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2007-09-12
Reducing the Possibility of Subjective Error in the Determination of the Structure-Function-Based Effective Thermal Conductivity of Boards
The thermal response function given to a unit-step dissipation accurately characterizes the thermal system. Instead of the thermal response function the so-called structure function describing three-dimensional as the equivalent model of one-dimensional heat-spreading, created from the thermal response function with the help of complex mathematical procedures, is often used. Using the structure function the partial thermal capacity and partial heat resistance of certain elements of the thermal system can be identified. If the geometrical measurements of a thermal system of simple geometry and homogeneous material (such as a homogeneous rod or board, etc.) are known, the coefficient of thermal conductivity of the material in question can be determined from two points of the structure function at 2-5 per cent of accuracy. In this paper a method is presented which applies a wide range/section instead of two points of the cumulative structure function to determine the thermal coefficient, thus reducing the subjective error deriving from the selection of the two points. The above method is presented and illustrated in simulated as well as measured thermal transient responses.
0709.1863v1
2008-01-22
Phase coherent transport in (Ga,Mn)As
Quantum interference effects and resulting quantum corrections of the conductivity have been intensively studied in disordered conductors over the last decades. The knowledge of phase coherence lengths and underlying dephasing mechanisms are crucial to understand quantum corrections to the resistivity in the different material systems. Due to the internal magnetic field and the associated breaking of time-reversal symmetry quantum interference effects in ferromagnetic materials have been scarcely explored. Below we describe the investigation of phase coherent transport phenomena in the newly discovered ferromagnetic semiconductor (Ga,Mn)As. We explore universal conductance fluctuations in mesoscopic (Ga,Mn)As wires and rings, the Aharonov-Bohm effect in nanoscale rings and weak localization in arrays of wires, made of the ferromagnetic semiconductor material. The experiments allow to probe the phase coherence length L_phi and the spin flip length L_SO as well as the temperature dependence of dephasing.
0801.3363v1
2008-08-03
Use of a nanoindentation fatigue test to characterize the ductile-brittle transition
When considering grinding of minerals, scaling effect induces competition between plastic deformation and fracture in brittle solids. The competition can be sketched by a critical size of the material, which characterizes the ductile-brittle transition. A first approach using Vickers indentation gives a good approximation of the critical size through an extrapolation from the macroscopic to the microscopic scales. Nanoindentation tests confirm this experimental value. According to the grain size compared to the indent size, it can reasonably be said that the mode of damage is deformation-induced intragranular microfracture. This technique also enables to perform cyclic indentations to examine calcite fatigue resistance. Repeated loadings with a nanoindenter on CaCO3 polycrystalline samples produce cumulative mechanical damage. It is also shown that the transition between ductile and brittle behaviour depends on the number of indentation cycles. The ductile domain can be reduced when the material is exposed to a fatigue process.
0808.0329v1
2008-10-02
Metallic conduction at organic charge-transfer interfaces
The electronic properties of interfaces between two different solids can differ strikingly from those of the constituent materials. For instance, metallic conductivity, and even superconductivity, have been recently discovered at interfaces formed by insulating transition metal oxides. Here we investigate interfaces between crystals of conjugated organic molecules, which are large gap undoped semiconductors, i.e. essentially insulators. We find that highly conducting interfaces can be realized with resistivity ranging from 1 to 30 kOhm square, and that, for the best samples, the temperature dependence of the conductivity is metallic. The observed electrical conduction originates from a large transfer of charge between the two crystals that takes place at the interface, on a molecular scale. As the interface assembly process is simple and can be applied to crystals of virtually any conjugated molecule, the conducting interfaces described here represent the first examples of a new class of electronic systems.
0810.0361v1
2009-11-13
Internal relaxation time in immersed particulate materials
We study the dynamics of the solid to liquid transition for a model material made of elastic particles immersed in a viscous fluid. The interaction between particle surfaces includes their viscous lubrication, a sharp repulsion when they get closer than a tuned steric length and their elastic deflection induced by those two forces. We use Soft Dynamics to simulate the dynamics of this material when it experiences a step increase in the shear stress and a constant normal stress. We observe a long creep phase before a substantial flow eventually establishes. We find that the typical creep time relies on an internal relaxation process, namely the separation of two particles driven by the applied stress and resisted by the viscous friction. This mechanism should be relevant for granular pastes, living cells, emulsions and wet foams.
0911.2531v1
2010-02-18
The influence of Ga$^+$-irradiation on the transport properties of mesoscopic conducting thin films
We studied the influence of 30keV Ga$^+$-ions -- commonly used in focused ion beam (FIB) devices -- on the transport properties of thin crystalline graphite flake, La$_{0.7}$Ca$_{0.3}$MnO$_3$ and Co thin films. The changes of the electrical resistance were measured in-situ during irradiation and also the temperature and magnetic field dependence before and after irradiation. Our results show that the transport properties of these materials strongly change at Ga$^+$ fluences much below those used for patterning and ion beam induced deposition (IBID), limiting seriously the use of FIB when the intrinsic properties of the materials of interest are of importance. We present a method that can be used to protect the sample as well as to produce selectively irradiation-induced changes.
1002.3565v1
2010-09-24
Photoemission induced gating of topological insulator
The recently discovered topological insulators exhibit topologically protected metallic surface states which are interesting from the fundamental point of view and could be useful for various applications if an appropriate electronic gating can be realized. Our photoemission study of Cu intercalated Bi2Se3 shows that the surface states occupancy in this material can be tuned by changing the photon energy and understood as a photoemission induced gating effect. Our finding provides an effective tool to investigate the new physics coming from the topological surface states and suggests the intercalation as a recipe for synthesis of the material suitable for electronic applications.
1009.4855v2
2011-08-23
Single-Crystal and Powder Neutron Diffraction Study of FeXMn1-XS Solid Solutions
FeXMn1-XS (0 <x< 0.3) synthesized on the basis of {\alpha}-MnS are the novel Mott-type substances with the rock salt structure. Neutron diffraction study shows that the shift of the Neel temperature of these materials from 150 (x = 0) to 200 K (x = 0.29) under the action of chemical pressure (x) is accompanied by a decrease in the cubic NaCl lattice parameters. The structural transition with a change in crystal symmetry and a decrease in resistance before the magnetic transition at x = 0.25 is found. Therefore, FeXMn1-XS are interesting materials for both fundamental study of the interrelation between the magnetic, electrical, and structural properties in systems with the strong electron correlations of a MnO-type and application.
1108.4537v2
2012-02-11
Temperature dependence of the conductivity of graphene on boron nitride
The substrate material of monolayer graphene influences the charge carrier mobility by various mechanisms. At room temperature, the scattering of conduction electrons by phonon modes localized at the substrate surface can severely limit the charge carrier mobility. We here show that for substrates made of the piezoelectric hexagonal boron nitride (hBN), in comparison to the widely used SiO$_2$, this mechanism of remote phonon scattering is --at room temperature-- weaker by almost an order of magnitude, and causes a resistivity of approximately 3\,$\Omega$. This makes hBN an excellent candidate material for future graphene based electronic devices operating at room temperature.
1202.2440v2
2012-10-15
Theory of Charge Order and Heavy-Electron Formation in the Mixed-Valence Compound KNi$_2$Se$_2$
The material KNi$_2$Se$_2$ has recently been shown to possess a number of striking physical properties, many of which are apparently related to the mixed valency of this system, in which there is on average one quasi-localized electron per every two Ni sites. Remarkably, the material exhibits a charge density wave (CDW) phase that disappears upon cooling, giving way to a low-temperature coherent phase characterized by an enhanced electron mass, reduced resistivity, and an enlarged unit cell free of structural distortion. Starting from an extended periodic Anderson model and using the slave-boson formulation, we develop a model for this system and study its properties within mean-field theory. We find a reentrant first-order transition from a CDW phase, in which the localized moments form singlet dimers, to a heavy Fermi liquid phase as temperature is lowered. The magnetic susceptibility is Pauli-like in both the high- and low-temperature regions, illustrating the lack of a single-ion Kondo regime such as that usually found in heavy-fermion materials.
1210.4041v3
2012-10-24
Magnetic phase diagram of CePt3B1-xSix
We present a study of the main bulk properties (susceptibility, magnetization, resistivity and specific heat) of CePt_3B_(1-x)Si-x, an alloying system that crystallizes in a noncentrosymmetric lattice, and derive the magnetic phase diagram. The materials at the end point of the alloying series have previously been studied, with CePt_3B established as a material with two different magnetic phases at low temperatures (antiferromagnetic below T_N = 7.8 K, weakly ferromagnetic below T_C ~ 5 K), while CePt3Si is a heavy fermion superconductor (T_c = 0.75 K) coexisting with antiferromagnetism (T_N = 2.2 K). From our experiments we conclude that the magnetic phase diagram is divided into two regions. In the region of low Si content (up to x ~ 0.7) the material properties resemble those of CePt3B. Upon increasing the Si concentration further the magnetic ground state continuously transforms into that of CePt3Si. In essence, we argue that CePt_3B can be understood as a low pressure variant of CePt3Si.
1210.6489v3
2013-04-26
Preparation and characterization of Bismaleimide resin/titania nanocomposites via sol-gel process
Bismaleimide (BMI) resin/ titania nanocomposites were synthesized from allylated-phenolic modified bismaleimide resin and TiO2 via the sol-gel process of tetrabutyltitanate (Ti(OnBu)4, TBT). These nanocomposite materials were characterized by FT-IR, XRD, FE-SEM, TGA and DMA. It was found that the nano-scale TiO2 particles were formed in the AP-BMI resin matrix, and the average primary particle size of the dispersed phase in the nanocomposites was less than 100nm, but the particle aggregates with bigger size existed. Obvious improvements of glass transition temperature and heat resistance properties of the AP-BMI resins were achieved by the introduction of nano-sized TiO2 inorganic phase, and the modulus of the material was also improved.
1304.7082v1
2013-10-05
Engineered spin-valve type magnetoresistance in Fe$_3$O$_4$-CoFe$_2$O$_4$ core-shell nanoparticles
Naturally occurring spin-valve-type magnetoresistance (SVMR), recently observed in Sr2FeMoO6 samples, suggests the possibility of decoupling the maximal resistance from the coercivity of the sample. Here we present the evidence that SVMR can be engineered in specifically designed and fabricated core-shell nanoparticle systems, realized here in terms of soft magnetic Fe3O4 as the core and hard magnetic insulator CoFe2O4 as the shell materials. We show that this provides a magnetically switchable tunnel barrier that controls the magnetoresistance of the system, instead of the magnetic properties of the magnetic grain material, Fe3O4, and thus establishing the feasibility of engineered SVMR structures.
1310.1469v1
2013-10-23
A simple method to characterize the electrical and mechanical properties of micro-fibers
A procedure to characterize the electrical and mechanical properties of micro-fibers is presented here. As the required equipment can be found in many teaching laboratories, it can be carried out by physics and mechanical/electrical engineering students. The electrical resistivity, mass density and Young's modulus of carbon micro-fibers have been determined using this procedure, obtaining values in very good agreement with the reference values. The Young's modulus has been obtained by measuring the resonance frequency of carbon fiber based cantilevers. In this way, one can avoid common approaches based on tensile or bending tests which are difficult to implement for microscale materials. Despite the simplicity of the experiments proposed here, they can be used to trigger in the students interest on the electrical and mechanical properties of microscale materials.
1310.6134v1
2014-07-31
Quantum Criticality Based on Large Ising Spins: YbCo$_2$Ge$_4$ with New 1-2-4 Structure Type
We present a new type of quantum critical material YbCo$_2$Ge$_4$, having the largest quantum-critical pseudospin size ever. The YbCo$_2$Ge$_4$-type structure is new, forms in the orthorhombic $Cmcm$ system, and is related to the well-known ThCr$_2$Si$_2$ structure. Heavy rare earth (Tm,Yb,Lu, or Y) members are also possible to be grown. YbCo$_2$Ge$_4$ possesses the Ising-type ground-state doublet, namely the simplest ones of uniaxially up or down, $|\pm \sim 7/2\rangle$. It is clearly manifested through comprehensive resistivity, magnetization, specific heat, and NQR/NMR experiments. Large pseudospin state usually tends to order in simple magnetisms, or hard to be screened by Kondo effect. Therefore, the discovery of the quantum criticality of the fluctuating large spins opens a new door to new-material search and theoretical studies.
1407.8274v1
2014-09-19
Analysis of the internal heat losses in a thermoelectric generator
A 3D thermoelectric numerical model is used to investigate different internal heat loss mechanisms for a thermoelectric generator with bismuth telluride p- and n-legs. The model considers all thermoelectric effects, temperature dependent material parameters and simultaneous convective, conductive and radiative heat losses, including surface to surface radiation. For radiative heat losses it is shown that for the temperatures considered here, surface to ambient radiation is a good approximation of the heat loss. For conductive heat transfer the module efficiency is shown to be comparable to the case of radiative losses. Finally, heat losses due to internal natural convection in the module is shown to be negligible for the millimetre sized modules considered here. The combined case of radiative and conductive heat transfer resulted in the lowest efficiency. The optimized load resistance is found to decrease for increased heat loss. The leg dimensions are varied for all heat losses cases and it is shown that the ideal way to construct a TEG module with minimal heat losses and maximum efficiency is to either use a good insulating material between the legs or evacuate the module completely, and use small and wide legs closely spaced.
1409.6743v1
2015-01-17
Superconductivity in the orthorhombic phase of thermoelectric CsPbxBi4-xTe6 with 0.3=<x=<1.0
Experimental measurements clearly reveal the presence of bulk superconductivity in the CsPbxBi4-xTe6 (0.3=<x=<1.0) materials, i.e. the first member of the thermoelectric series of Cs[PbmBi3Te5+m], these materials have the layered orthorhombic structure containing infinite anionic [PbBi3Te6]- slabs separated with Cs+ cations. Temperature dependences of electrical resistivity, magnetic susceptibility, and specific heat have consistently demonstrated that the superconducting transition in CsPb0.3Bi3.7Te6 occurs at Tc=3.1K, with a superconducting volume fraction close to 100% at 1.8 K. Structural study using aberration-corrected STEM/TEM reveals a rich variety of microstructural phenomena in correlation with the Pb-ordering and chemical inhomogeneity. The superconducting material CsPb0.3Bi3.7Te6 with the highest Tc shows a clear ordered structure with a modulation wave vector of q=a*/2+ c*/1.35 on the a-c plane. Our study evidently demonstrates that superconductivity deriving upon doping of narrow-gap semiconductor is a viable approach for exploration of novel superconductors.
1501.04184v1
2015-01-22
DFT+U simulation of the Ti${}_4$O${}_7$-TiO${}_2$ interface
The formation of conducting channels of Ti${}_4$O${}_7$ inside TiO${}_2$-based memristors is believed to be the origin for the change in electric resistivity of these devices. While the properties of the bulk materials are reasonably known, the interface between them has not been studied up to now mostly due to their different crystalline structures. In this work we present a way to match the interfaces between TiO${}_2$ and Ti${}_4$O${}_7$ and subsequently the band offset between these materials is obtained from density functional theory based calculations. The results show that while the valence band is located at the Ti${}_4$O${}_7$, the conduction band is found at the TiO${}_2$ structure, resulting into a type II interface. In this case, the Ti${}_4$O${}_7$ would act as a donor to the TiO${}_2$ matrix.
1501.05564v1
2015-02-09
A theory of finite deformation magneto-viscoelasticity
This paper deals with the mathematical modelling of large strain magneto-viscoelastic deformations. Energy dissipation is assumed to occur both due to the mechanical viscoelastic effects as well as the resistance offered by the material to magnetisation. Existence of internal damping mechanisms in the body is considered by decomposing the deformation gradient and the magnetic induction into `elastic' and `viscous' parts. Constitutive laws for material behaviour and evolution equations for the non-equilibrium fields are derived that agree with the laws of thermodynamics. To illustrate the theory the problems of stress relaxation, magnetic field relaxation, time dependent magnetic induction and strain are formulated and solved for a specific form of the constitutive law. The results, that show the effect of several modelling parameters on the deformation and magnetisation process, are illustrated graphically.
1502.02482v1
2015-08-06
Odd-parity magnetoresistance in pyrochlore iridate thin films with broken time-reversal symmetry
A new class of materials termed topological insulators have been intensively investigated due to their unique Dirac surface state carrying dissipationless edge spin currents. Recently, it has been theoretically proposed that the three dimensional analogue of this type of band structure, the Weyl Semimetal phase, is materialized in pyrochlore oxides with strong spin-orbit coupling, accompanied by all-in-all-out spin ordering. Here, we report on the fabrication and magnetotransport of Eu2Ir2O7 single crystalline thin films. We reveal that one of the two degenerate all-in-all-out domain structures, which are connected by time-reversal operation, can be selectively formed by the polarity of the cooling magnetic field. Once formed, the domain is robust against an oppositely polarised magnetic field, as evidenced by an unusual odd field dependent term in the magnetoresistance and an anomalous term in the Hall resistance. Our findings pave the way for exploring the predicted novel quantum transport phenomenon at the surfaces/interfaces or magnetic domain walls of pyrochlore iridates.
1508.01318v1
2015-09-04
Hall effect in the extremely large magnetoresistance semimetal WTe$_2$
We systematically measured the Hall effect in the extremely large magnetoresistance semimetal WTe$_2$. By carefully fitting the Hall resistivity to a two-band model, the temperature dependencies of the carrier density and mobility for both electron- and hole-type carriers were determined. We observed a sudden increase of the hole density below $\sim$160~K, which is likely associated with the temperature-induced Lifshitz transition reported by a previous photoemission study. In addition, a more pronounced reduction in electron density occurs below 50~K, giving rise to comparable electron and hole densities at low temperature. Our observations indicate a possible electronic structure change below 50~K, which might be the direct driving force of the electron-hole ``compensation'' and the extremely large magnetoresistance as well. Numerical simulations imply that this material is unlikely to be a perfectly compensated system.
1509.01463v2
2015-11-19
`Ferroelectric' Metals Reexamined: Fundamental Mechanisms and Design Considerations for New Materials
The recent observation of a ferroelectric-like structural transition in metallic LiOsO$_3$ has generated a flurry of interest in the properties of polar metals. Such materials are thought to be rare because free electrons screen out the long-range electrostatic forces that favor a polar structure with a dipole moment in every unit cell. In this work, we question whether long-range electrostatic forces are always the most important ingredient in driving polar distortions. We use crystal chemical models, in combination with first-principles Density Functional Theory calculations, to explore the mechanisms of inversion-symmetry breaking in LiOsO$_3$ and both insulating and electron-doped ATiO$_3$ perovskites, A = Ba, Sr, Ca. Although electrostatic forces do play a significant role in driving the polar instability of BaTiO$_3$ (which is suppressed under electron doping), the polar phases of CaTiO$_3$ and LiOsO$_3$ emerge through a mechanism driven by local bonding preferences and this mechanism is `resistant' to the presence of charge carriers. Hence, our results suggest that there is no fundamental incompatibility between metallicity and polar distortions. We use the insights gained from our calculations to suggest design principles for new polar metals and promising avenues for further research.
1511.06187v2
2016-01-12
Superconductivity in Tl_{0.6}Bi_{2}Te_{3} Derived from a Topological Insulator
Bulk superconductivity has been discovered in Tl_{0.6}Bi_{2}Te_{3}, which is derived from the topological insulator Bi2Te3. The superconducting volume fraction of up to 95% (determined from specific heat) with Tc of 2.28 K was observed. The carriers are p-type with the density of ~1.8 x 10^{20} cm^{-3}. Resistive transitions under magnetic fields point to an unconventional temperature dependence of the upper critical field B_{c2}. The crystal structure appears to be unchanged from Bi2Te3 with a shorter c-lattice parameter, which, together with the Rietveld analysis, suggests that Tl ions are incorporated but not intercalated. This material is an interesting candidate of a topological superconductor which may be realized by the strong spin-orbit coupling inherent to topological insulators.
1601.02877v1
2016-05-06
Intrinsic Negative Poisson's Ratio for Single-Layer Graphene
Negative Poisson's ratio (NPR) materials have drawn significant interest because the enhanced toughness, shear resistance and vibration absorption that typically are seen in auxetic materials may enable a range of novel applications. In this work, we report that single-layer graphene exhibits an intrinsic NPR, which is robust and independent of its size and temperature. The NPR arises due to the interplay between two intrinsic deformation pathways (one with positive Poisson's ratio, the other with NPR), which correspond to the bond stretching and angle bending interactions in graphene. We propose an energy-based deformation pathway criteria, which predicts that the pathway with NPR has lower energy and thus becomes the dominant deformation mode when graphene is stretched by a strain above 6%, resulting in the NPR phenomenon.
1605.01827v2
2016-03-24
Isotoxal star-shaped polygonal voids and rigid inclusions in nonuniform antiplane shear fields. Part II: Singularities, annihilation and invisibility
Notch stress intensity factors and stress intensity factors are obtained analytically for isotoxal star-shaped polygonal voids and rigid inclusions (and also for the corresponding limit cases of star-shaped cracks and stiffeners), when loaded through remote inhomogeneous (self-equilibrated, polynomial) antiplane shear stress in an infinite linear elastic matrix. Usually these solutions show stress singularities at the inclusion corners. It is shown that an infinite set of geometries and loading conditions exist for which not only the singularity is absent, but the stress vanishes ('annihilates') at the corners. Thus the material, which even without the inclusion corners would have a finite stress, remains unstressed at these points in spite of the applied remote load. Moreover, similar conditions are determined in which a star-shaped crack or stiffener leaves the ambient stress completely unperturbed, thus reaching a condition of 'quasi-static invisibility'. Stress annihilation and invisibility define optimal loading modes for the overall strength of a composite and are useful for designing ultra-resistant materials.
1605.04942v1
2016-10-30
Characteristics of Interlayer Tunneling Field Effect Transistors Computed by a "DFT-Bardeen" Method
Theoretical predictions are made for the current-voltage characteristics of two-dimensional heterojunction interlayer tunneling field-effect transistors (Thin-TFETs), focusing on the magnitude of the current that is achievable in such devices. A theory based on the Bardeen tunneling method is employed, using wavefunctions from first-principles density-functional theory. This method permits convenient incorporation of differing materials into the source and drain electrodes, i.e. with different crystal structures, lattice constants, and/or band structures. Large variations in the tunnel currents are found, depending on the particular two-dimensional materials used for the source and drain electrodes. Tunneling between states derived from the center (Gamma-point) of the Brillouin zone (BZ) is found, in general, to lead to larger current than for zone-edge (e.g. K-point) states. Differences, as large as an order of magnitude, between the present results and various prior predictions are discussed. Predicted values for the tunneling currents, including subthreshold swing, are compared with benchmark values for low-power digital applications. Contact resistance is considered and its effect on the tunneling currents is demonstrated.
1610.09695v1
2016-10-31
Signature of Hanle Precession in Trilayer MoS2: Theory and Experiment
Valley-spin coupling in transition-metal dichalcogenides (TMDs) can result in unusual spin transport behaviors under an external magnetic field. Nonlocal resistance measured from 2D materials such as TMDs via electrical Hanle experiments are predicted to exhibit nontrivial features, compared with results from conventional materials due to the presence of intervalley scattering as well as a strong internal spin-orbit field. Here, for the first time, we report the all-electrical injection and non-local detection of spin polarized carriers in trilayer MoS_2 films. We calculate the Hanle curves theoretically when the separation between spin injector and detector is much larger than spin diffusion length, \lamda_s. The experimentally observed curve matches the theoretically-predicted Hanle shape under the regime of slow intervalley scattering. The estimated spin life-time was found to be around 110 ps at 30 K.
1611.00059v1
2016-11-23
Electron interactions, spin-orbit coupling, intersite correlations in pyrochlore iridates
We perform combined density functional and dynamical mean-field calculations to study the pyrochlore iridates Lu$_2$Ir$_2$O$_7$, Y$_2$Ir$_2$O$_7$ and Eu$_2$Ir$_2$O$_7$. Both single-site and cluster dynamical mean-field calculations are performed and spin-orbit coupling is included. Paramagnetic metallic phases, antiferromagnetic metallic phases with tilted Weyl cones and antiferromagnetic insulating phases are found. The magnetic phases display all-in/all-out magnetic ordering, consistent with previous studies. Unusually for electronically three dimensional materials, the single-site dynamical mean-field approximation fails to reproduce qualitative material trends, predicting in particular that the paramagnetic phase properties of Y$_2$Ir$_2$O$_7$ and Eu$_2$Ir$_2$O$_7$ are almost identical, although in experiments the Y compound has a much higher resistance than the Eu compound. This qualitative failure is attributed to the importance of intersite magnetic correlations in the physics of these materials.
1611.07997v2
2017-02-27
Quantum critical scaling and fluctuations in Kondo lattice materials
We propose a new phenomenological framework for three classes of Kondo lattice materials that incorporates the interplay between the fluctuations associated with the antiferromagnetic quantum critical point and those produced by the hybridization quantum critical point that marks the end of local moment behavior. We show that these fluctuations give rise to two distinct regions of quantum critical scaling: hybridization fluctuations are responsible for the logarithmic scaling in the density of states of the heavy electron Kondo liquid that emerges below the coherence temperature T*; while the unconventional power law scaling in the resistivity that emerges at lower temperatures below T_QC may reflect the combined effects of hybridization and antiferromagnetic quantum critical fluctuations. Our framework is supported by experimental measurements on CeCoIn5, CeRhIn5 and other heavy electron materials.
1702.08132v2
2017-06-30
Two-Dimensional h-BN and MoS2 as Diffusion Barriers for Ultra-Scaled Copper Interconnects
Copper interconnects in modern integrated circuits require ultra-thin barriers to prevent intermixing of Cu with surrounding dielectric materials. Conventional barriers rely on metals like TaN, however their finite thickness reduces the cross-sectional area and significantly increases the resistivity of nanoscale interconnects. In this study, a new class of two-dimensional (2D) Cu diffusion barriers, hexagonal boron nitride (h-BN) and molybdenum disulfide (MoS2), is demonstrated for the first time. Using time-dependent dielectric breakdown measurements and scanning transmission electron microscopy coupled with energy dispersive X-ray spectroscopy and electron energy loss spectroscopy, these 2D materials are shown to be promising barrier solutions for ultra-scaled interconnect technology. The predicted lifetime of devices with directly deposited 2D barriers can achieve three orders of magnitude improvement compared to control devices without barriers.
1706.10178v1
2017-08-31
Nonmonotonic dependence of polymer glass mechanical response on chain bending stiffness
We investigate the mechanical properties of amorphous polymers by means of coarse-grained simulations and nonaffine lattice dynamics theory. A small increase of polymer chain bending stiffness leads first to softening of the material, while hardening happens only upon further strengthening of the backbones. This nonmonotonic variation of the storage modulus $G'$ with bending stiffness is caused by a competition between additional resistance to deformation offered by stiffer backbones and decreased density of the material due to a necessary decrease in monomer-monomer coordination. This counter-intuitive finding suggests that the strength of polymer glasses may in some circumstances be enhanced by softening the bending of constituent chains.
1709.00024v2
2017-12-31
Geometry Effects on Switching Currents in Superconducting Ultra Thin Films
Vortex dynamics is strongly connected with the mechanisms responsible for the photon detection of superconducting devices. Indeed, the local suppression of superconductivity by photon absorption may trigger vortex nucleation and motion effects, which can make the superconducting state unstable. In addition, scaling down the thickness of the superconducting films and/or the width of the bridge geometry can strongly influence the transport properties of superconducting films, e.g. affecting its critical current as well as its switching current into the normal state. Understanding such instability can boost the performances of those superconducting devices based on nanowire geometries. We present an experimental study on the resistive switching in NbN and NbTiN ultra-thin films with a thickness of few nanometers. Despite both films were patterned with the same microbridge geometry, the two superconducting materials show different behaviors at very low applied magnetic fields. A comparison with other low temperature superconducting materials outlines the influence of geometry effects on the superconducting transport properties of these materials particularly useful for devices applications.
1801.00306v1
2018-02-22
Shear strength of wet granular materials: macroscopic cohesion and effective stress
Rheometric measurements on assemblies of wet polystyrene bead assemblies, in steady uniform quasistatic shear flow, for varying liquid content within the small saturation (pendular) range of isolated liquid bridges, are supplemented with a systematic study by discrete numerical simulations. Numerical results and experimental ones agree quantitatively is the intergranular friction coefficient is set to 0.09, suitable for the dry material. Shear resistance and solid fraction are recorded as functions of the reduced pressure p, comparing normal stress to capillary bridge tensile strength. The Mohr-Coulomb relation with p-independent cohesion c applies for p above 2. The assumption that contact force contributions to stress act as effective stresses predicts shear strength quite well throughout the numerically investigated range of parameters.. A generalized Mohr-Coulomb cohesion c is defined, which relates to the dry material internal friction, coordination numbers and capillary force network anisotropy. The Rumpf formula approximation, ignoring capillary shear stress is correct for the larger saturation range within the pendular regime, but fails to describe its decrease for small liquid contents.
1802.08172v1
2018-09-12
Elastoresistive and Elastocaloric Anomalies at Magnetic and Electronic-Nematic Critical Points
Using Ba(Fe$_{0.975}$Co$_{0.025}$)$_2$As$_{2}$ as an exemplar material exhibiting second order electronic-nematic and antiferromagnetic transitions, we present measurements that reveal anomalies in the elastoresistance $\left(\frac{\partial \rho_{ij}}{\partial\varepsilon_{kl}}\right)$ and elastocaloric effect $\left(\frac{\partial T}{\partial\varepsilon_{kl}}\right)$ at both phase transitions. Both effects are understood to arise from the effect of strain on the transition temperatures; in the region close to the phase transitions this leads to (1) similarity between the strain and temperature derivatives of the resistivity and (2) similarity between the elastocaloric effect and the singular part of the specific heat. These mechanisms for elastoresistance and elastocaloric effect should be anticipated for any material in which mechanical deformation changes the transition temperature. Furthermore, these measurements provide evidence that the Fisher-Langer relation $\rho^{(c)} \propto U^{(c)}$ between the scattering from critical degrees of freedom and their energy-density, respectively, holds near each of the Ne\'{e}l and electronic nematic transitions in the material studied.
1809.04582v1
2018-09-17
Electric-Field Control of Magnetic Order: From FeRh to Topological Antiferromagnetic Spintronics
Using an electric field instead of an electric current (or a magnetic field) to tailor the electronic properties of magnetic materials is promising for realizing ultralow energy-consuming memory devices because of the suppression of Joule heating, especially when the devices are scaled to the nanoscale. In the review, we summarize recent results on the giant magnetization and resistivity modulation in a metamagnetic intermetallic alloy - FeRh, which is achieved by electric-field-controlled magnetic phase transitions in multiferroic heterostructures. Furthermore, the approach is extended to topological antiferromagnetic spintronics, which is currently receiving attention in the magnetic society, and the antiferromagnetic order parameter has been able to switch back and forth by a small electric field. In the end, we envision the possibility of manipulating exotic physical phenomena in the emerging topological antiferromagnetic spintronics field via the electric-field approach.
1809.06011v1
2017-03-02
Morphology and properties evolution upon ring-opening polymerization during extrusion of cyclic butylene terephthalate and graphene-related-materials into thermally conductive nanocomposites
In this work, the study of thermal conductivity before and after in-situ ring-opening polymerization of cyclic butylene terephthalate into poly (butylene terephthalate) in presence of graphene-related materials (GRM) is addressed, to gain insight in the modification of nanocomposites morphology upon polymerization. Five types of GRM were used: one type of graphite nanoplatelets, two different grades of reduced graphene oxide (rGO) and the same rGO grades after thermal annealing for 1 hour at 1700{\deg}C under vacuum to reduce their defectiveness. Polymerization of CBT into pCBT, morphology and nanoparticle organization were investigated by means of differential scanning calorimetry, electron microscopy and rheology. Electrical and thermal properties were investigated by means of volumetric resistivity and bulk thermal conductivity measurement. In particular, the reduction of nanoflake aspect ratio during ring-opening polymerization was found to have a detrimental effect on both electrical and thermal conductivities in nanocomposites.
1703.00805v2
2015-05-18
Unique opportunity to harness polarization in GaN to override the conventional power electronics figure-of-merits
Owing to the large breakdown electric field, wide bandgap semiconductors such as SiC, GaN, Ga2O3 and diamond based power devices are the focus for next generation power switching applications. The unipolar trade-off relationship between the area specific-on resistance and breakdown voltage is often employed to compare the performance limitation among various materials. The GaN material system has a unique advantage due to its prominent spontaneous and piezoelectric polarization effects in GaN, AlN, InN, AlxInyGaN alloys and flexibility in inserting appropriate heterojunctions thus dramatically broaden the device design space.
1505.04651v1
2015-05-21
Impedance Matching of Atomic Thermal Interfaces Using Primitive Block Decomposition
We explore the physics of thermal impedance matching at the interface between two dissimilar materials by controlling the properties of a single atomic mass or bond. The maximum thermal current is transmitted between the materials when we are able to decompose the entire heterostructure solely in terms of primitive building blocks of the individual materials. Using this approach, we show that the minimum interfacial thermal resistance arises when the interfacial atomic mass is the arithmetic mean, while the interfacial spring constant is the harmonic mean of its neighbors. The contact induced broadening matrix for the local vibronic spectrum, obtained from the self-energy matrices, generalizes the concept of acoustic impedance to the nonlinear phonon dispersion or the short-wavelength (atomic) limit.
1505.05564v1
2017-11-06
On the relation between plasticity, friction, and geometry
Plasticity refers to thermodynamically irreversible deformation associated with a change of configuration of materials. Friction is a phenomenological law that describes the forces resisting sliding between two solids or across an embedded dislocation. These two types of constitutive behaviors explain the deformation of a wide range of engineered and natural materials. Yet, they are typically described with distinct physical laws that cloud their inherent connexion. Here, I introduce a multiplicative form of kinematic friction that closely resembles the power-law flow of viscoplastic materials and that regularizes the constitutive behavior at vanishing velocity, with important implications for rupture dynamics. Using a tensor-valued state variable that describes the degree of localization, I describe a constitutive framework compatible with viscoplastic theories that captures the continuum between distributed and localized deformation and for which the frictional response emerges when the deformed region collapses from three to two dimensions.
1711.01954v2
2018-10-12
Non-volatile ferroelectric memory effect in ultrathin α-In2Se3
Recent experiments on layered {\alpha}-In2Se3 have confirmed its room-temperature ferroelectricity under ambient condition. This observation renders {\alpha}-In2Se3 an excellent platform for developing two-dimensional (2D) layered-material based electronics with nonvolatile functionality. In this letter, we demonstrate non-volatile memory effect in a hybrid 2D ferroelectric field effect transistor (FeFET) made of ultrathin {\alpha}-In2Se3 and graphene. The resistance of graphene channel in the FeFET is tunable and retentive due to the electrostatic doping, which stems from the electric polarization of the ferroelectric {\alpha}-In2Se3. The electronic logic bit can be represented and stored with different orientations of electric dipoles in the top-gate ferroelectric. The 2D FeFET can be randomly re-written over more than $10^5$ cycles without losing the non-volatility. Our approach demonstrates a protype of re-writable non-volatile memory with ferroelectricity in van de Waals 2D materials.
1810.05328v1
2018-10-17
From plastic flow to brittle fracture: role of microscopic friction in amorphous solids
Plasticity in soft amorphous materials typically involves collective deformation patterns that emerge upon intense shearing. The microscopic basis of amorphous plasticity has been commonly established through the notion of "Eshelby"-type events, localized abrupt rearrangements that induce flow in the surrounding material via non-local elastic-type interactions. This universal mechanism in flowing disordered solids has been proposed despite their diversity in terms of scales, microscopic constituents, or interactions. However, we argue that the presence of frictional interactions in granular solids alters the dynamics of flow by nucleating micro shear cracks that continually coalesce to build up system-spanning fracture-like formations on approach to failure. The plastic-to-brittle failure transition is uniquely controlled by the degree of frictional resistance which is in essence similar to the role of heterogeneities that separate the abrupt and smooth yielding regimes in glassy structures.
1810.07418v1
2018-10-17
Modeling Heterogeneous Melting in Phase Change Memory Devices
We present thermodynamic crystallization and melting models and calculate phase change velocities in $Ge_2 Sb_2 Te_5$ based on kinetic and thermodynamic parameters. The calculated phase change velocities are strong functions of grain size, with smaller grains beginning to melt at lower temperatures. Phase change velocities are continuous functions of temperature which determine crystallization and melting rates. Hence, set and reset times as well as power and peak current requirements for switching are strong functions of grain size. Grain boundary amorphization can lead to a sufficient increase in cell resistance for small-grain phase change materials even if the whole active region does not completely amorphize. Isolated grains left in the amorphous regions, the quenched-in nuclei, facilitate templated crystal growth and significantly reduce set times for phase change memory cells. We demonstrate the significance of heterogeneous melting through 2-D electrothermal simulations coupled with a dynamic materials phase change model. Our results show reset and set times on the order of ~1 ns for 30 nm wide confined nanocrystalline (7.5 nm - 25 nm radius crystals) phase change memory cells.
1810.07764v1
2018-11-08
Magnetically-driven orbital-selective insulator-metal transition in double perovskite oxides
Interaction-driven metal-insulator transitions or Mott transitions are widely observed in condensed-matter systems. In multi-orbital systems, many-body physics is richer in which an orbital-selective metal-insulator transition is an intriguing and unique phenomenon. Here we use first-principles calculations to show that a magnetic transition (from paramagnetic to long-range magnetically ordered) can simultaneously induce an orbital-selective insulator-metal transition in rock-salt ordered double perovskite oxides $A_2BB'$O$_6$ where $B$ is a non-magnetic ion (Y$^{3+}$ and Sc$^{3+}$) and $B'$ a magnetic ion with a $d^3$ electronic configuration (Ru$^{5+}$ and Os$^{5+}$). The orbital selectivity originates from geometrical frustration of a face-centered-cubic lattice on which the magnetic ions $B'$ reside. Including realistic structural distortions and spin-orbit interaction do not affect the transition. The predicted orbital-selective transition naturally explains the anomaly observed in the electric resistivity of Sr$_2$YRuO$_6$. Implications of other available experimental data are also discussed. Our work shows that by exploiting geometrical frustration on non-bipartite lattices, novel electronic/magnetic/orbital-coupled phase transitions can occur in correlated materials that are in the vicinity of metal-insulator phase boundary.
1811.03465v1
2018-11-08
Giant anomalous Nernst effect in the magnetic Weyl semimetal Co3Sn2S2
In ferromagnetic solids, even in absence of magnetic field, a transverse voltage can be generated by a longitudinal temperature gradient. This thermoelectric counterpart of the Anomalous Hall effect (AHE) is dubbed the Anomalous Nernst effect (ANE). Expected to scale with spontaneous magnetization, both these effects arise because of the Berry curvature at the Fermi energy. Here, we report the observation of a giant ANE in a newly-discovered magnetic Weyl semimetal Co$_3$Sn$_2$S$_2$ crystal. Hall resistivity and Nernst signal both show sharp jumps at a threshold field and exhibit a clear hysteresis loop below the ferromagnetic transition temperature. The ANE signal peaks a maximum value of about 5 miuV/K which is comparable to the largest seen in any magnetic material. Moreover, the anomalous transverse thermoelectric conductivity becomes as large as about 10 A/K.m at 70 K, the largest in known semimetals. The observed ANE signal is much larger than what is expected according to the magnetization.
1811.03485v2
2018-11-23
Extremely large magnetoresistance induced by hidden three-dimensional Dirac bands in nonmagnetic semimetal InBi
Extremely large positive magnetoresistance (XMR) was found in a nonmagnetic semimetal InBi. Using several single crystals with different residual resistivity ratios (RRRs), we revealed that the XMR strongly depended on the RRR (sample quality). Assuming that there were no changes in effective mass m* and carrier concentrations in these single crystals, this dependence was explained by a semiclassical two-carrier model. First-principle calculations including the spin-orbit interactions (SOI) unveiled that InBi had a compensated carrier balance and SOI-induced "hidden" three-dimensional (3D) Dirac bands at the M and R points. Because the small m* and the large carrier mobilities will be realized, these hidden 3D Dirac bands should play an important role for the XMR in InBi. We suggest that this feature can be employed as a novel strategy for the creation of XMR semimetals.
1811.09383v2
2019-02-07
In situ control of diamagnetism by electric current in Ca$_3$(Ru$_{1-x}$Ti$_x$)$_2$O$_7$
Non-equilibrium steady state (NESS) conditions induced by DC current can alter the physical properties of strongly correlated electron systems (SCES). In this regard, it was recently shown that DC current can trigger novel electronic states, such as current-induced diamagnetism, which cannot be realized in equilibrium conditions. However, reversible control of diamagnetism has not been achieved yet. Here, we demonstrate reversible in situ control between a Mott insulating state and a diamagnetic semimetal-like state by DC current in the Ti-substituted bilayer ruthenate Ca$_3$(Ru$_{1-x}$Ti$_x$)$_2$O$_7$ ($x=0.5$%). By performing simultaneous magnetic and resistive measurements, we map out the temperature vs current-density phase diagram in the NESS of this material. The present results open up the possibility of creating novel electronic states in a variety of SCES under DC current.
1902.02515v1
2019-05-15
Unconventional Hall Effect induced by Berry Curvature
Berry phase and Berry curvature play a key role in the development of topology in physics and do contribute to the transport properties in solid state systems. In this paper, we report the finding of novel nonzero Hall effect in topological material ZrTe5 flakes when in-plane magnetic field is parallel and perpendicular to the current. Surprisingly, both symmetric and antisymmetric components with respect to magnetic field are detected in the in-plane Hall resistivity. Further theoretical analysis suggests that the magnetotransport properties originate from the anomalous velocity induced by Berry curvature in a tilted Weyl semimetal. Our work not only enriches the Hall family but also provides new insights into the Berry phase effect in topological materials.
1905.06040v2
2020-02-13
Guest-Tunable Dielectric Sensing Using a Single Crystal of HKUST-1
There is rising interest on low-k dielectric materials based on porous metal-organic frameworks (MOFs) for improved electrical insulation in microelectronics. Herein, we demonstrate the concept of MOF dielectric sensor built from a single crystal of HKUST-1. We study guest encapsulation effects of polar and non-polar molecules, by monitoring the transient dielectric response and AC conductivity of the crystal exposed to different vapors (water, I2, methanol, ethanol). The dielectric properties were measured along the <100> crystal direction in the frequency range of 100 Hz to 2 MHz. The dielectric data show the efficacy of MOF dielectric sensor for discriminating the guest analytes. The time-dependent transient response reveals dynamics of the molecular inclusion and exclusion processes in the nanoscale pores. Since dielectric response is ubiquitous to all MOF materials (unlike DC conductivity and fluorescence), our results demonstrate the potential of dielectric MOF sensors compared to resistive sensors and luminescence-based approaches.
2002.05705v1
2020-04-08
Nonreciprocal thermal transport in a multiferroic helimagnet
Breaking of spatial inversion symmetry (SIS) induces unique phenomena in condensed matter. Besides the classic examples such as natural optical activity and piezoelectricity, the spin-orbit interaction further enriches the effect of SIS breaking, as exemplified by the Rashba effect. In particular, by combining this symmetry with magnetic fields or another type of time-reversal symmetry (TRS) breaking, noncentrosymmetric materials can be made to exhibit nonreciprocal responses, which are responses that differ for rightward and leftward stimuli. For example, resistivity becomes directionally dependent; that is to say, rectification appears in noncentrosymmetric materials in a magnetic field. However, the effect of SIS breaking on thermal transport remains to be elucidated. Here we show nonreciprocal thermal transport in the multiferroic helimagnet TbMnO3. The longitudinal thermal conductivity depends on whether the thermal current is parallel or antiparallel to the vector product of the electric polarization and magnetization. This phenomenon is thermal rectification that is controllable with external fields in a uniform crystal. This discovery may pave the way to thermal diodes with controllability and scalability.
2004.03801v1
2012-01-13
Ferroelectric PbTiO$_{3}$/SrRuO$_{3}$ superlattices with broken inversion symmetry
We have fabricated PbTiO$_{3}$/SrRuO$_{3}$ superlattices with ultra-thin SrRuO$_{3}$ layers. Due to the superlattice geometry, the samples show a large anisotropy in their electrical resistivity, which can be controlled by changing the thickness of the PbTiO$_{3}$ layers. Therefore, along the ferroelectric direction, SrRuO$_{3}$ layers can act as dielectric, rather than metallic, elements. We show that, by reducing the concentration of PbTiO$_{3}$, an increasingly important effect of polarization asymmetry due to compositional inversion symmetry breaking occurs. The results are significant as they represent a new class of ferroelectric superlattices, with a rich and complex phase diagram. By expanding our set of materials we are able to introduce new behaviors that can only occur when one of the materials is not a perovskite titanate. Here, compositional inversion symmetry breaking in bi-color superlattices, due to the combined variation of A and B site ions within the superlattice, is demonstrated using a combination of experimental measurements and first principles density functional theory.
1201.2893v2
2012-01-31
Effect of starting materials on the superconducting properties of SmFeAsO1-xFx tapes
SmFeAsO1-xFx tapes were prepared using three kinds of starting materials. It shows that the starting materials have an obvious effect on the impurity phases in final superconducting tapes. Compared with the other samples, the samples fabricated by SmAs, FeO, Fe2As, and SmF3 have the smallest arsenide impurity phase and voids. As a result, these samples possess much denser structure and better grain connectivity. Moreover, among the three kinds of samples fabricated in this work, this kind of sample has the highest zero-resistivity temperature ~40 K and largest critical current density ~4600 A/cm^2 in self-field at 4.2 K. This is the highest Jc values reported so far for SmFeAsO1-xFx wires and tapes.
1201.6522v1
2014-01-05
Phase-coexistence and glass-like behavior in magnetic and dielectric solids with long range order
Phase-coexistence in the manganese-oxide compounds or manganites with colossal magneto-resistance (CMR) has been generally considered to be an inhomogeneous ground state. An alternative explanation of phase-coexistence as the manifestation of a disorder-broadened first order magnetic phase transition being interrupted by the glasslike arrest of kinetics is now gradually gaining ground. This kinetic arrest of a first order phase transitions, between two states with long-range magnetic order, has actually been observed in various other classes of magnetic materials in addition to the CMR manganites. The underlying common features of this kinetic arrest of a first order phase transition are discussed in terms of the phenomenology of glasses. The possible manifestations of such glass-like arrested states across disorder-influenced first order phase transitions in dielectric solids and in multiferroic materials, are also discussed.
1401.0891v2
2017-04-04
Mechanics of disordered auxetic metamaterials
Auxetic materials are of great engineering interest not only because of their fascinating negative Poisson's ratio, but also due to their increased toughness and indentation resistance. These materials are typically synthesized polyester foams with a very heterogeneous structure, but the role of disorder in auxetic behavior is not fully understood. Here, we provide a systematic theoretical and experimental investigation in to the effect of disorder on the mechanical properties of a paradigmatic auxetic lattice with a re-entrant hexagonal geometry. We show that disorder has a marginal effect on the Poisson's ratio unless the lattice topology is altered, and in all cases examined the disorder preserves the auxetic characteristics. Depending on the direction of loading applied to these disordered auxetic lattices, either brittle or ductile failure is observed. It is found that brittle failure is associated with a disorder-dependent tensile strength, whereas in ductile failure disorder does not affect strength. Our work thus provides general guidelines to optimize elasticity and strength of disordered auxetic metamaterials.
1704.00943v3
2017-05-31
Tuning of Magnetic and Electrical Properties in Complex oxide Thin Films Deposited By Pulsed Laser Deposition
Lanthanum manganite, LaMnO (LMO) is the parent compound for a class of hole doped(e.g. La1-xCaxMnO3, La1-xSrxMnO3) and electron doped (e.g. . La1-xCexMnO3, La1-xSnxMnO3) perovskite complex oxide materials. Strong correlation between the spin,lattice, charge and orbital degrees of freedom is a hallmark of these class of materials (popularly known as manganites). Competition and interplay of these degrees of freedom lead to a wide range of interesting electronic behavior including half-metallicity, colossal magneto-resistivity, etc. Although a lot of experimental research has been carried out on the hole doped and the electron doped counterparts, the parent system LMO remains less investigated. This could be attributed to the difficulty in making stoichiometric LMO (whether in bulk polycrystalline, single crystals or thin films). There exists phenomenon like double-exchange (DE) and anti-ferromagnetic super-exchange (SE) interactions which leads to ferromagnetism in LMO thin films. This project work is aimed at the fabrication and characterization of thin films of stoichiometric LMO and their structural, magnetic and electrical studies.
1705.11003v1
2017-07-04
Time-temperature superposition in grain and grain boundary response regime of A2HoRuO6 (A = Ba, Sr, Ca) double perovskite ceramics: A Conductivity Spectroscopic Analysis
The pursuit for an appropriate universal scaling factor to satisfy the time-temperature superposition principle for grain and grain boundary responses has been explored in the ac conductivity domain for polycrystalline double perovskite oxides A2HoRuO6 (AHR; A = Ba, Sr, Ca). The samples show different structural phases ranging from cubic to monoclinic with decreasing ionic radii. The degree of distortion in the materials is correlated to the strength of bonding through the bond valence sum (BVS). The conductivity spectra for all the samples obey the power law behaviour. The contribution of different microstructural features to the conduction process is established. Thermal variation of dc resistivity points towards a gradual crossover from nearest neighbour to variable range hopping. The activation energies obtained from dc conductivity, hopping frequency and relaxation frequency show close correlation between the conduction and relaxation mechanisms. The scaled conductivity curves for AHR showed the presence of two different conduction processes with dissimilar activation energies in the grain boundary and grain response regimes. It is thus concluded that a single scaling parameter is insufficient to satisfy the time temperature superposition principle universally when two different thermally activated regions are present simultaneously in the materials.
1707.00881v1
2017-07-18
Insulator to Metal Transition in WO$_3$ Induced by Electrolyte Gating
Tungsten oxide and its associated bronzes (compounds of tungsten oxide and an alkali metal) are well known for their interesting optical and electrical characteristics. We have modified the transport properties of thin WO$_3$ films by electrolyte gating using both ionic liquids and polymer electrolytes. We are able to tune the resistivity of the gated film by more than five orders of magnitude, and a clear insulator-to-metal transition is observed. To clarify the doping mechanism, we have performed a series of incisive operando experiments, ruling out both a purely electronic effect (charge accumulation near the interface) and oxygen-related mechanisms. We propose instead that hydrogen intercalation is responsible for doping WO$_3$ into a highly conductive ground state and provide evidence that it can be described as a dense polaronic gas.
1707.05748v1
2019-04-02
Solid Propellants
Solid propellants are energetic materials used to launch and propel rockets and missiles. Although their history dates to the use of black powder more than two millennia ago, greater performance demands and the need for "insensitive munitions" that are resistant to accidental ignition have driven much research and development over the past half-century. The focus of this review is the material aspects of propellants, rather than their performance, with an emphasis on the polymers that serve as binders for oxidizer particles and as fuel for composite propellants. The prevalent modern binders are discussed along with a discussion of the limitations of state-of-the-art modeling of composite motors.
1904.01510v1
2019-04-08
Superhydrophobic frictions
Contrasting with its sluggish behavior on standard solids, water is extremely mobile on superhydrophobic materials, as shown for instance by the continuous acceleration of drops on tilted water-repellent leaves. For much longer substrates, however, drops reach a terminal velocity that results from a balance between weight and friction, allowing us to question the nature of this friction. We report that the relationship between force and terminal velocity is non-linear. This is interpreted by showing that classical sources of friction are minimized, so that the aerodynamical resistance to motion becomes dominant, which eventually explains the matchless mobility of water. Our results are finally extended to viscous liquids, also known to be unusually quick on these materials.
1904.03913v1
2019-04-23
Hydrated lithium intercalation into the Kitaev spin liquid candidate material $α-$RuCl$_3$
We study on transport and magnetic properties of hydrated and lithium-intercalated $\alpha$-RuCl$_3$, Li$_x$RuCl$_3 \cdot y$H$_2$O, for investigating the effect on mobile-carrier doping into candidate materials for a realization of a Kitaev model. From thermogravitometoric and one-dimensional electron map analyses, we find two crystal structures of this system, that is, mono-layer hydrated Li$_x$RuCl$_3 \cdot y$H$_2$O~$(x\approx0.56, y\approx1.3)$ and bi-layer hydrated Li$_x$RuCl$_3 \cdot y$H$_2$O~$(x\approx0.56, y\approx3.9)$. The temperature dependence of the electrical resistivity shows a temperature hysteresis at 200-270 K, which is considered to relate with a formation of a charge order. The antiferromagnetic order at 7-13 K in pristine $\alpha$-RuCl$_3$~ is successfully suppressed down to 2 K in bi-layer hydrated Li$_x$RuCl$_3 \cdot y$H$_2$O, which is sensitive to not only an electronic state of Ru but also an interlayer distance between Ru-Cl planes.
1904.10231v2
2019-12-03
Large Resistance Change on Magnetic Tunnel Junction based Molecular Spintronics Devices
Molecular bridges covalently bonded to two ferromagnetic electrodes can transform ferromagnetic materials and produce intriguing spin transport characteristics. This paper discusses the impact of molecule induced strong coupling on spin transport. To study the molecular coupling effect organometallic molecular complex (OMC) was bridged between two ferromagnetic electrodes of a magnetic tunnel junction (Ta/Co/NiFe/AlOx/NiFe/Ta) along the exposed side edges. OMCs induced strong iter-ferromagnetic electrode coupling to yield drastic changes in transport properties of the magnetic tunnel junction testbed at the room temperature. These OMCs also transformed the magnetic properties of magnetic tunnel junctions. SQUID and ferromagnetic resonance studies provided insightful data to explain transport studies on the magnetic tunnel junction based molecular spintronics devices.
1912.01305v1
2021-01-04
Unraveling the optical contrast in Sb2Te and AgInSbTe phase-change materials
Chalcogenide phase-change materials (PCMs) show a significant contrast in optical reflectivity and electrical resistivity upon crystallization from the amorphous phase and are leading candidates for non-volatile photonic and electronic applications. In addition to the flagship Ge2Sb2Te5 phase-change alloy, doped Sb2Te alloys, in particular AgInSbTe used in rewritable optical discs, have been widely investigated for decades, and nevertheless the theoretical insights on the optical properties of this important family of PCMs are scarce. Here, we carry out thorough ab initio simulations to gain an atomistic understanding of the optical properties of Sb2Te and AgInSbTe. We show that the large optical contrast between the amorphous and crystalline phase stems from the change in bond type in the parent compound Sb2Te. Ag and In impurities serve mostly the purpose of stabilization of the amorphous phase, and have marginal impact on the large variation in the dielectric function upon the phase transitions.
2101.00789v2
2011-04-05
Viscoelastic Fracture of Biological Composites
Soft constituent materials endow biological composites, such as bone, dentin and nacre, with viscoelastic properties that may play an important role in their remarkable fracture resistance. In this paper we calculate the scaling properties of the quasi-static energy release rate and the viscoelastic contribution to the fracture energy of various biological composites, using both perturbative and non-perturbative approaches. We consider coarse-grained descriptions of three types of anisotropic structures: (i) Liquid-crystal-like composites (ii) Stratified composites (iii) Staggered composites, for different crack orientations. In addition, we briefly discuss the implications of anisotropy for fracture criteria. Our analysis highlights the dominant lengthscales and scaling properties of viscoelastic fracture of biological composites. It may be useful for evaluating crack velocity toughening effects and structure-dissipation relations in these materials.
1104.0814v1
2012-03-12
Circuital model for the Maxwell Fish Eye perfect drain
Perfect drain for the Maxwell Fish Eye (MFE) is a non-magnetic dissipative region placed in the focal point to absorb all the incident radiation without reflection or scattering. The perfect drain was recently designed as a material with complex electrical permittivity that depends on frequency. However, this material is only a theoretical material, so it can not be used in practical devices. Recently, the perfect drain has been claimed as necessary to achieve super-resolution [Leonhard 2009, New J. Phys. 11 093040], which has increased the interest for practical perfect drains suitable for manufacturing. Here, we analyze the super-resolution properties of a device equivalent to the MFE, known as Spherical Geodesic Waveguide (SGW), loaded with the perfect drain. In the SGW the source and drain are implemented with coaxial probes. The perfect drain is realized using a circuit (made of a resistance and a capacitor) connected to the drain coaxial probes. Super-resolution analysis for this device is done in Comsol Multiphysics. The results of simulations predict the super-resolution up to wavelength/3000 and optimum power transmission from the source to the drain.
1203.2424v1
2015-06-22
Fracture Toughness of Silicate Glasses: Insights from Molecular Dynamics Simulations
Understanding, predicting and eventually improving the resistance to fracture of silicate materials is of primary importance to design new glasses that would be tougher, while retaining their transparency. However, the atomic mechanism of the fracture in amorphous silicate materials is still a topic of debate. In particular, there is some controversy about the existence of ductility at the nano-scale during the crack propagation. Here, we present simulations of the fracture of three archetypical silicate glasses using molecular dynamics. We show that the methodology that is used provide realistic values of fracture energy and toughness. In addition, the simulations clearly suggest that silicate glasses can show different degrees of ductility, depending on their composition.
1506.06441v1
2015-06-26
Conduction through subsurface cracks in bulk topological insulators
Topological insulators (TIs) have the singular distinction of being electronic insulators while harboring metallic, conductive surfaces. In ordinary materials, defects such as cracks and deformations are barriers to electrical conduction, intuitively making the material more electrically resistive. Peculiarly, 3D TIs should become better conductors when they are cracked because the cracks themselves, which act as conductive topological surfaces, provide additional paths for the electrical current. Significantly, for a TI material, any surface or extended defect harbors such conduction. In this letter, we demonstrate that small subsurface cracks formed within the predicted 3D TI samarium hexaboride (SmB$_{6}$) via systematic scratching or sanding results in such an increase in the electrical conduction. SmB$_{6}$ is in a unique position among TIs to exhibit this effect because its single-crystals are thick enough to harbor cracks, and because it remarkably does not appear to suffer from conduction through bulk impurities. Our results not only strengthen the building case for SmB$_{6}$'s topological nature, but are relevant to all TIs with cracks, including TI films with grain boundaries.
1506.08233v1
2018-12-14
VI3 - a new layered ferromagnetic semiconductor
Two-dimensional (2D) materials are promising candidates for next-generation electronic devices. In this regime, insulating 2D ferromagnets, which remain rare, are of special importance due to their potential for enabling new device architectures. Here we report the discovery of ferromagnetism in a layered van der Waals semiconductor, VI3, which is based on honeycomb vanadium layers separated by an iodine-iodine van der Waals gap. It has a BiI3-type structure (R-3, No.148) at room temperature, and our experimental evidence suggests that it may undergo a subtle structural phase transition at 78 K. VI3 becomes ferromagnetic at 49 K, below which magneto-optical Kerr effect imaging clearly shows ferromagnetic domains, which can be manipulated by the applied external magnetic field. The optical band gap determined by reflectance measurements is 0.6 eV, and the material is highly resistive.
1812.05982v1
2019-01-06
Low-Frequency Noise Spectroscopy of Charge-Density-Wave Phase Transitions in Vertical Quasi-2D Devices
We report results regarding the electron transport in vertical quasi-2D layered 1T-TaS2 charge-density-wave devices. The low-frequency noise spectroscopy was used as a tool to study changes in the cross-plane electrical characteristics of the quasi-2D material below room temperature. The noise spectral density revealed strong peaks - changing by more than an order-of-magnitude - at the temperatures closely matching the electrical resistance steps. Some of the noise peaks appeared below the temperature of the commensurate to nearly-commensurate charge-density-wave transition, possibly indicating the presence of the debated "hidden" phase transitions. These results confirm the potential of the noise spectroscopy for investigations of electron transport and phase transitions in novel materials.
1901.01475v1
2019-06-12
Simulation and experimental studies of induction hardening behavior of a new medium-carbon, low-alloy wear resistance steel
Flux2D commercial software together with a Gleeble thermomechanical simulator has been employed to numerically and physically simulate the material properties profile of an induction hardened slurry transportation pipe made of a recently developed 0.4 wt.% C, Nb-microalloyed steel. After calculating the thermal history of a 400 mm diameter, 10 mm thick pipe at various positions through the thickness, different heating and cooling paths were physically simulated using the Gleeble machine to predict the through-thickness material microstructure and hardness profiles. The results showed that by coupling a phase transformation model considering the effect of heating rate on the austenite transformation temperatures which allows calculations for arbitrary cooling paths with calculated induction heating and quenching thermal cycles, it has been possible to design induction hardening parameters for a slurry transport pipe material.
1906.05007v1
2019-06-15
Nonlinear planar Hall effect
An intriguing property of three-dimensional (3D) topological insulator (TI) is the existence of surface states with spin-momentum locking, which offers a new frontier of exploration in spintronics. Here, we report the observation of a new type of Hall effect in a 3D TI Bi2Se3 film. The Hall resistance scales linearly with both the applied electric and magnetic fields and exhibits a {\pi}/2 angle offset with respect to its longitudinal counterpart, in contrast to the usual angle offset of {\pi}/4 between the linear planar Hall effect and the anisotropic magnetoresistance. This novel nonlinear planar Hall effect originates from the conversion of a nonlinear transverse spin current to a charge current due to the concerted actions of spin-momentum locking and time reversal symmetry breaking, which also exists in a wide class of non-centrosymmetric materials with a large span of magnitude. It provides a new way to characterize and utilize the nonlinear spin-to-charge conversion in a variety of topological quantum materials.
1906.06462v1
2019-06-15
Effect of tungsten on vacancy behaviors in Ta-W alloys from first-principles
Alloying elements play an important role in the design of plasma facing materials with good comprehensive properties. Based on first-principles calculations, the stability of alloying element W and its interaction with vacancy defects in Ta-W alloys are studied. The results show that W tends to distribute dispersedly in Ta lattice, and is not likely to form precipitation even with the coexistence of vacancy. The aggregation behaviors of W and vacancy can be affected by their concentration competition. The increase of W atoms has a negative effect on the vacancy clustering, as well as delays the vacancy nucleation process, which is favorable to the recovery of point defects. Our results are in consistent with the defect evolution observed in irradiation experiments in Ta-W alloys. Our calculations suggest that Ta is a potential repairing element that can be doped into Ta-based materials to improve their radiation resistance.
1906.06610v1
2019-06-24
Electrical and magnetic properties of thin films of the spin-filter material CrVTiAl
The spin-filter material CrVTiAl is a promising candidate for producing highly spin-polarized currents at room temperature in a nonmagnetic architecture. Thin films of compensated-ferrimagnetic CrVTiAl have been grown and their electrical and magnetic properties have been studied. The resistivity shows two-channel semiconducting behavior with one disordered gapless channel and a gapped channel with activation energy $\Delta E$=~0.1~-~0.2~eV. Magnetoresistance measurements to B~=~35~T provide values for the mobilities of the gapless channel, leading to an order of magnitude difference in the carrier effective masses, which are in reasonable accord with our density-functional-theory based results. The density of states and electronic band structure is computed for permutations of the four sublattices arranged differently along the (111) body diagonal, yielding metallic (Cr-V-Al-Ti), spin-gapless (Cr-V-Ti-Al) and spin-filtering (Cr-Ti-V-Al) phases. Robustness of the spin-gapless phase to substitutional disorder is also considered.
1906.10222v1
2019-11-25
Fracturing of polycrystalline MoS$_2$ nanofilms
The possibility of tailoring the critical strain of 2D materials will be crucial for the fabrication of flexible devices. In this paper, the fracture in polycrystalline MoS2 films with two different grain orientations is studied at the micro- and nanoscale using electron microscopy. The critical uniaxial strain is determined to be approximately 5% and independent of the sample morphology. However, electron beam irradiation is found to enhance the interaction between the MoS2 and the PDMS substrates, leading to an increased critical strain that can exceed 10%. This enhancement of strain resistance was used to fabricate a mechanically robust array of lines 1 mm in length. Finally, nanoscale crack propagation studied by transmission electron microscopy showed that cracks propagate along the grain boundaries as well as through the grains, preferentially along van der Waals bonding. These results provide insight regarding the fracture of polycrystalline 2D materials and a new method to tailor the critical strain and nanofabrication of ultra-thin MoS2 devices using well-developed tools, which will be of great interest to the flexible electronics industry.
1911.10769v1
2019-11-27
Large topological Hall effect in a geometrically frustrated kagome magnet Fe$_3$Sn$_2$
We report on the observation of a large topological Hall effect (THE) over a wide temperature region in a geometrically frustrated Fe3Sn2 magnet with a kagome-bilayer structure. We found that the magnitude of the THE resistivity increases with temperature and reaches -0.875 {\mu}{\Omega}.cm at 380 K. Moreover, the critical magnetic fields with the change of THE are consistent with the magnetic structure transformation, which indicates that the real-space fictitious magnetic field is proportional to the formation of magnetic skyrmions in Fe3Sn2. The results strongly suggest that the large THE originates from the topological magnetic spin textures and may open up further research opportunities in exploring emergent phenomena in kagome materials.
1911.12214v1
2020-01-21
Huge linear magnetoresistance due to open orbits in $γ$-PtBi$_2$
Some single-crystalline materials present an electrical resistivity which decreases between room temperature and low temperatures at zero magnetic field as in a good metal and switches to a nearly semiconductinglike behavior at low temperatures with the application of a magnetic field. Often, this is accompanied by a huge and nonsaturating linear magnetoresistance which remains difficult to explain. Here we present a systematic study of the magnetoresistance in single-crystal $\gamma$-PtBi$_2$. We observe that the angle between the magnetic field and the crystalline $c$ axis fundamentally changes the magnetoresistance, going from a saturating to a nonsaturating magnetic field dependence. In between, there is one specific angle where the magnetoresistance is perfectly linear with the magnetic field. We show that the linear dependence of the nonsaturating magnetoresistance is due to the formation of open orbits in the Fermi surface of $\gamma$-PtBi$_2$.
2001.07674v2
2020-01-22
Chemical segregation in Ge2Sb2Te5 thin films during in-situ heating
Germanium antimony telluride has been the most used and studied phase-change material for electronic memory due to its suitable crystallization temperature, amorphous to crystalline resistance contrast, and stability of the amorphous phase. In this work, the segregation of Ge in a Ge2Sb2Te5 film of 30 nm thickness during heating inside the transmission electron microscope was observed and characterized. The Ge2Sb2Te5 film was deposited using sputtering on a Protochips Fusion holder and left uncapped in atmosphere for about four months. Oxygen incorporated within the film played a significant role in the chemical segregation observed which resulted in amorphous Ge-O grain boundaries and Sb and Te rich crystalline domains. Such composition changes can occur when the phase-change material interfaces insulating oxide layers in an integrated device and would significantly impact its electrical and thermal properties.
2001.08100v1
2020-05-10
Determination of the magnetocaloric effect from thermophysical parameters and their relationships near magnetic phase transition in doped manganites
We present the results of a comparative analysis of the magnetocaloric effect (MCE) in Pr0.7Sr0.2Ca0.1MnO3, through direct and indirect measurements, using experimentally measured magnetization, specific heat, magnetostriction, resistivity, thermal diffusivity and thermal conductivity parameters. We have demonstrated that the change in each parameter in response to a magnetic field near the ferromagnetic-paramagnetic phase transition temperature of the material correlates with the change in magnetic entropy. These findings allow us to interrelate these parameters and provide an alternative, effective approach for accessing the usefulness of magnetocaloric materials.
2005.04569v1
2020-07-05
Deep Learning based Dimple Segmentation for Quantitative Fractography
In this work, we try to address the challenging problem of dimple detection and segmentation in Titanium alloys using machine learning methods, especially neural networks. The images i.e. fractographs are obtained using a Scanning Election Microscope (SEM). To determine the cause of fracture in metals we address the problem of segmentation of dimples in fractographs i.e. the fracture surface of metals using supervised machine learning methods. Determining the cause of fracture would help us in material property, mechanical property prediction and development of new fracture-resistant materials. This method would also help in correlating the topography of the fracture surface with the mechanical properties of the material. Our proposed novel model achieves the best performance as compared to other previous approaches. To the best of our knowledge, this is one the first work in fractography using fully convolutional neural networks with self-attention for supervised learning of dimple fractography, though it can be easily extended to account for brittle characteristics as well.
2007.02267v3
2020-07-10
Canted Spin Texture and Quantum Spin Hall Effect in WTe2
We report an unconventional quantum spin Hall phase in the monolayer T$_\text{d}$-WTe$_2$, which exhibits hitherto unknown features in other topological materials. The low-symmetry of the structure induces a canted spin texture in the $yz$ plane, which dictates the spin polarization of topologically protected boundary states. Additionally, the spin Hall conductivity gets quantized ($2e^2/h$) with a spin quantization axis parallel to the canting direction. These findings are based on large-scale quantum simulations of the spin Hall conductivity tensor and nonlocal resistances in multi-probe geometries using a realistic tight-binding model elaborated from first-principle methods. The observation of this canted quantum spin Hall effect, related to the formation of topological edge states with nontrivial spin polarization, demands for specific experimental design and suggests interesting alternatives for manipulating spin information in topological materials.
2007.05626v1
2020-07-14
Tuning Conductivity and Spin Dynamics in Few-Layer Graphene via In Situ Potassium Exposure
Chemical modification, such as intercalation or doping of novel materials is of great importance for exploratory material science and applications in various fields of physics and chemistry. In the present work, we report the systematic intercalation of chemically exfoliated few-layer graphene with potassium while monitoring the sample resistance using microwave conductivity. We find that the conductivity of the samples increases by about an order of magnitude upon potassium exposure. The increased of number of charge carriers deduced from the ESR intensity also reflects this increment. The doped phases exhibit two asymmetric Dysonian lines in ESR, a usual sign of the presence of mobile charge carriers. The width of the broader component increases with the doping steps, however, the narrow components seem to have a constant line width.
2007.07057v1
2020-07-31
Quantum breakdown of superconductivity in low-dimensional materials
In order to understand the emergence of superconductivity it is useful to study and identify the various pathways leading to the destruction of superconductivity. One way is to use the increase in Coulomb-repulsion due to the increase in disorder, which overpowers the attractive interaction responsible for Cooper-pair formation. A second pathway, applicable to uniformly disordered materials, is the competition between superconductivity and Anderson localization, which leads to electronic granularity in which phase and amplitude fluctuations of the superconducting order parameter play a role. Finally, a third pathway is an array of superconducting islands coupled by some form of proximity-effect, due to Andreev-reflections, and which leads from a superconducting state to a state with finite resistivity, which appears like a metallic groundstate. This review summarizes recent progress in understanding of these different pathways, including experiments in low dimensional materials and application in superconducting quantum devices.
2007.15870v1
2020-08-06
Creep in reactive colloidal gels: a nanomechanical study of cement hydrates
From soft polymeric gels to hardened cement paste, amorphous solids under constant load exhibit a pronounced time-dependent deformation called creep. The microscopic mechanism of such a phenomenon is poorly understood in amorphous materials and constitutes an even greater challenge in densely packed and chemically reactive granular systems. Both features are prominently present in hydrating cement pastes composed of calcium silicate hydrate (C-S-H) nanoparticles, whose packing density increases as a function of time, while cement hydration is taking place. Performing nano-indentation tests and porosity measurements on a large collection of samples at various stages of hydration, we show that the creep response of hydrating cement paste is mainly controlled by the inter-particle distance and results from slippage between (C-S-H) nanoparticles. Our findings provide a unique insight into the microscopic mechanism underpinning the creep response in aging granular materials, thus paving the way for the design of concrete with improved creep resistance.
2008.02617v3
2020-12-04
Epitaxial stabilization of SrCu$_3$O$_4$ with infinite Cu$_{3/2}$O$_2$ layers
We report the epitaxial thin film synthesis of SrCu$_3$O$_4$ with infinitely stacked Cu$_3$O$_4$ layers composed of edge-sharing CuO$_4$ square-planes, using molecular beam epitaxy. Experimental and theoretical characterizations showed that this material is a metastable phase that can exist by applying tensile biaxial strain from the (001)-SrTiO$_3$ substrate. SrCu$_3$O$_4$ shows an insulating electrical resistivity in accordance with the Cu$^{2+}$ valence state revealed X-ray photoelectron spectroscopy. First-principles calculations also indicated that the unoccupied $d_{3z^2-r^2}$ band becomes substantially stabilized owing to the absence of apical anions, in contrast to $A_2$Cu$_3$O$_4$Cl$_2$ ($A = $Sr, Ba) with an $A_2$Cl$_2$ block layer and therefore a trans-CuO$_4$Cl$_2$ octahedron. These results suggest that SrCu$_3$O$_4$ is a suitable parent material for electron-doped superconductivity based on the Cu$_3$O$_4$ plane.
2012.02433v1
2021-03-02
Bioinspired approaches to toughen calcium phosphate-based ceramics for bone repair
To respond to the increasing need for bone repair strategies, various types of biomaterials have been developed. Among those, calcium phosphate ceramics (CPCs) are promising since they possess a chemical composition similar to that of bones. To be suitable for implants, CPCs need to fulfill a number of biological and mechanical requirements. Fatigue resistance and toughness are two key mechanical properties that are still challenging to obtain in CPCs. This paper thus reviews and discusses current progress in the processing of CPCs with bioinspired microstructures for load-bearing applications. First, methods to obtain CPCs with bioinspired structure at individual lengthscales, namely nano-, micro-, and macroscale are discussed. Then, approaches to attain synergetic contribution of all lengthscales through a complex and biomimetic hierarchical structure are reviewed. The processing methods and their design capabilities are presented and the mechanical properties of the materials they can produce are analysed. Their limitations and challenges are finally discussed to suggest new directions for the fabrication of biomimetic bone implants with satisfactory properties. The paper could help biomedical researchers, materials scientists and engineers to join forces to create the next generation of bone implants.
2103.01443v1
2021-04-14
Combining AFM imaging and elementally resolved spectro-electrochemistry for understanding stability and quality of passive films formed on Alloy 600
Understanding elemental corrosion currents and visualizing corroding topographies provide a detailed insight into corrosion mechanisms at the nano-scale. Here, we develop a strategy to understand the elemental composition, corrosion resistivity and local stability of passive materials. Specifically, we utilize a pulse voltammetry approach in a novel electrochemical AFM cell and complement this data by real-time dissolution currents based on spectro-electrochemical online analysis in an ICP-MS flow cell. We study the oxide properties and their protective behaviour, when formed under different applied potentials using alloy 600 as model sample. Both AFM and ICP-MS data show that passive films formed on alloy 600 at around +0.3 to +0.4~V in neutral 1 mM NaCl solution are most stable during anodic corrosion at +1.0~V, while AFM further demonstrates that local dissolution occurs, indicating locally varying defect levels in the passive film. In combination of both techniques, our approach provide real-time elementally resolved and localized information of passive film quality under corrosive conditions, and it may prove useful for other corroding materials.
2104.07100v1
2021-06-11
Measurement of onset of structural relaxation in melt-quenched phase change materials
Chalcogenide phase change materials enable non-volatile, low-latency storage-class memory. They are also being explored for new forms of computing such as neuromorphic and in-memory computing. A key challenge, however, is the temporal drift in the electrical resistance of the amorphous states that encode data. Drift, caused by the spontaneous structural relaxation of the newly recreated melt-quenched amorphous phase, has consistently been observed to have a logarithmic dependence in time. Here, we show that this observation is valid only in a certain observable timescale. Using threshold-switching voltage as the measured variable, based on temperature-dependent and short timescale electrical characterization, we experimentally measure the onset of drift. This additional feature of the structural relaxation dynamics serves as a new benchmark to appraise the different classical models to explain drift.
2106.06270v1
2021-08-08
Strong-coupling superconductivity of SrIr2 and SrRh2: Phonon engineering of metallic Ir and Rh
Experimental and theoretical studies on superconductivity in SrIr$_2$ and SrRh$_2$ Laves phases are presented. The measured resistivity, heat capacity, and magnetic susceptibility confirm the superconductivity of these compounds with $T_c$ = 6.07 K and 5.41 K, respectively. Electronic structure calculations show that the Fermi surface is mostly contributed by 5$d$ (4$d$) electrons of Ir (Rh), with Sr atoms playing the role of electron donors. The effect of the spin-orbit coupling is analyzed and found to be important in both materials. Lattice dynamics and electron-phonon coupling (EPC) are studied and the strong electron-phonon interaction is found, contributed mostly by the low-frequency Ir and Rh vibrations. The enhancement of EPC when compared to weakly-coupled metallic Ir and Rh is explained by the strong modifications in the propagation of phonons in the network of Ir (Rh) tetrahedrons, which are the building blocks of the Laves phase, and originate from the metallic fcc structures of elemental iridium and rhodium.
2108.03692v1
2021-08-06
Manipulating thermal fields with inhomogeneous heat spreaders
We design a class of spatially inhomogeneous heat spreaders in the context of steady-state thermal conduction leading to spatially uniform thermal fields across a large convective surface. Each spreader has a funnel-shaped design, either in the form of a trapezoidal prism or truncated cone, and is forced by a thermal source at its base. We employ transformation-based techniques, commonly used to study metamaterials, to determine the require thermal conductivity for the spreaders. The obtained materials, although strongly anisotropic and inhomogeneous, can be accurately approximated by assembling isotropic, homogeneous layers, rendering them realisable. An alternative approach is then considered for the conical and trapezoidal spreaders by dividing them into two or three isotropic, homogeneous components respectively. We refer to these simple configurations as neutral layers. All designs are validated numerically both with and without the effects of thermal contact resistance between interfaces. Such novel designs pave the way for future materials that can manipulate and control the flow of heat, helping to solve traditional heat transfer problems such as controlling the temperature of an object and energy harvesting.
2108.04881v2
2021-08-20
Peak in the superconducting transition temperature of the nonmagnetic topological line-nodal material CaSb$_2$ under pressure
Investigating the pressure dependence of the superconducting (SC) transition temperature $T_{\rm c}$ is crucial for understanding the SC mechanism. Herein, we report on the pressure dependence of $T_{\rm c}$ in the nonmagnetic topological line-nodal material CaSb$_2$, based on measurements of electric resistance and alternating current magnetic susceptibility. $T_{\rm c}$ initially increases with increasing pressure and peaks at $\sim$ 3.1~GPa. With a further increase in pressure, $T_{\rm c}$ decreases and finally becomes undetectable at 5.9~GPa. Because no signs of phase transition or Lifshitz transition are observed in the normal state, the peculiar peak structure of $T_{\rm c}$ suggests that CaSb$_2$ has an unconventional SC character.
2108.08992v1
2021-09-09
Bias factor of dislocation loops in quasicrystalline materials
Vacancy swelling of quasicrystals under irradiation is considered. In quasicrystals, the evolution of dislocations is accompanied by the formation of phasons which are localized topological defects of the vacancy and interstitial types. At moderate temperatures the diffusivity of phasons is low which leads to the formation of ring-or disk-shaped phason trails inside dislocation loops. To find the capture efficiency of point defects by a dislocation loop with the complementary ring of phasons the steady-state drift-diffusional problem is solved in the toroidal geometry by the successive overrelaxation method. It is shown that phasons significantly reduce the bias of dislocations towards absorption of interstitial atoms. For this reason, quasicrystalline materials are predicted to exhibit increased resistance to vacancy swelling.
2109.04136v2
2021-09-20
Coexistence of superconductivity and weak anti-localization at KTaO3 (111) interfaces
The intersection of two-dimensional superconductivity and topologically nontrivial states hosts a wide range of quantum phenomena, including Majorana fermions. Coexistence of topologically nontrivial states and superconductivity in a single material, however, remains elusive. Here, we report on the observation of two-dimensional superconductivity and weak anti-localization at the TiOx/KTaO3(111) interfaces. A remnant, saturating resistance persists below the transition temperature as superconducting puddles fail to reach phase coherence. Signatures of weak anti-localization are observed below the superconducting transition, suggesting the coexistence of superconductivity and weak anti-localization. The superconducting interfaces show roughly one order of magnitude larger weak anti-localization correction, compared to non-superconducting interfaces, alluding to a relatively large coherence length in these interfaces.
2109.09786v1
2021-09-23
Plastic deformation of the CaMg$_{2}$ C14-Laves phase from 50-250$^\circ$C
Intermetallic phases can significantly improve the creep resistance of magnesium alloys, extending their use to higher temperatures. However, little is known about the deformation behaviour of these phases at application temperatures, which are commonly below their macroscopic brittle-to-ductile-transition temperature. In this study, we therefore investigate the activation of different slip systems of the CaMg$_2$ phase and the occurrence of serrated yielding in the temperature range from 50$^\circ$C to 250$^\circ$C. A decreasing amount of serrated flow with increasing temperature suggests that solute atoms govern the flow behaviour when the CaMg$_{2}$ phase is off-stoichiometric.
2109.11367v1
2021-11-08
Microstructure and the Boson-peak in thermally-treated In_{x}O films
We report on the correlation between the boson-peak and structural changes associated with thermally-treating amorphous indium-oxide films. In this process, the resistance of a given sample may decrease by a considerable margin while its amorphous structure is preserved. In the present study, we focus on the changes that result from the heat-treatment by employing electron-microscopy, X-ray, and Raman spectroscopy. These techniques were used on films with different stoichiometry and thus different carrier-concentration. The main effect of heat-treatment is material densification, which presumably results from elimination of micro-voids. The densified system presents better wavefunction-overlap and more efficient connectivity for the current flow. X-ray, and electron-beam diffraction experiments indicate that the heat-treated samples show significantly less spatial heterogeneity with only a moderate change of the radial-distribution function metrics. These results are consistent with the changes that occur in the boson-peak characteristics due to annealing as observed in their Raman spectra.
2111.04277v1
2021-11-11
NbReSi: A Noncentrosymetric Superconductor with Large Upper Critical Field
We report the discovery of superconductivity in noncentrosymmetric NbReSi, which crystallizes in a hexagonal ZrNiAl-type crystal structure with space group $P\bar{6}2m$ (No.~189). Bulk superconductivity, with $T_c$ = 6.5 K was characterized via electrical-resistivity, magnetization, and heat-capacity measurements. The low-temperature electronic specific heat suggests a fully gapped superconducting state in NbReSi, while a large upper critical field of $\mu_0H_\mathrm{c2}(0)$ $\sim$ 12.6 T is obtained, which is comparable to the weak-coupling Pauli limit. The electronic band-structure calculations show that the density of states at the Fermi level are dominated by Re and Nb $d$-orbitals, with a sizeable band splitting induced by the antisymmetric spin-orbit coupling. NbReSi represents another candidate material for revealing the puzzle of time-reversal symmetry breaking observed in some Re-based superconductors and its relation to the lack of inversion symmetry.
2111.06010v1
2021-11-14
Superconductivity in noncentrosymmetric NbReSi investigated by muon spin rotation and relaxation
Noncentrosymmetric materials are promising paradigm to explore unconventional superconductivity. In particular, several Re containing noncentrosymmetric materials have attracted considerable attention due to a superconducting state with a broken time reversal symmetry. A comprehensive study on the superconducting ground state of NbReSi was investigated using magnetization, resistivity, and muon spin rotation/relaxation measurements. Zero field muon spectroscopy results showed the absence of any spontaneous magnetic field below the superconducting transition temperature, T$ _{c} $ = 6.29 K, indicating the preserved time-reversal symmetry. Transverse field muon spin rotation measurements confirms a s-wave nature of the sample with $\Delta(0)/k_{B}T_{c} $ = 1.726. This study urges further investigation on more noncentrosymmetric materials to elucidate the selective appearance of unconventional nature and unveil its dependence on antisymmetric spin-orbit coupling strength.
2111.07247v1
2021-12-26
Tuning Ferroelectrics to Antiferroelectrics in Multiferroic LaxSr1-xFe12O19 Ceramics
The combination of antiferroelectricity (AFE) and ferromagnetism (FM) in one structure would allow the development of new type of multiferroic candidates, which be applicable not only in magnetoelectric memories but also in novel energy storage devices. Here we propose a novel type of multiferroic candidate LaxSr1-xFe12O19, whose room temperature state could betuned from ferroelectrics (FE) to antiferroelectrics by changing x from 0 to 0.5. The emphasis of this paper will be focused on the La0.5Sr0.5Fe12O19 system, in which full AFE and FM coexist. The pure antiferroelectric behavior in La0.5Sr0.5Fe12O19 ceramics is demonstrated by double polarization-electric field (P-E) hysteresis loops, which are fully separated by a linear antiferroelectric AFE component with zero net polarization. The material of La0.2Sr0.7Fe12O19 with the intermediate composition exhibits a hybrid ferroelectric/antiferroelectric state. The recoverable energy density of the antiferroelectric La0.5Sr0.5Fe12O19 phase reaches 14.3 J/cm3. This material demonstrates strong magnetoelectric coupling and giant magnetoresistance (GMR) effect. A 1.1T magnetic field generates electronic polarization up to 0.95uC/cm2, reduce the resistance by 117%, enhances dielectric constants by 540% and right shifts the maximum dielectric loss peak by 208 kHz. The combined functional responses provide an opportunity to develop novel multifunctional electric and energy storage devices.
2112.13307v1
2022-01-03
Aerogel from sustainably grown bacterial cellulose pellicle as thermally insulative film for building envelope
Improving building energy performance requires the development of new highly insulative materials. An affordable retrofitting solution comprising a thin film could improve the resistance to heat flow in both residential and commercial buildings and reduce overall energy consumption. Here we propose cellulose aerogel films formed from pellicles produced by the bacteria Gluconacetobacter hansenii as insulation materials. We studied the impact of density and nanostructure on the aerogels' thermal properties. Thermal conductivity as low as 13 mW/(K*m) was measured for native pellicle-based aerogels dried as-is with minimal post-treatment. The use of waste from the beer brewing industry as a solution to grow the pellicle maintained the cellulose yield obtained with standard Hestrin-Schramm medium, making our product more affordable and sustainable. In the future, our work can be extended through further diversification of the sources of substrate among food wastes, facilitating larger potential production and applications.
2201.00449v1
2022-03-13
Electronic and topological properties of the van der Waals layered superconductor PtTe
We report the crystal growth and structural and electronic properties of superconducting, van der Waals layered PtTe. Easily cleavable crystals with a plate-like morphology consistent with the layered structure were grown from a platinum rich flux. A consistent determination of $T_c = 0.57$ K is made from the onset of diamagnetism, the zero of resistivity, and the midpoint of the heat capacity jump. The observed behavior is consistent with type-II superconductivity, with upper critical field at $T=0$ estimated using the Werthamer-Helfand-Hohenberg theory to be 143 and 65 Oe for fields out of and in the plane, respectively. The heat capacity discontinuity is close to the weak coupling BCS value. Density functional theory calculations and analysis of the electronic structure finds that PtTe is a topological semimetal with numerous surface states, but suggests the superconducting state itself may be topologically trivial. Angle resolved photoemission spectroscopy reveals a normal-state Fermi surface in remarkable agreement with theory, and confirms the overall topological nature of the material by experimental identification of the surface bands. Together, these findings identify PtTe as an interesting example of a cleavable, topological, and superconducting material.
2203.06655v1
2022-04-28
Vacancy formation energies and migration barriers in multi-principal element alloys
Multi-principal element alloys (MPEAs) continue to garner interest as structural and plasma-facing materials due to their structure stability and increased resistance to radiation damage. Despite sensitivity of mechanical behavior to irradiation and point-defect formation, there has been scant attention on understanding vacancy stability and diffusion in refractory-based MPEAs. Using density-functional theory, we examine vacancy stability and diffusion barriers in body-centered cubic (Mo0.95W0.05)0.85Ta0.10(TiZr)0.05. The results in this MPEA show strong dependence on environment, originating from local lattice distortion associated with charge-transfer between neighboring atoms that vary with different chemical environments. We find a correlation between degree of lattice distortion and migration barrier: (Ti, Zr) with less distortion have lower barriers, while (Mo, W) with larger distortion have higher barriers, depending up local environments. Under irradiation, our findings suggest that (Ti, Zr) are significantly more likely to diffuse than (Mo, W) while Ta shows intermediate effect. As such, material degradation caused by vacancy diffusion can be controlled by tuning composition of alloying elements to enhance creep strength at extreme operating temperatures and harsh conditions.
2204.13616v1
2022-08-01
Boundary scattering in micro-size crystal of topological Kondo insulator SmB$_6$
We have studied the effects of phonon-boundary scattering on the thermal transport in topological Kondo insulator, SmB$_6$. The studies have been performed by using the $3\omega$ method in the temperature range 300K - 3K. We show that the observed thermal conductivity of micro-size SmB$_6$ is of the order of magnitude smaller than for a bulk single-crystal. Using the Callaway model we analyzed the low-temperature lattice thermal conductivity of the micro crystal and show that phonon scattering by sample boundaries plays a major role in the thermal resistance in this topological material. In addition, we show that the temperature dependence of the lattice thermal conductivity shows a double peak structure that suggests complex phonon-phonon or phonon-defects interactions in SmB$_6$. These findings provide guidance for the understanding of the thermal transport of advanced materials and devices at a micro-scale.
2208.01145v1
2022-08-09
Pressure-Independent Through-Plane Electrical Conductivity Measurements of Highly Filled Conductive Polymer Composites
Highly filled conductive polymer composites (CPCs) are widely used in applications such as bipolar plate materials for polymer electrolyte membrane fuel cells and redox flow batteries, electromagnetic interference shielding and sensors due to their useful electrical properties. A common method for determining through-plane electrical conductivities $\left(\sigma_{\rm tp} \right)$ of such highly filled CPCs applies a conductive carbon paper between electrodes and sample with application of external pressure to improve electrical contact. We show the pressure-dependence of the measured $\sigma_{\rm tp}$ can be eliminated by using a liquid metal such as the gallium-indium eutectic alloy (EGaIn) as contact material. Results indicate that EGaIn reduces contact resistances and cause three to five times larger $\sigma_{\rm tp}$ compared to measurements with carbon paper contacts and pressures up to 20 bar.
2208.04643v1