cm^-3, r_c \simeq 1 solar radius). We resolve cloud structure over 7 orders of magnitude in spatial extent and over 17 orders of magnitude in density contrast. For comparison, we calculate two models: resistive and ideal MHD models. Both models have the same initial condition, but the former includes dissipation process of magnetic field while the latter does not. The magnetic fluxes in resistive MHD model are extracted from the first core during 10^12 cm^-3 < n < 10^16 cm^-3 by Ohmic dissipation. Magnetic flux density of the formed stellar core (n \simeq 10^20 cm^-3) in resistive MHD model is two orders of magnitude smaller than that in ideal MHD model. Since magnetic braking is less effective in resistive MHD model, rapidly rotating stellar core (the second core) is formed. After stellar core formation, the magnetic field of the core is largely amplified both by magneto-rotational instability and the shearing motion between the stellar core and ambient medium. As a consequence, high speed (simeq 45 km,s^-1) jets are driven by the second core, which results in strong mass ejection. A cocoon-like structure around the second core also forms with clear bow shocks.
0603456v1
2018-05-07
Appearance of ferromagnetism property for Si nano-polycrystalline body and vanishing of electrical resistances at local high frequencies
Reduction in the skin effect for the sintered Si nanopolycrystalline body as an electricity conductor at a high frequency due to its nano-structure was studied. Singular vanishing of electrical resistances near a local high magnetic harmonic frequency of a few MHz was observed. This phenomenon has not been observed for conventional ferromagnetic metals. The measured electrical resistances changed to almost 0 m{\Omega} at room temperature. At the same time, negative resistance of the sintered Si nano-polycrystalline body was observed. It will be applicable to electronic transmittance lines or semiconductors. Numerical calculation was also performed on the electrical resistance with frequency dependency while considering the electric field and magnetic field in the sintered Si nanopolycrystalline body. The calculation could explain the variation of the relative permittivity of the Si nanopolycrystalline and the phenomenon for vanishing the resistivity at frequency of MHz theoretically. Reduced Si nanoparticles from SiO2 powder were synthesized by laser ablation in liquid. A Si nano-polycrystalline body made of the reduced Si nanoparticles was fabricated. It was found by measuring the magnetization property of the body that the sintered Si nano-polycrystalline body has ferromagnetism. High-density dangling bonds cause the sintered Si nanopolycrystalline to have ferromagnetism. In this study, the density of the unpaired electrons in the sintered Si nanopolycrystalline was observed using ESR. It has been clarified that the Si nanopowder and the sintered Si nanopolycrystalline have numerous dangling bonds. Both densities of the dangling bonds were evaluated.
1805.02312v1
2019-03-26
The micro-RWELL layouts for high particle rate
The $\mu$-RWELL is a single-amplification stage resistive Micro-Pattern Gaseous Detector (MPGD). The detector amplification element is realized with a single copper-clad polyimide foil micro-patterned with a blind hole (well) matrix and embedded in the readout PCB through a thin Diamond-Like-Carbon (DLC) sputtered resistive film. The introduction of the resistive layer, suppressing the transition from streamer to spark, allows to achieve large gains ($\geq$10$^4$) with a single amplification stage, while partially reducing the capability to stand high particle fluxes. The simplest resistive layout, designed for low-rate applications, is based on a single-resistive layer with edge grounding. At high particle fluxes this layout suffers of a non-uniform response. In order to get rid of such a limitation different current evacuation geometries have been designed. In this work we report the study of the performance of several high rate resistive layouts tested at the CERN H8-SpS and PSI $\pi$M1 beam test facilities. These layouts fulfill the requirements for the detectors at the HL-LHC and for the experiments at the next generation colliders FCC-ee/hh and CepC.
1903.11017v2
2018-04-15
$\mathrm{Co_2Fe_{1-x}Cr_xSi}$ Heusler Alloys : A promising material for spintronics application
In this article, we investigated the effect of Cr substitution in place of Fe on the structural, magnetic and transport properties of $\mathrm{Co_2FeSi}$ alloy. A comprehensive structural analysis is done using X-ray diffraction (XRD) and extended X-ray absorption fine structure (EXAFS) spectroscopy. Quaternary Heusler compounds $\mathrm{Co_2Fe_{1-x}Cr_xSi}$ with Cr content (x = 0.1, 0.3, 0.5) were found to crystallize in cubic structure. The synchrotron based EXAFS studies reveal that the anti-site disorder increases with the increase in Cr concentration. The saturation magnetization values in all the alloys are found to be less than those expected from the Slater-Pauling rule, which may be due to the some inherent disorder. A detailed resistivity analysis in the temperature range of 5-300 K is done, taking into account different scattering mechanisms. The residual resistivity ratio is found to decrease with increasing Cr concentration. A disorder induced resistivity minimum due to weak localization effect is seen for x = 0.5. The resistivity measurements also indicate that the half-metallic character survives upto 100 K for x = 0.1, whereas the alloys with x= 0.3 and 0.5 show signature of half- metallic nature even at higher temperatures. First principles calculation done with a more robust exchange correlation functional (namely HSE-06) confirms the half metallicity in the entire concentration range. Theoretically simulated band gap and magnetic moments compliment the experimental findings and are compared wherever possible. All these properties make $\mathrm{Co_2Fe_{1-x}Cr_xSi}$ a promising material for spintronics application.
1804.05321v1
2021-10-16
Giant magnetoresistance and topological Hall effect in the EuGa4 antiferromagnet
We report on systematic temperature- and magnetic field-dependent studies of the EuGa$_4$ binary compound, which crystallizes in a centrosymmetric tetragonal BaAl$_4$-type structure with space group $I4/mmm$. The electronic properties of EuGa$_4$ single crystals, with an antiferromagnetic (AFM) transition at $T_\mathrm{N} \sim 16.4$ K, were characterized via electrical resistivity and magnetization measurements. A giant nonsaturating magnetoresistance was observed at low temperatures, reaching $\sim 7 \times 10^4$ % at 2 K in a magnetic field of 9 T. In the AFM state, EuGa$_4$ undergoes a series of metamagnetic transitions in an applied magnetic field, clearly manifested in its field-dependent electrical resistivity. Below $T_\mathrm{N}$, in the $\sim$4-7 T field range, we observe also a clear hump-like anomaly in the Hall resistivity which is part of the anomalous Hall resistivity. We attribute such a hump-like feature to the topological Hall effect, usually occurring in noncentrosymmetric materials known to host topological spin textures (as e.g., magnetic skyrmions). Therefore, the family of materials with a tetragonal BaAl$_4$-type structure, to which EuGa$_4$ and EuAl$_4$ belong, seems to comprise suitable candidates on which one can study the interplay among correlated-electron phenomena (such as charge-density wave or exotic magnetism) with topological spin textures and topologically nontrivial bands.
2110.08522v1
2016-01-09
Field-induced resistivity plateau and unsaturated negative magnetoresistance in topological semimetal TaSb2
Several prominent transport properties have been identified as key signatures of topologicalmaterials. One is the resistivity plateau at low temperatures as observed in several topological insulators (TIs), another is the negative magnetoresistance (MR) when the applied magnetic field is parallel to the current direction as observed in several topological semimetals (TSMs) including Dirac semimetals (DSMs) and Weyl semimetals (WSMs). Usually, these two exotic phenomena emerge in distinct materials with or without time reversal symmetry (TRS), respectively. Here we report the discovery of a new member in TSMs, TaSb2, which clearly exhibits both of these phenomena in a single material. This compound crystallizes in a base-centered monoclinic, centrosymmetric structure, and is metallic with a low carrier density in the zero field. While applying magnetic field it exhibits insulating behavior before appearance of a resistivity plateau below Tc =13 K. In the plateau regime, the ultrahigh carrier mobility and extreme magnetoresistance (XMR) for the field perpendicular to the current are observed as in DSMs and WSMs, in addition to a quantum oscillation behavior with non-trivial Berry phases. In contrast to the most known DSMs and WSMs, the negative MR in TaSb2 does not saturate up to 9 T, which, together with the almost linear Hall resistivity, manifests itself an electron-hole non-compensated TMS. These findings indicate that the resistivity plateau could be a generic feature of topology-protected metallic states even in the absence of TRS and compatible with the negative MR depending on the field direction. Our experiment extends a materials basis represented by TaSb2 as a new platform for future theoretical investigations and device applications of topological materials.
1601.02062v1
2011-01-31
Encapsulation and Electronic Control of Epitaxial Graphene by Photosensitive Polymers and UV light
Electronic devices using epitaxial graphene on Silicon Carbide require encapsulation to avoid uncontrolled doping by impurities deposited in ambient conditions. Additionally, interaction of the graphene monolayer with the substrate causes relatively high level of electron doping in this material, which is rather difficult to change by electrostatic gating alone. Here we describe one solution to these problems, allowing both encapsulation and control of the carrier concentration in a wide range. We describe a novel heterostructure based on epitaxial graphene grown on silicon carbide combined with two polymers: a neutral spacer and a photoactive layer that provides potent electron acceptors under UV light exposure. Unexposed, the same double layer of polymers works well as capping material, improving the temporal stability and uniformity of the doping level of the sample. By UV exposure of this heterostructure we controlled electrical parameters of graphene in a non-invasive, non-volatile, and reversible way, changing the carrier concentration by a factor of 50. The electronic properties of the exposed SiC/ graphene/polymer heterostructures remained stable over many days at room temperature, but heating the polymers above the glass transition reversed the effect of light. The newly developed photochemical gating has already helped us to improve the robustness (large range of quantizing magnetic field, substantially higher opera- tion temperature and significantly enhanced signal-to-noise ratio due to significantly increased breakdown current) of a graphene resistance standard to such a level that it starts to compete favorably with mature semiconductor heterostructure standards. [2,3]
1101.6014v1
2020-11-20
Phase Transitions in Germanium Telluride Nanoparticle Phase-Change Materials Studied by Time-Resolved X-Ray Diffraction
Germanium telluride (GeTe), a phase-change material, is known to exhibit four different structural phases: three at room temperature (one amorphous and two crystalline, $\alpha$ and $\gamma$) and one at high temperature (crystalline $\beta$). Because transitions between the amorphous and crystalline phases lead to significant changes in material properties (e.g., refractive index and resistivity), GeTe has been investigated as a phase-change material for photonics, thermoelectrics, ferroelectrics, and spintronics. Consequently, the temperature-dependent phase transitions in GeTe have been studied for bulk and thin-film GeTe, both fabricated by sputtering. Colloidal synthesis of nanoparticles offers a more flexible fabrication approach for amorphous and crystalline GeTe. These nanoparticles are known to exhibit size-dependent properties, such as an increased crystallization temperature for the amorphous-to-$\alpha$ transition in sub-10\,nm GeTe particles. The $\alpha$-to-$\beta$ phase transition is also expected to vary with size, but this effect has not yet been investigated for GeTe. Here, we report time-resolved X-ray diffraction of GeTe nanoparticles with different diameters and from different synthetic protocols. We observe a non-volatile amorphous-to-$\alpha$ transition between 210$^{\circ}$C and 240$^{\circ}$C and a volatile $\alpha$-to-$\beta$ transition between 370$^{\circ}$C and 420$^{\circ}$C. The latter transition was reversible and repeatable. While the transition temperatures are shifted relative to the values known for bulk GeTe, the nanoparticle-based samples still exhibit the same structural phases reported for sputtered GeTe. Thus, colloidal GeTe maintains the same general phase behavior as bulk GeTe while allowing for more flexible and accessible fabrication. Therefore, nanoparticle-based GeTe films show great potential for applications, such as in active photonics.
2011.10633v1
2022-08-23
Electrochemical investigation of MoSeTe as an anode for sodium-ion batteries
Sodium ion batteries (SIBs) are considered as an efficient alternative for lithium-ion batteries (LIBs) owing to the natural abundance and low cost of sodium than lithium. In this context, the anode materials play a vital role in rechargeable batteries to acquire high energy and power density. In order to demonstrate transition metal dichalcogenide (TMD) as potential anode materials, we have synthesized MoSeTe sample by conventional flux method, and the structure and morphology are characterized using x-ray diffraction (XRD), field-emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), and Raman spectroscopy. These characterisations confirm the hexagonal crystal symmetry with p63/mmc space group and layered morphology of MoSeTe. We investigate the electrochemical performance of a MoSeTe as a negative electrode (anode) for SIBs in the working potential range of 0.01 to 3.0~V. In a half-cell configuration, the MoSeTe as an anode and Na metal as counter/reference electrode exhibits significant initial specific discharge capacities of around 475 and 355 mAhg$^{-1}$ at current densities of 50 and 100 mAg$^{-1}$, respectively. However, the capacity degraded significantly like $\approx$200~mAhg$^{-1}$ in 2nd cycle, but having $\approx$100\% Coulombic efficiency, which suggest for further modification in this material to improve its stability. The cyclic voltammetry (CV) study reveals the reversibility of the material after 1st cycle, resulting no change in the initial peak positions. The electrochemical impedance spectroscopy (EIS) measurements affirms the smaller charge transfer resistance of fresh cells than the cells after 10th cycle. Moreover, the extracted diffusion coefficient is found to be of the order of 10$^{-14}$ cm$^2$s$^{-1}$.
2208.10911v1
2024-05-13
Reducing the oxygen contamination in conductive (Ti,Zr)N coatings via RF-bias assisted reactive sputtering
Ternary transition metal nitride coatings are promising for many applications as they can offer improved hardness and oxidation resistance compared to binary counterparts. A common challenge in the deposition of functional nitride thin films is oxygen contamination. Even low amounts of oxygen contamination can adversely affect the functional properties of the thin films. Here, we present a practical approach for the growth of virtually oxygen-free (Ti, Zr)N thin films. To cover the complete compositional range of (Ti,Zr)N coatings we employ combinatorial reactive co-sputtering. The depositions are carried out with or without applying a low-power radio-frequency (RF) bias voltage to the substrate holder to study the possibility of decelerating energetic oxygen ions and effectively reducing oxygen contamination in the growing film. High-throughput structural analysis and functional property mapping are used to elucidate the synthesis-property relationships. The structural analysis indicates solid solution formation over the entire compositional range, as evidenced by Vegardian lattice scaling, regardless of the applied RF substrate bias. Irrespective of the composition of the films, the application of RF substrate bias leads to a dramatic reduction of oxygen contamination, as demonstrated by X-ray photoelectron spectroscopy (XPS) depth-profile mapping. This is reflected in a significant improvement in the films' conductivity and hardness. We demonstrate that the reduction in oxygen contamination is intrinsic to the process and not due to changes in the microstructure. The approach presented here is applicable to both conductive and insulating substrates and provides a practical route to synthesize nitride thin films with improved purity that can be applied in standard sputter chambers and on many different material systems.
2405.07789v1
2018-11-03
Pressure-induced Insulator to Metal Transition of Mixed Valence Compound Ce(O,F)SbS$_{2}$
Transport properties of Ce$_{0.85}$F0.15SbS$_{2}$ and undoped CeOSbS$_{2}$ under high pressure were investigated experimentally and theoretically. Electrical resistivity measurements of the Ce$_{0.85}$F0.15SbS$_{2}$ single crystals were performed under various high pressures using a diamond anvil cell with boron-doped diamond electrodes. The samples showed the insulator to metal transition by applying high pressure up to 30-40 GPa. On the other hand, the undoped CeOSbS$_{2}$ showed almost same transport property with the F-doped sample under high pressure. The valence state analysis using X-ray photoelectron spectroscopy revealed a simple valence state of Ce3+ in Ce$_{0.85}$F0.15SbS$_{2}$ and mixed valence state between Ce3+ and Ce4+ in undoped CeOSbS$_{2}$. The valence fluctuation in Ce carried out the comparable transport nature in the both samples. A band calculation suggests that the undoped CeOSbS$_{2}$ could be metallic under high pressure of 30 GPa in accordance with the experimental results. A superior thermoelectric property of power factor in CeOSbS$_{2}$ was estimated under high pressure around 20 GPa in comparison with that of ambient pressure.
1811.01151v1
2020-10-22
A photogrammetric method for target monitoring inside the MEG II detector
An automatic target monitoring method based on photographs taken by a CMOS photo-camera has been developed for the MEG II detector. The technique could be adapted for other fixed-target experiments requiring good knowledge of their target position to avoid biases and systematic errors in measuring the trajectories of the outcoming particles. A CMOS-based, high resolution, high radiation tolerant and high magnetic field resistant photo-camera was mounted inside the MEG II detector at the Paul Scherrer Institute (Switzerland). MEG II is used to search for lepton flavour violation in muon decays. The photogrammetric method's challenges, affecting measurements of low momentum particles' tracks, are high magnetic field of the spectrometer, high radiation levels, tight space constraints, and the need to limit the material budget in the tracking volume. The camera is focused on dot pattern drawn on the thin MEG II target, about 1 m away from the detector endcaps where the photo-camera is placed. Target movements and deformations are monitored by comparing images of the dots taken at various times during the measurement. The images are acquired with a Raspberry board and analyzed using a custom software. Global alignment to the spectrometer is guaranteed by corner cubes placed on the target support. As a result, the target monitoring fulfils the needs of the experiment.
2010.11576v2
2021-02-04
Disorder-robust high-field superconducting phase of FeSe single crystals
When exposed to high magnetic fields, certain materials manifest an exotic superconducting (SC) phase that has attracted considerable attention. A proposed explanation for the origin of the high-field SC phase is the Fulde-Ferrell-Larkin-Ovchinnikov (FFLO) state. This state is characterized by inhomogeneous superconductivity, where the Cooper pairs have finite center-of-mass momenta. Recently, the high-field SC phase was observed in FeSe, and it was deemed to originate from the FFLO state. Here, we synthesize FeSe single crystals with different levels of disorder. The level of disorder is expressed by the ratio of the mean free path to the coherence length and ranges between 35 and 1.2. The upper critical field \textit{B}$_{\rm{c}2}$ was obtained by both resistivity and magnetic torque measurements over a wide range of temperatures, which went as low as $\sim$0.5 K, and magnetic fields, which went up to $\sim$38 T along the \textit{c} axis and in the \textit{ab} plane. In the high-field region parallel to the \textit{ab} plane, an unusual SC phase was confirmed in all the crystals, and the phase was found to be robust against disorder. This result suggests that the high-field SC phase in FeSe is not a conventional FFLO state.
2102.02353v2
2021-03-03
On the early stages of precipitation during direct ageing of Alloy 718
The Ni-based superalloy Alloy 718 is used in aircraft engines as high-pressure turbine discs and must endure challenging demands on high-temperature yield strength, creep-, and oxidation-resistance. Nanoscale $\gamma^{\prime}$- and $\gamma^{\prime \prime}$-precipitates commonly found in duplet and triplet co-precipitate morphologies provide high-temperature strength under these harsh operating conditions. Direct ageing of Alloy 718 is an attractive alternative manufacturing route known to increase the yield strength at 650 $^{\deg}$C by at least +10 $\%$, by both retaining high dislocation densities and changing the nanoscale co-precipitate morphology. However, the detailed nucleation and growth mechanisms of the duplet and triplet co-precipitate morphologies of $\gamma^{\prime}$ and $\gamma^{\prime \prime}$ during the direct ageing process remain unknown. We provide a correlative high-resolution microscopy approach using transmission electron microscopy, high-angle annular dark-field imaging, and atom probe microscopy to reveal the early stages of precipitation during direct ageing of Alloy 718. Quantitative stereological analyses of the $\gamma^{\prime}$- and $\gamma^{\prime \prime}$-precipitate dispersions as well as their chemical compositions have allowed us to propose a qualitative model of the microstructural evolution. It is shown that fine $\gamma^{\prime}$- and $\gamma^{\prime \prime}$-precipitates nucleate homogeneously and grow coherently. However, $\gamma^{\prime \prime}$-precipitates also nucleate heterogeneously on dislocations and experience accelerated growth due to Nb pipe diffusion. Moreover, the co-precipitation reactions are largely influenced by solute availability and the potential for enrichment of Nb and rejection of Al+Ti.
2103.02763v1
2022-06-25
High-Mobility Tri-Gate $β$-Ga$_2$O$_3$ MESFETs with a Power Figure of Merit over 0.9 GW/cm$^2$
In this letter, fin-shape tri-gate $\beta$-Ga$_{2}$O$_{3}$ lateral MESFETs are demonstrated with a high power figure of merit of 0.95 GW/cm$^{2}$ - a record high for any $\beta$-Ga$_{2}$O$_{3}$ transistor to date. A low-temperature undoped buffer-channel stack design is developed which demonstrates record high Hall and drift electron mobilities in doped $\beta$-Ga$_{2}$O$_{3}$ channels allowing for low ON resistances R$_{ON}$ in $\beta$-Ga$_{2}$O$_{3}$ MESFETs. Fin-widths (W$_{fin}$) were 1.2-1.5 $\mu$m and there were 25 fins (N$_{fin}$) per device with a trench depth of $\sim$1$\mu$m. A $\beta$-Ga$_2$O$_3$ MESFET with a source-drain length of 6.4 $\mu$m exhibits a high ON current (187 mA/mm), low R$_{ON}$ (20.5 $\Omega$.mm) and a high average breakdown field (4.2 MV/cm). All devices show very low reverse leakage until catastrophic breakdown for breakdown voltages scaled from 1.1kV to $\sim$3kV. This work demonstrates the potential of channel engineering in improving $\beta$-Ga$_{2}$O$_{3}$ device performance toward lower conduction losses for low-to-medium voltage applications.
2206.12539v2
2023-10-22
Pressure-induced volumetric negative thermal expansion in CoZr2 superconductor
We investigate the thermal expansion and superconducting properties of a CuAl2-type (tetragonal) superconductor CoZr2 under high pressures. We perform high-pressure synchrotron X-ray diffraction in a pressure range of 2.9 GPa < P < 10.4 GPa and discover that CoZr2 exhibits volumetric negative thermal expansion under high pressures. Although the uniaxial positive thermal expansion (PTE) along the a-axis is observed under ambient pressure, that is suppressed by pressure, while the large uniaxial negative thermal expansion (NTE) along the c-axis is maintained under the pressure regime. As a result of a combination of the suppressed uniaxial PTE along the a-axis and uniaxial NTE along the c-axis, volumetric negative thermal expansion is achieved under high pressure in CoZr2. The mechanisms of volumetric NTE would be based on the flexible crystal structure caused by the soft Co-Co bond as seen in the iso-structural compound FeZr2, which exhibits uniaxial NTE along the c-axis. We also perform high-pressure electrical resistance measurements of CoZr2 to confirm the presence of superconductivity under the examined pressure regime in the range of 0.03 GPa < P < 41.9 GPa. We confirm the presence of superconductivity under all pressures and observe dome-like shape pressure dependence of superconducting transition temperature. Because of the coexistence of two phenomena, which are volumetric NTE and superconductivity, in CoZr2 under high pressure, the coexistence would be achievable under ambient pressure by tuning chemical compositions after our present observation.
2310.14254v2
2023-10-22
Superconductivity in the high-entropy ceramics Ti0.2Zr0.2Nb0.2Mo0.2Ta0.2Cx with possible nontrivial band topology
Topological superconductors have drawn significant interest from the scientific community due to the accompanying Majorana fermions. Here, we report the discovery of electronic structure and superconductivity in high-entropy ceramics Ti0.2Zr0.2Nb0.2Mo0.2Ta0.2Cx (x = 1 and 0.8) combined with experiments and first-principles calculations. The Ti0.2Zr0.2Nb0.2Mo0.2Ta0.2Cx high-entropy ceramics show bulk type-II superconductivity with Tc about 4.00 K (x = 1) and 2.65 K (x = 0.8), respectively. The specific heat jump is equal to 1.45 (x = 1) and 1.52 (x = 0.8), close to the expected value of 1.43 for the BCS superconductor in the weak coupling limit. The high-pressure resistance measurements show that a robust superconductivity against high physical pressure in Ti0.2Zr0.2Nb0.2Mo0.2Ta0.2C, with a slight Tc variation of 0.3 K within 82.5 GPa. Furthermore, the first-principles calculations indicate that the Dirac-like point exists in the electronic band structures of Ti0.2Zr0.2Nb0.2Mo0.2Ta0.2C, which is potentially a topological superconductor. The Dirac-like point is mainly contributed by the d orbitals of transition metals M and the p orbitals of C. The high-entropy ceramics provide an excellent platform for the fabrication of novel quantum devices, and our study may spark significant future physics investigations in this intriguing material.
2310.14271v1
2024-03-25
In situ growth of hydrophilic nickel-cobalt layered double hydroxides nanosheets on biomass waste-derived porous carbon for high-performance hybrid supercapacitors
Rational design and cost-effective fabrication of layered double hydroxides (LDHs) nanosheets with extraordinary electrochemical performance is a key challenge for hybrid supercapacitors (HSCs). Herein, we report a facile in situ growth methodology to eco-friendly synthesize hydrophilic NiCo-LDHs nanosheets on biomass waste-derived porous carbon (BC) for robust high-performance HSC cathode. The in situ growth process under ultrasonication realizes the rational arrangement of NiCo-LDHs nanosheets on the surface of BC, which effectively increases the specific surface area, promotes the electronic conductivity and enhances the wettability of NiCo-LDHs nanosheets without affecting their thickness values. With the beneficial effects of ultrathin thickness of LDHs nanosheets (6.20 nm), large specific surface area (2324.1 m2 g-1), low charge transfer resistance (1.65 ohm), and high wettability with electrolyte (34-35 degree), the obtained Ni2Co1-LDHs/BC50 electrode possesses an ultra-high specific capacitance of 2390 F g-1 (956 C g-1) at 1 A g-1, which is superior to most reported values. Furthermore, an assembled Ni2Co1-LDHs/BC50//YP-80F HSC delivers a maximum specific energy of 52.47 Wh kg-1 at 375 W kg-1, and maintains a high capacitance retention of 75.9% even after 4000 cycles. This work provides a facile approach to fabricate LDHs nanosheets based cathode materials for high-performance HSCs.
2403.16506v1
1997-01-08
Coupling between phonons and intrinsic Josephson oscillations in cuprate superconductors
The recently reported subgap structures observed in the current-voltage characteristic of intrinsic Josephson junctions in the high-T_c superconductors Tl_2Ba_2Ca_2Cu_3O_{10+\delta} and Bi_2Sr_2CaCu_2O_{8+\delta} are explained by the coupling between c-axis phonons and Josephson oscillations. A model is developed where c-axis lattice vibrations between adjacent superconducting multilayers are excited by the Josephson oscillations in a resistive junction. The voltages of the lowest structures correspond well to the frequencies of longitudinal c-axis phonons with large oscillator strength in the two materials, providing a new measurement technique for this quantity.
9701049v2
1997-07-17
Anomalous magnetotransport in wide quantum wells
We present magneto transport experiments of quasi 3D PbTe wide quantum wells. A plateau-like structure in the Hall resistance is observed, which corresponds to the Shubnikov de Haas oscillations in the same manner as known from the quantum Hall effect. The onsets of plateaux in Rxy do not correspond to 2D filling factors but coincide with the occupation of 3D (bulk-) Landau levels. At the same time a non-local signal is observed which corresponds to the structure in Rxx and Rxy and fulfils exactly the Onsager-Casimir relation (Rij,kl(B) = Rkl,ij(-B)). We explain the behaviour in terms of edge channel transport which is controlled by a permanent backscattering across a system of "percolative EC - loops" in the bulk region. Long range potential fluctuations with an amplitude of the order of the subband splitting are explained to play an essential role in this electron system.
9707173v1
1997-07-18
Edge Channel Dominated Magnetotransport in PbTe Wide Parabolic Quantum Wells
In PbTe wide parabolic quantum wells (WPQW) a plateau-like structure is observed in the Hall resistance, which corresponds to the Shubnikov-de Haas oscillations in the same manner as known from the quantum Hall effect. At the same time a non-local signal is observed which corresponds to the structure in Rxx and Rxy. We find a striking correspondence between a standard quantum Hall system and this quasi 3D WPQW system.
9707188v1
1997-10-28
Investigation of acceptor levels and hole scattering mechanisms in p-gallium selenide by means of transport measurements under pressure
The effect of pressure on acceptor levels and hole scattering mechanisms in p-GaSe is investigated through Hall effect and resistivity measurements under quasi-hydrostatic conditions up to 4 GPa. The pressure dependence of the hole concentration is interpreted through a carrier statistics equation with a single (nitrogen) or double (tin) acceptor whose ionization energies decrease under pressure due to the dielectric constant increase. The pressure effect on the hole mobility is also accounted for by considering the pressure dependencies of both the phonon frequencies and the hole-phonon coupling constants involved in the scattering rates.
9710296v1
1998-12-24
Electron Correlations in Molecular Systems
A short review of correlated electrons in molecular systems has been performed. Main attention has been focussed on ET salts, which are the d=2 systems. They show the Mott transition in high temperatures and the transition from the antiferromagnetic to the superconducting phase in low temperatures, under a (chemical) pressure. Physical properties (the electrical resistivity, the specific heat, the magnetic susceptibility, the photoemission spectra, the optical conductivity) of ET salts have been compared with those ones in other strongly correlated systems. The optical conductivity is described in the framework of the Hubbard model, with a low frequency peak as an evidence for the Abrikosov-Suhl resonance.
9812392v1
1998-12-30
Giant transverse magnetoresistance in an asymmetric system of three GaAs/AlGaAs quantum wells in a strong magnetic field at room temperature
The giant transverse magnetoresistance is observed in the case of photoinduced nonequilibrium carriers in an asymmetric undoped system of three GaAs/AlGaAs quantum wells at room temperature. In a magnetic field of 75 kOe, the resistance of nanostructure being studied increases by a factor of 1.85. The magnetoresistance depends quadratically on the magnetic field in low fields and tends to saturation in high fields. This phenomenon is attributed to the rearrangement of the electron wave function in magnetic field. Using the fact that the incoherent part of the scattering probability for electron scattering on impurities and bulk defects is proportional to the integral of the forth power of the envelope wave function, the calculated field dependence of the magnetoresistance is shown to be similar to that observed experimentally.
9812426v1
1999-03-03
Non linear flux flow in TiN superconducting thin film
We have studied the superconducting behavior of 100 nm Titanium Nitride (TiN) thin film in a perpendicular magnetic field. We found a zero field transition temperature of 4.6 K and a slope in the H-T plane of -0.745 T/K. At 4.2 K, we have performed careful transport measurements by measuring both the differential resistivity and voltage as a function of a DC current. Our results are analyzed in the framework of linear and non linear flux flow behavior. In particular, we have observed an electronic instability at high vortex velocities and from its dependence with respect to the applied magnetic field, we can exctract the inelastic scattering time and diffusion length of the quasiparticles.
9903060v2
1999-08-26
Destruction of the Mott Insulating Ground State of Ca_2RuO_4 by a Structural Transition
We report a first-order phase transition at T_M=357 K in single crystal Ca_2RuO_4, an isomorph to the superconductor Sr_2RuO_4. The discontinuous decrease in electrical resistivity signals the near destruction of the Mott insulating phase and is triggered by a structural transition from the low temperature orthorhombic to a high temperature tetragonal phase. The magnetic susceptibility, which is temperature dependent but not Curie-like decreases abruptly at TM and becomes less temperature dependent. Unlike most insulator to metal transitions, the system is not magnetically ordered in either phase, though the Mott insulator phase is antiferromagnetic below T_N=110 K.
9908390v1
1999-08-29
Anomalous microwave response of high-temperature superconducting thin-film microstrip resonator in weak dc magnetic fields
We have studied an anomalous microwave (mw) response of superconducting YBa_{2}Cu_{3}O_{7-delta} (YBCO) microstrip resonators in the presence of a weak dc magnetic field, H_{dc}. The surface resistance (R_{s}) and reactance (X_{s}) show a correlated non-monotonic behaviour as a function of H_{dc}. R_{s} and X_{s} were found to initially decrease with elevated H_{dc} and then increase after H_{dc} reaches a crossover field, H_{c}, which is independent of the amplitude and frequency of the input mw signal within the measurements. The frequency dependence of R_{s} is almost linear at fixed H_{dc} with different magnitudes (<H_{c}, =H_{c} and >H_{c}). The impedance plane analysis demonstrates that r_{H}, which is defined as the ratio of the change in R_{s}(H_{dc}) and that in X_{s}(H_{dc}), is about 0.6 at H_{dc}<H_{c} and 0.1 at H_{dc}>H_{c}. The H_{dc} dependence of the surface impedance is qualitatively independent of the orientation of H_{dc}.
9908429v1
2000-05-11
Magnetic Field resulting from non-linear electrical transport in single crystals of charge-ordered Pr$_{0.63}$ Ca$_{0.37}$ MnO$_{3}$}
In this letter we report that the current induced destabilization of the charge ordered (CO) state in a rare-earth manganite gives rise to regions with ferromagnetic correlation. We did this experiment by measurement of the I-V curves in single crystal of the CO system Pr$_{0.63}$Ca$_{0.37}$MnO$_{3}$ and simultanously measuring the magnetization of the current carrying conductor using a high T$_c$ SQUID working at T = 77K. We have found that the current induced destabilization of the CO state leads to a regime of negative differential resistance which leads to a small enhancement of the magnetization of the sample, indicating ferromagnetically aligned moments.
0005194v1
2000-06-22
High field magnetotransport in composite conductors: the effective medium approximation revisited
The self consistent effective medium approximation (SEMA) is used to study three-dimensional random conducting composites under the influence of a strong magnetic field {\bf B}, in the case where all constituents exhibit isotropic response. Asymptotic analysis is used to obtain almost closed form results for the strong field magnetoresistance and Hall resistance in various types of two- and three-constituent isotropic mixtures for the entire range of compositions. Numerical solutions of the SEMA equations are also obtained, in some cases, and compared with those results. In two-constituent free-electron-metal/perfect-insulator mixtures, the magnetoresistance is asymptotically proportional to $|{\bf B}|$ at {\em all concentrations above the percolation threshold}. In three-constituent metal/insulator/superconductor mixtures a line of critical points is found, where the strong field magnetoresistance switches abruptly from saturating to non-saturating dependence on $|{\bf B}|$, at a certain value of the insulator-to-superconductor concentration ratio. This transition appears to be related to the phenomenon of anisotropic percolation.
0006351v1
2000-08-02
The Zeno effect and an inter-layer pairing mechanism for high-temperature superconductivity in layered materials
Quantum Zeno Effect (QZE) is the suppression of the inter-subspace transition by a relatively fast intra-subspace decoherence. Earlier, we had proposed a QZE-based mechanism for the temperature-dependent normal-state c-axis resistivity of the layered high-T$_c$ cuprate superconductors in which the single-particle inter-layer tunneling is blocked by the strong intra-layer decoherence (entanglement). We now argue that while the single-particle inter-layer tunneling is thus blocked, the tunneling of the bosonic BCS-like pairs must remain unblocked inasmuch as a BCS pairing condensate is an eigenstate of the pair annihilation operator. This pair tunneling stabilizes
0008023v1
2000-12-14
Electronic Transmission Through Metallic Nanowires: Generalized Scattering Matrix Approach
An easy to implement and powerful method for the solution of 3D scattering problems that can be well described by Helmholtz equation is presented. The matrix algebra used provides excellent stability versus the number of junctions as well as great computational speed. The matrix truncation method yields an easy single-parameter convergence procedure. Subsequently, some aspects of the electronic transport through metal nanowires are studied by the use of Landauer's scattering approach to the conductance. We predict the existence of current vortex-rings patterns due to sharp enough narrow-wide connections in atomic size point contacts. Longitudinal resonances between scattering centers provide a simple physical picture for the understanding of negative differential resistance in ideal monoatomic contacts. Relatively long nanowires with high geometrical perfection -like those recently observed by Transmission Electron Microscopy- are modelled exhibiting resonant tunnelling and total reflection at given incident energy intervals.
0012250v1
2001-03-16
Giant Magnetoresistance by Exchange Springs in DyFe$_2$/YFe$_2$ Superlattices
Magnetization and magnetoresistance measurements are reported for antiferromagnetically coupled DyFe$_2$/YFe$_2$ multilayers in fields up to 23 T. We demonstrate that the formation of short exchange springs (~ 2 nm) in the magnetically soft YFe$_2$ layers results in a giant magneto-resistance as high as 32% in the spring region. It is shown that both the magnitude of the effect, and its dependence on magnetic field, are in good agreement with the theory of Levy and Zhang for giant magnetoresistance due to domain wall like structures.
0103354v1
2001-04-05
Fractal Nature and Scaling Exponent of Non-Drude Currents in Non-Fermi Liquids
In many oxides of the perovskite and pseudoperovskite families there are phase transitions between insulating and normal metallic (Fermi liquid) phases that are separated by an intermediate phase that is often called a non-Fermi liquid (NFL). The dc resistivity of the intermediate or NFL phase often exhibits a T temperature dependence, in contrast to the T2 dependence expected from a bad normal metal. The same alloys exhibit a non-Drude (ND) w2alpha frequency dependence, with alpha ~ 0.5, in contrast to the Drude dependence w2 characteristic of samples with the T2 behavior. Various attempts have been made to modify the algebra of continuum Fermi liquid theory (FLT) to derive the ND exponent alpha, but these have been based on artifices designed to explain only this one parameter. The discrete filamentary model has been used to calculate many properties of high temperature superconductors, and to explain the asymmetric nature of the intermediate phase. Here it is used to derive a by the same rules previously used for several other discrete relaxation calculations that are in excellent agreement with other quite different experiments. The results are: (cubic) perovskites, alpha = 0.45, and planar conductivity of bilayered pseudoperovskites, alpha = 0.70. The corresponding experimental values are (0.4, 0.5) and 0.7.
0104095v1
2001-04-06
Evidence for high inter-granular current flow in single-phase polycrystalline MgB2 superconductor
The distribution of magnetic field in single-phase polycrystalline bulk MgB2 has been measured using a Magneto-Optical (MO) technique for an external magnetic field applied perpendicular to the sample surface. The MO studies indicate that an inter-granular current network is readily established in this material and the current is not limited by weak-linked grain boundaries. The grain boundaries are observed to resist preferential magnetic field penetration, with the inter-grain mechanism dominating the current flow in the sample at temperatures up to 30K. The results provide clear evidence that the intra-granular current flow is isotropic. A critical current density of ~10^4 Acm-2 was estimated at 30K in a field of 150mT from the MO measurements. These results provide further evidence of the considerable potential for MgB2 for engineering applications.
0104114v1
2002-04-17
Epitaxial Growth of La$_{1/3}$Sr$_{2/3}$FeO$_3$ thin films by laser ablation
We report on the synthesis of high quality La$_{1/3}$Sr$_{2/3}$FeO$_3$ (LSFO) thin films using the pulsed laser deposition technique on both SrTiO$_3$ (STO) and LaAlO$_3$ (LAO) substrates (100)-oriented. From X-Ray diffraction (XRD) studies, we find that the films have an out-of-plane lattice parameter around 0.3865nm, almost independent of the substrate (i.e. the nature of the strains). The transport properties reveal that, while LSFO films deposited on STO exhibit an anomaly in the resistivity vs temperature at 180K (corresponding to the charge-ordered transition and associated with a transition from a paramagnetic to an antiferromagnetic state), the films grown on LAO display a very small magnetoresistance behavior and present an hysteresis around 270K under the application of a 4T magnetic field. The changes in transport properties between both substrates are discussed and compared with the corresponding single crystals.
0204370v1
2002-05-24
The Hall effect and hole densities in high Tc GaMnAs thin films
By studying the Hall effect in a series of low resistivity Ga1-xMnxAs samples, accurate values for the hole density p, Mn concentration x, and Curie temperature Tc are obtained over the range 0.015=<x=<0.08. The hole density corresponds to 90% of the Mn concentration at low x, and has a maximum value of 1.0x10-27 m-3 when Tc=125K for x=0.06. This data allows the first meaningful comparison of mean field predicted Curie temperatures with experiment over a wide range of x. The theory is in qualitative agreement with experiment, but overestimates Tc at large x and underestimates TC at low x.
0205517v3
2002-06-19
Transport and magnetic properties of LT annealed Ga1-xMnxAs
We present the results of low temperature (LT) annealing studies of Ga1-xMnxAs epilayers grown by low temperature molecular beam epitaxy in a wide range of Mn concentrations (0.01<x<0.084). Transport measurements in low and high magnetic fields as well as SQUID measurements were performed on a wide range of samples, serving to establish optimal conditions of annealing. Optimal annealing procedure succeeded in the Curie temperatures higher than 110K. The highest value of Curie temperature estimated from the maximum in the temperature dependence of zero-field resistivity (Tr) was 127K. It is generally observed that annealing leads to large changes in the magnetic and transport properties of GaMnAs in the very narrow range of annealing temperature close to the growth temperature.
0206371v1
2002-07-08
Magnetic behavior of single crystalline Ho$_2$PdSi$_3$
The magnetic behavior of single-crystal Ho$_2$PdSi$_3$, crystallizing in an AlB$_2$-derived hexagonal structure, is investigated by magnetic susceptibility ($\chi$) and electrical resistivity ($\rho$) measurements along two directions. There is no dramatic anisotropy in the high temperature Curie-Weiss parameter or in the $\rho$ and isothermal magnetization data, though there is a noticeable anisotropy in the magnitude of $\rho$ between two perpendicular orientations. The degree of anisotropy is overall less prominent than in the Gd (which is an S-state ion!) and Tb analogues. A point of emphasis is that this compound undergoes long range magnetic ordering below 8 K as in the case of analogous Gd and Dy compounds. Considering this fact for these compounds with well-localised f-orbital, the spin glass freezing noted for isomorphous U compounds in the recent literature could be attributed to the role of the f-ligand hybridization, rather than just Pd-Si disorder.
0207199v1
2002-10-22
Unipolar transport and shot noise in metal-semiconductor-metal structures
We carry out a self-consistent analytical theory of unipolar current and noise properties of metal-semiconductor-metal structures made of highly resistive semiconductors in the presence of an applied bias of arbitrary strength. By including the effects of the diffusion current we succeed to study the whole range of carrier injection conditions going from low level injection, where the structure behaves as a linear resistor, to high level injection, where the structure behaves as a space charge limited diode. We show that these structures display shot noise at the highest voltages. Remarkably the crossover from Nyquist noise to shot noise exhibits a complicate behavior with increasing current where an initial square root dependence (double thermal noise) is followed by a cubic power law.
0210484v1
2002-11-14
Synthesis and Properties of YbB2
We report temperature and field dependent measurements of the magnetic susceptibility, specific heat and resistivity of sintered YbB2 pellets, prepared via two distinct reaction routes, utilizing different temperatures, pressures and sintering times. Sample behavior is affected by the preparation procedure, as a consequence of different secondary phases, most of which were identified via x-ray diffraction. These experiments show that YbB2 is a metal with the Yb atoms in or very close to their 3+ state. YbB2 appears to order anti-ferromagnetically at TN ~ 5.6 K, which can be considered a relatively high ordering temperature for an ytterbium-based intermetallic compound.
0211288v1
2003-07-07
Mn Interstitial Diffusion in (Ga,Mn)As
We present a combined theoretical and experimental study of the ferromagnetic semiconductor (Ga,Mn)As which explains the remarkably large changes observed on low temperature annealing. Careful control of the annealing conditions allows us to obtain samples with ferromagnetic transition temperatures up to 159 K. Ab initio calculations, and resistivity measurements during annealing, show that the observed changes are due to out-diffusion of Mn interstitials towards the surface, governed by an energy barrier of about 0.7-0.8 eV. The Mn interstitial is a double donor resulting in compensation of charge carriers and suppression of ferromagnetism. Electric fields induced by high concentrations of substitutional Mn acceptors have a significant effect on the diffusion.
0307140v1
2003-07-09
Direct Observation of Long-Term Durability of Superconductivity in YBa$_2$Cu$_3$O$_7$-Ag$_2$O Composites
We report direct observation of long-term durability of superconductivity of several YBa$_2$Cu$_3$O$_7$-Ag$_2$O composites that were first prepared and studied almost 14 years ago [J. J. Lin {\it et al}., Jpn. J. Appl. Phys. {\bf 29}, 497 (1990)]. Remeasurements performed recently on both resistances and magnetizations indicate a sharp critical transition temperature at 91 K. We also find that such long-term environmental stability of high-temperature superconductivity can only be achieved in YBa$_2$Cu$_3$O$_7$ with Ag$_2$O addition, but not with pure Ag addition.
0307187v1
2003-07-18
Probing quasiparticle dynamics in Bi2Sr2CaCu2O(8+delta) with a driven Josephson vortex lattice
We show that the flux-flow transport of the Josephson vortex lattice (JVL) in layered high-temperature superconductors provides a convenient probe for both components of quasiparticle conductivity, $\sigma_{c}$ and $\sigma_{ab}$. We found that the JVL flux-flow resistivity, $\rho_{ff}$, in a wide range of magnetic fields is mainly determined by the in-plane dissipation. In the dense lattice regime ($B>1$ T) $\rho_{ff}(B)$ dependence is well fitted by the theoretical formula for that limit. That allows us to independently extract from the experimental data the values of $\sigma_{c}$ and of the ratio $\sigma _{ab}/(\sigma_{c}\gamma ^{4})$. The extracted temperature dependence $\sigma _{ab}(T)$ is consistent with microwave data. The shape of the current-voltage characteristics is also sensitive to the frequency dependence of $\sigma_{ab}$ and that allows us to estimate the quasiparticle relaxation time and relate it to the impurity bandwidth using data obtained for the same crystal.
0307450v1
2003-09-02
The enhancement of phase separation aspect in electron doped manganite Ca0.8Sm0.16Nd0.04MnO3
The complex lanthanide doping of electron manganites results in enhancement of various phase separation effects in physical properties of these compounds. Selecting Ca0.8Sm0.16Nd0.04MnO3 as a model case we show that the first order structural phase transition from paramagnetic semi-metallic phase into anti-ferromagnetic semi-metallic phase at TS ~ 158 +- 4 K is marked by an abrupt decrease in magnetization, a step like anomaly DL/L = 10-4 in thermal expansion and large latent heat DQ = 610 J/mol. In a certain temperature range below TS, the high field magnetization exhibits hysteretic metamagnetic behavior due to field-induced first order transformation. ac-susceptibility, magnetization and resistivity data suggest rather a non-uniform state in Ca0.8Sm0.16Nd0.04MnO3 at low temperatures. The metal - insulator transition occurs at TMI ~112 +- 3 K, accompanied by a step-like increase in magnetization. These features could be ascribed to "sponging" of electrons from neighboring anti-ferromagnetic matrix by clusters undergoing the ferromagnetic ordering.
0309065v1