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From hathaway at cns.fas.harvard.edu Tue Jul 18 17:51:55 2023
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From: hathaway at cns.fas.harvard.edu (Hathaway, Malcolm R)
|
Date: Tue, 18 Jul 2023 21:51:55 +0000
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Subject: [labnetwork] TTIP Cylinder Overheated - Request for Advise
|
Message-ID: <MN2PR07MB6526683338D9DA35ACD0C64ECB38A@MN2PR07MB6526.namprd07.prod.outlook.com>
|
Hey all,
|
We (not CNS, but another lab) have an issue with a TTIP cylinder (Cambridge Nano/swagelok-style) which got over-heated to an unknown temp, whereupon the bottle acquired a bulge. It was closed at the time, and so is still under pressure to an unknown degree. The bottle label melted, for reference.
|
Questions:
|
Are the contents likely to be decomposition products?
|
Would these products be flammable or explosive?
|
Can a bottle burst under the flexural stress of slow depressurization?
|
Is there a safe way to depressurize?
|
We came up with the idea of attaching a second valve (these are all VCR), and alternating opening inner valve (then closing) and opening outer valve (then closing), to step-wise vent the bottle. Has anyone heard of such a technique causing the bottle to burst along the way?
|
Suggestion welcome.
|
Mac
|
--
|
Mac Hathaway
|
Senior Process and Systems Engineer
|
Harvard Center for Nanoscale Systems
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11 Oxford St.
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Cambridge, MA 02138
|
617-495-9012
|
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From s.etienne at ucl.ac.uk Wed Jul 19 04:29:09 2023
|
From: s.etienne at ucl.ac.uk (Etienne, Steve)
|
Date: Wed, 19 Jul 2023 08:29:09 +0000
|
Subject: [labnetwork] Job opportunity in London
|
Message-ID: <PA4PR01MB933115A90E879C3261C4E2ADB939A@PA4PR01MB9331.eurprd01.prod.exchangelabs.com>
|
Hi everyone,
|
I'd like to make you aware of this position available at UCL.
|
https://www.ucl.ac.uk/work-at-ucl/search-ucl-jobs/details?jobId=12592&jobTitle=Cleanroom+Manager
|
Best Regards
|
Steve
|
Stephen Etienne | Cleanroom Manager
|
I retire at end of July 2023, and my current email will become inactive.
|
Please use lcn.crteam at ucl.ac.uk<mailto:lcn.crteam at ucl.ac.uk> for ongoing communications.
|
London Centre for Nanotechnology | UCL | 17-19 Gordon Street | London | WC1H 0AH
|
Tel: +44 (0)207 679 2570 | www.london-nano.com<http://www.london-nano.com> lcn.crteam at ucl.ac.uk<mailto:lcn.crteam at ucl.ac.uk>
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From deonc69 at illinois.edu Thu Jul 20 14:55:00 2023
|
From: deonc69 at illinois.edu (Collins, Deon)
|
Date: Thu, 20 Jul 2023 18:55:00 +0000
|
Subject: [labnetwork] TTIP Cylinder Overheated - Request for Advise
|
In-Reply-To: <MN2PR07MB6526683338D9DA35ACD0C64ECB38A@MN2PR07MB6526.namprd07.prod.outlook.com>
|
References: <MN2PR07MB6526683338D9DA35ACD0C64ECB38A@MN2PR07MB6526.namprd07.prod.outlook.com>
|
Message-ID: <DM6PR11MB31622313B095B7441827AA21D73EA@DM6PR11MB3162.namprd11.prod.outlook.com>
|
I would have the bottle disposed of ASAP. The structural integrity of the cylinder has been compromised.
|
Deon D. Collins
|
FACILITY MANAGER
|
The Grainger College Of Engineering UIUC
|
Holonyak Micro & Nanotechnology Lab
|
208 N Wright St Rm. 1114 | MC-249
|
Urbana, IL 61801
|
217-300-7531 | deonc69 at illinois.edu<mailto:deonc69 at illinois.edu>
|
[cid:image001.png at 01D9BB11.CB783070]<http://illinois.edu/>
|
Under the Illinois Freedom of Information Act any written communication to or from university employees regarding university business is a public record and may be subject to public disclosure.
|
Life is not about watching other people live it. It's about you living your own!
|
From: labnetwork <labnetwork-bounces at mtl.mit.edu> On Behalf Of Hathaway, Malcolm R
|
Sent: Tuesday, July 18, 2023 4:52 PM
|
To: Labnetwork Mailing List <labnetwork at mtl.mit.edu>
|
Subject: [labnetwork] TTIP Cylinder Overheated - Request for Advise
|
Hey all,
|
We (not CNS, but another lab) have an issue with a TTIP cylinder (Cambridge Nano/swagelok-style) which got over-heated to an unknown temp, whereupon the bottle acquired a bulge. It was closed at the time, and so is still under pressure to an unknown degree. The bottle label melted, for reference.
|
Questions:
|
Are the contents likely to be decomposition products?
|
Would these products be flammable or explosive?
|
Can a bottle burst under the flexural stress of slow depressurization?
|
Is there a safe way to depressurize?
|
We came up with the idea of attaching a second valve (these are all VCR), and alternating opening inner valve (then closing) and opening outer valve (then closing), to step-wise vent the bottle. Has anyone heard of such a technique causing the bottle to burst along the way?
|
Suggestion welcome.
|
Mac
|
--
|
Mac Hathaway
|
Senior Process and Systems Engineer
|
Harvard Center for Nanoscale Systems
|
11 Oxford St.
|
Cambridge, MA 02138
|
617-495-9012
|
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From hathaway at cns.fas.harvard.edu Thu Jul 20 17:17:56 2023
|
From: hathaway at cns.fas.harvard.edu (Hathaway, Malcolm R)
|
Date: Thu, 20 Jul 2023 21:17:56 +0000
|
Subject: [labnetwork] TTIP Cylinder Overheated - Request for Advise
|
In-Reply-To: <DM6PR11MB31622313B095B7441827AA21D73EA@DM6PR11MB3162.namprd11.prod.outlook.com>
|
References: <MN2PR07MB6526683338D9DA35ACD0C64ECB38A@MN2PR07MB6526.namprd07.prod.outlook.com>
|
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